# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Mn(pyldach)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 387.99 _exptl_crystal_F_000 1044.00 _reflns_d_resolution_high 0.7983 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.8283 _cell_length_b 12.4842 _cell_length_c 14.1340 _cell_angle_alpha 97.971 _cell_angle_beta 91.017 _cell_angle_gamma 98.036 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 141.63 20.56 6.61 o 2 0 0 11471.15 9804.19 179.93 o 3 0 0 862.52 1426.33 35.59 o 4 0 0 5102.50 4811.28 73.16 o 5 0 0 1329.11 1448.23 83.72 o 6 0 0 3115.90 3121.34 57.81 o 7 0 0 15603.41 16073.24 142.68 o 8 0 0 435.34 290.82 61.32 o 9 0 0 3656.58 3589.76 109.56 o 10 0 0 2188.34 1990.95 146.51 o 11 0 0 320.62 331.21 87.39 o 12 0 0 165.53 117.14 74.91 o 13 0 0 306.84 366.46 104.28 o 14 0 0 180.87 198.65 95.47 o -14 1 0 195.71 160.83 88.49 o -13 1 0 15.57 52.88 69.40 o -12 1 0 82.74 135.13 70.87 o -11 1 0 2567.95 2280.30 159.00 o -10 1 0 3311.94 3234.65 177.72 o -9 1 0 550.38 621.57 49.43 o -8 1 0 3.75 1.24 14.31 o -7 1 0 30.75 57.31 14.54 o -6 1 0 2.50 -4.90 16.41 o -5 1 0 42.10 44.10 18.43 o -4 1 0 1679.40 1860.04 52.41 o -3 1 0 25121.29 29891.97 689.23 o -2 1 0 5715.15 9582.56 91.50 o -1 1 0 832.93 223.96 12.05 o 0 1 0 7581.45 5506.14 73.81 o 1 1 0 1929.35 825.83 33.78 o 2 1 0 408.68 192.78 24.97 o 3 1 0 1293.05 1752.64 73.81 o 4 1 0 3169.92 3385.98 74.17 o 5 1 0 150.08 183.39 19.50 o 6 1 0 6.58 42.93 15.24 o 7 1 0 3260.73 3134.54 72.87 o 8 1 0 2353.45 1513.22 114.57 o 9 1 0 3096.84 3170.02 170.75 o 10 1 0 1903.44 2016.80 96.19 o 11 1 0 846.92 942.97 120.44 o 12 1 0 11.04 46.63 66.10 o 13 1 0 8.26 16.52 68.30 o 14 1 0 336.48 258.51 106.12 o -14 2 0 1.39 -6.24 69.40 o -13 2 0 381.83 553.37 114.20 o -12 2 0 1025.62 971.97 126.32 o -11 2 0 906.99 914.32 113.83 o -10 2 0 1672.47 1646.15 128.15 o -9 2 0 2633.40 2715.46 75.97 o -8 2 0 369.20 347.59 24.63 o -7 2 0 1649.27 1601.59 47.07 o -6 2 0 19971.86 20825.58 186.15 o -5 2 0 15513.54 15283.83 195.70 o -4 2 0 39.52 24.38 7.89 o -3 2 0 8543.17 8733.06 107.23 o -2 2 0 10311.76 8897.87 101.35 o -1 2 0 12968.08 11103.49 107.41 o 0 2 0 18491.35 17611.94 182.13 o 1 2 0 9876.58 14215.33 114.38 o 2 2 0 49.84 162.30 26.07 o 3 2 0 3478.66 4417.40 123.01 o 4 2 0 37161.60 37551.17 422.28 o 5 2 0 255.94 356.55 52.51 o 6 2 0 1479.13 1696.09 107.59 o 7 2 0 9406.48 9258.17 252.63 o 8 2 0 332.18 278.70 64.26 o 9 2 0 1053.71 1075.89 109.43 o 10 2 0 7082.64 6873.59 264.02 o 11 2 0 1372.09 1374.34 93.27 o 12 2 0 230.77 275.03 92.90 o 13 2 0 11.04 24.60 72.71 o 14 2 0 10.25 -9.91 75.28 o -14 3 0 426.04 475.15 113.10 o -13 3 0 3.27 25.34 67.20 o -12 3 0 649.70 621.30 108.69 o -11 3 0 1394.48 1299.88 129.25 o -10 3 0 1909.34 1828.18 71.95 o -9 3 0 99.69 79.09 27.42 o -8 3 0 5.68 7.24 27.17 o -7 3 0 7005.85 7491.21 116.50 o -6 3 0 1685.49 1731.53 38.75 o -5 3 0 92.67 51.28 20.80 o -4 3 0 669.07 629.93 37.55 o -3 3 0 3416.35 2787.41 66.25 o -2 3 0 1133.52 741.94 56.92 o -1 3 0 13717.77 17096.39 215.55 o 0 3 0 8908.16 12471.16 167.44 o 1 3 0 37.14 27.17 15.42 o 2 3 0 1983.67 1344.43 36.09 o 3 3 0 1725.49 1379.93 75.64 o 4 3 0 0.16 36.72 27.54 o 5 3 0 463.01 390.70 57.28 o 6 3 0 4257.35 4439.80 168.18 o 7 3 0 4317.18 4096.83 176.99 o 8 3 0 2364.91 2674.67 156.06 o 9 3 0 2034.97 1874.18 139.54 o 10 3 0 746.84 748.35 107.59 o 11 3 0 3.19 35.99 59.49 o 12 3 0 89.61 66.59 57.47 o 13 3 0 116.89 62.79 78.21 o -14 4 0 3.55 -16.52 66.46 o -13 4 0 321.99 277.97 91.43 o -12 4 0 2181.77 2204.29 168.18 o -11 4 0 914.15 901.84 112.36 o -10 4 0 3616.82 3308.85 95.94 o -9 4 0 170.87 213.71 62.42 o -8 4 0 151.07 206.34 39.06 o -7 4 0 564.12 546.34 49.26 o -6 4 0 1157.41 1149.18 59.59 o -5 4 0 18978.69 20248.77 220.78 o -4 4 0 17.20 77.44 20.63 o -3 4 0 16792.46 18233.03 184.59 o -2 4 0 1178.99 1021.87 43.34 o -1 4 0 21302.89 27071.33 313.59 o 0 4 0 1384.03 1953.86 76.01 o 1 4 0 6185.80 5624.74 114.57 o 2 4 0 5331.11 6236.68 89.28 o 3 4 0 868.19 1191.71 30.40 o 4 4 0 34356.90 36965.49 465.24 o 5 4 0 262.23 192.04 50.67 o 6 4 0 1303.86 1429.14 107.96 o 7 4 0 8.16 10.28 38.19 o 8 4 0 32.14 76.01 54.71 o 9 4 0 8.22 30.48 53.61 o 10 4 0 1779.29 1552.51 141.00 o 11 4 0 2930.33 2822.65 192.78 o 12 4 0 127.78 56.42 50.79 o 13 4 0 10.27 55.08 72.34 o -14 5 0 327.62 388.86 107.96 o -13 5 0 14.70 -6.98 67.20 o -12 5 0 533.59 481.76 99.88 o -11 5 0 839.17 871.63 61.88 o -10 5 0 63.37 74.27 31.67 o -9 5 0 368.39 348.11 49.45 o -8 5 0 1565.69 1681.79 82.82 o -7 5 0 7635.29 7505.64 153.58 o -6 5 0 1801.21 1748.86 98.78 o -5 5 0 1333.29 1438.12 64.82 o -4 5 0 459.58 581.08 42.35 o -3 5 0 9022.90 10875.19 221.24 o -2 5 0 1446.44 912.86 67.20 o -1 5 0 8122.96 6897.82 158.63 o 0 5 0 167.05 405.02 44.80 o 1 5 0 4607.21 4981.05 124.11 o 2 5 0 400.69 464.51 34.04 o 3 5 0 2184.58 1897.13 42.89 o 4 5 0 1292.29 1117.25 40.89 o 5 5 0 86.81 37.82 42.23 o 6 5 0 1653.66 1635.13 120.44 o 7 5 0 1039.63 854.84 96.21 o 8 5 0 207.44 143.57 63.89 o 9 5 0 551.48 390.70 90.70 o 10 5 0 46.43 84.82 71.60 o 11 5 0 1046.58 906.61 125.21 o 12 5 0 262.06 157.25 59.85 o 13 5 0 332.48 457.31 81.67 o -14 6 0 223.42 309.92 105.75 o -13 6 0 135.66 156.43 85.19 o -12 6 0 128.52 195.81 57.69 o -11 6 0 676.49 795.40 62.15 o -10 6 0 1894.90 1680.55 75.47 o -9 6 0 3544.52 3325.98 120.86 o -8 6 0 3090.86 3409.07 164.14 o -7 6 0 201.24 156.92 37.22 o -6 6 0 1495.20 1324.72 70.13 o -5 6 0 2729.87 2275.97 84.47 o -4 6 0 3.90 0.85 20.65 o -3 6 0 13677.94 14526.70 185.50 o -2 6 0 6978.95 8421.33 200.86 o -1 6 0 4173.07 3536.12 125.95 o 0 6 0 15.22 -6.98 27.17 o 1 6 0 3845.48 3294.50 111.63 o 2 6 0 5912.53 5224.23 102.52 o 3 6 0 10415.59 10933.61 163.99 o 4 6 0 8302.62 8222.67 232.44 o 5 6 0 6386.86 6749.84 223.99 o 6 6 0 1923.31 1947.99 133.29 o 7 6 0 264.11 221.05 69.77 o 8 6 0 252.91 274.66 77.48 o 9 6 0 137.49 243.82 81.15 o 10 6 0 166.53 243.45 88.13 o 11 6 0 1887.26 2079.08 178.46 o 12 6 0 168.14 206.83 76.01 o -13 7 0 13.69 32.68 72.34 o -12 7 0 250.52 290.25 54.13 o -11 7 0 456.01 535.60 59.62 o -10 7 0 25.66 11.58 30.88 o -9 7 0 8.20 8.81 32.62 o -8 7 0 5714.61 5370.94 147.61 o -7 7 0 4106.24 4123.61 123.55 o -6 7 0 113.36 93.53 32.99 o -5 7 0 1421.44 1506.41 74.71 o -4 7 0 396.17 301.52 39.72 o -3 7 0 1654.94 1506.98 103.92 o -2 7 0 1086.48 1311.27 95.84 o -1 7 0 264.94 394.37 59.49 o 0 7 0 4451.29 4436.12 148.35 o 1 7 0 2201.69 1991.32 98.78 o 2 7 0 520.74 587.49 45.52 o 3 7 0 4274.77 4471.74 82.29 o 4 7 0 159.55 208.20 61.32 o 5 7 0 110.44 100.61 53.98 o 6 7 0 213.21 254.10 70.50 o 7 7 0 98.53 87.76 60.22 o 8 7 0 3.07 4.04 55.81 o 9 7 0 178.71 228.03 82.62 o 10 7 0 946.26 1090.58 138.07 o 11 7 0 977.15 1243.33 157.90 o 12 7 0 225.17 249.29 72.65 o -13 8 0 415.96 397.78 61.95 o -12 8 0 92.81 124.61 49.42 o -11 8 0 335.11 363.26 55.38 o -10 8 0 39.32 45.21 36.09 o -9 8 0 522.63 557.53 64.15 o -8 8 0 5013.45 4797.44 208.94 o -7 8 0 7.60 16.46 33.47 o -6 8 0 7423.18 7418.74 164.69 o -5 8 0 310.76 342.07 46.74 o -4 8 0 18.81 28.27 45.53 o -3 8 0 188.12 269.89 62.79 o -2 8 0 935.81 841.62 84.09 o -1 8 0 6459.98 6374.20 194.98 o 0 8 0 127.12 188.74 51.41 o 1 8 0 15590.58 16370.44 289.35 o 2 8 0 81.63 108.32 51.04 o 3 8 0 998.81 1104.90 106.85 o 4 8 0 6.87 7.71 40.02 o 5 8 0 1178.79 1098.66 109.79 o 6 8 0 2605.84 2641.26 167.44 o 7 8 0 122.94 131.09 71.97 o 8 8 0 1432.06 1520.20 142.84 o 9 8 0 10.68 9.55 62.42 o 10 8 0 197.34 159.73 85.92 o 11 8 0 2.97 -9.18 74.54 o -13 9 0 304.85 301.67 61.96 o -12 9 0 321.28 364.07 61.22 o -11 9 0 228.74 173.03 51.69 o -10 9 0 239.89 188.19 48.21 o -9 9 0 93.42 77.48 62.79 o -8 9 0 1164.95 1122.08 83.75 o -7 9 0 835.67 730.72 68.45 o -6 9 0 142.40 121.99 41.09 o -5 9 0 245.42 212.61 69.03 o -4 9 0 2786.49 2973.21 159.36 o -3 9 0 1164.44 1238.56 110.16 o -2 9 0 148.74 125.95 58.02 o -1 9 0 327.63 284.95 63.89 o 0 9 0 1276.06 1432.81 103.92 o 1 9 0 7.71 19.09 45.90 o 2 9 0 4187.28 4211.75 137.79 o 3 9 0 1329.01 1287.76 116.77 o 4 9 0 1215.36 1244.44 118.97 o 5 9 0 290.29 258.87 73.07 o 6 9 0 471.77 461.57 92.53 o 7 9 0 137.36 125.95 72.34 o 8 9 0 43.11 -27.17 56.18 o 9 9 0 168.74 290.45 94.00 o 10 9 0 1210.91 1201.84 155.69 o -12 10 0 41.78 38.75 46.47 o -11 10 0 145.05 153.66 51.02 o -10 10 0 332.90 285.63 55.67 o -9 10 0 368.50 376.01 86.29 o -8 10 0 1692.68 1787.04 102.73 o -7 10 0 63.38 68.10 44.14 o -6 10 0 152.20 61.32 64.99 o -5 10 0 4145.61 3940.41 193.15 o -4 10 0 3399.44 3123.76 169.28 o -3 10 0 350.19 377.48 77.11 o -2 10 0 1143.89 1063.41 105.02 o -1 10 0 4002.95 3692.55 171.85 o 0 10 0 226.54 186.90 63.89 o 2 10 0 1912.68 2239.91 150.18 o 3 10 0 706.91 853.00 106.12 o 4 10 0 18.72 -29.74 49.57 o 5 10 0 919.58 894.13 113.10 o 6 10 0 712.87 829.13 120.07 o 7 10 0 50.94 87.39 69.03 o 8 10 0 889.22 758.26 125.95 o 9 10 0 124.47 180.66 92.53 o -11 11 0 105.56 101.55 52.76 o -10 11 0 157.28 91.98 48.77 o -9 11 0 416.68 466.54 61.66 o -8 11 0 387.78 327.91 83.72 o -7 11 0 55.63 73.81 69.40 o -6 11 0 153.33 183.60 84.46 o -5 11 0 101.34 80.05 66.83 o -4 11 0 2422.74 2269.29 159.00 o -3 11 0 722.41 588.25 98.04 o -2 11 0 1314.13 1320.08 125.58 o -1 11 0 226.71 164.50 68.30 o 1 11 0 920.80 926.10 60.38 o 2 11 0 192.92 255.57 74.91 o 3 11 0 65.78 70.13 59.12 o 4 11 0 1820.47 1863.53 151.65 o 5 11 0 7.05 -29.74 56.92 o 6 11 0 553.55 708.33 119.71 o 7 11 0 515.28 559.61 116.03 o 8 11 0 23.08 -6.24 67.93 o -10 12 0 341.44 305.22 61.44 o -9 12 0 1366.54 1259.44 115.66 o -8 12 0 67.90 45.71 56.92 o -1 12 0 749.37 804.49 76.32 o 0 12 0 173.27 229.70 56.60 o 1 12 0 192.30 260.71 80.42 o 2 12 0 122.12 78.58 66.46 o 3 12 0 1446.59 1884.46 159.36 o 4 12 0 247.85 275.40 86.66 o 5 12 0 1592.02 1747.86 159.00 o 6 12 0 220.94 300.74 94.37 o -9 13 0 91.91 97.23 68.13 o -8 13 0 162.52 200.65 68.54 o -7 13 0 3.78 61.39 56.95 o -6 13 0 392.97 406.17 75.68 o -5 13 0 597.10 488.73 76.83 o -4 13 0 271.88 287.93 65.04 o -3 13 0 103.40 132.63 54.66 o -2 13 0 99.79 160.27 59.72 o -1 13 0 11.75 42.02 50.75 o 1 13 0 59.61 77.48 67.56 o 2 13 0 44.01 30.48 55.81 o 3 13 0 496.39 490.58 109.43 o 4 13 0 2.62 -1.10 59.12 o -8 14 0 322.57 372.48 86.24 o -7 14 0 29.46 19.96 60.70 o -6 14 0 10.42 36.89 63.20 o -5 14 0 642.04 676.79 92.25 o -4 14 0 963.03 921.73 100.35 o -3 14 0 300.93 220.71 66.17 o -2 14 0 426.14 428.76 76.86 o 0 14 0 320.01 423.75 98.41 o -5 15 0 5.73 -11.01 61.89 o -4 15 0 38.00 -0.92 68.85 o -3 15 0 4.89 53.87 57.50 o -2 15 0 6.76 3.13 50.10 o 2 -15 1 107.03 117.19 60.41 o 3 -15 1 420.78 458.70 79.71 o 4 -15 1 433.64 564.95 85.19 o 5 -15 1 146.37 169.97 69.79 o 1 -14 1 723.70 758.87 80.48 o 4 -14 1 28.13 -18.36 74.17 o 8 -14 1 374.89 363.55 82.43 o 1 -13 1 252.67 295.23 89.60 o 2 -13 1 1268.96 1363.77 136.23 o 3 -13 1 50.19 57.65 70.13 o 4 -13 1 1201.05 1156.67 136.60 o 5 -13 1 55.71 8.08 75.28 o 6 -13 1 144.99 190.21 94.37 o 7 -13 1 329.79 285.68 108.69 o -3 -12 1 117.96 126.68 68.30 o -2 -12 1 79.80 44.80 56.55 o -1 -12 1 312.24 337.46 84.09 o 0 -12 1 2830.35 3170.39 176.62 o 1 -12 1 54.42 17.26 57.28 o 2 -12 1 4.54 50.31 66.83 o 3 -12 1 29.69 31.21 67.20 o 4 -12 1 2.36 -21.30 66.10 o 5 -12 1 520.89 504.53 104.28 o 6 -12 1 113.82 135.86 78.58 o 7 -12 1 1255.24 1365.61 151.65 o 8 -12 1 847.04 980.42 133.66 o 9 -12 1 27.32 33.21 52.06 o 10 -12 1 105.68 50.67 70.50 o -6 -11 1 744.52 847.49 118.97 o -5 -11 1 33.58 57.65 55.45 o -4 -11 1 2747.62 2673.94 174.42 o -3 -11 1 9.12 66.46 57.28 o -2 -11 1 76.51 108.69 58.02 o -1 -11 1 1251.65 1469.02 85.05 o 0 -11 1 1849.00 1754.84 129.25 o 1 -11 1 926.19 1023.38 107.22 o 2 -11 1 2186.58 2014.45 144.68 o 3 -11 1 2784.53 2416.17 155.69 o 4 -11 1 1334.89 1338.07 127.79 o 5 -11 1 746.50 640.03 104.28 o 6 -11 1 416.76 352.88 92.53 o 7 -11 1 330.17 317.99 88.86 o 8 -11 1 1402.52 1506.59 99.52 o 9 -11 1 2123.14 2037.09 162.49 o 10 -11 1 31.26 38.19 66.83 o 11 -11 1 10.09 -11.73 42.04 o -9 -10 1 149.66 203.80 88.86 o -8 -10 1 4.58 44.43 63.89 o -7 -10 1 378.73 406.86 95.10 o -6 -10 1 1000.26 874.30 114.93 o -5 -10 1 946.60 870.26 107.59 o -4 -10 1 880.05 707.22 95.47 o -3 -10 1 8.40 0.00 44.80 o -2 -10 1 171.25 224.36 63.53 o -1 -10 1 782.64 870.63 93.64 o 0 -10 1 546.44 494.98 78.21 o 1 -10 1 1410.76 1402.33 113.83 o 2 -10 1 249.55 308.81 72.34 o 3 -10 1 4795.42 4581.53 202.33 o 4 -10 1 4571.58 4711.89 207.47 o 5 -10 1 19.72 60.59 61.32 o 6 -10 1 1487.54 1495.58 89.12 o 7 -10 1 1903.81 1835.65 99.85 o 8 -10 1 146.26 91.70 46.14 o 9 -10 1 266.89 235.34 56.55 o 10 -10 1 2.26 -7.17 44.64 o 11 -10 1 265.48 257.41 87.39 o 12 -10 1 380.03 391.71 64.51 o -10 -9 1 474.05 519.94 84.87 o -9 -9 1 90.75 109.43 76.38 o -8 -9 1 2.61 42.96 67.20 o -7 -9 1 144.93 95.47 68.67 o -6 -9 1 3744.60 3525.47 193.15 o -5 -9 1 2.75 12.48 47.00 o -4 -9 1 2577.83 2614.82 158.26 o -3 -9 1 654.49 812.61 94.74 o -2 -9 1 1022.27 876.62 61.51 o -1 -9 1 45.29 49.57 45.90 o 0 -9 1 12.47 29.38 44.43 o 1 -9 1 1697.96 1660.84 113.46 o 2 -9 1 244.53 331.21 67.20 o 3 -9 1 6185.32 5863.42 209.67 o 4 -9 1 1253.47 1241.86 111.26 o 5 -9 1 657.57 557.62 57.25 o 6 -9 1 1161.55 1089.05 74.60 o 7 -9 1 3.13 0.86 33.70 o 8 -9 1 67.28 67.95 41.76 o 9 -9 1 1887.86 1776.46 145.23 o 10 -9 1 1561.47 1432.79 97.74 o 11 -9 1 977.05 927.54 122.64 o 12 -9 1 150.67 148.73 50.18 o 13 -9 1 1052.85 1111.76 86.97 o -11 -8 1 139.31 110.32 60.04 o -10 -8 1 111.18 73.81 74.91 o -9 -8 1 77.44 42.23 58.75 o -8 -8 1 798.91 643.70 105.02 o -7 -8 1 255.99 300.37 79.68 o -6 -8 1 97.70 94.37 56.55 o -5 -8 1 6289.89 6529.89 235.01 o -4 -8 1 265.21 263.28 64.26 o -3 -8 1 56.89 39.78 26.71 o -2 -8 1 1.14 -3.11 24.40 o -1 -8 1 520.20 628.64 68.30 o 0 -8 1 198.36 188.01 50.67 o 1 -8 1 2692.64 2936.85 139.54 o 2 -8 1 3769.83 4180.19 166.71 o 3 -8 1 10616.21 11690.86 282.38 o 4 -8 1 3287.06 3075.01 277.05 o 5 -8 1 409.73 372.33 46.28 o 6 -8 1 208.73 170.84 39.08 o 7 -8 1 1643.33 1677.68 87.05 o 8 -8 1 247.04 223.00 47.41 o 9 -8 1 60.01 94.84 40.93 o 10 -8 1 1805.25 1850.91 103.06 o 11 -8 1 2166.86 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