# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 030902H in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 352.47 _exptl_crystal_F_000 1142.00 _reflns_d_resolution_high 0.7964 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.1973 _cell_length_b 12.3936 _cell_length_c 16.8968 _cell_angle_alpha 73.715 _cell_angle_beta 73.060 _cell_angle_gamma 86.618 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5117.69 2103.24 47.57 o 2 0 0 575.04 829.63 15.78 o 3 0 0 13.19 16.51 7.33 o 4 0 0 11810.81 11066.93 199.34 o 5 0 0 118.99 126.41 15.86 o 6 0 0 911.41 869.71 25.35 o 7 0 0 2789.61 2705.81 146.11 o 8 0 0 708.86 709.01 50.97 o 9 0 0 10.19 -33.98 33.98 o 10 0 0 358.13 391.88 46.44 o 11 0 0 8.09 9.06 41.91 o 12 0 0 66.15 67.96 45.30 o 13 0 0 0.01 -44.17 44.17 o -13 1 0 0.03 -46.44 46.44 o -12 1 0 11.88 -40.77 40.77 o -11 1 0 4.83 9.06 33.98 o -10 1 0 7.94 32.85 37.38 o -9 1 0 1088.77 1001.22 62.29 o -8 1 0 1173.93 1219.81 63.43 o -7 1 0 1.41 11.45 19.82 o -6 1 0 4774.42 4800.01 180.65 o -5 1 0 8912.92 8408.46 115.12 o -4 1 0 442.31 546.59 27.18 o -3 1 0 1.32 24.22 10.19 o -2 1 0 2416.56 1708.94 49.83 o -1 1 0 18753.90 17284.64 311.47 o 1 1 0 2156.75 2467.94 50.97 o 2 1 0 67.66 43.61 7.21 o 3 1 0 124235.59 109903.09 3221.12 o 4 1 0 9726.69 9419.70 228.79 o 5 1 0 786.15 628.92 27.18 o 6 1 0 2.70 -14.23 14.23 o 7 1 0 4.54 11.50 15.48 o 8 1 0 550.75 514.20 47.57 o 9 1 0 4.01 65.69 32.85 o 10 1 0 398.44 371.49 47.57 o 11 1 0 63.78 66.82 40.77 o 12 1 0 1.93 4.53 38.51 o 13 1 0 6.54 -33.98 47.57 o -13 2 0 27.23 13.59 40.77 o -12 2 0 0.17 -30.58 32.85 o -11 2 0 12.37 69.09 36.24 o -10 2 0 156.55 96.27 35.11 o -9 2 0 19.46 -10.19 30.58 o -8 2 0 769.48 856.25 54.36 o -7 2 0 0.94 -6.67 31.71 o -6 2 0 7784.64 7580.67 108.49 o -5 2 0 6784.07 6982.07 99.07 o -4 2 0 7.08 -1.13 9.42 o -3 2 0 8747.01 9821.52 126.51 o -2 2 0 216.19 475.18 13.61 o -1 2 0 674.65 426.55 14.72 o 0 2 0 737.46 627.46 21.52 o 1 2 0 142.21 49.83 10.19 o 3 2 0 43.80 54.36 23.22 o 4 2 0 1623.74 1633.98 34.99 o 5 2 0 732.06 675.71 37.38 o 6 2 0 10346.51 9894.39 139.54 o 7 2 0 3.39 7.28 16.59 o 8 2 0 59.49 100.80 33.98 o 9 2 0 324.83 271.82 41.91 o 10 2 0 10.65 -37.38 39.64 o 11 2 0 3.06 -29.45 36.24 o 12 2 0 24.37 -22.65 39.64 o 13 2 0 17.33 35.11 50.97 o -13 3 0 0.81 7.93 40.77 o -12 3 0 194.65 161.96 41.91 o -11 3 0 248.17 253.70 47.57 o -10 3 0 71.44 97.40 38.51 o -9 3 0 339.75 416.80 46.44 o -8 3 0 28.07 57.76 29.45 o -7 3 0 1333.66 1297.79 34.27 o -6 3 0 1024.44 1030.37 29.39 o -5 3 0 685.55 720.54 31.15 o -4 3 0 10867.44 10970.64 237.28 o -3 3 0 22487.43 21174.47 259.18 o -2 3 0 1903.53 1972.60 39.07 o -1 3 0 1013.25 1254.78 26.82 o 0 3 0 10871.92 10255.23 136.15 o 1 3 0 7323.66 7504.74 182.35 o 2 3 0 5029.31 5167.94 74.36 o 3 3 0 2559.39 2676.86 48.03 o 4 3 0 0.95 23.62 13.86 o 5 3 0 14647.37 13900.12 235.58 o 6 3 0 643.73 748.93 30.21 o 7 3 0 474.66 414.78 25.29 o 8 3 0 24.03 16.99 31.71 o 9 3 0 149.66 86.08 41.91 o 10 3 0 20.29 -39.64 39.64 o 11 3 0 2.23 18.12 45.30 o 12 3 0 30.28 -3.40 44.17 o 13 3 0 0.23 0.00 53.23 o -13 4 0 77.45 74.75 48.70 o -12 4 0 29.10 27.18 41.91 o -11 4 0 171.51 175.55 44.17 o -10 4 0 34.29 61.16 35.11 o -9 4 0 1655.88 1772.52 78.15 o -8 4 0 89.09 50.97 32.85 o -7 4 0 207.42 253.74 20.67 o -6 4 0 4.24 -5.75 15.96 o -5 4 0 321.98 330.29 30.58 o -4 4 0 5442.86 6053.53 89.27 o -3 4 0 2231.14 2350.69 36.54 o -2 4 0 4320.13 4262.01 69.66 o -1 4 0 20282.09 20177.48 259.87 o 0 4 0 259.16 314.18 15.06 o 1 4 0 3.56 -0.23 9.42 o 2 4 0 835.51 801.31 31.71 o 3 4 0 2611.69 2680.71 50.01 o 4 4 0 4242.95 3715.15 65.67 o 5 4 0 391.41 433.57 53.23 o 6 4 0 931.36 861.69 33.38 o 7 4 0 239.76 165.89 23.06 o 8 4 0 808.33 755.45 60.03 o 9 4 0 10.99 44.17 37.38 o 10 4 0 0.13 -14.72 44.17 o 11 4 0 2.35 -38.51 46.44 o 12 4 0 24.78 20.39 52.10 o -12 5 0 0.67 49.83 44.17 o -11 5 0 15.22 15.86 40.77 o -10 5 0 2460.60 2679.74 103.07 o -9 5 0 727.05 720.33 54.36 o -8 5 0 32.11 72.49 33.98 o -7 5 0 760.96 883.19 49.83 o -6 5 0 1936.52 2069.22 47.61 o -5 5 0 19.48 35.20 15.48 o -4 5 0 46.01 56.32 13.69 o -3 5 0 2778.03 2850.49 56.42 o -2 5 0 4170.80 4416.90 81.55 o -1 5 0 3832.39 3573.12 63.21 o 0 5 0 148.58 147.18 11.28 o 1 5 0 3681.13 3360.34 55.51 o 2 5 0 7536.32 7487.50 107.22 o 3 5 0 775.53 692.34 27.09 o 4 5 0 0.76 2.27 16.82 o 5 5 0 421.12 429.09 43.04 o 6 5 0 54.65 87.54 23.22 o 7 5 0 87.45 77.00 24.18 o 8 5 0 0.03 -19.25 33.98 o 9 5 0 116.51 148.37 45.30 o 10 5 0 0.72 72.49 40.77 o 11 5 0 6.37 -3.40 49.83 o 12 5 0 0.48 -4.53 47.57 o -12 6 0 132.24 150.64 48.70 o -11 6 0 224.76 156.30 46.44 o -10 6 0 8.03 -27.18 37.38 o -9 6 0 50.33 178.95 39.64 o -8 6 0 730.87 885.69 56.63 o -7 6 0 13367.13 14150.73 277.49 o -6 6 0 156.95 153.55 21.51 o -5 6 0 58.56 106.23 18.63 o -4 6 0 160.54 203.12 15.96 o -3 6 0 76.78 119.63 18.42 o -2 6 0 614.51 641.17 26.43 o -1 6 0 67.30 75.43 18.42 o 0 6 0 5778.24 5720.33 78.32 o 1 6 0 4646.48 4245.19 68.85 o 2 6 0 39.79 62.33 17.56 o 3 6 0 1568.24 1317.36 37.23 o 4 6 0 6.92 -17.30 20.95 o 5 6 0 961.02 983.38 45.87 o 6 6 0 32.43 9.88 28.32 o 7 6 0 3.16 55.65 32.85 o 8 6 0 85.46 80.33 50.40 o 9 6 0 20.53 -19.25 43.04 o 10 6 0 0.52 32.85 47.57 o 11 6 0 10.53 96.27 53.23 o 12 6 0 0.25 -29.45 49.83 o -12 7 0 11.18 11.33 47.57 o -11 7 0 0.62 60.36 32.85 o -10 7 0 28.74 65.87 39.64 o -9 7 0 140.21 135.03 29.16 o -8 7 0 4447.68 4471.78 111.56 o -7 7 0 217.72 204.63 26.43 o -6 7 0 524.66 725.20 74.29 o -5 7 0 24.81 -10.29 18.16 o -4 7 0 11758.69 11702.71 153.88 o -3 7 0 213.77 221.73 22.38 o -2 7 0 319.29 302.92 24.34 o -1 7 0 2054.93 2079.82 52.10 o 0 7 0 170.52 212.96 15.01 o 1 7 0 97.40 134.49 16.61 o 2 7 0 177.07 202.97 24.92 o 3 7 0 3319.73 2918.70 60.61 o 4 7 0 344.71 270.17 24.48 o 5 7 0 44.69 48.70 35.11 o 6 7 0 99.50 92.43 37.94 o 7 7 0 1.88 -10.90 23.18 o 8 7 0 49.46 78.42 26.28 o 9 7 0 3.15 -14.72 43.04 o 10 7 0 1.54 32.85 41.91 o 11 7 0 3.55 15.86 50.97 o -11 8 0 1.25 75.88 47.57 o -10 8 0 524.47 497.21 60.03 o -9 8 0 3.55 67.96 37.38 o -8 8 0 58.55 76.45 27.23 o -7 8 0 63.19 88.84 28.32 o -6 8 0 1609.99 1678.05 58.09 o -5 8 0 15223.61 15572.01 179.57 o -4 8 0 137.21 176.02 31.12 o -3 8 0 1815.94 2111.92 57.66 o -2 8 0 126.73 50.55 21.58 o -1 8 0 1197.84 1266.36 42.71 o 0 8 0 2.46 -35.25 39.07 o 1 8 0 3.68 20.80 15.26 o 2 8 0 1370.01 1355.96 37.92 o 3 8 0 698.35 657.53 43.61 o 4 8 0 417.36 418.86 28.30 o 5 8 0 628.20 582.65 56.06 o 6 8 0 13.40 13.16 23.18 o 7 8 0 68.28 42.57 29.45 o 8 8 0 0.00 -6.05 49.83 o 9 8 0 16.00 7.93 47.57 o 10 8 0 0.01 -48.70 48.70 o 11 8 0 0.55 -36.24 52.10 o -10 9 0 290.02 351.11 57.76 o -9 9 0 23.95 62.29 44.17 o -8 9 0 4.22 18.12 39.64 o -7 9 0 366.71 296.74 48.70 o -6 9 0 1024.35 1019.80 46.45 o -5 9 0 7.12 44.17 26.43 o -4 9 0 1488.33 1487.42 96.27 o -3 9 0 9.07 5.98 53.80 o -2 9 0 7297.28 7163.16 126.51 o -1 9 0 43.31 6.26 25.14 o 0 9 0 1080.64 943.12 46.44 o 1 9 0 119.47 121.19 39.64 o 2 9 0 243.56 232.18 43.04 o 3 9 0 15.89 -16.99 33.98 o 4 9 0 11.20 -6.80 29.45 o 5 9 0 642.10 697.68 55.50 o 6 9 0 0.14 22.65 36.24 o 7 9 0 2.17 -5.72 25.14 o 8 9 0 32.37 -1.08 28.42 o 9 9 0 0.04 23.78 46.44 o 10 9 0 1.74 -1.13 55.50 o -10 10 0 35.74 137.04 52.10 o -9 10 0 219.99 252.57 54.36 o -8 10 0 661.62 746.38 69.09 o -7 10 0 148.75 165.36 46.44 o -6 10 0 24.49 19.42 68.52 o -5 10 0 15.22 -16.65 26.75 o -4 10 0 1228.81 1341.93 52.04 o -3 10 0 3059.10 2922.00 105.90 o -2 10 0 393.93 465.49 36.38 o -1 10 0 1656.87 1706.17 57.76 o 0 10 0 61.91 81.15 27.55 o 1 10 0 316.62 383.95 49.83 o 2 10 0 9.56 -32.85 32.85 o 3 10 0 53.28 15.86 33.98 o 4 10 0 21.88 -36.24 36.24 o 5 10 0 20.61 30.58 39.64 o 6 10 0 46.40 45.30 41.91 o 7 10 0 8.28 73.62 43.04 o 8 10 0 3.73 58.90 49.83 o -9 11 0 65.37 -7.93 49.83 o -8 11 0 321.69 371.49 58.90 o -7 11 0 25.94 19.25 46.44 o -6 11 0 266.63 251.68 35.80 o -5 11 0 318.75 317.99 36.43 o -4 11 0 12.10 2.22 29.03 o -3 11 0 1.65 -8.06 28.88 o -2 11 0 316.12 336.42 33.86 o -1 11 0 6.23 15.86 36.24 o 0 11 0 657.82 783.76 63.43 o 1 11 0 140.77 141.58 41.91 o 2 11 0 476.47 496.08 56.63 o 3 11 0 37.45 147.24 45.30 o 4 11 0 84.95 122.32 45.30 o 5 11 0 2.24 -7.93 36.24 o 6 11 0 28.80 61.16 46.44 o 7 11 0 46.34 144.97 48.70 o 8 11 0 0.79 50.97 48.70 o -8 12 0 19.50 -15.86 50.97 o -7 12 0 477.59 522.13 67.96 o -6 12 0 331.61 344.31 58.90 o -5 12 0 22.85 95.19 38.04 o -4 12 0 39.85 116.66 49.83 o -3 12 0 46.61 -16.99 41.91 o -2 12 0 501.63 574.23 58.90 o -1 12 0 85.31 95.14 41.91 o 0 12 0 62.14 66.82 45.30 o 1 12 0 167.65 186.88 49.83 o 2 12 0 2.14 -22.65 37.38 o 3 12 0 0.98 62.29 45.30 o 4 12 0 4.37 20.39 46.44 o 5 12 0 29.70 -23.78 44.17 o 6 12 0 0.20 30.58 43.04 o 7 12 0 0.95 -3.40 49.83 o -5 13 0 1.75 -24.92 60.03 o -4 13 0 292.35 289.95 63.43 o -3 13 0 84.39 112.13 54.36 o -2 13 0 21.18 5.66 49.83 o -1 13 0 7.11 -16.99 46.44 o 0 13 0 0.02 47.57 48.70 o 1 13 0 1.86 -26.05 47.57 o 2 13 0 13.02 -2.27 47.57 o 3 13 0 19.04 27.18 44.17 o 4 13 0 14.68 87.21 44.17 o 5 13 0 22.91 20.39 50.97 o 6 13 0 0.29 37.38 52.10 o -4 14 0 92.85 106.46 65.69 o -3 14 0 35.72 129.12 63.43 o -2 14 0 59.01 129.12 58.90 o -1 14 0 20.67 47.57 56.63 o 0 14 0 54.94 88.34 55.50 o 1 14 0 3.06 31.71 49.83 o 2 14 0 13.55 -31.71 46.44 o 3 14 0 0.97 -41.91 53.23 o 4 14 0 0.40 33.98 56.63 o -3 -14 1 0.90 55.50 56.63 o -2 -14 1 3.72 46.44 49.83 o -1 -14 1 170.25 161.96 58.90 o 0 -14 1 35.76 52.10 56.63 o 1 -14 1 18.67 77.02 55.50 o 2 -14 1 22.84 14.72 56.63 o 3 -14 1 12.97 35.11 55.50 o 4 -14 1 4.55 97.40 63.43 o -5 -13 1 22.83 -7.93 52.10 o -4 -13 1 1.94 38.51 45.30 o -3 -13 1 2.56 54.36 49.83 o -2 -13 1 29.33 63.43 43.04 o -1 -13 1 37.90 123.45 45.30 o 0 -13 1 3.42 -21.52 48.70 o 1 -13 1 1.48 21.52 44.17 o 2 -13 1 85.60 97.40 49.83 o 3 -13 1 23.74 107.60 54.36 o 4 -13 1 90.25 134.78 58.90 o 5 -13 1 262.97 410.00 67.96 o -7 -12 1 23.56 67.96 53.23 o -6 -12 1 26.54 72.49 49.83 o -5 -12 1 80.09 60.03 48.70 o -4 -12 1 4.96 38.51 41.91 o -3 -12 1 0.01 -4.53 43.04 o -2 -12 1 19.50 -15.86 43.04 o -1 -12 1 1.68 12.46 45.30 o 0 -12 1 36.96 35.11 45.30 o 1 -12 1 577.66 534.59 61.16 o 2 -12 1 63.02 33.98 45.30 o 3 -12 1 161.52 296.74 56.63 o 4 -12 1 122.15 117.13 37.18 o 5 -12 1 90.44 106.77 39.64 o 6 -12 1 10.81 -9.06 48.70 o 7 -12 1 49.17 22.65 52.10 o 8 -12 1 148.89 209.53 57.76 o -8 -11 1 0.03 64.56 52.10 o -7 -11 1 5.24 16.99 47.57 o -6 -11 1 20.26 32.85 45.30 o -5 -11 1 49.72 82.68 45.30 o -4 -11 1 130.96 209.53 48.70 o -3 -11 1 134.06 126.85 45.30 o -2 -11 1 162.06 210.66 47.57 o -1 -11 1 196.85 282.02 49.83 o 0 -11 1 2.00 47.57 43.04 o 1 -11 1 315.56 244.45 37.94 o 2 -11 1 32.97 24.44 45.30 o 3 -11 1 62.05 59.53 29.39 o 4 -11 1 141.18 104.83 29.96 o 5 -11 1 3.42 -32.03 32.03 o 6 -11 1 410.36 371.49 55.50 o 7 -11 1 558.57 526.66 60.03 o 8 -11 1 5.65 -29.45 46.44 o 9 -11 1 42.03 5.66 48.70 o -8 -10 1 0.05 35.11 46.44 o -7 -10 1 0.51 -24.92 41.91 o -6 -10 1 1.54 0.00 39.64 o -5 -10 1 82.01 70.22 40.77 o -4 -10 1 13.55 -1.13 39.64 o -3 -10 1 529.92 482.49 54.36 o -2 -10 1 327.52 292.21 47.57 o -1 -10 1 0.64 -7.93 32.85 o 0 -10 1 47.62 69.23 26.02 o 1 -10 1 5.35 12.89 25.80 o 2 -10 1 418.70 448.00 43.61 o 3 -10 1 477.00 447.51 36.43 o 4 -10 1 45.41 45.11 28.42 o 5 -10 1 320.19 335.53 34.03 o 6 -10 1 39.51 -42.47 42.47 o 7 -10 1 49.45 78.15 41.91 o 8 -10 1 262.07 192.54 50.97 o 9 -10 1 108.63 112.13 50.97 o 10 -10 1 99.30 161.96 54.36 o -8 -9 1 8.25 70.22 46.44 o -7 -9 1 0.59 58.90 39.64 o -6 -9 1 26.18 39.64 32.85 o -5 -9 1 0.10 37.38 36.24 o -4 -9 1 155.56 234.45 39.64 o -3 -9 1 156.53 97.40 33.98 o -2 -9 1 536.17 473.43 46.44 o -1 -9 1 88.07 5.66 31.71 o 0 -9 1 1383.13 1536.71 50.62 o 1 -9 1 1696.44 1608.06 52.42 o 2 -9 1 44.99 30.66 32.28 o 3 -9 1 11.46 32.28 26.62 o 4 -9 1 74.30 40.18 26.82 o 5 -9 1 452.12 409.39 68.52 o 6 -9 1 32.80 -11.47 26.93 o 7 -9 1 7.22 -19.25 36.24 o 8 -9 1 523.27 455.31 56.63 o 9 -9 1 187.70 144.97 43.04 o 10 -9 1 30.62 22.65 39.64 o -10 -8 1 0.15 7.93 49.83 o -9 -8 1 3.45 46.44 45.30 o -8 -8 1 147.23 90.80 50.40 o -7 -8 1 2.30 -24.83 24.83 o -6 -8 1 43.50 52.55 25.22 o -5 -8 1 79.01 50.73 27.75 o -4 -8 1 70.26 90.64 22.31 o -3 -8 1 36.21 6.80 32.85 o -2 -8 1 103.14 89.48 35.11 o -1 -8 1 2148.91 1856.33 78.15 o 0 -8 1 631.67 577.76 32.25 o 1 -8 1 220.85 141.10 26.82 o 2 -8 1 2317.56 2433.15 62.06 o 3 -8 1 4.70 -22.81 22.81 o 4 -8 1 1121.97 1188.03 74.19 o 5 -8 1 134.35 70.70 104.20 o 6 -8 1 1056.65 1070.62 73.05 o 7 -8 1 192.37 215.19 45.30 o 8 -8 1 47.17 16.99 38.51 o 9 -8 1 18.29 46.44 41.91 o 10 -8 1 212.16 161.96 47.57 o 11 -8 1 72.95 120.06 47.57 o -11 -7 1 2.27 -35.11 53.23 o -10 -7 1 0.16 52.10 47.57 o -9 -7 1 26.42 19.25 37.38 o -8 -7 1 67.64 148.37 43.04 o -7 -7 1 29.50 63.48 25.14 o -6 -7 1 18.04 11.33 23.23 o -5 -7 1 154.28 120.91 28.88 o -4 -7 1 21.56 19.46 19.61 o -3 -7 1 549.68 486.85 26.67 o -2 -7 1 2879.59 2942.36 57.66 o -1 -7 1 47.87 10.88 14.23 o 0 -7 1 719.99 680.36 20.50 o 1 -7 1 26.04 11.53 20.39 o 2 -7 1 3064.64 2810.74 63.27 o 3 -7 1 1457.59 1280.38 29.68 o 4 -7 1 9.26 -9.31 15.81 o 5 -7 1 4261.00 4395.25 66.79 o 6 -7 1 213.81 209.79 38.50 o 7 -7 1 278.22 312.97 30.15 o 8 -7 1 0.11 -24.92 47.57 o 9 -7 1 522.00 543.08 59.46 o 10 -7 1 263.71 288.96 35.21 o 11 -7 1 0.31 -33.98 33.98 o 12 -7 1 11.00 15.86 45.30 o -11 -6 1 1.46 -47.57 49.83 o -10 -6 1 0.07 -38.51 46.44 o -9 -6 1 2.28 50.97 43.04 o -8 -6 1 73.73 70.12 26.02 o -7 -6 1 190.64 178.08 27.09 o -6 -6 1 1061.98 925.04 38.84 o -5 -6 1 0.15 -21.45 21.45 o -4 -6 1 1040.87 1081.46 37.08 o -3 -6 1 756.23 751.65 30.45 o -2 -6 1 809.60 721.90 28.88 o -1 -6 1 1073.92 1072.99 28.27 o 0 -6 1 107.22 149.53 12.00 o 1 -6 1 10006.47 10086.81 148.56 o 2 -6 1 51.84 -6.66 16.40 o 3 -6 1 1273.58 1131.23 26.07 o 4 -6 1 2718.89 2604.48 43.94 o 5 -6 1 0.66 -18.71 23.90 o 6 -6 1 139.93 198.56 19.96 o 7 -6 1 11.09 -22.11 69.66 o 8 -6 1 3722.90 3623.07 81.75 o 9 -6 1 63.09 24.23 25.22 o 10 -6 1 21.23 22.65 39.64 o 11 -6 1 35.62 54.36 44.17 o 12 -6 1 1.38 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