Acta Cryst. (2007). E63, m2618  [ doi:10.1107/S1600536807046272 ]

Bis(-N,2-di-3-pyridylisoindoline-1-imine-²N,N')bis[aqua(perchlorato-O)cadmium(II)] bis(perchlorate) methanol disolvate

L.-N. Zhu, S. Gao and S. W. Ng

Key indicators

• Single-crystal X-ray study
• T = 295 K
• Mean (C-C) = 0.008 Å
• R factor = 0.056
• wR factor = 0.181
• Data-to-parameter ratio = 16.7

checkCIF/PLATON results

No syntax errors found




Alert level B
ABSTM02_ALERT_3_B  The ratio of expected to reported Tmax/Tmin(RR') is < 0.75
            Tmin and Tmax reported:      0.399     0.842
            Tmin(prime) and Tmax expected:      0.781     0.836
            RR(prime) =      0.507
            Please check that your absorption correction is appropriate.
PLAT061_ALERT_3_B Tmax/Tmin Range Test RR' too Large .............       0.50      
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for        Cl1     

Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT230_ALERT_2_C Hirshfeld Test Diff for    Cl1    -   O1      ..       6.11 su   
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        Cl2     
PLAT720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........          2      

Alert level G
PLAT794_ALERT_5_G Check Predicted Bond Valency for Cd1         (2)       1.97      
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......         17      

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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