# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1 in Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 299.95 _exptl_crystal_F_000 1432.00 _reflns_d_resolution_high 0.8405 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 8.5905 _cell_length_b 14.8361 _cell_length_c 20.9045 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6612.86 6929.04 86.54 o 4 0 0 20442.93 20192.60 244.94 o 6 0 0 7643.40 7436.66 117.17 o 8 0 0 1466.77 1499.31 53.11 o 2 1 0 15517.20 15301.02 122.88 o 4 1 0 7583.90 7676.77 75.65 o 6 1 0 610.13 590.88 24.28 o 8 1 0 3198.33 3380.83 57.10 o 10 1 0 445.16 392.47 44.29 o 0 2 0 23460.24 23407.85 365.68 o 2 2 0 89967.95 81550.61 704.12 o 4 2 0 2631.90 2496.49 34.96 o 6 2 0 7.87 -9.31 11.58 o 8 2 0 376.40 381.90 24.66 o 10 2 0 221.64 240.02 40.82 o 2 3 0 4894.85 5240.49 68.62 o 4 3 0 10250.42 11807.15 106.82 o 6 3 0 475.87 502.74 20.54 o 8 3 0 32.41 11.73 17.95 o 10 3 0 108.42 83.59 65.85 o 0 4 0 64.32 48.27 6.95 o 2 4 0 3149.79 3455.17 38.03 o 4 4 0 45.26 103.26 11.69 o 6 4 0 25.64 -0.82 10.77 o 8 4 0 1103.47 1063.75 51.61 o 2 5 0 9922.28 8813.96 102.95 o 4 5 0 21286.56 21378.18 256.44 o 6 5 0 10962.23 11146.00 134.29 o 8 5 0 3993.55 4045.63 98.73 o 0 6 0 10652.91 10717.78 109.75 o 2 6 0 838.08 1112.96 18.83 o 4 6 0 7648.85 7393.96 92.53 o 6 6 0 6899.92 7044.30 245.19 o 8 6 0 460.09 522.57 45.53 o 2 7 0 8330.64 7709.25 93.46 o 4 7 0 11086.12 11556.33 166.55 o 6 7 0 8053.42 8025.18 140.64 o 8 7 0 1580.04 1552.00 64.23 o 0 8 0 1468.92 1369.58 29.03 o 2 8 0 28.34 12.14 6.23 o 4 8 0 980.42 991.97 41.32 o 6 8 0 2234.59 2306.77 70.38 o 8 8 0 199.77 228.14 38.43 o 2 9 0 770.72 771.87 21.31 o 4 9 0 1572.37 1637.29 53.75 o 6 9 0 1008.66 876.75 60.95 o 8 9 0 50.66 -23.48 28.20 o 0 10 0 18186.92 18436.31 187.61 o 2 10 0 12.62 9.27 10.52 o 4 10 0 7186.58 7232.90 127.86 o 6 10 0 2264.83 2159.35 72.26 o 8 10 0 3.27 22.69 31.48 o 2 11 0 9305.15 9064.25 109.35 o 4 11 0 2002.87 2037.62 52.96 o 6 11 0 396.44 482.80 43.32 o 0 12 0 13963.88 14267.03 202.03 o 2 12 0 52.39 25.99 13.18 o 4 12 0 5320.55 5384.48 83.01 o 6 12 0 1336.49 1264.60 59.21 o 2 13 0 1173.32 1267.38 36.13 o 4 13 0 96.06 99.16 21.10 o 6 13 0 1220.53 1224.51 61.29 o 0 14 0 1681.65 1691.11 58.54 o 2 14 0 63.09 50.05 21.65 o 4 14 0 342.56 416.86 32.62 o 6 14 0 2.85 -15.95 43.40 o 2 15 0 1824.16 1831.81 55.58 o 4 15 0 16.00 28.18 26.15 o 0 16 0 195.78 169.91 45.46 o 2 16 0 0.45 12.49 30.84 o 4 16 0 407.59 423.78 91.67 o 2 17 0 1130.24 1186.64 126.13 o 1 1 1 13361.22 13430.78 202.48 o 2 1 1 1241.85 1241.39 24.72 o 3 1 1 2830.87 2888.72 28.44 o 4 1 1 1163.49 1312.54 17.33 o 5 1 1 299.64 333.41 11.43 o 6 1 1 7.15 8.67 7.79 o 7 1 1 2927.01 2917.47 34.76 o 8 1 1 49.15 66.57 11.99 o 9 1 1 3.04 -0.43 16.80 o 10 1 1 6.91 15.04 22.51 o 0 2 1 22750.92 22228.37 648.25 o 1 2 1 30615.54 29306.57 306.49 o 2 2 1 50485.00 48636.13 409.61 o 3 2 1 4662.18 4834.29 39.54 o 4 2 1 289.15 224.06 13.47 o 5 2 1 10685.38 10873.73 73.91 o 6 2 1 1591.84 1617.05 27.84 o 7 2 1 190.49 198.14 12.75 o 8 2 1 790.13 750.80 20.57 o 9 2 1 2466.23 2507.56 48.03 o 10 2 1 456.86 501.44 33.91 o 1 3 1 33040.65 32657.96 178.74 o 2 3 1 74373.16 70548.97 404.62 o 3 3 1 11614.29 11315.06 80.28 o 4 3 1 1258.88 1186.37 16.48 o 5 3 1 645.52 738.50 14.88 o 6 3 1 929.12 878.87 17.89 o 7 3 1 4727.39 4681.88 45.98 o 8 3 1 876.61 917.93 29.20 o 9 3 1 6.86 -3.82 18.88 o 10 3 1 10.35 -5.94 21.66 o 0 4 1 5184.74 5719.85 64.32 o 1 4 1 7368.55 7309.36 58.65 o 2 4 1 49.76 37.26 5.90 o 3 4 1 597.71 564.58 12.85 o 4 4 1 7685.53 7634.58 57.41 o 5 4 1 4001.90 3721.91 37.63 o 6 4 1 1263.27 1278.32 21.06 o 7 4 1 127.55 128.13 15.99 o 8 4 1 327.79 351.93 26.63 o 9 4 1 2492.89 2695.97 66.29 o 1 5 1 5695.65 5843.27 32.65 o 2 5 1 480.37 446.49 10.19 o 3 5 1 26.16 23.22 7.86 o 4 5 1 873.44 1028.48 18.05 o 5 5 1 167.26 179.36 10.26 o 6 5 1 427.34 478.66 18.87 o 7 5 1 2528.94 2522.19 44.61 o 8 5 1 58.58 57.22 19.67 o 9 5 1 253.08 255.56 40.60 o 0 6 1 713.51 724.68 13.09 o 1 6 1 24.64 19.03 4.47 o 2 6 1 586.48 779.94 13.71 o 3 6 1 587.01 767.63 15.77 o 4 6 1 2451.65 2457.16 32.44 o 5 6 1 466.40 519.43 19.67 o 6 6 1 40.93 72.88 17.83 o 7 6 1 50.71 34.57 16.48 o 8 6 1 37.20 12.04 18.70 o 9 6 1 33.59 25.40 21.77 o 1 7 1 935.10 830.87 10.63 o 2 7 1 3156.61 3123.00 36.33 o 3 7 1 2731.35 2659.18 39.41 o 4 7 1 63.33 71.97 24.95 o 5 7 1 614.17 698.16 27.05 o 6 7 1 145.45 150.71 20.06 o 7 7 1 2169.37 2135.50 49.79 o 8 7 1 317.73 303.30 27.82 o 9 7 1 337.21 295.06 30.17 o 0 8 1 1623.68 1350.15 20.53 o 1 8 1 4340.03 3976.75 27.69 o 2 8 1 1070.65 1186.67 15.18 o 3 8 1 1159.38 1132.74 23.85 o 4 8 1 4431.25 4380.68 62.55 o 5 8 1 6704.40 6760.11 86.96 o 6 8 1 4401.95 4160.50 104.37 o 7 8 1 746.26 716.59 36.16 o 8 8 1 44.50 34.81 20.92 o 9 8 1 1437.57 1523.16 49.07 o 1 9 1 6805.85 6921.11 46.53 o 2 9 1 3221.30 3220.01 30.27 o 3 9 1 9580.68 9657.98 85.43 o 4 9 1 317.10 327.06 19.48 o 5 9 1 397.18 378.59 25.13 o 6 9 1 82.62 75.75 19.18 o 7 9 1 1506.63 1599.83 48.28 o 8 9 1 1039.30 1022.02 50.40 o 0 10 1 94.26 67.77 13.29 o 1 10 1 2257.46 2304.92 24.74 o 2 10 1 43.05 22.84 7.70 o 3 10 1 32.15 8.81 9.45 o 4 10 1 1149.76 1215.96 31.42 o 5 10 1 2907.14 3086.40 58.69 o 6 10 1 761.36 781.81 33.15 o 7 10 1 107.29 75.16 24.07 o 8 10 1 203.82 231.63 27.56 o 1 11 1 1347.70 1316.50 21.14 o 2 11 1 461.30 482.88 14.33 o 3 11 1 1989.92 1981.81 30.53 o 4 11 1 81.42 107.49 17.03 o 5 11 1 779.72 709.60 30.87 o 6 11 1 24.95 16.48 18.34 o 7 11 1 520.36 611.42 36.14 o 0 12 1 0.93 14.11 13.73 o 1 12 1 149.08 142.21 10.62 o 2 12 1 59.73 33.16 9.75 o 3 12 1 812.51 802.69 21.72 o 4 12 1 541.72 579.53 22.53 o 5 12 1 0.34 0.91 18.03 o 6 12 1 26.32 -23.53 19.74 o 7 12 1 59.94 43.58 27.73 o 1 13 1 784.52 777.90 20.40 o 2 13 1 1700.34 1681.88 27.23 o 3 13 1 1101.36 1102.36 25.14 o 4 13 1 437.05 425.94 32.36 o 5 13 1 27.56 27.25 18.81 o 6 13 1 243.18 296.71 28.80 o 0 14 1 644.97 652.51 31.48 o 1 14 1 3803.10 3778.88 48.31 o 2 14 1 91.86 80.99 16.00 o 3 14 1 989.45 973.20 24.87 o 4 14 1 959.70 932.22 29.65 o 5 14 1 1871.40 2009.21 47.19 o 6 14 1 24.09 -15.53 23.55 o 1 15 1 423.63 502.47 25.03 o 2 15 1 434.98 468.64 29.60 o 3 15 1 2140.92 2207.70 48.76 o 4 15 1 4.78 4.77 17.46 o 5 15 1 23.21 46.63 24.63 o 0 16 1 1213.15 1161.74 46.83 o 1 16 1 361.50 401.80 31.47 o 2 16 1 417.31 353.72 26.70 o 3 16 1 124.73 132.37 22.82 o 4 16 1 363.69 446.09 41.12 o 1 17 1 95.56 58.16 24.12 o 2 17 1 220.13 249.90 44.83 o 0 0 2 17055.47 15837.40 251.12 o 1 0 2 47017.85 41273.44 440.82 o 2 0 2 1131.48 1049.96 36.11 o 3 0 2 4443.10 4628.50 48.42 o 4 0 2 6883.75 7117.12 71.71 o 5 0 2 14141.84 13867.67 127.01 o 6 0 2 8388.78 8677.83 116.17 o 7 0 2 295.87 263.90 27.23 o 8 0 2 1822.74 1864.41 53.89 o 9 0 2 685.96 732.53 31.54 o 10 0 2 28.28 37.11 67.95 o 1 1 2 18854.14 18432.97 172.09 o 2 1 2 326.03 271.45 11.18 o 3 1 2 7647.44 7598.92 50.12 o 4 1 2 2794.45 2839.18 26.89 o 5 1 2 46.32 32.78 6.65 o 6 1 2 497.26 459.02 15.65 o 7 1 2 2641.48 2641.06 33.06 o 8 1 2 1113.46 1104.23 23.90 o 9 1 2 148.20 137.78 17.17 o 10 1 2 124.13 90.48 22.67 o 0 2 2 32.16 4.40 7.45 o 1 2 2 17815.22 17543.02 123.41 o 2 2 2 106.38 111.45 8.95 o 3 2 2 6167.47 6583.55 64.72 o 4 2 2 3211.43 3149.12 28.77 o 5 2 2 2917.83 2770.73 29.04 o 6 2 2 1606.45 1590.06 23.52 o 7 2 2 52.15 37.64 9.65 o 8 2 2 1581.95 1503.41 32.10 o 9 2 2 676.33 692.24 28.60 o 10 2 2 101.95 135.42 25.40 o 1 3 2 2128.02 2346.91 29.33 o 2 3 2 66393.51 64382.18 707.98 o 3 3 2 553.85 545.39 10.55 o 4 3 2 77.67 59.38 6.48 o 5 3 2 99.18 127.00 10.90 o 6 3 2 90.52 89.26 9.48 o 7 3 2 10.99 5.96 9.45 o 8 3 2 48.81 47.42 15.95 o 9 3 2 36.04 9.72 24.10 o 10 3 2 0.31 -15.00 22.49 o 0 4 2 5235.37 5555.21 68.91 o 1 4 2 3227.82 3186.36 22.93 o 2 4 2 9845.13 10913.32 79.45 o 3 4 2 289.71 331.96 9.58 o 4 4 2 922.04 928.68 15.71 o 5 4 2 3357.09 3447.96 35.49 o 6 4 2 985.74 979.58 18.99 o 7 4 2 157.46 151.46 14.66 o 8 4 2 14.81 19.01 15.62 o 9 4 2 857.98 793.11 34.71 o 1 5 2 10472.02 10516.18 70.79 o 2 5 2 3207.64 3190.48 36.16 o 3 5 2 31407.42 31040.79 205.58 o 4 5 2 9445.98 10361.60 73.40 o 5 5 2 2.23 7.69 7.67 o 6 5 2 954.99 965.00 26.16 o 7 5 2 7354.73 7496.02 84.45 o 8 5 2 430.82 474.64 37.85 o 9 5 2 219.08 231.50 25.33 o 0 6 2 2465.91 2417.93 25.49 o 1 6 2 11663.16 11589.54 62.12 o 2 6 2 411.30 610.88 12.64 o 3 6 2 1387.76 1262.11 20.98 o 4 6 2 642.56 759.90 26.39 o 5 6 2 10910.61 10880.80 99.50 o 6 6 2 72.47 51.12 14.38 o 7 6 2 132.05 123.95 19.51 o 8 6 2 518.45 522.44 31.35 o 9 6 2 872.85 905.97 38.04 o 1 7 2 1070.38 922.08 11.25 o 2 7 2 19713.28 20549.03 134.01 o 3 7 2 4842.35 4528.28 44.96 o 4 7 2 1829.50 1900.52 30.97 o 5 7 2 0.87 -11.18 12.58 o 6 7 2 207.64 227.30 22.05 o 7 7 2 5320.06 5500.47 82.49 o 8 7 2 1584.75 1575.21 45.92 o 9 7 2 118.39 96.80 24.26 o 0 8 2 9721.15 10576.37 80.79 o 1 8 2 206.56 124.73 6.96 o 2 8 2 10.37 5.20 5.24 o 3 8 2 1246.59 1207.71 26.69 o 4 8 2 265.00 304.21 18.75 o 5 8 2 2850.36 2844.71 53.58 o 6 8 2 1.84 18.76 17.11 o 7 8 2 11.80 -16.87 17.54 o 8 8 2 1.95 0.06 20.28 o 9 8 2 21.12 51.92 24.13 o 1 9 2 2.66 -5.87 4.89 o 2 9 2 217.28 272.47 18.29 o 3 9 2 102.27 104.26 12.40 o 4 9 2 142.07 238.03 76.89 o 5 9 2 899.45 854.61 31.14 o 6 9 2 25.81 21.82 20.29 o 7 9 2 274.82 249.73 25.64 o 8 9 2 5.51 7.65 21.38 o 0 10 2 735.44 703.15 17.36 o 1 10 2 2120.46 2064.16 21.99 o 2 10 2 1890.30 1910.97 23.71 o 3 10 2 2178.02 2160.87 30.37 o 4 10 2 351.40 360.33 30.39 o 5 10 2 3276.38 3259.63 65.10 o 6 10 2 3.80 32.69 18.76 o 7 10 2 348.55 303.99 42.99 o 8 10 2 547.17 479.86 34.91 o 1 11 2 2743.19 2670.63 28.42 o 2 11 2 859.32 867.69 18.71 o 3 11 2 4889.27 4785.86 49.22 o 4 11 2 214.72 248.17 18.68 o 5 11 2 122.25 133.23 22.17 o 6 11 2 81.11 79.30 21.03 o 7 11 2 1538.67 1588.12 48.10 o 0 12 2 6808.30 6920.91 139.92 o 1 12 2 5590.10 5623.75 49.30 o 2 12 2 1309.22 1289.95 23.02 o 3 12 2 1081.30 1082.36 24.06 o 4 12 2 4104.93 4039.30 51.27 o 5 12 2 2069.81 2245.20 51.41 o 6 12 2 402.98 443.03 31.92 o 7 12 2 10.64 2.06 22.55 o 1 13 2 857.49 849.91 23.10 o 2 13 2 8.19 28.84 10.50 o 3 13 2 799.14 871.41 22.89 o 4 13 2 64.27 63.12 16.34 o 5 13 2 7.64 6.29 18.17 o 6 13 2 122.97 98.95 29.42 o 0 14 2 396.67 421.68 26.78 o 1 14 2 1043.84 1027.69 26.36 o 2 14 2 107.09 106.51 16.84 o 3 14 2 341.22 323.29 20.22 o 4 14 2 789.12 758.25 28.48 o 5 14 2 355.94 401.68 28.15 o 6 14 2 56.67 80.39 23.27 o 1 15 2 7.53 -12.31 15.56 o 2 15 2 175.07 188.28 21.85 o 3 15 2 306.71 283.90 33.51 o 4 15 2 63.96 43.77 18.00 o 5 15 2 51.19 15.06 21.52 o 0 16 2 639.33 644.50 64.20 o 1 16 2 449.83 465.03 32.54 o 2 16 2 476.53 517.74 30.90 o 3 16 2 71.02 51.25 21.38 o 4 16 2 6.12 -2.19 23.85 o 1 17 2 443.54 447.68 51.00 o 2 17 2 200.02 221.88 54.92 o 1 1 3 4186.45 4306.65 45.68 o 2 1 3 6017.02 6025.70 45.78 o 3 1 3 474.06 513.78 15.04 o 4 1 3 3168.11 3171.58 40.86 o 5 1 3 3.80 -7.11 6.04 o 6 1 3 1029.25 1041.24 19.46 o 7 1 3 373.87 428.87 16.33 o 8 1 3 930.76 901.74 21.99 o 9 1 3 1.41 -11.72 14.67 o 10 1 3 7.45 -7.31 25.50 o 0 2 3 10838.77 10425.82 86.78 o 1 2 3 7026.86 7043.85 46.99 o 2 2 3 319.27 301.10 7.79 o 3 2 3 36.64 24.23 5.91 o 4 2 3 11364.55 11230.45 90.27 o 5 2 3 8.30 11.60 6.60 o 6 2 3 3620.66 3528.37 51.63 o 7 2 3 5.63 -9.90 9.05 o 8 2 3 746.52 758.02 24.34 o 9 2 3 1.15 -4.51 15.80 o 10 2 3 1641.60 1638.95 47.53 o 1 3 3 2506.99 2559.88 20.70 o 2 3 3 27601.88 27057.63 162.14 o 3 3 3 9125.12 9901.28 74.40 o 4 3 3 3198.68 3132.50 41.14 o 5 3 3 797.36 856.22 16.04 o 6 3 3 7206.41 7271.85 81.10 o 7 3 3 12.95 -14.29 10.70 o 8 3 3 3113.15 3150.63 46.36 o 9 3 3 165.63 132.91 20.45 o 0 4 3 22714.50 21948.92 163.16 o 1 4 3 12.25 11.72 3.11 o 2 4 3 654.66 628.47 13.11 o 3 4 3 570.00 568.24 11.59 o 4 4 3 15412.20 15526.40 171.91 o 5 4 3 29.50 22.05 7.64 o 6 4 3 6898.29 6844.18 66.85 o 7 4 3 0.48 -16.69 11.13 o 8 4 3 1973.60 1875.47 47.58 o 9 4 3 1.04 -11.76 20.10 o 1 5 3 7.13 1.87 4.18 o 2 5 3 6350.10 6480.39 58.33 o 3 5 3 2844.71 2989.52 34.07 o 4 5 3 31.33 86.17 17.03 o 5 5 3 1640.33 1658.93 25.87 o 6 5 3 1284.95 1255.23 26.37 o 7 5 3 127.49 170.97 18.84 o 8 5 3 868.90 872.73 36.04 o 9 5 3 0.36 -28.75 19.17 o 0 6 3 863.62 811.40 13.85 o 1 6 3 8.37 6.20 3.37 o 2 6 3 1081.22 1144.32 18.69 o 3 6 3 193.93 197.37 11.02 o 4 6 3 7961.22 8156.35 91.72 o 5 6 3 52.62 61.78 12.53 o 6 6 3 16.01 12.07 14.26 o 7 6 3 469.37 476.52 24.96 o 8 6 3 17.67 13.57 18.29 o 9 6 3 61.20 61.95 23.04 o 1 7 3 1.64 1.69 3.85 o 2 7 3 1025.65 941.02 13.72 o 3 7 3 844.73 1034.89 20.17 o 4 7 3 36.40 32.33 9.56 o 5 7 3 1082.39 1080.56 31.54 o 6 7 3 5059.68 4892.58 110.32 o 7 7 3 5.78 39.90 18.49 o 8 7 3 326.24 355.99 29.16 o 9 7 3 21.59 10.75 21.67 o 0 8 3 9022.39 8613.11 68.67 o 1 8 3 1611.24 1785.23 16.86 o 2 8 3 1624.52 1610.31 18.06 o 3 8 3 173.22 152.79 14.20 o 4 8 3 6394.56 6539.88 73.14 o 5 8 3 1436.45 1455.14 37.45 o 6 8 3 14.99 11.05 16.41 o 7 8 3 0.22 -19.36 18.27 o 8 8 3 1127.29 1100.80 45.05 o 9 8 3 0.67 3.15 23.71 o 1 9 3 1112.67 1283.71 16.45 o 2 9 3 22076.76 22287.36 117.16 o 3 9 3 24.54 12.54 11.39 o 4 9 3 3659.34 3717.31 53.08 o 5 9 3 107.78 98.67 17.64 o 6 9 3 3450.15 3360.95 61.83 o 7 9 3 346.15 349.72 28.38 o 8 9 3 940.95 1029.29 40.19 o 0 10 3 11679.67 11335.67 89.53 o 1 10 3 499.05 542.50 12.18 o 2 10 3 3594.82 3621.33 47.14 o 3 10 3 36.47 42.90 10.81 o 4 10 3 4779.35 4694.60 62.60 o 5 10 3 23.66 29.50 17.32 o 6 10 3 2725.11 2734.31 57.01 o 7 10 3 7.30 -5.65 20.39 o 8 10 3 155.07 141.98 26.08 o 1 11 3 290.91 329.61 12.39 o 2 11 3 1676.04 1606.73 24.42 o 3 11 3 281.54 290.91 15.62 o 4 11 3 37.50 32.47 13.20 o 5 11 3 220.66 205.33 23.43 o 6 11 3 178.56 219.36 28.90 o 7 11 3 5.73 -3.17 22.82 o 0 12 3 2326.98 2340.07 60.73 o 1 12 3 296.06 325.36 15.57 o 2 12 3 173.27 159.90 12.58 o 3 12 3 0.25 0.69 11.46 o 4 12 3 30.69 62.16 23.65 o 5 12 3 61.72 35.20 19.32 o 6 12 3 26.28 14.33 20.96 o 7 12 3 5.40 17.39 23.15 o 1 13 3 594.73 545.15 20.10 o 2 13 3 304.94 309.73 18.38 o 3 13 3 43.00 44.90 13.46 o 4 13 3 226.41 219.12 19.43 o 5 13 3 0.18 -19.11 18.16 o 6 13 3 630.67 652.72 40.61 o 0 14 3 1516.57 1580.61 48.28 o 1 14 3 7.67 -8.70 13.83 o 2 14 3 3.22 -9.06 13.35 o 3 14 3 118.85 110.70 17.93 o 4 14 3 2131.86 2317.87 44.88 o 5 14 3 0.30 6.36 19.06 o 6 14 3 573.56 665.02 36.61 o 1 15 3 513.90 581.34 32.46 o 2 15 3 4268.87 4572.61 68.99 o 3 15 3 5.38 -2.42 16.68 o 4 15 3 673.53 745.26 35.13 o 5 15 3 120.77 90.98 22.87 o 0 16 3 2210.79 2092.78 113.53 o 1 16 3 105.05 75.54 23.32 o 2 16 3 310.91 370.87 34.77 o 3 16 3 2.18 -4.53 21.56 o 4 16 3 771.55 826.20 42.08 o 1 17 3 292.52 225.89 35.96 o 2 17 3 711.59 757.85 47.54 o 0 0 4 38315.50 37165.25 567.21 o 1 0 4 2628.75 2700.76 41.89 o 2 0 4 178.14 209.86 20.13 o 3 0 4 5929.99 5994.26 81.70 o 4 0 4 4587.41 4555.10 52.67 o 5 0 4 9337.26 8949.81 206.68 o 6 0 4 84.67 65.09 13.49 o 7 0 4 124.25 119.86 16.54 o 8 0 4 380.19 395.27 25.43 o 9 0 4 680.68 718.92 39.54 o 10 0 4 3019.98 3019.21 260.92 o 1 1 4 2007.44 2110.40 20.26 o 2 1 4 10961.49 10811.08 70.44 o 3 1 4 4276.65 4074.07 33.83 o 4 1 4 1013.00 1024.80 16.01 o 5 1 4 43.03 44.24 7.18 o 6 1 4 4236.50 4338.95 71.66 o 7 1 4 5713.60 5814.83 72.30 o 8 1 4 535.12 578.57 25.47 o 9 1 4 84.42 56.55 17.99 o 10 1 4 69.46 81.20 51.33 o 0 2 4 1876.88 1895.37 30.19 o 1 2 4 22513.59 22688.40 135.47 o 2 2 4 8612.44 8941.07 60.62 o 3 2 4 1062.04 1024.64 14.50 o 4 2 4 1766.28 1775.87 25.18 o 5 2 4 7855.23 7846.04 74.49 o 6 2 4 878.55 895.24 18.35 o 7 2 4 61.50 50.65 11.04 o 8 2 4 269.45 247.62 17.93 o 9 2 4 1778.87 1781.75 52.21 o 10 2 4 418.58 488.55 46.21 o 1 3 4 94.49 88.55 7.88 o 2 3 4 2228.97 2421.87 23.24 o 3 3 4 648.74 676.56 13.60 o 4 3 4 641.59 759.54 14.33 o 5 3 4 81.62 71.85 9.78 o 6 3 4 43.56 36.92 9.59 o 7 3 4 6.89 -2.33 10.96 o 8 3 4 0.25 -3.51 13.35 o 9 3 4 587.76 549.89 43.20 o 0 4 4 5566.99 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446.67 501.22 90.88 o 1 16 7 8.80 14.70 23.27 o 2 16 7 34.33 -3.26 22.77 o 3 16 7 110.73 101.64 31.96 o 0 0 8 630.74 611.30 22.01 o 1 0 8 3467.75 3042.88 36.95 o 2 0 8 3059.97 3407.99 89.31 o 3 0 8 29184.26 30472.46 765.74 o 4 0 8 2262.46 2282.18 52.61 o 5 0 8 20403.79 19740.79 527.41 o 6 0 8 30.68 18.87 12.79 o 7 0 8 11.77 -7.84 16.39 o 8 0 8 38.43 13.95 20.69 o 9 0 8 1494.21 1587.42 64.46 o 1 1 8 694.62 554.27 12.73 o 2 1 8 213.28 173.23 10.05 o 3 1 8 36141.60 36588.54 554.75 o 4 1 8 49.98 66.07 7.73 o 5 1 8 787.83 814.82 20.03 o 6 1 8 148.22 128.40 12.36 o 7 1 8 6547.85 6398.39 102.49 o 8 1 8 1.08 1.81 15.23 o 9 1 8 42.35 34.90 18.19 o 0 2 8 96.41 110.44 9.76 o 1 2 8 19634.92 20352.29 181.92 o 2 2 8 1114.51 1189.48 23.99 o 3 2 8 20.76 37.75 5.64 o 4 2 8 1168.44 1168.34 19.07 o 5 2 8 1765.79 1696.57 28.08 o 6 2 8 276.38 276.40 15.06 o 7 2 8 100.89 87.16 14.15 o 8 2 8 121.83 148.24 18.90 o 9 2 8 46.10 25.85 18.15 o 1 3 8 6708.69 7534.59 105.27 o 2 3 8 233.89 281.87 10.64 o 3 3 8 1941.03 2141.40 26.45 o 4 3 8 114.24 112.31 9.92 o 5 3 8 39.06 29.02 9.81 o 6 3 8 51.01 85.55 21.20 o 7 3 8 196.33 189.08 16.75 o 8 3 8 146.95 169.29 17.86 o 9 3 8 0.11 -29.77 19.85 o 0 4 8 561.32 619.25 27.18 o 1 4 8 8664.08 8944.55 88.17 o 2 4 8 919.14 1059.67 17.80 o 3 4 8 4016.70 4150.19 39.94 o 4 4 8 403.10 419.68 13.92 o 5 4 8 3417.40 3401.21 80.46 o 6 4 8 95.28 131.49 16.28 o 7 4 8 2611.34 2545.46 52.57 o 8 4 8 226.55 255.14 21.68 o 9 4 8 836.96 781.25 42.81 o 1 5 8 12413.03 12846.23 79.20 o 2 5 8 758.35 759.52 15.65 o 3 5 8 8429.97 8311.66 86.13 o 4 5 8 1254.57 1294.02 23.75 o 5 5 8 434.38 507.57 20.73 o 6 5 8 109.77 73.29 14.78 o 7 5 8 3140.04 3248.51 70.21 o 8 5 8 1092.82 1057.47 37.28 o 9 5 8 70.90 52.56 21.40 o 0 6 8 1800.87 1826.42 27.54 o 1 6 8 20952.10 20599.94 118.45 o 2 6 8 146.35 147.94 12.12 o 3 6 8 2579.01 2459.67 31.61 o 4 6 8 997.04 980.61 31.89 o 5 6 8 1285.04 1243.11 29.95 o 6 6 8 15.07 34.24 13.96 o 7 6 8 1017.09 988.48 36.08 o 8 6 8 54.97 90.92 19.74 o 9 6 8 2355.56 2275.77 71.88 o 1 7 8 1800.46 1660.32 21.00 o 2 7 8 589.63 524.47 16.75 o 3 7 8 5422.41 5345.63 55.97 o 4 7 8 153.74 151.01 13.82 o 5 7 8 7.59 -8.40 12.30 o 6 7 8 91.33 98.31 19.04 o 7 7 8 2430.60 2447.42 72.72 o 8 7 8 719.19 672.69 31.50 o 0 8 8 188.60 215.22 16.82 o 1 8 8 6955.33 7229.28 53.25 o 2 8 8 1.31 5.76 8.00 o 3 8 8 2775.72 2831.37 38.90 o 4 8 8 38.20 30.44 11.22 o 5 8 8 384.39 414.26 23.66 o 6 8 8 491.34 466.68 29.14 o 7 8 8 83.10 51.48 20.06 o 8 8 8 45.77 66.18 21.13 o 1 9 8 322.06 347.20 13.77 o 2 9 8 73.84 52.70 10.23 o 3 9 8 17.43 25.41 11.15 o 4 9 8 67.15 63.30 19.17 o 5 9 8 645.26 563.98 25.93 o 6 9 8 9.89 42.27 18.38 o 7 9 8 5.58 38.90 20.34 o 8 9 8 9.82 34.08 24.05 o 0 10 8 380.32 411.73 27.01 o 1 10 8 4272.21 4185.96 54.52 o 2 10 8 73.83 60.84 10.43 o 3 10 8 107.06 84.85 14.23 o 4 10 8 43.61 41.86 14.71 o 5 10 8 1642.68 1649.68 40.08 o 6 10 8 194.99 169.56 23.80 o 7 10 8 1.01 0.73 21.22 o 1 11 8 3557.70 3572.46 43.78 o 2 11 8 115.69 118.43 15.71 o 3 11 8 5828.78 5882.31 84.71 o 4 11 8 410.57 377.39 23.67 o 5 11 8 28.16 6.24 16.77 o 6 11 8 75.08 45.40 21.09 o 7 11 8 4924.56 4936.39 112.66 o 0 12 8 188.54 130.93 23.72 o 1 12 8 3319.87 3299.21 54.80 o 2 12 8 1.23 2.38 13.24 o 3 12 8 1184.67 1123.23 29.59 o 4 12 8 265.21 232.49 20.43 o 5 12 8 2790.38 2789.89 53.74 o 6 12 8 556.21 561.08 34.77 o 1 13 8 26.52 5.67 15.95 o 2 13 8 351.22 350.26 24.48 o 3 13 8 1671.99 1702.78 41.48 o 4 13 8 33.58 27.79 16.76 o 5 13 8 23.17 7.58 17.81 o 6 13 8 13.98 30.99 23.76 o 0 14 8 382.68 409.45 43.11 o 1 14 8 3.48 23.76 19.87 o 2 14 8 58.34 64.53 19.04 o 3 14 8 78.17 71.45 20.28 o 4 14 8 3.26 7.89 19.43 o 5 14 8 361.45 367.67 27.29 o 1 15 8 792.09 802.51 38.71 o 2 15 8 226.11 251.66 28.76 o 3 15 8 39.99 35.86 22.01 o 4 15 8 0.27 10.31 21.96 o 0 16 8 3.70 -17.59 33.62 o 1 16 8 1028.52 1069.16 43.10 o 2 16 8 17.84 -2.73 24.01 o 1 1 9 944.88 945.68 17.27 o 2 1 9 6818.63 6921.59 93.93 o 3 1 9 840.46 813.98 16.63 o 4 1 9 4.99 9.05 7.06 o 5 1 9 222.09 244.10 14.04 o 6 1 9 1882.60 1902.39 30.18 o 7 1 9 33.19 53.13 13.60 o 8 1 9 41.44 25.40 18.50 o 9 1 9 47.96 10.37 18.21 o 0 2 9 11589.43 10889.60 102.47 o 1 2 9 17.99 12.43 6.16 o 2 2 9 3.59 6.86 6.37 o 3 2 9 2168.83 2189.18 24.04 o 4 2 9 5368.54 5246.12 72.15 o 5 2 9 3373.69 3399.51 62.68 o 6 2 9 3006.56 2952.62 71.67 o 7 2 9 70.38 52.24 13.50 o 8 2 9 1780.51 1677.42 39.67 o 9 2 9 37.20 12.05 18.46 o 1 3 9 3380.11 3562.31 43.12 o 2 3 9 29789.87 29667.69 343.00 o 3 3 9 719.67 733.54 16.06 o 4 3 9 2728.48 2699.86 58.35 o 5 3 9 8.37 24.88 10.19 o 6 3 9 5475.00 5406.48 116.92 o 7 3 9 595.29 554.23 22.72 o 8 3 9 2593.06 2576.71 59.03 o 9 3 9 89.67 46.93 23.38 o 0 4 9 23273.82 22913.79 171.65 o 1 4 9 6898.37 7490.17 78.78 o 2 4 9 2212.03 2331.29 27.89 o 3 4 9 220.88 247.50 11.39 o 4 4 9 6595.83 6240.12 95.23 o 5 4 9 1256.71 1273.45 25.41 o 6 4 9 5707.69 5696.74 129.99 o 7 4 9 98.17 92.26 15.26 o 8 4 9 24.69 30.14 15.69 o 9 4 9 68.82 44.20 22.18 o 1 5 9 3044.02 3388.66 28.35 o 2 5 9 2707.44 2635.36 38.34 o 3 5 9 64.24 66.04 8.77 o 4 5 9 1333.09 1251.82 22.44 o 5 5 9 57.85 58.21 12.90 o 6 5 9 31.38 44.88 14.63 o 7 5 9 128.76 150.20 18.47 o 8 5 9 91.95 102.17 19.38 o 9 5 9 3.85 -15.84 20.17 o 0 6 9 903.99 941.58 20.45 o 1 6 9 810.06 876.87 13.72 o 2 6 9 307.56 361.04 12.90 o 3 6 9 3.72 10.62 7.87 o 4 6 9 25.16 60.68 28.88 o 5 6 9 869.08 842.06 41.38 o 6 6 9 1595.17 1488.47 48.20 o 7 6 9 461.79 426.64 28.64 o 8 6 9 5.26 1.22 18.55 o 1 7 9 8.52 11.25 8.85 o 2 7 9 5217.18 5228.80 57.22 o 3 7 9 2501.85 2613.65 45.58 o 4 7 9 2273.38 2362.75 39.93 o 5 7 9 7.67 -0.59 12.23 o 6 7 9 28.85 33.02 17.85 o 7 7 9 33.55 66.57 22.72 o 8 7 9 232.34 278.77 36.08 o 0 8 9 14007.41 13629.97 228.07 o 1 8 9 2347.82 2468.44 30.08 o 2 8 9 217.46 191.17 12.42 o 3 8 9 1093.31 1136.90 26.07 o 4 8 9 329.42 332.28 25.10 o 5 8 9 491.48 529.35 25.48 o 6 8 9 1919.32 1873.14 59.68 o 7 8 9 59.73 15.90 20.63 o 8 8 9 617.49 670.90 40.12 o 1 9 9 304.82 287.81 13.25 o 2 9 9 6728.85 6620.47 77.85 o 3 9 9 1516.21 1558.41 36.51 o 4 9 9 425.31 479.18 24.42 o 5 9 9 2.97 -5.57 14.47 o 6 9 9 4761.74 4737.25 126.94 o 7 9 9 122.41 125.42 23.58 o 0 10 9 6094.51 5837.68 110.53 o 1 10 9 88.27 75.75 10.41 o 2 10 9 7.70 9.36 10.37 o 3 10 9 557.08 525.42 21.90 o 4 10 9 3801.18 3838.86 78.05 o 5 10 9 372.29 370.01 24.74 o 6 10 9 1331.51 1392.68 83.89 o 7 10 9 2.47 -34.99 25.04 o 1 11 9 39.26 32.59 13.14 o 2 11 9 1536.69 1565.50 29.78 o 3 11 9 3.75 35.50 13.99 o 4 11 9 612.64 599.44 25.70 o 5 11 9 52.92 16.14 17.46 o 6 11 9 173.70 143.54 25.05 o 7 11 9 213.70 271.96 29.61 o 0 12 9 1228.85 1273.38 43.11 o 1 12 9 1189.54 1195.63 33.70 o 2 12 9 286.01 305.25 22.72 o 3 12 9 53.58 27.31 14.74 o 4 12 9 36.71 35.32 16.70 o 5 12 9 258.95 245.71 24.33 o 6 12 9 20.83 -32.97 21.98 o 1 13 9 22.67 37.77 16.63 o 2 13 9 1203.25 1181.12 37.73 o 3 13 9 139.13 134.48 20.14 o 4 13 9 253.23 293.67 22.16 o 5 13 9 0.08 -26.20 17.47 o 0 14 9 5904.31 5811.85 129.79 o 1 14 9 307.97 349.42 36.38 o 2 14 9 90.52 64.64 19.75 o 3 14 9 329.31 327.00 29.87 o 4 14 9 1407.33 1427.54 42.63 o 5 14 9 392.57 419.00 29.83 o 1 15 9 137.58 143.35 25.55 o 2 15 9 1820.98 1857.14 53.84 o 3 15 9 141.25 152.74 31.42 o 0 16 9 1905.72 1987.00 80.42 o 1 16 9 3.80 -10.30 36.75 o 2 16 9 67.50 4.89 27.94 o 0 0 10 7098.24 6536.71 95.98 o 1 0 10 9360.71 9199.05 147.73 o 2 0 10 1165.72 1218.45 24.02 o 3 0 10 5301.44 5685.02 186.54 o 4 0 10 16346.95 16520.91 240.68 o 5 0 10 2234.04 2104.33 53.19 o 6 0 10 1062.10 1069.23 48.58 o 7 0 10 27.24 16.95 18.61 o 8 0 10 902.22 890.77 75.19 o 9 0 10 3182.65 3222.60 302.43 o 1 1 10 1206.27 1091.27 16.81 o 2 1 10 8123.83 7732.42 93.01 o 3 1 10 1220.89 982.61 23.92 o 4 1 10 5677.52 5818.29 109.69 o 5 1 10 7.41 -8.55 9.20 o 6 1 10 1640.82 1556.24 50.42 o 7 1 10 2254.66 2169.12 38.74 o 8 1 10 2656.06 2608.08 70.42 o 9 1 10 393.91 453.31 48.35 o 0 2 10 1954.88 1883.95 37.38 o 1 2 10 4517.88 4634.86 49.38 o 2 2 10 779.66 793.87 21.08 o 3 2 10 300.54 250.59 10.82 o 4 2 10 3022.02 3147.61 91.48 o 5 2 10 131.16 111.44 16.30 o 6 2 10 6.21 7.64 10.70 o 7 2 10 195.35 197.01 22.90 o 8 2 10 813.81 794.94 30.56 o 9 2 10 327.26 378.91 28.10 o 1 3 10 754.34 899.03 18.78 o 2 3 10 59.52 28.37 7.23 o 3 3 10 0.54 -3.23 6.93 o 4 3 10 202.24 199.64 12.74 o 5 3 10 1186.82 1304.13 55.71 o 6 3 10 46.99 39.00 16.21 o 7 3 10 339.20 373.61 26.85 o 8 3 10 1.14 6.24 17.51 o 9 3 10 233.89 230.41 27.29 o 0 4 10 5140.25 5337.57 87.82 o 1 4 10 6022.28 6345.53 66.23 o 2 4 10 192.10 169.00 11.30 o 3 4 10 340.42 376.55 13.85 o 4 4 10 3487.45 3496.54 73.81 o 5 4 10 388.61 409.66 20.82 o 6 4 10 1111.33 1191.96 45.85 o 7 4 10 647.31 623.11 25.33 o 8 4 10 34.79 28.19 16.18 o 9 4 10 464.44 537.96 35.03 o 1 5 10 2653.58 2530.26 25.44 o 2 5 10 6308.52 6206.94 74.66 o 3 5 10 4652.56 4487.48 44.82 o 4 5 10 6.32 8.67 9.94 o 5 5 10 4.34 -1.76 12.10 o 6 5 10 659.72 623.58 24.76 o 7 5 10 1621.40 1586.59 70.28 o 8 5 10 528.96 576.24 34.50 o 0 6 10 14138.64 14191.31 117.51 o 1 6 10 221.05 155.49 11.23 o 2 6 10 1976.46 2103.90 28.20 o 3 6 10 1382.83 1462.35 24.07 o 4 6 10 6242.56 6123.60 64.72 o 5 6 10 2690.25 2674.44 75.54 o 6 6 10 1666.63 1689.72 63.32 o 7 6 10 0.19 -14.81 18.88 o 8 6 10 547.76 576.82 31.07 o 1 7 10 49.76 22.41 6.64 o 2 7 10 10846.79 10859.71 85.68 o 3 7 10 2341.34 2237.95 35.04 o 4 7 10 27.00 45.36 12.50 o 5 7 10 320.45 324.95 20.11 o 6 7 10 762.80 777.18 32.34 o 7 7 10 1447.05 1464.66 43.77 o 8 7 10 850.62 807.33 32.71 o 0 8 10 2477.17 2463.71 43.16 o 1 8 10 415.14 417.92 14.32 o 2 8 10 477.03 493.06 17.15 o 3 8 10 903.08 895.36 30.03 o 4 8 10 51.78 49.27 12.81 o 5 8 10 2210.86 2226.65 61.39 o 6 8 10 869.72 839.94 37.02 o 7 8 10 52.32 63.40 20.94 o 8 8 10 1.46 -32.34 21.56 o 1 9 10 594.69 598.12 16.83 o 2 9 10 117.92 112.63 12.41 o 3 9 10 2069.63 1958.22 34.13 o 4 9 10 1023.74 943.14 25.83 o 5 9 10 16.37 -9.55 15.70 o 6 9 10 290.62 319.04 27.53 o 7 9 10 2.43 -12.18 20.14 o 0 10 10 831.63 899.38 35.45 o 1 10 10 96.24 93.65 12.21 o 2 10 10 1482.90 1487.27 28.00 o 3 10 10 1907.82 1899.32 36.10 o 4 10 10 816.18 835.07 29.19 o 5 10 10 1882.46 1837.64 42.38 o 6 10 10 2.69 18.40 21.02 o 7 10 10 266.18 245.86 29.33 o 1 11 10 3691.01 3730.52 51.72 o 2 11 10 2406.30 2357.30 39.62 o 3 11 10 403.61 437.14 22.71 o 4 11 10 1132.71 1123.53 30.96 o 5 11 10 7.54 -4.51 16.87 o 6 11 10 583.31 589.33 35.24 o 0 12 10 448.24 461.33 41.88 o 1 12 10 1572.78 1584.75 35.11 o 2 12 10 612.34 556.34 32.15 o 3 12 10 1052.70 1084.00 29.82 o 4 12 10 2237.50 2298.44 44.01 o 5 12 10 746.67 743.74 33.54 o 6 12 10 541.44 555.58 35.96 o 1 13 10 623.17 645.36 29.62 o 2 13 10 1906.83 1848.47 58.43 o 3 13 10 361.13 357.08 52.86 o 4 13 10 529.40 573.54 34.82 o 5 13 10 54.83 24.89 19.43 o 0 14 10 6.45 -44.03 29.35 o 1 14 10 1657.79 1502.25 40.77 o 2 14 10 14.19 -5.52 21.41 o 3 14 10 26.60 -0.65 21.40 o 4 14 10 199.23 227.33 27.81 o 1 15 10 69.93 48.92 23.76 o 2 15 10 50.53 83.10 50.99 o 3 15 10 19.20 -0.96 23.97 o 0 16 10 518.30 532.68 69.18 o 1 16 10 286.12 321.39 33.78 o 1 1 11 680.73 507.36 12.77 o 2 1 11 662.70 813.68 14.59 o 3 1 11 2887.01 2735.43 57.73 o 4 1 11 993.24 1092.68 33.06 o 5 1 11 141.21 130.38 13.09 o 6 1 11 30.01 31.25 12.09 o 7 1 11 1358.75 1429.43 34.76 o 8 1 11 56.03 58.99 18.37 o 9 1 11 87.56 96.02 40.10 o 0 2 11 113.33 114.83 9.93 o 1 2 11 11681.04 11173.39 88.55 o 2 2 11 851.54 868.32 18.98 o 3 2 11 275.02 190.88 12.67 o 4 2 11 117.29 106.44 11.30 o 5 2 11 6210.46 6011.53 122.81 o 6 2 11 218.78 177.65 14.49 o 7 2 11 41.78 60.33 15.95 o 8 2 11 943.42 926.49 67.33 o 9 2 11 1878.06 1808.75 68.77 o 1 3 11 4255.59 3837.72 42.39 o 2 3 11 1369.98 1398.63 22.45 o 3 3 11 10503.26 10085.13 163.91 o 4 3 11 14.79 17.04 8.62 o 5 3 11 692.28 643.45 25.14 o 6 3 11 3.92 1.60 12.84 o 7 3 11 4860.69 4723.43 132.02 o 8 3 11 751.54 717.75 31.54 o 9 3 11 302.21 336.54 37.85 o 0 4 11 2600.36 2801.77 37.52 o 1 4 11 4796.51 4488.61 40.91 o 2 4 11 1058.62 1197.33 21.12 o 3 4 11 1338.91 1315.21 32.03 o 4 4 11 424.17 414.19 15.96 o 5 4 11 8083.88 7982.09 231.00 o 6 4 11 651.15 695.84 25.91 o 7 4 11 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