# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' blg3 in P-1 C14H10N6OBR2 Z=4' _shelx_refln_list_code 4 _shelx_F_calc_maximum 497.07 _exptl_crystal_F_000 856.00 _reflns_d_resolution_high 0.6617 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.1647 _cell_length_b 12.2833 _cell_length_c 14.0288 _cell_angle_alpha 86.532 _cell_angle_beta 84.218 _cell_angle_gamma 78.747 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 16274.30 16984.54 350.47 o 4 0 0 11583.78 12397.69 181.46 o 5 0 0 515.16 567.41 14.80 o 6 0 0 3145.97 3176.27 68.48 o 7 0 0 2010.44 2136.85 49.18 o 8 0 0 2626.19 2813.39 24.34 o 9 0 0 2.49 -0.05 8.12 o 10 0 0 1734.79 1844.22 138.24 o 11 0 0 429.57 503.65 39.84 o 12 0 0 2.23 38.68 68.17 o 13 0 0 137.44 159.18 51.89 o -13 1 0 108.71 135.99 84.34 o -12 1 0 43.65 98.31 74.61 o -11 1 0 117.68 176.28 43.52 o -10 1 0 834.75 925.97 42.06 o -9 1 0 204.36 208.98 32.55 o -8 1 0 21.82 -1.66 19.68 o -7 1 0 3194.44 3539.25 130.71 o -6 1 0 222.61 347.38 11.35 o -5 1 0 1.14 7.30 5.06 o -4 1 0 884.27 1120.90 22.98 o -3 1 0 2253.11 2104.37 38.63 o -2 1 0 3359.84 3722.93 47.92 o 3 1 0 9330.38 10597.93 287.45 o 4 1 0 97.43 106.90 10.21 o 5 1 0 11.02 7.21 9.34 o 6 1 0 339.56 376.22 18.43 o 7 1 0 157.76 178.94 15.95 o 8 1 0 1907.54 2106.72 59.05 o 9 1 0 1.95 39.00 28.46 o 10 1 0 51.70 67.49 28.34 o 11 1 0 271.77 295.00 38.25 o 12 1 0 0.93 8.79 30.04 o 13 1 0 4.75 5.16 17.47 o -12 2 0 19.26 115.25 80.72 o -11 2 0 20.07 100.53 77.46 o -10 2 0 70.50 89.77 48.66 o -9 2 0 11.90 9.93 35.85 o -8 2 0 572.85 693.67 47.91 o -7 2 0 331.34 344.68 11.45 o -6 2 0 1999.31 1963.65 91.98 o -5 2 0 5360.51 5361.78 41.18 o -4 2 0 421.29 397.62 15.06 o -3 2 0 3735.45 3673.80 54.34 o -2 2 0 1153.03 1311.52 19.11 o 2 2 0 16750.29 17074.75 142.96 o 3 2 0 1672.16 1644.35 26.70 o 4 2 0 1245.18 1154.38 33.37 o 5 2 0 9676.02 10152.66 383.52 o 6 2 0 693.63 776.10 19.94 o 7 2 0 151.28 157.85 21.60 o 8 2 0 984.86 1040.83 61.76 o 9 2 0 143.06 169.74 19.01 o 10 2 0 181.95 184.56 33.91 o 11 2 0 27.78 42.53 32.05 o 12 2 0 169.05 167.46 36.39 o 13 2 0 52.59 6.98 18.18 o -12 3 0 26.98 7.97 112.16 o -11 3 0 52.60 220.58 85.59 o -10 3 0 109.49 156.45 73.86 o -9 3 0 18.75 30.71 38.54 o -8 3 0 909.99 1141.72 155.83 o -7 3 0 460.83 495.84 25.40 o -6 3 0 367.74 373.15 20.53 o -5 3 0 2231.26 2156.10 24.96 o -4 3 0 208.30 201.75 12.99 o -3 3 0 795.98 843.75 24.67 o -2 3 0 6.63 5.11 3.32 o -1 3 0 0.19 -1.11 3.78 o 0 3 0 2389.40 2670.29 21.49 o 1 3 0 1926.22 1899.42 33.12 o 2 3 0 1402.80 1422.71 18.30 o 3 3 0 4107.40 4148.42 66.02 o 4 3 0 0.27 9.57 8.88 o 5 3 0 832.17 777.43 15.39 o 6 3 0 274.38 293.52 15.02 o 7 3 0 13.56 11.27 12.20 o 8 3 0 0.78 31.42 25.12 o 9 3 0 30.11 21.80 15.35 o 10 3 0 71.85 75.12 22.21 o 11 3 0 110.10 140.41 32.02 o 12 3 0 11.97 10.46 35.31 o 13 3 0 64.45 62.72 50.60 o -12 4 0 159.22 507.28 110.29 o -11 4 0 6.17 301.17 97.31 o -10 4 0 478.32 527.99 87.08 o -9 4 0 1325.31 1211.18 78.85 o -8 4 0 4.86 371.04 61.38 o -7 4 0 2968.88 3032.05 118.27 o -6 4 0 1249.47 1183.39 53.65 o -5 4 0 65.94 68.47 11.04 o -4 4 0 303.08 319.52 26.03 o -3 4 0 2199.87 2182.42 120.44 o -2 4 0 5051.09 4896.35 56.54 o -1 4 0 13725.56 13525.37 156.91 o 0 4 0 2883.16 3198.73 42.28 o 1 4 0 21624.66 20737.45 146.62 o 2 4 0 1694.68 1663.85 41.31 o 3 4 0 714.71 641.13 22.02 o 4 4 0 3637.06 3424.84 50.31 o 5 4 0 1188.59 1095.56 18.11 o 6 4 0 60.68 52.11 13.75 o 7 4 0 54.54 62.45 16.95 o 8 4 0 752.55 750.18 27.91 o 9 4 0 952.28 964.16 27.03 o 10 4 0 0.84 -0.33 6.13 o 11 4 0 274.92 269.53 33.21 o 12 4 0 217.63 242.81 37.08 o 13 4 0 2.36 13.97 64.38 o -11 5 0 500.74 586.13 104.55 o -10 5 0 172.24 176.16 97.31 o -9 5 0 795.79 692.92 90.58 o -8 5 0 12.57 74.07 39.18 o -7 5 0 241.11 231.62 37.30 o -6 5 0 1141.47 1015.45 114.16 o -5 5 0 298.41 271.65 13.65 o -4 5 0 6.18 1.52 3.29 o -3 5 0 212.67 250.91 9.29 o -2 5 0 11160.73 11450.18 133.77 o -1 5 0 6518.27 5815.78 71.44 o 0 5 0 4522.24 5425.76 43.25 o 1 5 0 19156.42 19209.88 633.05 o 2 5 0 5631.28 5503.16 65.77 o 3 5 0 1247.13 1231.71 47.95 o 4 5 0 2377.71 2408.17 43.54 o 5 5 0 1742.99 1637.31 78.59 o 6 5 0 2.31 23.93 25.39 o 7 5 0 336.64 348.06 18.93 o 8 5 0 222.71 184.63 21.67 o 9 5 0 1004.61 1040.63 45.37 o 10 5 0 245.77 229.69 33.38 o 11 5 0 258.18 226.41 30.91 o 12 5 0 175.39 131.82 52.77 o 13 5 0 24.85 19.96 71.86 o -9 6 0 25.97 82.59 54.40 o -8 6 0 3.24 67.87 48.91 o -7 6 0 1125.99 1101.86 464.24 o -6 6 0 232.16 222.32 45.41 o -5 6 0 3614.51 3651.38 137.98 o -4 6 0 1044.38 1005.26 106.73 o -3 6 0 6.79 0.58 10.29 o -2 6 0 172.89 215.20 11.45 o -1 6 0 5335.51 5333.75 66.15 o 0 6 0 178.48 148.21 9.10 o 1 6 0 429.44 422.92 44.69 o 2 6 0 129.92 113.39 27.95 o 3 6 0 4339.41 3997.71 71.66 o 4 6 0 4230.22 4051.51 175.16 o 5 6 0 480.78 407.64 41.80 o 6 6 0 1355.09 1330.13 21.56 o 7 6 0 511.05 467.72 19.00 o 8 6 0 31.88 -3.47 8.84 o 9 6 0 139.71 113.82 24.44 o 10 6 0 187.22 88.15 37.82 o 12 6 0 34.38 49.11 44.58 o 13 6 0 3.59 27.45 73.11 o -9 7 0 192.92 323.13 62.13 o -8 7 0 581.54 725.11 60.63 o -7 7 0 2300.48 2091.76 472.22 o -6 7 0 1039.82 1087.62 167.80 o -5 7 0 210.77 271.62 20.84 o -4 7 0 8840.68 8710.12 163.29 o -3 7 0 2368.55 2402.99 192.88 o -2 7 0 984.60 980.46 21.51 o -1 7 0 1385.14 1320.34 21.11 o 0 7 0 1900.66 1782.34 37.67 o 1 7 0 6140.21 5903.85 152.77 o 2 7 0 612.92 634.11 38.10 o 3 7 0 15691.53 15045.25 136.39 o 4 7 0 11059.88 10625.79 152.41 o 5 7 0 7.73 6.28 13.97 o 6 7 0 3622.80 3556.38 100.93 o 7 7 0 3111.93 3451.48 211.10 o 8 7 0 28.32 46.16 24.41 o 9 7 0 2.93 9.98 46.91 o 10 7 0 406.27 323.35 84.46 o 11 7 0 796.30 761.70 45.85 o 12 7 0 1.78 43.84 59.51 o 13 7 0 318.55 278.94 91.33 o -10 8 0 40.34 40.17 115.28 o -9 8 0 85.99 228.49 57.37 o -8 8 0 11.16 54.89 64.38 o -7 8 0 327.88 273.25 144.60 o -6 8 0 727.10 712.15 49.42 o -5 8 0 10.42 70.36 59.51 o -4 8 0 1094.99 1180.00 31.07 o -3 8 0 31.66 24.29 79.85 o -2 8 0 183.15 124.79 11.63 o -1 8 0 311.32 305.23 13.59 o 0 8 0 233.11 250.71 17.71 o 1 8 0 593.06 608.76 20.90 o 2 8 0 1176.08 1150.82 56.67 o 3 8 0 66.15 55.74 11.28 o 4 8 0 2084.08 2029.25 58.98 o 5 8 0 218.38 238.18 16.50 o 6 8 0 213.94 207.80 46.16 o 7 8 0 1.73 40.15 33.69 o 8 8 0 8.67 57.11 34.06 o 9 8 0 24.05 14.48 26.58 o 10 8 0 70.20 81.18 38.07 o 11 8 0 22.31 79.34 60.26 o 12 8 0 85.01 133.40 48.49 o 13 8 0 80.10 291.01 109.04 o -9 9 0 8.75 126.01 105.05 o -8 9 0 186.46 231.06 78.85 o -7 9 0 82.22 48.38 44.91 o -5 9 0 0.25 33.13 46.20 o -4 9 0 39.08 105.80 56.64 o -3 9 0 511.43 484.81 50.28 o -2 9 0 1906.96 1653.68 51.37 o -1 9 0 21.56 42.80 13.94 o 0 9 0 4930.25 5151.22 34.36 o 1 9 0 1028.51 981.19 26.72 o 2 9 0 1890.92 1649.93 25.41 o 3 9 0 1125.22 1143.67 26.65 o 4 9 0 1.11 20.42 17.07 o 5 9 0 238.08 238.46 29.66 o 6 9 0 12.76 77.85 53.65 o 7 9 0 164.89 180.86 63.88 o 8 9 0 327.36 343.24 50.53 o 9 9 0 146.09 123.02 39.90 o 10 9 0 151.08 161.89 39.94 o 11 9 0 22.63 83.59 71.36 o 12 9 0 5.54 5.47 36.31 o 13 9 0 2.57 114.03 79.10 o -9 10 0 0.89 16.47 106.30 o -8 10 0 1.12 132.25 89.33 o -6 10 0 391.23 81.47 167.55 o -5 10 0 147.48 42.20 102.93 o -4 10 0 280.84 298.66 132.00 o -3 10 0 1628.06 1589.36 119.65 o -2 10 0 70.75 11.32 21.38 o -1 10 0 861.12 959.40 24.99 o 0 10 0 75.96 127.04 20.42 o 1 10 0 228.10 232.90 32.31 o 2 10 0 1089.78 938.08 24.89 o 3 10 0 217.35 184.62 44.33 o 4 10 0 699.84 679.46 22.13 o 5 10 0 945.84 948.71 32.23 o 6 10 0 21.53 170.36 70.49 o 7 10 0 598.57 561.58 76.35 o 8 10 0 161.13 235.95 112.04 o 9 10 0 0.27 112.04 83.84 o 12 10 0 35.83 7.48 14.76 o -8 11 0 256.73 350.06 93.95 o -6 11 0 795.74 783.71 312.78 o -5 11 0 1494.72 1477.61 345.46 o -4 11 0 252.13 227.96 77.73 o -3 11 0 1132.13 1252.52 48.41 o -2 11 0 1325.62 1301.23 41.52 o -1 11 0 1687.73 1729.52 49.52 o 0 11 0 1838.45 1874.33 19.22 o 1 11 0 1809.57 1888.69 32.63 o 2 11 0 1458.96 1373.82 28.99 o 3 11 0 646.97 597.01 40.42 o 4 11 0 2439.09 2391.55 68.11 o 5 11 0 4843.61 4710.25 100.59 o 6 11 0 128.37 239.74 44.03 o 7 11 0 773.71 969.44 42.48 o 8 11 0 450.14 629.10 133.04 o 9 11 0 68.57 347.43 54.65 o 10 11 0 1.80 374.53 69.62 o 11 11 0 211.64 170.92 47.99 o 12 11 0 109.42 10.98 320.89 o -6 12 0 216.59 3.11 108.79 o -5 12 0 865.50 905.90 134.87 o -4 12 0 17.15 58.39 62.13 o -3 12 0 2270.50 2420.26 53.71 o -2 12 0 1848.26 1765.12 29.43 o -1 12 0 867.59 799.69 23.94 o 0 12 0 4.23 16.77 17.96 o 1 12 0 1206.76 1254.61 22.53 o 2 12 0 921.91 921.62 58.56 o 3 12 0 27.25 56.64 50.90 o 4 12 0 1152.07 1117.45 83.30 o 5 12 0 639.04 679.23 44.49 o 6 12 0 272.47 330.69 32.20 o 7 12 0 267.59 357.11 65.42 o 8 12 0 408.00 579.58 102.50 o 9 12 0 19.41 251.65 138.36 o 10 12 0 12.17 279.71 70.12 o 11 12 0 9.84 313.46 176.66 o -7 13 0 23.27 8.73 83.59 o -6 13 0 212.01 262.67 75.48 o -5 13 0 22.42 45.66 71.61 o -4 13 0 238.09 179.80 46.85 o -3 13 0 752.39 725.81 45.89 o -2 13 0 71.39 123.04 29.50 o -1 13 0 1150.60 1170.16 46.22 o 0 13 0 1003.09 999.29 48.35 o 1 13 0 289.40 287.11 21.60 o 2 13 0 299.64 243.74 34.31 o 3 13 0 6.83 56.87 39.76 o 4 13 0 260.93 187.10 61.14 o 5 13 0 187.71 151.13 52.13 o 6 13 0 36.98 -12.73 172.67 o 7 13 0 505.78 514.17 40.48 o 8 13 0 32.11 76.18 50.33 o 9 13 0 5.50 179.05 69.61 o 10 13 0 117.08 287.28 55.36 o -6 14 0 0.43 32.49 62.41 o -4 14 0 92.79 -0.66 13.35 o -3 14 0 562.91 557.61 58.24 o -2 14 0 1.56 51.18 37.75 o -1 14 0 941.40 1003.66 42.09 o 0 14 0 367.68 415.74 40.43 o 1 14 0 127.22 162.22 35.91 o 2 14 0 233.53 267.74 30.28 o 3 14 0 58.40 188.27 55.64 o 4 14 0 28.63 186.39 64.13 o 5 14 0 414.28 393.81 97.19 o 6 14 0 48.89 70.86 73.11 o 7 14 0 607.43 460.55 54.46 o 8 14 0 110.01 8.14 38.43 o 9 14 0 87.27 192.14 61.76 o -5 15 0 149.34 159.92 62.86 o -4 15 0 149.34 3.54 29.94 o -3 15 0 125.89 58.60 57.29 o -2 15 0 298.62 244.28 53.80 o -1 15 0 0.76 13.84 24.51 o 0 15 0 190.85 199.85 33.52 o 1 15 0 5.07 91.41 41.21 o 2 15 0 103.44 135.90 54.06 o 3 15 0 324.47 399.40 56.36 o 4 15 0 113.69 172.70 48.53 o 5 15 0 145.59 293.94 71.61 o 6 15 0 194.62 376.03 77.60 o 7 15 0 0.42 220.08 81.84 o 8 15 0 31.36 264.99 89.33 o -2 16 0 450.25 498.54 59.34 o -1 16 0 124.67 150.19 44.11 o 0 16 0 0.17 26.49 42.21 o 1 16 0 1.06 106.80 70.37 o 2 16 0 13.07 172.61 48.80 o 3 16 0 176.67 257.39 57.96 o 4 16 0 37.00 208.60 73.61 o 5 16 0 89.45 368.05 76.10 o 6 16 0 17.76 232.06 83.59 o 7 16 0 33.14 238.29 88.33 o -1 17 0 14.98 42.11 52.05 o 0 17 0 451.63 558.27 46.26 o 1 17 0 201.27 203.01 65.87 o 2 17 0 0.02 171.80 54.03 o 3 17 0 6.52 57.71 56.55 o 5 17 0 61.77 140.48 82.34 o 6 17 0 152.54 463.36 87.33 o 0 18 0 212.56 232.55 85.84 o 1 18 0 174.26 244.03 84.59 o 2 18 0 94.66 217.82 54.42 o 3 18 0 162.97 171.67 76.35 o 5 18 0 99.94 27.70 90.83 o -5 -18 1 0.99 79.35 86.83 o -3 -18 1 25.40 97.59 71.61 o -2 -18 1 9.06 137.12 72.11 o -1 -18 1 28.23 82.44 54.36 o -6 -17 1 69.72 373.29 91.08 o -5 -17 1 128.01 348.08 81.59 o -4 -17 1 160.72 45.76 51.61 o -3 -17 1 68.31 98.18 45.02 o -2 -17 1 16.81 124.72 51.44 o -1 -17 1 80.28 125.07 56.17 o 0 -17 1 1.64 49.98 44.21 o 1 -17 1 1.64 54.73 50.55 o -7 -16 1 31.11 245.78 90.83 o -6 -16 1 809.54 838.85 256.01 o -5 -16 1 28.60 240.04 75.85 o -4 -16 1 144.21 306.55 134.12 o -3 -16 1 587.24 701.53 49.31 o -2 -16 1 10.85 94.26 39.20 o -1 -16 1 567.41 926.05 65.68 o 0 -16 1 90.10 87.79 37.18 o 1 -16 1 78.03 105.96 36.25 o 2 -16 1 68.91 47.18 46.19 o 3 -16 1 261.18 295.16 62.28 o -8 -15 1 74.87 59.39 90.58 o -7 -15 1 276.66 315.40 86.83 o -6 -15 1 67.20 108.54 78.85 o -5 -15 1 40.11 24.70 72.11 o -4 -15 1 1371.30 1336.77 40.84 o -3 -15 1 632.05 717.91 85.72 o -2 -15 1 31.17 76.37 31.77 o -1 -15 1 559.26 648.92 44.73 o 0 -15 1 449.09 584.53 45.60 o 1 -15 1 2.38 -5.39 29.88 o 2 -15 1 216.37 268.01 36.21 o 3 -15 1 68.08 123.76 96.07 o 4 -15 1 5.90 14.22 203.86 o 5 -15 1 130.73 97.56 77.60 o -10 -14 1 0.66 222.07 83.34 o -9 -14 1 4.22 104.40 58.40 o -8 -14 1 39.97 60.78 68.99 o -7 -14 1 13.26 119.19 55.85 o -6 -14 1 9.59 40.22 64.38 o -5 -14 1 0.89 24.91 59.01 o -4 -14 1 5.40 15.26 49.53 o -3 -14 1 451.85 487.85 54.33 o -2 -14 1 101.34 202.80 58.26 o -1 -14 1 879.72 902.47 30.83 o 0 -14 1 502.29 526.57 40.41 o 1 -14 1 128.75 144.78 26.65 o 2 -14 1 352.77 348.42 29.46 o 3 -14 1 8.48 15.83 47.53 o 5 -14 1 10.20 12.98 88.58 o 6 -14 1 38.67 57.12 62.41 o -10 -13 1 18.11 299.94 53.87 o -9 -13 1 78.56 322.64 42.11 o -8 -13 1 0.18 167.43 39.18 o -7 -13 1 40.26 85.23 36.44 o -6 -13 1 159.75 171.46 57.28 o -5 -13 1 9.68 72.47 36.20 o -4 -13 1 190.65 213.05 57.80 o -3 -13 1 6.36 60.54 26.61 o -2 -13 1 19.06 97.06 48.41 o -1 -13 1 37.95 127.58 39.57 o 0 -13 1 1.86 27.31 16.73 o 1 -13 1 241.19 278.12 25.13 o 2 -13 1 91.91 132.22 27.29 o 3 -13 1 197.28 185.82 38.10 o 4 -13 1 167.40 155.55 58.26 o 5 -13 1 1.38 24.45 72.61 o 6 -13 1 24.99 12.86 62.23 o 7 -13 1 5.35 -9.73 34.93 o -10 -12 1 36.29 345.79 53.21 o -9 -12 1 7.33 260.82 63.00 o -8 -12 1 249.82 503.91 37.06 o -7 -12 1 67.57 199.93 33.07 o -6 -12 1 19.58 94.31 32.23 o -5 -12 1 18.09 56.50 28.77 o -4 -12 1 136.40 175.39 32.50 o -3 -12 1 212.59 112.90 54.06 o -2 -12 1 135.91 151.95 16.67 o -1 -12 1 121.04 157.11 28.86 o 0 -12 1 1334.87 1480.23 31.91 o 1 -12 1 62.74 62.53 22.96 o 2 -12 1 468.95 488.19 25.91 o 3 -12 1 42.57 50.76 36.88 o 4 -12 1 5.94 20.21 62.38 o 5 -12 1 57.39 72.36 70.61 o 6 -12 1 48.77 9.48 58.39 o 7 -12 1 190.84 198.12 87.33 o -11 -11 1 110.91 62.09 55.34 o -10 -11 1 245.38 343.22 75.02 o -9 -11 1 104.42 16.59 27.17 o -8 -11 1 227.61 438.21 102.05 o -7 -11 1 222.55 467.96 55.90 o -6 -11 1 707.58 715.84 36.94 o -5 -11 1 1847.94 1794.38 79.59 o -4 -11 1 167.09 168.17 26.51 o -3 -11 1 5786.92 5535.57 76.92 o -2 -11 1 3942.87 3879.81 103.07 o -1 -11 1 33.04 56.46 15.62 o 0 -11 1 2749.80 2920.39 41.64 o 1 -11 1 1809.63 1985.58 38.76 o 2 -11 1 709.16 636.39 30.69 o 3 -11 1 316.43 303.81 36.52 o 4 -11 1 460.29 522.52 48.26 o 5 -11 1 983.38 915.48 187.64 o 6 -11 1 134.37 64.13 77.10 o 7 -11 1 22.54 51.15 88.33 o 8 -11 1 777.49 753.63 105.05 o -12 -10 1 25.53 84.84 83.59 o -11 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