(IUCr) Crystallography Journals Online checkcif report

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Acta Cryst. (2008). E64, m387-m388 [ doi:10.1107/S1600536808001372 ]

Bis(4,4'-bipyridinium) di--hydroxido-bis[dihydroxido(pyridine-2,6-dicarboxylato)antimonate(III,V)] octahydrate

J. Soleimannejad, H. Aghabozorg, Y. M. A. Golenji, J. Attar Gharamaleki and H. Adams

Key indicators

Single-crystal X-ray study
T = 150 K
Mean (C-C) = 0.003 Å
R factor = 0.023
wR factor = 0.060
Data-to-parameter ratio = 16.6

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT048_ALERT_1_C MoietyFormula Not Given ........................          ?
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.95      
PLAT154_ALERT_1_C The su's on the Cell Angles are Equal  (x 10000)        200 Deg. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H8B    ..  O3      ..       2.61 Ang. 
PLAT717_ALERT_1_C D...A   Unknown or Inconsistent Label ..........    CG1(N2/     

Alert level G
ABSTM02_ALERT_3_G  When printed, the submitted absorption T values will be
            replaced by the scaled T values. Since the ratio of scaled T's
            is identical to the ratio of reported T values, the scaling
            does not imply a change to the absorption corrections used in
            the study.
            Ratio of Tmax expected/reported      0.949
            Tmax scaled      0.583 Tmin scaled      0.557

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check