# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' nuchptm in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 439.85 _exptl_crystal_F_000 1828.80 _reflns_d_resolution_high 0.7996 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 13.9051 _cell_length_b 15.3559 _cell_length_c 17.1261 _cell_angle_alpha 71.930 _cell_angle_beta 72.045 _cell_angle_gamma 87.621 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8192.38 9865.09 244.54 o 3 0 0 40066.70 42724.20 720.59 o 4 0 0 4571.88 4530.49 91.47 o 5 0 0 20962.61 21817.87 378.70 o 6 0 0 34445.59 37332.51 639.31 o 7 0 0 4599.00 4233.59 223.14 o 8 0 0 1112.85 1014.95 61.66 o 9 0 0 10367.45 10079.22 201.48 o 10 0 0 1864.83 2099.32 126.65 o 11 0 0 1257.84 1047.81 115.56 o 12 0 0 15379.09 14797.16 301.47 o 13 0 0 3292.82 3090.05 188.22 o 14 0 0 345.37 382.67 123.34 o 15 0 0 8118.80 8273.14 306.79 o 16 0 0 562.37 813.58 154.08 o -16 1 0 2319.55 2224.02 181.51 o -15 1 0 282.97 209.33 130.15 o -14 1 0 452.63 443.19 92.11 o -13 1 0 8336.23 8182.48 285.98 o -12 1 0 11655.66 11488.36 353.10 o -11 1 0 923.21 833.42 114.78 o -10 1 0 782.27 675.06 103.89 o -9 1 0 9250.83 9227.40 254.17 o -8 1 0 380.82 408.39 70.91 o -7 1 0 13987.29 14469.03 267.96 o -6 1 0 20336.95 20649.20 365.51 o -5 1 0 3274.86 3209.25 85.21 o -4 1 0 1824.17 2080.93 58.36 o -3 1 0 13620.72 14780.41 258.88 o -2 1 0 10953.98 12055.25 210.26 o 1 1 0 19489.04 18827.30 456.59 o 2 1 0 88485.06 96960.32 1755.07 o 3 1 0 160479.06 164875.41 2722.93 o 4 1 0 96598.19 104527.45 1418.19 o 5 1 0 726.93 678.35 32.61 o 6 1 0 147.46 170.08 40.00 o 7 1 0 10237.28 10095.20 151.01 o 8 1 0 47477.00 49633.95 594.39 o 9 1 0 19966.87 19970.20 370.84 o 10 1 0 8231.82 7824.16 176.20 o 11 1 0 128.16 105.13 66.60 o 12 1 0 6454.42 6064.26 159.18 o 13 1 0 209.73 231.90 110.70 o 14 1 0 6062.52 5940.38 247.26 o 15 1 0 3774.89 3863.04 213.41 o 16 1 0 849.38 858.71 159.33 o -16 2 0 899.44 1161.81 163.22 o -15 2 0 5477.13 6085.12 270.03 o -14 2 0 13503.69 13324.26 416.91 o -13 2 0 9992.33 9741.55 326.44 o -12 2 0 653.13 662.61 124.12 o -11 2 0 4851.14 4642.58 194.35 o -10 2 0 8496.25 8443.34 187.45 o -9 2 0 62573.28 63773.08 1093.20 o -8 2 0 10911.02 10777.35 213.98 o -7 2 0 45.32 -0.46 51.14 o -6 2 0 10830.60 10844.87 207.68 o -5 2 0 2442.62 2668.07 138.22 o -4 2 0 13766.26 13981.01 251.31 o -3 2 0 31037.80 32251.50 450.36 o -2 2 0 2983.85 2861.63 44.79 o -1 2 0 8954.64 10529.78 130.35 o 0 2 0 1620.87 1253.37 28.60 o 1 2 0 1488.57 2227.93 133.16 o 2 2 0 6165.98 5748.66 109.81 o 3 2 0 49637.82 52007.29 710.46 o 4 2 0 25465.13 28068.01 390.48 o 5 2 0 28264.97 30343.44 422.95 o 6 2 0 31910.12 35242.99 564.77 o 7 2 0 19963.33 19635.54 283.72 o 8 2 0 647.86 622.68 43.96 o 9 2 0 1176.28 1191.68 98.34 o 10 2 0 5496.56 5434.74 137.64 o 11 2 0 17058.33 17755.34 377.22 o 12 2 0 12495.97 12706.78 386.75 o 13 2 0 4424.92 4334.42 203.69 o 14 2 0 423.96 431.89 130.15 o 15 2 0 736.57 1026.80 157.77 o 16 2 0 40.27 -21.40 150.58 o -16 3 0 5284.72 5153.45 268.86 o -15 3 0 8005.77 8043.19 313.41 o -14 3 0 2000.73 2119.55 172.75 o -13 3 0 462.60 271.19 133.26 o -12 3 0 1738.81 1746.80 146.69 o -11 3 0 1391.91 1287.68 185.69 o -10 3 0 1689.12 1737.11 90.95 o -9 3 0 3032.14 2819.61 213.22 o -8 3 0 786.69 656.72 64.37 o -7 3 0 59216.25 61685.43 1054.79 o -6 3 0 69701.77 71918.00 1221.31 o -5 3 0 21736.93 22460.83 330.25 o -4 3 0 973.78 911.92 30.90 o -3 3 0 550.33 425.68 25.88 o -2 3 0 56.30 65.82 23.30 o -1 3 0 5915.99 6169.03 83.58 o 0 3 0 33411.12 32554.13 390.10 o 1 3 0 18693.49 20657.90 289.01 o 2 3 0 8.02 -5.59 34.84 o 3 3 0 2269.07 2512.59 82.49 o 4 3 0 94.86 130.19 35.87 o 5 3 0 63237.78 65832.39 901.98 o 6 3 0 52069.59 52234.10 721.21 o 7 3 0 32786.04 35763.21 502.31 o 8 3 0 22.09 70.10 43.49 o 9 3 0 3308.16 3378.93 102.74 o 10 3 0 1542.30 1822.87 125.29 o 11 3 0 181.58 45.91 102.14 o 12 3 0 472.82 563.01 118.09 o 13 3 0 469.56 663.20 129.76 o 14 3 0 5437.86 5602.06 248.43 o 15 3 0 8010.65 8142.99 318.47 o 16 3 0 1346.48 1190.02 180.93 o -16 4 0 4.49 3.89 175.28 o -15 4 0 46.54 156.02 151.74 o -14 4 0 3014.68 2818.54 193.18 o -13 4 0 8904.17 9092.36 319.05 o -12 4 0 24766.93 24702.31 669.62 o -11 4 0 20411.34 20028.04 386.18 o -10 4 0 10293.58 10513.60 614.17 o -9 4 0 27.73 6.08 65.69 o -8 4 0 563.69 512.32 64.38 o -7 4 0 9091.15 8826.11 184.95 o -6 4 0 5057.84 4648.66 129.43 o -5 4 0 1289.34 1328.38 40.57 o -4 4 0 55031.39 57011.14 679.37 o -3 4 0 42047.89 43743.63 538.46 o -2 4 0 47700.74 49216.14 586.59 o -1 4 0 8288.71 8007.57 106.71 o 0 4 0 1064.69 1040.20 30.92 o 1 4 0 1996.46 2233.73 52.10 o 2 4 0 7468.24 7441.74 162.35 o 3 4 0 27633.90 28096.56 484.81 o 4 4 0 2746.86 2776.53 75.75 o 5 4 0 1280.40 1126.90 43.36 o 6 4 0 1107.12 1004.66 46.78 o 7 4 0 16599.00 17999.61 265.96 o 8 4 0 35452.97 35733.11 506.09 o 9 4 0 23407.54 23431.75 624.29 o 10 4 0 3139.72 3150.04 165.17 o 11 4 0 7528.37 7171.44 261.47 o 12 4 0 40.41 1.36 115.56 o 13 4 0 2971.02 2793.06 182.48 o 14 4 0 3342.76 3618.50 213.22 o 15 4 0 3646.36 3618.11 227.23 o -16 5 0 2411.85 2693.84 223.14 o -15 5 0 5062.89 4952.48 251.93 o -14 5 0 1138.90 900.15 160.50 o -13 5 0 62.97 190.46 133.46 o -12 5 0 158.47 151.34 86.99 o -11 5 0 628.65 684.66 87.66 o -10 5 0 16085.33 15748.09 314.25 o -9 5 0 31059.41 30383.37 550.28 o -8 5 0 33526.72 32662.74 583.79 o -7 5 0 19837.46 20476.54 391.57 o -6 5 0 17771.35 18636.14 337.94 o -5 5 0 265.36 169.50 34.07 o -4 5 0 77078.44 78261.44 929.66 o -3 5 0 43506.14 43795.24 526.54 o -2 5 0 3839.74 4131.83 67.96 o -1 5 0 21045.40 22392.43 283.39 o 0 5 0 15268.50 15729.74 198.29 o 1 5 0 5989.98 5995.91 85.81 o 2 5 0 481.86 383.68 51.94 o 3 5 0 1094.46 1228.72 44.25 o 4 5 0 445.86 623.89 57.13 o 5 5 0 7796.89 7111.47 152.98 o 6 5 0 20920.85 20911.76 506.77 o 7 5 0 2423.17 2429.10 86.77 o 8 5 0 44.29 20.26 59.78 o 9 5 0 150.93 159.48 66.96 o 10 5 0 217.29 174.31 104.86 o 11 5 0 13631.50 14018.78 423.52 o 12 5 0 15182.58 14891.89 453.48 o 13 5 0 2544.42 2333.93 178.79 o 14 5 0 1578.10 1757.50 177.23 o 15 5 0 899.40 976.41 174.70 o -15 6 0 1117.53 1247.61 180.34 o -14 6 0 24.47 -42.80 150.38 o -13 6 0 4563.89 5006.57 236.76 o -12 6 0 8763.45 8446.87 542.48 o -11 6 0 279.89 318.14 84.92 o -10 6 0 1329.50 1473.03 94.27 o -9 6 0 3073.29 2887.44 109.15 o -8 6 0 1003.04 990.60 77.38 o -7 6 0 20887.93 21864.68 530.39 o -6 6 0 28318.68 28324.78 485.44 o -5 6 0 29467.47 30722.63 379.79 o -4 6 0 2462.17 2498.72 56.23 o -3 6 0 440.04 574.25 52.50 o -2 6 0 37815.52 39345.21 476.63 o -1 6 0 110014.39 112742.35 1530.44 o 0 6 0 79986.95 81126.04 963.10 o 1 6 0 3258.10 3278.49 58.69 o 2 6 0 818.17 749.42 43.90 o 3 6 0 11980.06 11315.09 176.06 o 4 6 0 10289.98 10348.37 162.89 o 5 6 0 1168.74 1059.86 69.27 o 6 6 0 6157.63 6292.53 171.78 o 7 6 0 7.84 6.58 62.83 o 8 6 0 5927.26 5488.68 139.28 o 9 6 0 16920.44 16238.42 314.17 o 10 6 0 60.29 46.88 104.47 o 11 6 0 4410.47 4359.13 206.22 o 12 6 0 3959.62 3362.09 193.38 o 13 6 0 238.03 260.88 142.60 o 14 6 0 3584.00 3487.96 221.78 o 15 6 0 2788.74 2562.72 215.94 o -15 7 0 42.33 163.03 170.03 o -14 7 0 31.68 116.14 154.27 o -13 7 0 4372.50 4559.04 162.25 o -12 7 0 3143.34 3055.97 130.82 o -11 7 0 134.09 152.27 84.93 o -10 7 0 5238.87 4908.57 328.49 o -9 7 0 9175.54 8438.24 198.08 o -8 7 0 589.15 588.78 75.31 o -7 7 0 2792.34 2774.77 80.08 o -6 7 0 10337.19 10238.89 175.08 o -5 7 0 2978.93 2924.17 64.62 o -4 7 0 2881.54 2787.99 62.03 o -3 7 0 20201.67 20367.06 262.58 o -2 7 0 7468.50 8043.01 214.44 o -1 7 0 6074.00 6679.12 101.31 o 0 7 0 1282.17 1467.16 53.18 o 1 7 0 22120.14 22282.63 279.44 o 2 7 0 79027.00 78402.98 1078.35 o 3 7 0 72570.60 74423.71 1024.68 o 4 7 0 15790.51 15444.86 234.42 o 5 7 0 817.95 737.15 70.50 o 6 7 0 1160.97 1212.92 142.99 o 7 7 0 3509.63 3492.97 114.19 o 8 7 0 13497.61 13148.61 267.11 o 9 7 0 9795.49 9489.86 211.39 o 10 7 0 37.00 -112.45 112.45 o 11 7 0 3215.29 2994.60 186.76 o 12 7 0 1754.07 1771.70 167.11 o 13 7 0 492.14 288.90 147.27 o 14 7 0 2242.41 2524.39 206.02 o -15 8 0 8736.69 9276.79 367.10 o -14 8 0 7123.87 7270.47 308.35 o -13 8 0 809.47 860.77 113.83 o -12 8 0 88.07 -7.76 95.72 o -11 8 0 1788.94 1490.54 104.79 o -10 8 0 12994.85 12027.99 264.60 o -9 8 0 13783.82 13663.88 326.83 o -8 8 0 405.07 436.76 61.29 o -7 8 0 535.14 684.87 155.56 o -6 8 0 6218.87 6203.57 116.22 o -5 8 0 2720.68 2759.59 81.21 o -4 8 0 12456.60 12512.09 173.03 o -3 8 0 32582.77 34893.49 430.95 o -2 8 0 4943.85 4761.60 83.83 o -1 8 0 1865.69 2028.36 54.41 o 0 8 0 4089.24 4181.30 89.27 o 1 8 0 3454.35 3170.04 63.80 o 2 8 0 13874.04 13605.86 181.03 o 3 8 0 17634.74 18106.64 274.57 o 4 8 0 4432.17 4407.58 95.44 o 5 8 0 26597.43 26509.59 632.75 o 6 8 0 6113.71 5750.12 161.76 o 7 8 0 7689.17 7472.58 182.77 o 8 8 0 276.88 293.71 174.80 o 9 8 0 2295.98 2283.51 107.81 o 10 8 0 2815.83 2729.63 177.81 o 11 8 0 10152.93 9899.91 348.62 o 12 8 0 8007.27 7763.83 311.85 o 13 8 0 289.20 307.57 158.94 o 14 8 0 353.96 27.43 170.23 o -14 9 0 888.34 795.30 126.96 o -13 9 0 626.69 673.51 116.19 o -12 9 0 5250.99 5264.82 172.28 o -11 9 0 3918.94 3805.22 142.51 o -10 9 0 2748.87 2605.80 118.85 o -9 9 0 0.29 44.33 81.30 o -8 9 0 15152.49 15005.35 249.48 o -7 9 0 26040.58 24909.91 379.64 o -6 9 0 29060.85 29659.08 385.93 o -5 9 0 3056.20 2948.34 70.57 o -4 9 0 419.60 383.17 45.89 o -3 9 0 274.41 194.40 43.33 o -2 9 0 1250.66 1191.95 71.58 o -1 9 0 22691.25 22511.54 289.16 o 0 9 0 22179.01 21708.03 318.85 o 1 9 0 17149.87 17199.35 226.29 o 2 9 0 140.53 209.36 52.74 o 3 9 0 2962.82 3048.61 85.50 o 4 9 0 11204.22 10756.91 230.60 o 5 9 0 28504.34 27762.74 1249.65 o 6 9 0 13862.78 13139.33 273.80 o 7 9 0 2658.62 2532.78 113.29 o 8 9 0 2089.08 2083.40 105.88 o 9 9 0 2111.83 2109.48 110.78 o 10 9 0 1356.14 973.69 149.02 o 11 9 0 102.76 196.10 143.38 o 12 9 0 27.35 96.69 152.13 o 13 9 0 869.22 877.97 179.95 o -14 10 0 3638.05 3755.32 172.29 o -13 10 0 7438.31 7441.00 220.51 o -12 10 0 10490.64 10383.58 258.66 o -11 10 0 3212.76 3011.96 136.85 o -10 10 0 690.50 623.02 95.95 o -9 10 0 6042.08 5949.92 171.82 o -8 10 0 945.70 1022.96 72.67 o -7 10 0 1099.19 1128.57 89.06 o -6 10 0 186.53 150.85 50.74 o -5 10 0 7603.24 7786.00 127.31 o -4 10 0 29212.71 29408.24 374.51 o -3 10 0 12920.36 12705.41 180.48 o -2 10 0 5208.13 5256.37 109.62 o -1 10 0 18.25 40.82 44.02 o 0 10 0 4.01 -38.53 42.42 o 1 10 0 9104.69 8755.96 158.65 o 2 10 0 17448.46 17207.21 270.70 o 3 10 0 20240.37 19857.45 305.95 o 4 10 0 4211.66 3691.13 126.14 o 5 10 0 152.90 342.48 84.10 o 6 10 0 423.60 297.07 85.36 o 7 10 0 4102.43 4013.70 139.86 o 8 10 0 18367.65 17780.73 358.65 o 9 10 0 10744.88 10035.29 238.25 o 10 10 0 3916.09 3509.56 212.25 o 11 10 0 393.93 503.09 160.89 o 12 10 0 51.97 215.36 165.75 o 13 10 0 334.58 277.61 181.12 o -13 11 0 36.74 -29.64 116.51 o -12 11 0 101.05 172.16 109.91 o -11 11 0 1545.36 1407.43 119.47 o -10 11 0 13525.89 13577.78 300.98 o -9 11 0 12756.43 13014.19 233.09 o -8 11 0 22087.79 21253.48 340.09 o -7 11 0 1282.95 1163.39 81.53 o -6 11 0 849.96 821.53 59.87 o -5 11 0 2555.37 2327.45 72.77 o -4 11 0 14898.49 14954.69 210.97 o -3 11 0 1142.51 1158.62 59.30 o -2 11 0 40.84 112.15 69.86 o -1 11 0 12206.25 12176.37 187.21 o 0 11 0 8068.06 7832.62 150.35 o 1 11 0 2647.46 2285.60 101.13 o 2 11 0 68.88 78.20 61.37 o 3 11 0 69.14 33.05 79.18 o 4 11 0 145.00 102.32 85.17 o 5 11 0 12377.19 12336.44 271.19 o 6 11 0 437.59 581.52 95.54 o 7 11 0 1637.24 1451.07 110.23 o 8 11 0 1989.01 1900.19 143.57 o 9 11 0 1222.48 1151.30 133.65 o 10 11 0 4524.84 4671.18 250.18 o 11 11 0 7107.50 7022.23 310.69 o 12 11 0 4724.39 4582.07 269.25 o -13 12 0 1640.43 1517.13 142.81 o -12 12 0 1160.30 1059.82 128.55 o -11 12 0 20.74 -45.60 107.02 o -10 12 0 893.69 834.24 87.65 o -9 12 0 953.66 962.49 84.35 o -8 12 0 1997.27 2015.76 99.76 o -7 12 0 12734.78 12033.55 217.57 o -6 12 0 16411.76 16104.90 229.51 o -5 12 0 5730.09 5708.35 123.55 o -4 12 0 15.12 40.42 54.37 o -3 12 0 4625.70 4247.04 92.85 o -2 12 0 9944.71 10024.26 155.81 o -1 12 0 23076.72 23301.76 358.81 o 0 12 0 16004.20 16417.75 554.55 o 1 12 0 67.05 108.28 68.57 o 2 12 0 1646.05 1825.69 85.18 o 3 12 0 2152.90 1822.69 109.41 o 4 12 0 139.15 212.94 91.56 o 5 12 0 930.45 801.91 144.45 o 6 12 0 4856.96 4660.36 160.16 o 7 12 0 1801.99 1973.69 122.63 o 8 12 0 4897.94 4337.47 161.14 o 9 12 0 1099.95 1111.48 121.40 o 10 12 0 368.71 300.37 164.78 o 11 12 0 218.18 371.77 181.51 o -12 13 0 402.45 573.08 130.20 o -11 13 0 44.15 -14.21 114.23 o -10 13 0 1054.61 1004.82 95.64 o -9 13 0 237.50 238.66 81.25 o -8 13 0 2651.51 2384.81 139.79 o -7 13 0 6640.77 6300.19 159.00 o -6 13 0 4303.06 4453.24 119.20 o -5 13 0 1059.82 1077.12 68.14 o -4 13 0 5157.56 5403.76 175.53 o -3 13 0 4739.29 4361.61 115.31 o -2 13 0 989.80 955.87 74.53 o -1 13 0 309.91 274.88 68.70 o 0 13 0 327.56 445.93 73.08 o 1 13 0 21670.96 21953.31 518.04 o 2 13 0 14587.02 14009.97 301.24 o 3 13 0 8268.41 8845.80 222.58 o 4 13 0 1899.28 1980.73 168.57 o 5 13 0 4.23 -96.88 96.88 o 6 13 0 3.11 14.97 100.99 o 7 13 0 2559.62 2438.51 205.92 o 8 13 0 4862.05 5092.76 179.56 o 9 13 0 1934.43 1838.37 137.50 o 10 13 0 135.24 -1.56 172.95 o -11 14 0 2242.75 2078.76 147.97 o -10 14 0 3665.23 3928.69 133.85 o -9 14 0 1443.17 1515.26 100.39 o -8 14 0 114.73 -18.18 81.85 o -7 14 0 54.38 70.72 78.41 o -6 14 0 16.88 -30.13 75.00 o -5 14 0 3004.47 3029.28 91.22 o -4 14 0 3455.74 3844.18 166.73 o -3 14 0 6353.43 6522.28 147.86 o -2 14 0 80.34 90.61 71.44 o -1 14 0 186.91 232.86 72.79 o 0 14 0 63.08 14.66 71.97 o 1 14 0 3352.58 3182.33 133.55 o 2 14 0 53.88 231.42 94.50 o 3 14 0 330.31 328.75 102.90 o 4 14 0 5983.76 6013.96 187.16 o 5 14 0 6203.54 5613.00 299.30 o 6 14 0 5505.65 6210.15 196.39 o 7 14 0 1174.04 1158.65 125.97 o 8 14 0 265.87 187.90 118.71 o 9 14 0 389.73 207.70 124.96 o -10 15 0 342.52 365.55 101.52 o -9 15 0 918.53 975.48 100.74 o -8 15 0 4932.63 5157.64 185.60 o -7 15 0 6631.08 6660.18 163.62 o -6 15 0 4974.46 4791.51 170.82 o -5 15 0 921.78 909.08 89.52 o -4 15 0 9.20 8.15 78.17 o -3 15 0 56.25 101.23 76.99 o -2 15 0 2226.09 2172.54 99.33 o -1 15 0 10939.12 11112.61 211.83 o 0 15 0 5688.53 5442.10 252.67 o 1 15 0 149.89 159.39 134.72 o 2 15 0 135.72 243.53 102.47 o 3 15 0 565.66 825.05 113.39 o 4 15 0 3992.31 4073.92 375.57 o 5 15 0 1936.44 2217.31 143.69 o 6 15 0 113.94 265.76 119.16 o 7 15 0 586.49 756.14 129.17 o 8 15 0 2260.85 2649.70 319.15 o -8 16 0 251.24 481.13 166.04 o -7 16 0 224.21 124.60 113.42 o -6 16 0 285.23 353.46 114.95 o -5 16 0 6152.25 6390.50 200.54 o -4 16 0 5919.07 5633.46 260.89 o -3 16 0 4635.89 4767.85 233.30 o -2 16 0 243.31 133.24 85.31 o -1 16 0 155.89 120.90 84.68 o 0 16 0 150.30 46.13 100.95 o 1 16 0 6104.50 6118.18 408.44 o 2 16 0 4609.53 4719.62 249.02 o 3 16 0 2684.84 2657.97 212.34 o 4 16 0 23.70 62.37 115.75 o 5 16 0 0.21 -98.62 129.57 o 6 16 0 335.70 319.75 127.40 o 7 16 0 3656.20 3843.76 311.17 o -6 17 0 13.04 22.22 120.07 o -5 17 0 847.21 847.83 102.45 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