# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 602.97 _exptl_crystal_F_000 1600.00 _reflns_d_resolution_high 0.7964 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.5716 _cell_length_b 13.7737 _cell_length_c 15.8867 _cell_angle_alpha 75.301 _cell_angle_beta 69.112 _cell_angle_gamma 65.617 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11250.58 13917.92 637.11 o 2 0 0 485.66 506.78 36.09 o 3 0 0 86079.45 103603.23 4738.52 o 4 0 0 37041.63 42814.07 1963.69 o 5 0 0 54546.61 66311.13 3045.72 o 6 0 0 162657.59 191382.67 8722.53 o 7 0 0 4735.69 5258.87 276.27 o 8 0 0 17.65 43.44 32.19 o 9 0 0 4513.76 4975.10 331.60 o 10 0 0 35743.40 39199.23 2153.41 o 11 0 0 11786.94 12360.50 744.99 o 12 0 0 6288.37 6574.12 667.05 o 13 0 0 19191.32 19649.39 1679.30 o -13 1 0 3128.43 3301.20 491.57 o -12 1 0 23108.74 24178.50 2021.23 o -11 1 0 11909.22 12378.70 1109.83 o -10 1 0 15432.99 16561.68 966.65 o -9 1 0 19483.92 21260.88 1203.66 o -8 1 0 1692.52 1761.81 127.73 o -7 1 0 856.55 1010.69 89.11 o -6 1 0 150531.59 174502.48 7920.75 o -5 1 0 461.86 486.40 66.14 o -4 1 0 14121.42 15756.82 739.06 o -3 1 0 9051.37 9570.88 459.84 o -2 1 0 110540.88 125489.50 5698.08 o -1 1 0 59044.00 65438.76 3001.65 o 0 1 0 357890.78 167741.75 13818.98 o 1 1 0 8355.59 9503.32 438.34 o 2 1 0 22361.58 27686.07 1274.57 o 3 1 0 1269.83 1582.17 84.90 o 4 1 0 256627.30 306108.00 13952.54 o 5 1 0 71254.05 85902.42 3924.78 o 6 1 0 73597.73 89949.03 4115.23 o 7 1 0 34602.38 41519.13 1921.69 o 8 1 0 1487.89 1951.80 128.57 o 9 1 0 2967.38 3296.55 237.46 o 10 1 0 44221.17 51837.91 2812.20 o 11 1 0 3681.73 3706.86 274.80 o 12 1 0 12.15 -7.65 117.46 o 13 1 0 18918.66 21137.63 1767.45 o 14 1 0 2184.38 2488.20 407.53 o -13 2 0 532.38 536.26 213.60 o -12 2 0 32369.16 28684.24 2381.61 o -11 2 0 1750.90 2460.32 401.79 o -10 2 0 4129.71 4563.12 723.21 o -9 2 0 15941.97 18306.41 1056.28 o -8 2 0 11425.89 11352.43 569.32 o -7 2 0 16971.30 18816.28 898.49 o -6 2 0 105221.12 117839.98 5379.64 o -5 2 0 14923.77 16694.08 792.54 o -4 2 0 1539.66 1681.74 111.60 o -3 2 0 4134.88 4306.03 221.84 o -2 2 0 81791.31 85682.45 3927.82 o -1 2 0 40601.24 41594.78 2239.34 o 0 2 0 24896.55 19187.73 882.81 o 1 2 0 31300.57 32272.74 1483.88 o 2 2 0 8289.06 9480.32 439.53 o 3 2 0 44.92 111.23 41.20 o 4 2 0 175968.97 198639.61 9048.35 o 5 2 0 6238.82 7621.58 367.88 o 6 2 0 57.67 54.42 23.03 o 7 2 0 43500.76 47479.24 2191.52 o 8 2 0 13946.70 14977.95 988.49 o 9 2 0 1231.12 1122.31 120.18 o 10 2 0 22957.93 24523.16 1362.74 o 11 2 0 1495.18 1888.25 182.00 o 12 2 0 3527.49 3895.31 289.04 o 13 2 0 14070.70 14899.87 888.03 o 14 2 0 4939.96 4954.27 546.92 o -12 3 0 22814.30 20061.83 1749.82 o -11 3 0 587.43 239.43 157.43 o -10 3 0 382.27 525.19 206.22 o -9 3 0 5530.41 5442.80 375.33 o -8 3 0 36942.58 37847.79 1776.69 o -7 3 0 28575.39 30599.72 1445.22 o -6 3 0 38820.00 41656.69 1942.72 o -5 3 0 17683.34 18097.93 866.72 o -4 3 0 1919.09 1917.45 124.53 o -3 3 0 70.75 218.21 37.22 o -2 3 0 105739.40 109655.43 6287.18 o -1 3 0 5313.56 5165.96 411.79 o 0 3 0 325.43 477.22 120.54 o 1 3 0 91804.23 89965.38 4098.78 o 2 3 0 17673.26 18191.38 844.96 o 3 3 0 4118.14 4104.19 202.01 o 4 3 0 103959.13 116297.77 5289.29 o 5 3 0 18601.64 20028.91 1087.42 o 6 3 0 29475.49 35434.26 1627.20 o 7 3 0 27868.18 29599.95 1374.92 o 8 3 0 29101.50 32657.25 1518.05 o 9 3 0 5801.11 6205.11 381.64 o 10 3 0 2548.01 2500.88 192.35 o 11 3 0 53988.78 55286.77 2991.73 o 12 3 0 1604.13 1761.93 178.62 o 13 3 0 4467.90 4275.57 315.16 o 14 3 0 11899.09 11478.78 1016.35 o -12 4 0 9078.64 8008.25 844.98 o -11 4 0 5662.00 5433.13 621.13 o -10 4 0 3260.33 2386.53 397.28 o -9 4 0 182.81 145.54 136.94 o -8 4 0 84443.01 85227.46 3933.59 o -7 4 0 5774.03 5327.09 297.64 o -6 4 0 2662.28 2802.36 179.88 o -5 4 0 43913.77 43657.33 4266.72 o -4 4 0 13689.37 13748.59 667.95 o -3 4 0 13096.67 11561.05 636.37 o -2 4 0 93275.15 71429.76 6424.48 o -1 4 0 24060.22 16579.82 1297.19 o 0 4 0 14793.44 14494.56 732.70 o 1 4 0 7568.79 6437.52 403.64 o 2 4 0 23980.48 23463.18 1086.52 o 3 4 0 314.57 423.39 51.83 o 4 4 0 4084.16 4343.13 216.22 o 5 4 0 116033.66 126976.01 5771.81 o 6 4 0 11841.96 12971.67 614.23 o 7 4 0 4536.51 5050.18 258.94 o 8 4 0 34999.49 37646.63 2034.09 o 9 4 0 1080.48 1095.14 113.61 o 10 4 0 2802.37 2887.43 209.88 o 11 4 0 79257.26 79318.20 4254.15 o 12 4 0 483.02 515.74 131.61 o 13 4 0 235.28 312.14 84.18 o 14 4 0 5227.26 5586.24 387.60 o -11 5 0 6273.59 5656.57 648.60 o -10 5 0 7717.53 5575.81 625.64 o -9 5 0 2036.17 1502.60 312.41 o -8 5 0 41757.09 30252.44 2455.81 o -7 5 0 7433.43 7799.53 419.26 o -6 5 0 225.69 258.38 61.32 o -5 5 0 11043.68 10974.61 577.56 o -4 5 0 55835.66 56291.47 3259.72 o -3 5 0 15383.20 14275.97 708.20 o -2 5 0 35063.88 28063.09 1678.36 o -1 5 0 130856.85 116250.30 5255.09 o 0 5 0 1620.08 1557.57 113.79 o 1 5 0 492.04 593.49 144.33 o 2 5 0 48053.74 44064.66 2015.23 o 3 5 0 4.58 33.29 14.93 o 4 5 0 7103.73 7396.12 359.26 o 5 5 0 180588.44 191542.14 8709.91 o 6 5 0 373.68 508.54 50.79 o 7 5 0 29.90 22.30 22.98 o 8 5 0 19446.54 20892.65 980.57 o 9 5 0 21806.70 21823.18 1203.68 o 10 5 0 22102.97 22867.46 1265.86 o 11 5 0 41317.55 42393.61 2304.58 o 12 5 0 6473.56 6786.88 430.65 o 13 5 0 34.75 25.61 75.44 o 14 5 0 271.18 260.68 120.54 o -10 6 0 9557.31 9241.49 915.91 o -9 6 0 2822.11 3045.78 446.06 o -8 6 0 10962.26 11606.70 1061.45 o -7 6 0 21466.94 20028.01 1257.64 o -6 6 0 505.33 441.35 114.92 o -5 6 0 1054.35 1049.00 112.45 o -4 6 0 36688.11 34512.98 1613.45 o -3 6 0 39.64 148.44 87.74 o -2 6 0 720.03 878.49 97.02 o -1 6 0 111138.59 111126.29 5090.94 o 0 6 0 2666.45 3297.83 193.94 o 1 6 0 5876.65 5903.02 309.96 o 2 6 0 20358.16 16624.92 1014.92 o 3 6 0 12932.57 11967.07 568.24 o 4 6 0 43845.84 43822.55 2014.39 o 5 6 0 95666.07 98577.34 4487.88 o 6 6 0 18942.28 19000.44 892.34 o 7 6 0 430.36 493.39 55.43 o 8 6 0 1468.66 1516.87 103.45 o 9 6 0 67394.14 67681.55 3623.36 o 10 6 0 21857.75 21396.77 1187.88 o 11 6 0 10087.67 9980.85 591.92 o 12 6 0 18563.64 17244.33 983.48 o 13 6 0 2439.85 2454.84 256.45 o 14 6 0 772.29 1105.83 150.16 o -10 7 0 14278.33 16043.15 1421.42 o -9 7 0 142.02 116.03 145.54 o -8 7 0 299.28 448.93 185.72 o -7 7 0 27795.53 28296.97 2978.55 o -6 7 0 5.40 83.45 90.17 o -5 7 0 35.39 82.73 60.14 o -4 7 0 17020.91 17672.41 1007.83 o -3 7 0 5992.73 6019.19 450.65 o -2 7 0 14683.75 15100.34 1133.56 o -1 7 0 64200.24 73142.16 3388.94 o 0 7 0 4798.16 4424.88 250.79 o 1 7 0 1216.58 1233.60 167.96 o 2 7 0 12241.19 10859.56 614.85 o 3 7 0 79389.40 74486.63 3358.65 o 4 7 0 36019.09 35239.86 1628.83 o 5 7 0 34060.09 34995.73 1620.58 o 6 7 0 30203.78 29273.21 1359.43 o 7 7 0 3797.98 3678.23 201.08 o 8 7 0 3871.39 4315.34 232.59 o 9 7 0 64044.25 59511.49 4443.43 o 10 7 0 4293.24 4024.40 269.83 o 11 7 0 749.05 621.42 94.56 o 12 7 0 9837.67 9425.12 658.44 o 13 7 0 14546.06 14197.55 828.53 o 14 7 0 3147.01 3063.57 243.97 o -9 8 0 1597.23 2028.20 355.87 o -8 8 0 2863.69 4051.48 508.79 o -7 8 0 15626.19 17833.54 3035.33 o -6 8 0 2663.34 2725.78 449.96 o -5 8 0 507.31 625.27 175.68 o -4 8 0 3292.03 3147.00 347.49 o -3 8 0 40489.31 51483.13 3962.92 o -2 8 0 14757.31 16729.55 1125.29 o -1 8 0 25064.11 29766.65 1415.12 o 0 8 0 15490.19 18408.94 887.43 o 1 8 0 6383.22 7039.47 372.11 o 2 8 0 235.56 409.03 104.33 o 4 8 0 2830.68 2576.13 152.54 o 5 8 0 6048.99 6173.10 316.99 o 6 8 0 28782.04 29578.20 1731.85 o 7 8 0 21847.01 21791.04 1029.59 o 8 8 0 12466.73 12384.73 603.43 o 9 8 0 65465.19 65263.83 3500.15 o 10 8 0 1833.77 1765.54 153.76 o 11 8 0 1215.77 1143.41 127.32 o 12 8 0 3229.14 3019.80 227.19 o 13 8 0 22657.46 22002.51 1241.07 o 14 8 0 4581.42 4514.20 321.88 o -7 9 0 5997.89 3874.36 575.21 o -6 9 0 6076.31 8131.25 756.42 o -5 9 0 4.22 12.85 113.57 o -4 9 0 1237.92 1499.65 223.21 o -3 9 0 71676.65 78009.62 7116.53 o -2 9 0 7860.58 9002.00 480.64 o -1 9 0 4102.46 5248.87 303.64 o 0 9 0 17005.71 20394.60 1260.63 o 1 9 0 13002.63 13448.34 857.24 o 2 9 0 13643.99 12721.14 2098.51 o 3 9 0 91814.16 85016.27 6432.27 o 4 9 0 1731.37 1537.40 168.18 o 5 9 0 70.14 -42.90 44.28 o 6 9 0 5787.99 5632.90 388.62 o 7 9 0 50254.04 52100.98 2397.51 o 8 9 0 9004.40 8742.10 439.88 o 9 9 0 33962.64 33801.73 1842.99 o 10 9 0 25937.01 25560.93 1413.34 o 11 9 0 3037.91 2935.85 221.04 o 12 9 0 89.63 132.52 85.28 o 13 9 0 29463.14 28562.06 2261.48 o 14 9 0 1091.22 1205.77 227.54 o -7 10 0 611.45 422.29 255.01 o -6 10 0 8390.06 6887.76 844.98 o -5 10 0 3078.28 3157.71 529.29 o -4 10 0 2246.27 2771.09 494.44 o -3 10 0 40842.76 46944.39 3551.50 o -2 10 0 38.52 55.28 78.39 o -1 10 0 72.43 29.18 71.13 o 0 10 0 5858.52 6669.45 484.09 o 1 10 0 44484.19 42062.07 3247.09 o 2 10 0 17817.77 16322.35 1330.40 o 3 10 0 32654.10 29888.93 3856.33 o 4 10 0 30333.29 26335.54 1869.95 o 5 10 0 1504.93 1335.95 165.80 o 6 10 0 8.35 -39.80 52.68 o 7 10 0 58312.57 56885.34 3850.38 o 8 10 0 3633.67 3575.27 282.72 o 9 10 0 1973.18 1897.00 259.52 o 10 10 0 23634.24 21755.48 1735.88 o 11 10 0 5648.69 4962.88 489.11 o 12 10 0 2537.24 2300.84 308.31 o 13 10 0 17958.02 17599.05 1449.71 o 14 10 0 2797.15 2429.17 337.83 o -6 11 0 1601.39 1358.28 377.19 o -5 11 0 16827.27 17321.49 1784.67 o -4 11 0 10533.11 11709.60 1278.75 o -3 11 0 12165.29 13166.69 1398.05 o -2 11 0 10040.25 12679.35 852.78 o -1 11 0 160.56 316.44 122.30 o 0 11 0 436.28 635.50 135.98 o 1 11 0 45601.97 53287.65 3166.11 o 2 11 0 2221.96 2496.33 252.76 o 3 11 0 1048.09 1153.92 396.46 o 4 11 0 25865.98 23366.49 1696.32 o 5 11 0 25301.75 22306.44 1355.46 o 6 11 0 8618.14 7921.38 540.03 o 7 11 0 24686.73 21909.78 2759.20 o 8 11 0 3106.90 3414.00 527.86 o 9 11 0 1890.60 1734.65 268.13 o 10 11 0 12266.62 12072.03 1025.78 o 11 11 0 16087.17 17239.49 1416.91 o 12 11 0 1232.82 1492.35 256.65 o 13 11 0 4475.62 4189.23 450.57 o -5 12 0 26270.02 32099.01 3107.69 o -4 12 0 1827.94 2088.88 460.82 o -3 12 0 2078.66 2709.19 507.56 o -2 12 0 16925.63 21869.46 2172.51 o -1 12 0 4985.35 5988.41 457.36 o 0 12 0 5109.35 6455.64 484.36 o 1 12 0 38806.07 45739.84 4637.35 o 2 12 0 15.62 -26.23 71.67 o 3 12 0 783.38 640.09 273.26 o 4 12 0 11785.90 10765.27 1547.90 o 5 12 0 19152.73 17443.56 1111.68 o 6 12 0 10414.06 9913.94 667.60 o 7 12 0 9661.08 8321.32 576.76 o 8 12 0 15895.57 14930.64 1824.23 o 9 12 0 1544.16 1603.86 270.59 o 10 12 0 2139.31 2331.59 328.81 o 11 12 0 22689.43 21358.21 1737.52 o 12 12 0 6.24 206.22 113.57 o 13 12 0 40.76 173.83 127.10 o -4 13 0 232.35 191.87 248.04 o -3 13 0 22.15 163.58 207.04 o -2 13 0 6222.56 8182.90 965.93 o -1 13 0 18275.93 26084.93 2546.01 o 0 13 0 5641.34 6859.31 713.17 o 1 13 0 15525.85 17665.29 1127.11 o 2 13 0 12371.07 13677.63 1160.46 o 3 13 0 832.00 947.14 168.05 o 4 13 0 2153.75 2341.93 372.88 o 5 13 0 34318.17 32624.40 3096.62 o 6 13 0 3242.04 3012.57 352.18 o 7 13 0 834.27 826.22 155.65 o 8 13 0 32520.32 31717.88 2419.74 o 9 13 0 285.50 316.51 153.74 o 10 13 0 812.67 544.46 189.41 o 11 13 0 18684.28 18340.71 1528.43 o 12 13 0 1862.28 2271.32 343.98 o -3 14 0 67.22 210.32 244.35 o -2 14 0 123.91 242.30 228.77 o -1 14 0 22059.57 28161.10 2739.52 o 0 14 0 1771.46 3006.43 515.76 o 1 14 0 954.73 1101.70 175.90 o 2 14 0 23533.13 26485.43 2993.10 o 3 14 0 732.81 770.16 158.03 o 4 14 0 96.97 53.93 84.47 o 5 14 0 20030.13 19073.60 3110.36 o 6 14 0 3227.59 3523.33 593.86 o 7 14 0 2712.73 3216.47 323.46 o 8 14 0 17631.77 17965.37 1159.56 o 9 14 0 6253.66 6098.95 631.38 o 10 14 0 2443.55 2287.72 366.12 o 11 14 0 2845.77 3132.70 439.91 o -1 15 0 11487.06 14016.59 1500.55 o 0 15 0 1504.90 1699.39 397.69 o 1 15 0 994.30 1383.29 346.85 o 2 15 0 14986.25 16869.31 1091.72 o 3 15 0 3891.32 4382.03 372.84 o 4 15 0 1347.45 1381.41 207.30 o 5 15 0 3525.86 3500.16 567.42 o 6 15 0 12264.91 12077.02 2046.24 o 7 15 0 4938.65 5126.58 622.15 o 8 15 0 6030.98 6653.45 521.50 o 9 15 0 9760.81 9955.68 948.71 o 10 15 0 117.84 251.73 203.76 o 2 16 0 3395.77 4381.11 636.71 o 3 16 0 7034.55 7877.19 585.44 o 4 16 0 5.51 -55.40 99.42 o 5 16 0 313.35 318.70 128.54 o 6 16 0 19957.01 20666.07 2691.15 o 7 16 0 1375.64 1568.10 248.07 o 8 16 0 450.30 484.95 156.99 o 9 16 0 6917.29 6729.92 740.84 o -8 -16 1 2535.10 3172.88 495.67 o -7 -16 1 1025.36 1162.49 211.65 o -6 -16 1 1971.58 2104.04 531.96 o -5 -16 1 9.84 -64.22 107.01 o -4 -16 1 615.87 803.45 169.73 o -3 -16 1 1407.67 1758.84 388.67 o -2 -16 1 10092.46 13174.89 1400.92 o -10 -15 1 1081.66 729.36 251.32 o -9 -15 1 456.11 371.86 213.60 o -8 -15 1 3787.89 4154.18 572.34 o -7 -15 1 1339.22 1679.16 251.08 o -6 -15 1 1812.98 1534.63 394.00 o -5 -15 1 1.04 47.00 92.39 o -4 -15 1 2513.18 2786.06 304.97 o -3 -15 1 2104.40 2356.84 372.47 o -2 -15 1 9597.89 12242.58 1311.54 o -1 -15 1 411.02 214.42 182.03 o 0 -15 1 538.21 868.35 307.08 o 1 -15 1 346.87 191.05 248.86 o -11 -14 1 122.23 324.71 179.16 o -10 -14 1 1626.57 1696.11 307.49 o -9 -14 1 2370.83 2890.40 416.14 o -8 -14 1 6759.74 7045.13 532.93 o -7 -14 1 31.10 30.96 100.44 o -6 -14 1 1959.24 2045.87 316.71 o -5 -14 1 498.57 493.10 141.08 o -4 -14 1 5621.87 6035.91 825.51 o -3 -14 1 8659.67 9372.52 1457.09 o -2 -14 1 4374.79 4722.92 403.43 o -1 -14 1 30.77 -34.03 135.30 o 0 -14 1 569.88 1121.72 309.13 o 1 -14 1 1086.31 1288.59 369.81 o 2 -14 1 9393.68 12881.34 1406.25 o 3 -14 1 1751.22 2068.79 478.45 o -12 -13 1 2397.59 2039.68 323.89 o -11 -13 1 242.14 360.38 177.93 o -10 -13 1 4672.59 5066.60 533.80 o -9 -13 1 5403.87 5433.13 562.09 o -8 -13 1 7495.82 6840.31 508.46 o -7 -13 1 17.86 70.36 235.74 o -6 -13 1 862.48 1049.53 181.11 o -5 -13 1 1595.64 1482.82 213.04 o -4 -13 1 8532.70 8434.19 1620.47 o -3 -13 1 5988.74 6388.50 819.15 o -2 -13 1 3302.74 3113.60 357.30 o -1 -13 1 603.27 629.45 134.75 o 0 -13 1 1825.75 2085.60 428.03 o 1 -13 1 3794.02 4930.49 672.79 o 2 -13 1 10298.89 12165.10 1337.37 o 3 -13 1 90.86 173.83 216.06 o 4 -13 1 531.14 503.87 301.34 o -12 -12 1 4526.44 4101.09 449.75 o -11 -12 1 1574.99 2015.90 308.72 o -10 -12 1 4630.46 4731.65 490.34 o -9 -12 1 1664.44 1787.13 290.68 o -8 -12 1 682.26 677.18 139.85 o -7 -12 1 143.82 108.89 86.47 o -6 -12 1 6943.02 7302.10 526.26 o -5 -12 1 6866.93 6593.90 488.37 o -4 -12 1 13606.98 12786.19 2417.28 o -3 -12 1 169.25 230.76 215.04 o -2 -12 1 1045.70 1091.98 175.18 o -1 -12 1 876.25 1142.56 177.93 o 0 -12 1 1734.96 1929.86 234.79 o 1 -12 1 2215.77 2956.00 507.15 o 2 -12 1 5212.49 6655.71 834.32 o 3 -12 1 770.37 1250.05 354.23 o 4 -12 1 290.03 297.65 247.22 o 5 -12 1 3.11 -53.30 227.95 o -13 -11 1 1932.49 2331.18 332.09 o -12 -11 1 2522.87 2314.37 323.07 o -11 -11 1 112.02 209.50 109.47 o -10 -11 1 3555.62 2789.13 349.72 o -9 -11 1 1477.79 1056.12 207.86 o -8 -11 1 3968.37 3562.36 297.05 o -7 -11 1 1965.46 2078.03 221.45 o -6 -11 1 7767.52 7640.24 532.02 o -5 -11 1 3636.48 3655.35 693.29 o -4 -11 1 1736.07 1595.89 235.54 o -3 -11 1 2836.66 2898.10 640.19 o -2 -11 1 87.48 58.31 73.42 o -1 -11 1 1564.97 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