data_I # to in P2(1)/c _audit_creation_date 07-11-08 _audit_creation_method CRYSTALS _cell_length_a 13.6900(10) _cell_angle_alpha 90 _cell_length_b 6.5920(10) _cell_angle_beta 106.580(10) _cell_length_c 11.3450(10) _cell_angle_gamma 90 # NOTE Fc on scale of Fo, 0.21263 # Status flags: # o - used in refinement # < - excluded by I/sigmaI cutoff # x - excluded for another reason loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 585.46 0.00 32.34 x 3 0 0 1.93 1.99 0.20 o 4 0 0 1056.11 1111.06 38.65 o 5 0 0 0.27 0.88 0.17 < 6 0 0 1324.00 1314.63 44.14 o 7 0 0 0.72 0.03 0.87 < 8 0 0 1077.58 1117.53 34.93 o 9 0 0 5.81 0.55 0.98 o 10 0 0 92.86 82.02 3.28 o 11 0 0 5.25 4.83 0.46 o 12 0 0 414.50 386.96 15.89 o 13 0 0 1.20 0.38 0.42 < 14 0 0 263.19 266.94 11.41 o 1 1 0 2.03 0.00 0.13 x 2 1 0 0.16 0.21 0.08 < 3 1 0 12.42 6.37 0.39 o 4 1 0 4.86 2.58 0.22 o 5 1 0 471.10 439.30 12.72 o 6 1 0 33.34 34.99 1.08 o 7 1 0 48.89 45.39 1.25 o 8 1 0 21.45 21.40 0.69 o 9 1 0 3.96 2.51 0.35 o 10 1 0 12.44 12.51 0.51 o 11 1 0 17.64 16.28 0.82 o 12 1 0 0.08 0.32 0.14 < 13 1 0 2.11 1.08 0.31 o 14 1 0 1.43 1.67 0.28 o 0 2 0 1625.06 1711.87 51.89 o 1 2 0 4.61 5.95 0.28 o 2 2 0 147.04 174.82 3.97 o 3 2 0 217.46 220.18 5.65 o 4 2 0 509.90 543.53 11.71 o 5 2 0 23.63 19.83 0.74 o 6 2 0 719.53 748.25 15.53 o 7 2 0 36.87 36.86 1.11 o 8 2 0 996.70 996.76 23.51 o 9 2 0 0.74 0.23 0.50 < 10 2 0 180.91 161.02 5.25 o 11 2 0 8.96 7.98 0.52 o 12 2 0 652.46 609.67 17.72 o 13 2 0 0.05 0.05 0.13 < 14 2 0 197.39 211.66 6.45 o 1 3 0 221.13 204.58 5.40 o 2 3 0 3.11 3.08 0.30 o 3 3 0 1.42 1.65 0.27 o 4 3 0 0.13 0.04 0.17 < 5 3 0 55.73 54.05 1.53 o 6 3 0 0.36 0.19 0.29 < 7 3 0 5.49 6.05 0.44 o 8 3 0 0.28 1.08 0.36 < 9 3 0 6.79 8.38 0.52 o 10 3 0 3.69 3.74 0.41 o 11 3 0 8.03 7.48 0.69 o 12 3 0 8.78 8.21 0.62 o 13 3 0 13.00 13.64 0.91 o 14 3 0 0.95 0.60 1.13 < 0 4 0 1256.17 1350.94 37.38 o 1 4 0 2.28 3.49 0.34 o 2 4 0 336.94 327.65 7.00 o 3 4 0 29.59 31.91 1.02 o 4 4 0 1152.32 1084.92 24.55 o 5 4 0 12.42 9.65 0.62 o 6 4 0 421.74 434.17 10.12 o 7 4 0 40.21 37.98 1.32 o 8 4 0 709.90 710.53 16.44 o 9 4 0 0.30 0.67 0.43 < 10 4 0 274.80 245.30 7.03 o 11 4 0 8.34 8.52 0.72 o 12 4 0 480.24 450.63 14.52 o 13 4 0 4.50 3.52 0.74 o 1 5 0 0.15 0.27 0.33 < 2 5 0 57.83 55.15 1.86 o 3 5 0 1.07 1.76 0.46 < 4 5 0 3.68 4.40 0.47 o 5 5 0 12.13 14.94 0.76 o 6 5 0 15.08 13.07 0.88 o 7 5 0 1.16 0.38 0.57 < 8 5 0 3.58 1.97 0.76 o 9 5 0 9.53 9.02 0.76 o 10 5 0 1.03 0.49 0.59 < 11 5 0 0.43 0.24 0.72 < 12 5 0 3.96 4.13 0.76 o 0 6 0 484.70 488.95 16.47 o 1 6 0 4.29 5.12 0.78 o 2 6 0 143.60 138.74 3.68 o 3 6 0 1.01 0.02 0.55 < 4 6 0 440.49 401.72 10.17 o 5 6 0 0.11 0.92 0.36 < 6 6 0 196.11 203.98 5.32 o 7 6 0 2.84 3.39 0.92 o 8 6 0 341.83 341.36 9.31 o 9 6 0 4.63 4.87 0.81 o 10 6 0 96.12 101.12 3.44 o 1 7 0 0.29 0.34 0.74 < 2 7 0 2.81 3.01 0.67 o 3 7 0 1.62 2.59 0.80 < 4 7 0 5.50 6.17 1.16 o 5 7 0 2.91 3.20 0.91 o 6 7 0 1.48 1.01 0.97 < 7 7 0 14.73 17.62 1.09 o -15 1 1 519.39 524.44 16.45 o -14 1 1 9.05 9.52 0.61 o -13 1 1 96.45 82.82 2.71 o -12 1 1 4.75 5.80 0.53 o -11 1 1 518.18 509.53 11.75 o -10 1 1 4.39 5.40 0.41 o -9 1 1 686.04 722.13 15.57 o -8 1 1 10.12 16.04 0.49 o -7 1 1 642.20 618.03 16.29 o -6 1 1 40.74 44.01 1.21 o -5 1 1 176.72 187.75 5.14 o -4 1 1 10.49 9.95 0.41 o -3 1 1 1795.06 1777.48 61.86 o -2 1 1 1.59 1.21 0.16 o -1 1 1 592.67 0.00 17.81 x 0 1 1 0.56 0.00 0.16 < 1 1 1 1677.54 1722.98 93.07 o 2 1 1 0.10 0.01 0.05 o 3 1 1 613.11 592.25 17.22 o 4 1 1 6.69 7.55 0.26 o 5 1 1 1674.34 1624.82 78.63 o 6 1 1 0.29 0.01 0.14 < 7 1 1 668.19 645.65 15.99 o 8 1 1 22.71 25.63 0.70 o 9 1 1 808.65 768.93 18.30 o 10 1 1 -0.22 0.00 0.17 < 11 1 1 179.11 200.22 5.82 o 12 1 1 9.33 7.04 0.38 o 13 1 1 517.29 499.20 22.80 o -15 2 1 2.64 2.32 0.50 o -14 2 1 1.14 2.24 0.43 < -13 2 1 0.02 0.29 0.13 < -12 2 1 2.83 3.57 0.51 o -11 2 1 0.81 1.40 0.68 < -10 2 1 31.04 29.64 1.00 o -9 2 1 18.84 17.42 0.63 o -8 2 1 16.89 18.29 0.73 o -7 2 1 13.63 15.19 0.55 o -6 2 1 16.01 17.58 0.66 o -5 2 1 14.49 12.19 0.60 o -4 2 1 71.44 74.14 1.93 o -3 2 1 0.29 0.08 0.20 < -2 2 1 3.18 3.91 0.31 o -1 2 1 4.90 5.84 0.31 o 0 2 1 54.66 55.70 1.37 o 1 2 1 0.24 0.00 0.17 < 2 2 1 145.30 131.67 3.72 o 3 2 1 49.96 53.52 1.39 o 4 2 1 26.10 29.43 0.72 o 5 2 1 14.69 15.18 0.54 o 6 2 1 126.35 116.86 3.10 o 7 2 1 2.30 2.71 0.25 o 8 2 1 4.90 4.88 0.32 o 9 2 1 24.97 25.37 1.02 o 10 2 1 0.94 0.55 0.52 < 11 2 1 4.21 3.40 0.39 o 12 2 1 22.44 22.47 0.83 o 13 2 1 3.17 3.40 0.38 o 14 2 1 0.95 0.64 0.84 < -15 3 1 320.35 351.96 12.39 o -14 3 1 0.29 0.23 0.53 < -13 3 1 103.94 95.76 3.27 o -12 3 1 3.14 5.06 0.59 o -11 3 1 603.35 570.00 18.66 o -10 3 1 4.19 4.65 0.55 o -9 3 1 498.56 520.31 11.52 o -8 3 1 5.08 6.64 0.47 o -7 3 1 779.29 729.04 19.85 o -6 3 1 12.62 14.84 0.67 o -5 3 1 396.95 384.81 8.66 o -4 3 1 30.52 30.83 0.98 o -3 3 1 1596.43 1655.95 33.79 o -2 3 1 42.93 39.51 1.26 o -1 3 1 361.35 385.24 8.54 o 0 3 1 15.30 16.17 0.60 o 1 3 1 656.46 668.69 14.79 o 2 3 1 2.90 1.98 0.36 o 3 3 1 584.36 599.99 15.53 o 4 3 1 101.48 95.44 2.52 o 5 3 1 1056.82 1110.45 22.59 o 6 3 1 6.67 7.54 0.49 o 7 3 1 162.21 154.78 4.34 o 8 3 1 1.02 0.91 0.35 < 9 3 1 775.77 720.54 18.81 o 10 3 1 1.43 0.55 0.35 o 11 3 1 311.63 316.02 9.40 o 12 3 1 0.69 0.81 0.66 < 13 3 1 422.72 410.67 15.30 o 14 3 1 9.41 11.80 1.37 o -14 4 1 0.71 0.02 1.25 < -13 4 1 0.68 2.47 1.12 < -12 4 1 10.51 10.10 0.78 o -11 4 1 7.27 5.81 0.70 o -10 4 1 19.63 19.16 1.05 o -9 4 1 0.21 0.00 0.42 < -8 4 1 30.08 32.69 1.17 o -7 4 1 -0.02 0.34 0.12 < -6 4 1 6.86 6.43 0.53 o -5 4 1 20.29 21.36 0.86 o -4 4 1 -0.17 0.04 0.29 < -3 4 1 5.97 6.16 0.52 o -2 4 1 0.96 1.13 0.74 < -1 4 1 10.79 9.25 0.63 o 0 4 1 0.80 1.15 0.57 < 1 4 1 1.21 1.39 0.35 o 2 4 1 30.98 27.34 1.02 o 3 4 1 0.08 0.01 0.18 < 4 4 1 7.76 9.86 0.57 o 5 4 1 2.30 1.87 0.40 o 6 4 1 0.94 0.22 0.81 < 7 4 1 6.51 6.81 0.58 o 8 4 1 9.94 11.26 0.72 o 9 4 1 7.67 5.63 0.59 o 10 4 1 3.09 4.11 0.47 o 11 4 1 0.58 0.28 0.78 < 12 4 1 -0.01 0.33 0.09 < 13 4 1 -0.22 0.22 0.44 < -12 5 1 3.61 4.20 0.78 o -11 5 1 542.55 511.70 13.21 o -10 5 1 3.83 2.61 0.63 o -9 5 1 320.26 327.33 7.85 o -8 5 1 1.55 2.85 0.53 < -7 5 1 526.81 494.33 11.95 o -6 5 1 2.55 1.90 0.60 o -5 5 1 287.07 274.72 6.65 o -4 5 1 2.94 2.39 0.50 o -3 5 1 1187.80 1196.25 23.93 o -2 5 1 3.63 2.84 0.48 o -1 5 1 112.69 117.56 3.14 o 0 5 1 0.50 0.37 0.61 < 1 5 1 573.58 520.46 13.64 o 2 5 1 17.85 14.75 0.91 o 3 5 1 396.75 397.39 9.23 o 4 5 1 0.46 0.02 0.60 < 5 5 1 700.98 718.01 15.26 o 6 5 1 0.53 0.17 0.71 < 7 5 1 83.73 77.63 2.47 o 8 5 1 8.81 8.31 0.77 o 9 5 1 518.60 478.65 12.86 o 10 5 1 1.60 2.31 0.61 < 11 5 1 252.85 268.80 7.63 o 12 5 1 1.48 0.83 0.75 < -10 6 1 0.58 1.77 1.05 < -9 6 1 -0.16 0.12 0.62 < -8 6 1 7.26 8.29 1.00 o -7 6 1 8.09 8.13 0.86 o -6 6 1 12.40 14.35 1.01 o -5 6 1 12.94 14.17 0.95 o -4 6 1 0.55 1.94 1.13 < -3 6 1 2.26 3.64 0.68 o -2 6 1 7.63 7.01 0.88 o -1 6 1 12.97 11.93 1.04 o 0 6 1 4.32 5.71 0.83 o 1 6 1 1.92 2.07 0.74 < 2 6 1 22.18 21.79 1.02 o 3 6 1 2.19 1.60 0.69 o 4 6 1 6.03 5.38 0.79 o 5 6 1 13.95 13.69 1.01 o 6 6 1 6.35 6.82 0.84 o 7 6 1 1.28 1.38 0.69 < 8 6 1 0.62 0.64 1.34 < 9 6 1 -0.21 0.02 0.62 < 10 6 1 4.37 4.11 0.82 o -8 7 1 1.46 0.93 0.94 < -7 7 1 214.48 222.83 5.35 o -6 7 1 9.21 10.08 1.18 o -5 7 1 161.76 155.12 4.70 o -4 7 1 0.56 1.20 1.21 < -3 7 1 517.89 505.39 13.53 o -2 7 1 0.29 0.03 0.99 < -1 7 1 157.67 157.20 5.23 o 0 7 1 4.09 4.31 0.90 o 1 7 1 383.50 351.50 10.29 o 2 7 1 6.39 4.31 1.06 o 3 7 1 300.27 295.17 7.95 o 4 7 1 0.77 0.67 1.37 < 5 7 1 322.44 329.12 8.58 o 6 7 1 0.28 0.79 0.88 < 7 7 1 77.08 83.77 2.95 o -16 0 2 190.18 185.66 8.86 o -15 0 2 -0.53 1.39 0.83 < -14 0 2 539.56 508.40 20.75 o -13 0 2 70.40 65.81 3.64 o -12 0 2 271.64 304.91 9.06 o -11 0 2 0.50 2.14 0.65 < -10 0 2 746.31 711.25 23.72 o -9 0 2 24.48 22.66 1.22 o -8 0 2 744.53 691.56 24.35 o -7 0 2 2.39 0.49 0.48 o -6 0 2 885.08 900.21 29.67 o -5 0 2 0.62 0.14 0.43 < -4 0 2 341.37 333.84 13.73 o -3 0 2 10.25 20.06 0.57 o -2 0 2 1679.91 1777.35 56.77 o -1 0 2 8.30 0.00 0.52 x 0 0 2 510.03 0.00 22.86 x 1 0 2 3.27 0.14 0.24 o -16 1 2 4.57 5.46 0.57 o -15 1 2 -0.01 0.14 0.08 < -14 1 2 3.00 2.22 0.50 o -13 1 2 5.91 6.52 0.53 o -12 1 2 3.85 2.70 0.50 o -11 1 2 22.48 22.24 0.88 o -10 1 2 0.31 0.01 0.29 < -9 1 2 3.98 4.24 0.41 o -8 1 2 95.53 101.72 2.49 o -7 1 2 46.96 41.88 1.47 o -6 1 2 1.53 3.32 0.25 o -5 1 2 38.93 44.10 1.15 o -4 1 2 53.08 60.18 1.50 o -3 1 2 0.69 1.91 0.33 < -2 1 2 0.41 0.90 0.19 < -1 1 2 15.72 14.16 0.56 o 0 1 2 0.53 0.01 0.23 < 1 1 2 10.43 11.78 0.34 o 2 1 2 0.63 0.66 0.17 < 3 1 2 112.37 102.30 2.75 o 4 1 2 1.47 1.32 0.12 o 5 1 2 46.74 44.23 1.31 o 6 1 2 30.46 29.92 0.98 o 7 1 2 26.40 25.60 0.79 o 8 1 2 1.35 0.98 0.13 o 9 1 2 4.17 3.85 0.43 o 10 1 2 37.29 37.10 2.82 o -16 2 2 53.85 60.70 2.56 o -15 2 2 13.82 16.16 0.83 o -14 2 2 482.99 466.14 13.73 o -13 2 2 0.44 0.38 0.66 < -12 2 2 213.35 229.68 5.83 o -11 2 2 7.63 5.86 0.55 o -10 2 2 550.05 514.35 13.49 o -9 2 2 1.09 1.84 0.38 < -8 2 2 300.20 274.51 7.04 o -7 2 2 16.16 14.00 0.67 o -6 2 2 818.92 874.55 17.73 o -5 2 2 19.99 13.59 0.74 o -4 2 2 279.30 297.71 6.71 o -3 2 2 135.92 131.28 3.68 o -2 2 2 635.60 670.96 15.58 o -1 2 2 10.98 10.08 0.46 o 0 2 2 547.70 534.53 13.94 o 1 2 2 30.38 30.61 0.80 o 2 2 2 1159.05 1226.27 27.94 o 3 2 2 13.49 14.90 0.47 o 4 2 2 504.04 494.48 11.79 o 5 2 2 14.07 16.31 0.52 o 6 2 2 1229.20 1148.40 29.92 o 7 2 2 0.43 0.87 0.24 < 8 2 2 430.15 462.29 10.48 o 9 2 2 33.65 30.67 1.08 o 10 2 2 925.12 917.36 23.51 o 11 2 2 18.71 21.14 0.72 o 12 2 2 201.58 187.92 9.91 o 13 2 2 14.10 13.78 0.92 o -15 3 2 2.39 1.86 0.53 o -14 3 2 1.05 1.95 0.62 < -13 3 2 3.59 4.70 0.61 o -12 3 2 9.49 8.97 0.68 o -11 3 2 8.74 10.20 0.75 o -10 3 2 0.91 1.38 0.80 < -9 3 2 48.69 47.74 1.38 o -8 3 2 9.24 9.47 0.60 o -7 3 2 49.07 43.63 1.52 o -6 3 2 1.92 2.04 0.32 o -5 3 2 0.89 0.33 0.58 < -4 3 2 4.79 6.49 0.42 o -3 3 2 0.15 0.46 0.21 < -2 3 2 0.74 1.20 0.45 < -1 3 2 260.77 240.29 5.76 o 0 3 2 5.96 6.07 0.39 o 1 3 2 158.85 144.70 3.82 o 2 3 2 3.66 2.34 0.32 o 3 3 2 138.35 141.30 3.14 o 4 3 2 39.50 37.77 1.13 o 5 3 2 3.07 3.60 0.35 o 6 3 2 1.20 1.53 0.28 o 7 3 2 17.45 17.17 0.79 o 8 3 2 -0.03 0.09 0.09 < 9 3 2 16.74 17.26 0.75 o 10 3 2 0.10 0.07 0.17 < 11 3 2 9.65 10.16 0.63 o 12 3 2 3.69 3.02 0.46 o 13 3 2 0.11 0.72 0.32 < -14 4 2 277.40 295.04 6.73 o -13 4 2 1.62 1.24 0.68 < -12 4 2 387.84 383.14 9.26 o -11 4 2 2.99 2.48 0.57 o -10 4 2 470.15 445.67 10.83 o -9 4 2 24.80 23.62 1.08 o -8 4 2 311.13 280.34 7.23 o -7 4 2 2.04 2.23 0.49 o -6 4 2 1541.70 1546.27 32.03 o -5 4 2 0.08 0.03 0.23 < -4 4 2 660.04 671.64 15.54 o -3 4 2 2.34 2.05 0.40 o -2 4 2 1118.60 1063.76 22.54 o -1 4 2 -0.17 0.09 0.28 < 0 4 2 439.68 424.11 9.86 o 1 4 2 33.08 33.33 1.05 o 2 4 2 1130.62 1164.57 24.63 o 3 4 2 1.31 2.21 0.44 o 4 4 2 195.24 180.75 4.72 o 5 4 2 0.59 0.00 0.54 < 6 4 2 489.73 448.82 11.74 o 7 4 2 3.94 6.81 0.47 o 8 4 2 116.98 126.54 3.44 o 9 4 2 4.79 5.50 0.53 o 10 4 2 503.70 492.09 15.04 o 11 4 2 4.63 4.77 0.62 o 12 4 2 116.81 113.05 3.69 o -13 5 2 -0.47 0.24 1.17 < -12 5 2 0.82 0.12 1.05 < -11 5 2 20.65 20.00 1.19 o -10 5 2 1.51 0.62 0.75 < -9 5 2 1.80 0.35 0.74 < -8 5 2 0.51 0.20 0.87 < -7 5 2 13.29 10.94 1.03 o -6 5 2 0.17 0.50 0.50 < -5 5 2 3.51 3.33 0.60 o -4 5 2 58.99 53.20 1.83 o -3 5 2 -0.15 0.08 0.34 < -2 5 2 0.14 0.40 0.38 < -1 5 2 61.52 61.22 1.96 o 0 5 2 14.72 16.31 0.83 o 1 5 2 2.06 2.76 0.53 o 2 5 2 3.55 6.31 0.54 o 3 5 2 25.13 25.95 1.01 o 4 5 2 -0.12 0.04 0.30 < 5 5 2 5.95 6.05 0.62 o 6 5 2 2.52 1.82 0.50 o 7 5 2 0.06 0.02 0.24 < 8 5 2 2.07 0.71 0.54 o 9 5 2 -0.83 0.26 1.20 < 10 5 2 1.06 0.52 0.58 < 11 5 2 0.17 0.29 0.41 < -11 6 2 0.88 1.57 1.41 < -10 6 2 295.23 306.47 9.76 o -9 6 2 7.99 7.24 0.93 o -8 6 2 83.09 79.42 2.76 o -7 6 2 1.11 2.50 0.74 < -6 6 2 582.00 571.77 14.56 o -5 6 2 3.03 1.90 0.72 o -4 6 2 219.18 221.08 5.61 o -3 6 2 3.10 2.64 0.70 o -2 6 2 389.79 348.37 8.91 o -1 6 2 3.37 1.46 0.70 o 0 6 2 196.84 190.98 4.74 o 1 6 2 3.67 4.12 0.73 o 2 6 2 689.70 683.58 14.33 o 3 6 2 10.22 11.16 0.94 o 4 6 2 277.57 268.66 6.92 o 5 6 2 -0.24 0.10 0.50 < 6 6 2 347.52 331.78 8.46 o 7 6 2 -0.70 0.06 1.27 < 8 6 2 183.41 188.17 5.63 o 9 6 2 0.15 0.10 0.47 < -8 7 2 0.26 1.25 0.91 < -7 7 2 -1.64 0.29 0.80 < -6 7 2 4.46 1.89 1.12 o -5 7 2 2.71 1.44 0.91 o -4 7 2 -0.29 0.02 0.86 < -3 7 2 16.76 16.64 1.44 o -2 7 2 3.91 4.99 0.95 o -1 7 2 0.39 1.11 1.04 < 0 7 2 0.28 0.34 0.76 < 1 7 2 -1.65 0.06 0.77 < 2 7 2 1.45 0.36 0.78 < 3 7 2 2.07 2.35 0.89 < 4 7 2 -0.43 0.08 1.25 < 5 7 2 8.13 12.19 1.13 o 6 7 2 1.17 0.70 0.76 < -16 1 3 0.75 0.26 1.13 < -15 1 3 236.94 241.31 7.01 o -14 1 3 14.77 12.40 0.85 o -13 1 3 549.18 534.11 15.17 o -12 1 3 36.04 34.97 1.38 o -11 1 3 277.05 247.72 6.64 o -10 1 3 0.74 4.84 0.65 < -9 1 3 1132.60 1125.97 26.83 o -8 1 3 1.25 0.64 0.34 o -7 1 3 576.25 613.15 14.05 o -6 1 3 13.36 20.62 0.58 o -5 1 3 384.38 420.38 9.99 o -4 1 3 43.86 42.14 1.26 o -3 1 3 347.17 359.01 8.53 o -2 1 3 103.97 91.49 2.84 o -1 1 3 1660.19 1615.61 41.02 o 0 1 3 46.56 43.09 1.38 o 1 1 3 164.52 179.55 4.36 o 2 1 3 115.72 102.42 3.12 o 3 1 3 763.76 777.19 17.76 o 4 1 3 37.92 42.58 1.06 o 5 1 3 705.11 710.86 17.71 o 6 1 3 4.53 5.82 0.26 o -16 2 3 1.60 0.58 0.55 < -15 2 3 6.42 5.70 0.79 o -14 2 3 1.67 1.94 0.71 < -13 2 3 1.56 1.68 0.62 < -12 2 3 3.72 4.12 0.55 o -11 2 3 0.58 1.45 0.65 < -10 2 3 55.51 57.83 1.66 o -9 2 3 7.55 6.52 0.60 o -8 2 3 16.14 15.01 0.74 o -7 2 3 29.08 22.54 1.01 o -6 2 3 15.80 17.90 0.64 o -5 2 3 0.78 0.07 0.44 < -4 2 3 282.94 262.63 6.47 o -3 2 3 4.33 4.15 0.32 o -2 2 3 0.99 1.07 0.68 < -1 2 3 0.40 0.24 0.27 < 0 2 3 228.18 223.66 5.43 o 1 2 3 8.15 8.19 0.42 o 2 2 3 37.36 38.51 1.02 o 3 2 3 17.40 19.72 0.65 o 4 2 3 5.67 6.78 0.33 o 5 2 3 8.49 10.54 0.38 o 6 2 3 27.62 27.52 0.84 o 7 2 3 13.18 14.64 0.51 o 8 2 3 13.42 15.69 0.51 o 9 2 3 0.33 0.27 0.18 < 10 2 3 9.63 9.37 0.56 o 11 2 3 11.32 12.75 0.74 o -15 3 3 82.02 106.15 3.04 o -14 3 3 4.32 2.55 0.90 o -13 3 3 417.21 415.75 13.19 o -12 3 3 0.69 0.35 0.95 < -11 3 3 188.06 172.33 4.86 o -10 3 3 12.91 16.97 0.78 o -9 3 3 633.49 638.89 13.81 o -8 3 3 0.06 0.01 0.16 < -7 3 3 451.86 471.60 9.93 o -6 3 3 5.45 7.54 0.52 o -5 3 3 1241.54 1157.27 26.08 o -4 3 3 -0.04 0.22 0.11 < -3 3 3 543.45 522.30 11.69 o -2 3 3 -0.22 0.00 0.24 < -1 3 3 1116.63 1185.50 27.97 o 0 3 3 36.01 37.86 1.14 o 1 3 3 809.19 826.32 16.69 o 2 3 3 1.16 0.52 0.29 o 3 3 3 733.55 707.83 16.35 o 4 3 3 1.30 2.68 0.26 o 5 3 3 229.85 247.87 5.50 o 6 3 3 2.88 2.10 0.33 o 7 3 3 923.41 916.72 20.47 o 8 3 3 13.40 15.16 0.57 o 9 3 3 116.88 107.42 3.25 o 10 3 3 18.15 18.71 0.70 o 11 3 3 447.88 431.90 14.76 o 12 3 3 9.80 8.91 0.65 o -14 4 3 5.18 4.38 0.86 o -13 4 3 1.24 0.36 0.67 < -12 4 3 7.55 7.74 0.80 o -11 4 3 6.47 7.51 0.68 o -10 4 3 1.23 0.69 0.48 < -9 4 3 0.23 0.02 0.43 < -8 4 3 0.12 0.28 0.30 < -7 4 3 13.77 15.08 0.78 o -6 4 3 25.02 25.65 1.05 o -5 4 3 1.83 2.10 0.45 o -4 4 3 18.94 18.96 0.90 o -3 4 3 -0.25 0.08 0.44 < -2 4 3 1.13 0.86 0.35 o -1 4 3 8.93 7.12 0.59 o 0 4 3 9.70 10.42 0.70 o 1 4 3 5.93 5.21 0.52 o 2 4 3 -0.14 0.10 0.23 < 3 4 3 3.50 3.54 0.46 o 4 4 3 1.81 2.30 0.43 o 5 4 3 14.11 15.08 0.77 o 6 4 3 -0.23 0.12 0.35 < 7 4 3 1.75 2.26 0.38 o 8 4 3 15.34 17.94 0.76 o 9 4 3 0.40 0.11 0.54 < 10 4 3 0.47 1.23 0.63 < 11 4 3 0.84 1.22 0.82 < 12 4 3 3.67 5.13 0.75 o -13 5 3 309.50 333.08 9.37 o -12 5 3 2.35 2.12 0.95 < -11 5 3 182.70 170.58 5.98 o -10 5 3 5.63 8.86 0.86 o -9 5 3 385.62 390.34 10.53 o -8 5 3 3.99 4.98 0.60 o -7 5 3 269.16 284.96 6.53 o -6 5 3 0.73 0.10 1.30 < -5 5 3 1001.54 931.16 22.60 o -4 5 3 2.57 1.31 0.58 o -3 5 3 182.45 177.96 4.22 o -2 5 3 24.67 25.63 1.10 o -1 5 3 775.51 792.49 17.48 o 0 5 3 12.47 12.37 0.85 o 1 5 3 461.97 439.22 10.51 o 2 5 3 3.84 2.38 0.53 o 3 5 3 727.89 655.91 16.42 o 4 5 3 14.36 18.05 0.81 o 5 5 3 149.26 152.60 3.93 o 6 5 3 0.26 0.35 0.56 < 7 5 3 575.12 556.63 15.08 o 8 5 3 -0.41 0.25 0.64 < 9 5 3 145.54 141.94 5.33 o 10 5 3 5.33 5.51 0.67 o 11 5 3 249.82 260.58 8.05 o -11 6 3 0.30 0.01 0.96 < -10 6 3 6.30 5.67 1.04 o -9 6 3 -0.41 0.04 1.15 < -8 6 3 5.99 6.34 1.01 o -7 6 3 -0.33 0.57 0.80 < -6 6 3 2.13 3.40 0.65 o -5 6 3 8.53 8.00 1.05 o -4 6 3 0.20 1.47 0.53 < -3 6 3 25.39 27.48 1.26 o -2 6 3 8.66 7.71 0.91 o -1 6 3 -0.13 0.05 0.47 < 0 6 3 41.97 44.75 1.79 o 1 6 3 2.80 3.59 0.67 o 2 6 3 7.73 7.36 0.92 o 3 6 3 6.46 6.26 0.75 o 4 6 3 3.56 2.95 0.72 o 5 6 3 2.16 3.47 0.83 < 6 6 3 3.42 2.63 0.86 o 7 6 3 -0.92 0.06 1.53 < 8 6 3 0.47 0.27 1.08 < 9 6 3 3.53 1.99 0.76 o -8 7 3 8.65 11.33 1.46 o -7 7 3 163.87 177.95 6.00 o -6 7 3 -0.49 0.62 1.11 < -5 7 3 412.27 382.28 12.03 o -4 7 3 0.75 1.31 1.39 < -3 7 3 148.97 142.09 4.32 o -2 7 3 49.13 51.27 2.28 o -1 7 3 429.30 435.14 11.93 o 0 7 3 3.29 3.67 0.93 o 1 7 3 242.53 240.03 6.84 o 2 7 3 1.15 0.00 0.94 < 3 7 3 332.97 320.48 10.48 o 4 7 3 0.19 0.00 0.75 < 5 7 3 175.00 191.37 5.74 o 6 7 3 1.09 0.17 0.94 < -16 0 4 437.13 446.54 16.79 o -15 0 4 13.03 15.39 1.50 o -14 0 4 170.89 150.14 6.40 o -13 0 4 25.91 30.19 1.74 o -12 0 4 776.09 756.15 28.41 o -11 0 4 10.67 9.29 1.05 o -10 0 4 805.93 832.31 23.61 o -9 0 4 4.31 1.63 0.61 o -8 0 4 1284.58 1219.44 37.12 o -7 0 4 1.29 0.00 0.48 < -6 0 4 313.88 304.40 9.86 o -5 0 4 358.31 413.05 12.79 o -4 0 4 1244.91 1283.53 63.56 o -3 0 4 131.11 120.47 5.39 o -2 0 4 746.28 740.63 28.01 o -1 0 4 77.60 80.71 3.23 o 0 0 4 342.14 397.49 15.68 o 1 0 4 180.59 177.35 6.94 o 2 0 4 5.90 0.53 0.42 o 3 0 4 142.66 150.86 5.26 o 4 0 4 1313.97 1279.53 56.21 o -16 1 4 1.85 1.60 0.77 < -15 1 4 9.34 9.90 0.99 o -14 1 4 0.02 0.24 0.18 < -13 1 4 2.88 3.87 0.62 o -12 1 4 4.15 4.28 0.54 o -11 1 4 0.14 0.02 0.32 < -10 1 4 23.26 20.81 0.89 o -9 1 4 4.55 5.91 0.65 o -8 1 4 0.36 0.25 0.38 < -7 1 4 37.20 37.88 1.28 o -6 1 4 67.50 72.90 1.77 o -5 1 4 66.74 64.47 1.73 o -4 1 4 1.53 1.62 0.32 o -3 1 4 440.88 423.32 9.87 o -2 1 4 8.52 9.75 0.44 o -1 1 4 0.28 0.63 0.20 < 0 1 4 12.09 10.75 0.49 o 1 1 4 30.03 31.39 0.99 o 2 1 4 1.38 0.87 0.17 o 3 1 4 8.78 9.78 0.36 o 4 1 4 20.47 18.26 0.61 o 5 1 4 0.47 0.54 0.14 < 6 1 4 8.37 8.62 0.49 o -16 2 4 447.36 453.84 11.61 o -15 2 4 1.86 2.54 0.79 < -14 2 4 94.96 88.55 2.88 o -13 2 4 13.95 20.16 0.89 o -12 2 4 591.61 577.96 13.94 o -11 2 4 0.08 0.51 0.23 < -10 2 4 346.25 375.95 8.00 o -9 2 4 6.54 10.40 0.59 o -8 2 4 831.51 812.92 18.34 o -7 2 4 9.78 8.53 0.57 o -6 2 4 224.96 218.68 5.23 o -5 2 4 5.80 5.97 0.44 o -4 2 4 1081.94 1112.61 22.87 o -3 2 4 159.86 162.98 3.74 o -2 2 4 1121.47 1117.08 25.49 o -1 2 4 54.48 57.10 1.43 o 0 2 4 615.32 624.62 13.96 o 1 2 4 3.98 6.94 0.31 o 2 2 4 794.97 775.71 17.89 o 3 2 4 7.12 6.81 0.40 o 4 2 4 1476.27 1473.91 30.38 o 5 2 4 45.25 56.27 1.20 o 6 2 4 330.87 321.06 8.98 o 7 2 4 31.68 34.26 0.94 o 8 2 4 843.02 797.95 23.44 o 9 2 4 14.33 12.50 0.78 o -15 3 4 5.43 5.15 0.86 o -14 3 4 8.51 9.44 0.99 o -13 3 4 0.43 0.09 0.85 < -12 3 4 -0.30 0.28 0.55 < -11 3 4 12.01 12.30 0.89 o -10 3 4 30.66 33.06 1.33 o -9 3 4 6.31 5.78 0.63 o -8 3 4 11.02 11.35 0.74 o -7 3 4 0.15 0.02 0.28 < -6 3 4 19.81 18.68 0.88 o -5 3 4 1.75 1.64 0.45 o -4 3 4 3.74 4.07 0.48 o -3 3 4 20.27 21.90 0.95 o -2 3 4 24.85 22.95 0.93 o -1 3 4 67.04 67.45 1.82 o 0 3 4 7.24 7.60 0.51 o 1 3 4 65.98 64.27 1.62 o 2 3 4 47.20 48.91 1.48 o 3 3 4 10.90 11.41 0.53 o 4 3 4 39.97 34.35 1.21 o 5 3 4 6.41 9.61 0.47 o 6 3 4 4.63 4.26 0.41 o 7 3 4 23.64 23.70 0.93 o 8 3 4 -0.12 0.06 0.19 < 9 3 4 2.29 2.62 0.32 o 10 3 4 0.82 1.33 0.49 < 11 3 4 7.82 9.18 0.79 o -14 4 4 143.53 142.65 4.98 o -13 4 4 2.14 5.05 0.85 < -12 4 4 344.84 340.81 9.06 o -11 4 4 1.10 0.27 0.60 < -10 4 4 229.48 243.25 5.84 o -9 4 4 6.48 6.10 0.79 o -8 4 4 619.56 593.94 14.46 o -7 4 4 7.49 6.62 0.73 o -6 4 4 254.12 244.58 5.90 o -5 4 4 125.59 131.90 3.03 o -4 4 4 1206.51 1226.33 25.53 o -3 4 4 6.53 8.03 0.59 o -2 4 4 372.82 393.08 8.50 o -1 4 4 2.68 3.40 0.48 o 0 4 4 698.55 637.20 15.61 o 1 4 4 5.40 11.46 0.58 o 2 4 4 484.08 470.69 10.84 o 3 4 4 7.42 9.23 0.57 o 4 4 4 746.18 764.70 15.18 o 5 4 4 4.69 7.07 0.52 o 6 4 4 27.42 25.89 1.02 o 7 4 4 5.48 6.31 0.54 o 8 4 4 480.78 444.73 12.33 o 9 4 4 3.55 5.42 0.43 o 10 4 4 177.44 183.78 5.70 o 11 4 4 1.77 2.31 0.52 o -13 5 4 0.26 1.30 0.68 < -12 5 4 7.96 6.85 1.17 o -11 5 4 8.16 8.80 1.07 o -10 5 4 1.09 1.83 0.65 < -9 5 4 1.47 3.10 0.65 < -8 5 4 0.56 0.28 0.87 < -7 5 4 0.65 1.47 1.03 < -6 5 4 1.53 1.00 0.73 < -5 5 4 0.76 0.69 0.89 < -4 5 4 2.30 2.07 0.61 o -3 5 4 37.50 34.79 1.51 o -2 5 4 -0.05 0.18 0.25 < -1 5 4 11.77 13.07 0.82 o 0 5 4 24.79 26.36 1.07 o 1 5 4 84.50 81.55 2.26 o 2 5 4 5.81 7.93 0.76 o 3 5 4 4.88 4.65 0.62 o 4 5 4 2.67 2.69 0.73 o 5 5 4 1.18 0.23 0.46 < 6 5 4 -0.02 0.06 0.14 < 7 5 4 1.00 0.42 1.10 < 8 5 4 0.66 0.09 1.04 < 9 5 4 -0.04 0.62 0.24 < 10 5 4 2.38 1.67 0.67 o -10 6 4 110.76 111.40 3.54 o -9 6 4 11.79 13.06 1.11 o -8 6 4 401.51 376.73 12.02 o -7 6 4 8.43 7.86 0.92 o -6 6 4 174.63 168.51 5.29 o -5 6 4 3.54 6.72 0.92 o -4 6 4 555.21 549.88 14.11 o -3 6 4 10.31 9.10 0.99 o -2 6 4 207.91 208.84 5.22 o -1 6 4 1.23 1.37 0.65 < 0 6 4 524.74 485.19 12.40 o 1 6 4 0.81 0.46 1.08 < 2 6 4 420.61 396.98 9.44 o 3 6 4 7.49 9.24 0.75 o 4 6 4 584.86 581.31 15.39 o 5 6 4 4.82 3.99 0.82 o 6 6 4 167.98 168.73 5.42 o 7 6 4 6.42 6.92 0.94 o 8 6 4 441.53 448.76 13.64 o -7 7 4 -0.61 0.32 1.56 < -6 7 4 0.83 2.11 2.08 < -5 7 4 13.21 11.81 1.28 o -4 7 4 -1.28 1.47 0.96 < -3 7 4 2.63 2.56 1.00 < -2 7 4 3.88 2.90 1.01 o -1 7 4 16.14 15.28 1.13 o 0 7 4 4.32 4.24 1.04 o 1 7 4 1.55 4.25 0.90 < 2 7 4 2.55 5.28 0.97 < 3 7 4 6.38 6.70 1.06 o 4 7 4 1.08 0.15 0.94 < 5 7 4 0.64 0.24 1.34 < -16 1 5 12.79 14.08 1.00 o -15 1 5 327.29 318.27 9.77 o -14 1 5 0.52 0.23 0.71 < -13 1 5 211.08 207.42 5.73 o -12 1 5 0.77 0.01 0.93 < -11 1 5 1074.22 1043.35 22.82 o -10 1 5 8.11 7.62 0.67 o -9 1 5 320.66 308.35 8.06 o -8 1 5 83.93 113.72 2.31 o -7 1 5 1082.58 1091.53 25.53 o -6 1 5 72.66 71.88 1.93 o -5 1 5 848.38 894.44 19.36 o -4 1 5 33.72 18.52 1.17 o -3 1 5 958.34 982.94 21.89 o -2 1 5 0.32 0.04 0.32 < -1 1 5 652.88 614.30 15.12 o 0 1 5 46.38 57.48 1.43 o 1 1 5 875.25 894.05 24.51 o 2 1 5 -0.15 0.76 0.15 < 3 1 5 227.16 227.92 5.87 o 4 1 5 13.45 11.18 0.49 o 5 1 5 993.86 914.86 26.60 o 6 1 5 0.59 1.33 0.28 < -16 2 5 14.03 12.07 1.33 o -15 2 5 1.68 1.88 0.75 < -14 2 5 3.24 5.04 0.80 o -13 2 5 1.38 0.60 0.64 < -12 2 5 9.22 8.85 0.84 o -11 2 5 1.59 4.37 0.63 < -10 2 5 18.84 20.02 1.01 o -9 2 5 0.35 0.41 0.62 < -8 2 5 9.41 9.00 0.64 o