# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 061224f in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 624.46 _exptl_crystal_F_000 1140.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.4316 _cell_length_b 11.8404 _cell_length_c 15.9838 _cell_angle_alpha 88.998 _cell_angle_beta 83.562 _cell_angle_gamma 73.210 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 20258.25 21193.92 530.74 o 2 0 0 475.58 545.12 27.41 o 3 0 0 1720.52 1611.79 57.53 o 4 0 0 5712.46 5692.21 114.79 o 5 0 0 21082.34 20347.84 396.02 o 6 0 0 1869.22 1868.80 82.59 o 7 0 0 18.98 15.71 48.47 o 8 0 0 1275.91 1463.30 102.73 o 9 0 0 358.18 270.42 139.03 o 10 0 0 140.19 -38.98 136.61 o 11 0 0 228.70 214.97 173.18 o 12 0 0 618.08 521.94 207.76 o -12 1 0 209.31 235.86 196.09 o -11 1 0 53.68 -12.05 177.60 o -10 1 0 591.25 570.16 167.14 o -9 1 0 149.02 323.46 153.90 o -8 1 0 826.50 867.09 125.75 o -7 1 0 1804.46 1874.18 102.70 o -6 1 0 4883.34 4876.82 180.38 o -5 1 0 506.34 536.32 49.70 o -4 1 0 3725.61 3752.18 90.99 o -3 1 0 11881.11 11761.93 191.36 o -2 1 0 2505.52 2471.53 72.00 o -1 1 0 7836.56 6878.35 201.29 o 0 1 0 15788.02 14936.30 380.48 o 1 1 0 23876.44 25732.78 876.87 o 2 1 0 192.98 212.88 24.95 o 3 1 0 1444.82 1517.15 198.70 o 4 1 0 264.53 292.40 33.44 o 5 1 0 2856.01 2722.89 76.40 o 6 1 0 5715.22 5785.97 122.62 o 7 1 0 370.16 351.67 56.84 o 8 1 0 5280.56 4884.82 164.50 o 9 1 0 1.80 50.18 73.45 o 10 1 0 388.99 544.84 155.89 o 11 1 0 67.42 -45.00 147.45 o 12 1 0 7.79 -87.59 179.19 o 13 1 0 743.94 720.46 228.25 o -12 2 0 226.44 372.88 204.92 o -11 2 0 765.65 692.33 198.48 o -10 2 0 888.18 1072.85 187.23 o -9 2 0 221.63 271.63 143.04 o -8 2 0 23.03 -28.54 95.70 o -7 2 0 10.12 49.99 87.81 o -6 2 0 212.84 241.96 47.07 o -5 2 0 19239.10 19035.51 306.38 o -4 2 0 15142.83 15131.28 297.72 o -3 2 0 770.95 877.79 97.43 o -2 2 0 11776.22 10996.52 337.49 o -1 2 0 687.12 675.46 87.59 o 0 2 0 1523.14 1466.90 63.30 o 1 2 0 93.16 138.12 44.60 o 2 2 0 63.65 68.45 17.94 o 3 2 0 39598.58 41081.26 786.27 o 4 2 0 2520.65 2423.33 137.23 o 5 2 0 3985.18 3720.50 121.13 o 6 2 0 10039.44 9697.69 360.59 o 7 2 0 2307.44 2019.28 112.81 o 8 2 0 3.86 -42.92 65.43 o 9 2 0 1375.77 1275.19 108.75 o 10 2 0 2438.84 2120.89 133.08 o 11 2 0 220.76 273.23 172.78 o 12 2 0 43.69 -10.45 169.97 o 13 2 0 167.26 278.05 211.75 o -11 3 0 870.31 663.01 203.30 o -10 3 0 134.97 22.91 163.14 o -9 3 0 1265.02 1294.63 187.23 o -8 3 0 2886.76 2963.42 178.38 o -7 3 0 889.35 900.60 115.07 o -6 3 0 3739.46 3959.81 258.36 o -5 3 0 112.48 131.86 71.90 o -4 3 0 126.13 114.52 115.72 o -3 3 0 45242.46 45287.43 1180.01 o -2 3 0 867.60 824.92 113.70 o -1 3 0 5763.59 5763.09 218.97 o 0 3 0 3.54 1.83 184.63 o 1 3 0 262.50 258.45 91.61 o 2 3 0 39627.62 40545.07 899.57 o 3 3 0 16621.82 16204.47 259.81 o 4 3 0 6609.89 6759.67 361.19 o 5 3 0 900.91 885.73 65.66 o 6 3 0 647.83 666.21 81.98 o 7 3 0 1661.56 1703.73 103.94 o 8 3 0 1066.48 1101.34 158.12 o 9 3 0 1039.80 1043.90 111.34 o 10 3 0 306.57 317.25 94.61 o 11 3 0 1032.02 1035.37 119.83 o 12 3 0 123.60 -9.24 168.36 o 13 3 0 687.28 681.09 212.58 o -11 4 0 25.14 265.60 211.75 o -10 4 0 91.00 40.98 165.14 o -9 4 0 1322.86 1930.32 218.20 o -8 4 0 3.96 -29.18 108.97 o -7 4 0 3458.86 3503.13 180.11 o -6 4 0 5390.44 5708.60 205.85 o -5 4 0 3618.15 3370.39 237.09 o -4 4 0 35.02 -44.60 110.49 o -3 4 0 357.72 289.71 130.59 o -2 4 0 9424.64 8702.80 318.61 o -1 4 0 3525.41 3483.87 92.52 o 0 4 0 14089.83 13851.56 276.22 o 1 4 0 293.20 309.54 89.61 o 2 4 0 4744.90 4646.17 159.70 o 3 4 0 6057.02 6179.63 147.50 o 4 4 0 5550.65 5376.86 101.99 o 5 4 0 7283.83 7208.53 178.36 o 6 4 0 100.98 70.37 53.00 o 7 4 0 2061.12 1958.43 143.65 o 8 4 0 4.44 -37.30 101.45 o 9 4 0 189.23 129.56 88.48 o 10 4 0 811.29 668.89 102.07 o 11 4 0 88.81 37.50 146.25 o 12 4 0 22.05 -35.39 153.89 o 13 4 0 179.75 -4.42 188.05 o -10 5 0 46.65 135.81 184.43 o -9 5 0 9.51 44.48 211.14 o -8 5 0 4693.30 5268.60 226.51 o -7 5 0 42.78 -156.68 150.68 o -6 5 0 780.73 920.58 152.29 o -5 5 0 4573.00 5038.23 310.97 o -4 5 0 45.94 -43.79 129.37 o -3 5 0 418.81 376.90 135.01 o -2 5 0 12.60 7.95 26.56 o -1 5 0 9930.21 9359.28 276.22 o 0 5 0 18677.03 18854.46 367.86 o 1 5 0 19949.84 19584.95 388.72 o 2 5 0 1988.82 1828.61 88.44 o 3 5 0 375.07 382.47 57.53 o 4 5 0 8574.26 8360.50 189.88 o 5 5 0 2091.17 2036.05 60.70 o 6 5 0 11923.60 12088.53 273.18 o 7 5 0 1745.57 1756.40 108.37 o 8 5 0 61.67 -11.29 111.50 o 9 5 0 1042.93 987.40 150.08 o 10 5 0 233.86 60.69 94.61 o 11 5 0 4.25 -61.07 97.77 o 12 5 0 344.92 310.14 116.69 o 13 5 0 29.00 38.70 113.55 o -10 6 0 37.61 169.16 190.86 o -9 6 0 134.34 39.35 139.63 o -8 6 0 128.66 390.33 259.16 o -7 6 0 1211.41 1471.94 144.99 o -6 6 0 1890.54 2441.01 289.72 o -5 6 0 677.11 1175.71 241.91 o -4 6 0 110.36 70.32 192.47 o -3 6 0 1858.95 1950.41 209.77 o -2 6 0 654.42 654.64 48.03 o -1 6 0 36.86 19.84 39.18 o 0 6 0 23637.48 23376.13 451.42 o 1 6 0 3020.02 3200.19 115.59 o 2 6 0 17654.54 19242.63 388.00 o 3 6 0 3581.71 3701.90 224.41 o 4 6 0 5059.10 5043.42 145.09 o 5 6 0 10636.05 10337.43 272.40 o 6 6 0 69.46 45.78 30.80 o 7 6 0 3725.17 3656.55 179.81 o 8 6 0 865.47 1132.67 100.80 o 9 6 0 1064.05 1044.53 180.42 o 10 6 0 476.42 558.66 136.22 o 11 6 0 210.14 159.02 130.39 o 12 6 0 105.14 214.79 114.90 o 13 6 0 21.69 72.36 120.57 o -9 7 0 55.31 41.04 164.94 o -8 7 0 0.68 326.18 137.23 o -7 7 0 79.42 55.13 257.37 o -6 7 0 139.94 34.56 182.82 o -5 7 0 807.80 1158.03 227.85 o -4 7 0 953.04 1097.36 243.51 o -3 7 0 3104.73 3747.70 296.55 o -2 7 0 1205.20 1393.07 209.36 o -1 7 0 18.14 -41.71 42.60 o 0 7 0 676.94 683.92 67.91 o 1 7 0 2156.21 2303.46 251.53 o 2 7 0 13910.86 13930.83 306.13 o 3 7 0 2169.69 2137.75 118.67 o 4 7 0 286.20 215.18 62.24 o 5 7 0 622.13 679.30 180.42 o 6 7 0 0.94 -16.07 108.89 o 7 7 0 44.58 8.44 129.38 o 8 7 0 497.92 375.08 222.60 o 9 7 0 16.00 105.90 89.33 o 10 7 0 69.79 25.29 150.27 o 11 7 0 9.69 -50.14 96.66 o 12 7 0 12.07 23.17 114.59 o 13 7 0 0.47 9.44 132.19 o -8 8 0 50.18 205.29 146.39 o -7 8 0 25.23 64.94 165.34 o -6 8 0 549.89 450.83 230.66 o -5 8 0 2910.92 3346.29 302.17 o -4 8 0 88.31 141.03 211.75 o -3 8 0 5.42 -109.68 168.34 o -2 8 0 3989.05 4240.31 303.34 o -1 8 0 1970.03 2256.16 258.78 o 0 8 0 338.58 290.05 68.96 o 1 8 0 3015.28 3148.43 134.23 o 2 8 0 116.78 114.88 68.07 o 3 8 0 8343.38 8613.95 227.98 o 4 8 0 605.37 564.26 123.36 o 5 8 0 3872.98 3657.44 185.44 o 6 8 0 394.13 347.57 133.80 o 7 8 0 1497.98 1603.64 211.77 o 8 8 0 1384.87 1258.47 190.84 o 9 8 0 1079.57 1303.67 124.57 o 10 8 0 315.74 353.93 110.23 o 11 8 0 248.40 532.90 140.44 o 12 8 0 1.59 -41.62 109.37 o -7 9 0 27.09 241.18 153.89 o -6 9 0 21.17 -14.06 232.25 o -5 9 0 306.13 363.64 231.45 o -4 9 0 338.35 67.10 213.36 o -3 9 0 3065.37 3754.53 308.20 o -2 9 0 25.10 24.11 170.77 o -1 9 0 948.41 1131.91 217.00 o 0 9 0 1577.96 1822.60 229.45 o 1 9 0 1.77 -35.92 67.92 o 2 9 0 565.11 597.23 89.49 o 3 9 0 134.22 140.68 79.73 o 4 9 0 1299.68 1378.60 161.93 o 5 9 0 104.01 187.04 81.91 o 6 9 0 157.89 -1.61 139.43 o 7 9 0 1450.62 1622.12 204.50 o 8 9 0 917.97 845.81 179.99 o 9 9 0 336.71 484.18 179.59 o 10 9 0 383.45 585.82 173.97 o 11 9 0 20.48 -78.75 157.09 o 12 9 0 7.69 62.55 121.51 o -6 10 0 272.66 305.38 251.53 o -5 10 0 2.35 71.52 223.41 o -4 10 0 26.12 -109.68 213.38 o -3 10 0 82.62 54.65 181.62 o -2 10 0 1957.57 2577.21 299.76 o -1 10 0 612.40 495.02 196.47 o 0 10 0 102.29 60.27 174.79 o 1 10 0 3505.80 3809.57 296.55 o 2 10 0 1240.84 1248.80 115.60 o 3 10 0 206.51 213.92 88.47 o 4 10 0 462.88 434.65 99.44 o 5 10 0 1373.70 1602.49 130.17 o 6 10 0 273.35 245.91 149.88 o 7 10 0 761.30 822.91 188.43 o 8 10 0 1332.77 1317.94 218.60 o 9 10 0 89.09 255.15 182.42 o 10 10 0 44.79 92.82 164.74 o 11 10 0 138.26 280.06 178.40 o -5 11 0 275.07 319.04 241.49 o -4 11 0 271.30 480.96 243.92 o -3 11 0 402.63 610.73 239.90 o -2 11 0 42.42 207.74 223.00 o -1 11 0 179.51 209.34 189.26 o 0 11 0 20.06 144.25 173.98 o 1 11 0 53.60 -151.87 177.58 o 2 11 0 106.62 173.58 180.41 o 3 11 0 568.19 718.35 106.36 o 4 11 0 2053.65 2195.69 139.02 o 5 11 0 452.66 417.88 140.62 o 6 11 0 487.37 351.99 155.50 o 7 11 0 134.09 150.28 165.14 o 8 11 0 1451.51 1796.49 245.93 o 9 11 0 122.68 233.86 197.29 o 10 11 0 42.52 32.55 184.03 o 11 11 0 3.50 140.23 199.70 o -3 12 0 300.54 341.54 238.28 o -2 12 0 242.49 308.19 225.41 o -1 12 0 28.73 -130.17 209.77 o 0 12 0 35.27 67.91 209.75 o 1 12 0 46.77 -102.85 192.85 o 2 12 0 8.90 -14.87 179.61 o 3 12 0 69.72 85.59 166.35 o 4 12 0 183.59 144.75 101.26 o 5 12 0 23.49 13.26 134.20 o 6 12 0 49.45 174.79 158.31 o 7 12 0 642.73 771.89 186.42 o 8 12 0 181.95 306.98 197.69 o 9 12 0 491.25 878.36 216.19 o 10 12 0 55.56 56.25 194.48 o -1 13 0 5.21 -89.19 215.39 o 0 13 0 11.90 -164.33 208.96 o 1 13 0 32.42 187.25 192.07 o 2 13 0 125.17 175.19 195.28 o 3 13 0 3.25 356.81 193.27 o 4 13 0 898.85 1348.47 225.84 o 5 13 0 434.13 632.87 168.74 o 6 13 0 568.71 601.90 188.83 o 7 13 0 645.14 866.70 196.07 o 8 13 0 73.20 36.16 173.98 o 3 14 0 30.82 -4.02 193.27 o -3 -14 1 1705.53 1912.64 255.97 o -8 -13 1 643.86 835.37 231.46 o -7 -13 1 8.47 113.71 189.26 o -6 -13 1 535.68 378.91 180.81 o -5 -13 1 50.34 278.05 159.92 o -4 -13 1 525.16 809.25 187.63 o -3 -13 1 2264.49 3056.97 284.09 o -2 -13 1 795.29 838.58 220.61 o -1 -13 1 50.74 22.91 196.49 o 0 -13 1 396.24 484.98 232.26 o 1 -13 1 132.07 110.10 198.90 o -9 -12 1 288.37 578.19 229.05 o -8 -12 1 114.48 125.77 176.80 o -7 -12 1 29.22 115.72 156.31 o -6 -12 1 311.01 50.63 164.74 o -5 -12 1 1019.60 1167.27 184.41 o -4 -12 1 642.05 834.41 114.25 o -3 -12 1 97.11 167.96 161.13 o -2 -12 1 324.01 387.35 173.98 o -1 -12 1 72.46 -74.73 173.57 o 0 -12 1 638.22 631.27 231.86 o 1 -12 1 69.31 -34.96 188.85 o 2 -12 1 258.31 244.30 229.84 o 3 -12 1 249.18 159.92 208.94 o -11 -11 1 189.70 18.88 178.00 o -10 -11 1 24.04 -62.68 189.64 o -9 -11 1 71.59 134.20 196.09 o -8 -11 1 8.56 57.06 181.22 o -7 -11 1 1320.65 1289.41 214.99 o -6 -11 1 2547.12 2944.07 241.10 o -5 -11 1 198.61 358.02 145.86 o -4 -11 1 875.19 1129.46 118.05 o -3 -11 1 176.24 228.58 92.83 o -2 -11 1 912.86 1149.19 210.97 o -1 -11 1 1043.52 1266.91 212.18 o 0 -11 1 1016.27 1304.28 246.33 o 1 -11 1 73.43 289.71 215.37 o 2 -11 1 186.60 349.98 231.45 o 3 -11 1 47.18 -150.26 186.42 o 4 -11 1 3.46 208.94 213.36 o 5 -11 1 140.80 120.54 211.75 o -11 -10 1 277.99 253.54 193.67 o -10 -10 1 108.91 275.24 170.37 o -9 -10 1 1546.09 1843.90 249.54 o -8 -10 1 1.56 116.53 166.75 o -7 -10 1 254.51 496.23 158.30 o -6 -10 1 1892.51 2184.24 214.19 o -5 -10 1 244.95 216.57 83.06 o -4 -10 1 244.88 297.67 89.21 o -3 -10 1 123.92 126.91 114.12 o -2 -10 1 11.98 -16.99 76.25 o -1 -10 1 528.66 603.50 199.68 o 0 -10 1 56.67 104.47 186.44 o 1 -10 1 377.32 26.52 196.09 o 2 -10 1 16.29 -113.70 197.27 o 3 -10 1 97.90 58.26 184.43 o 4 -10 1 733.81 556.90 222.22 o 5 -10 1 611.81 610.33 251.95 o 6 -10 1 89.49 160.32 214.16 o -12 -9 1 619.61 567.57 131.01 o -11 -9 1 490.60 662.91 123.84 o -10 -9 1 77.90 -64.69 143.03 o -9 -9 1 379.99 255.55 169.56 o -8 -9 1 3798.49 4241.92 292.09 o -7 -9 1 327.21 82.37 155.50 o -6 -9 1 11.33 -73.52 129.77 o -5 -9 1 350.54 374.44 93.22 o -4 -9 1 730.20 763.60 93.03 o -3 -9 1 4035.03 3706.90 185.02 o -2 -9 1 697.78 641.08 91.92 o -1 -9 1 88.17 67.39 67.88 o 0 -9 1 3757.80 3677.79 271.24 o 1 -9 1 821.17 941.43 206.91 o 2 -9 1 172.29 -192.45 172.76 o 3 -9 1 59.67 -93.21 199.68 o 4 -9 1 584.36 665.42 239.50 o 5 -9 1 1960.10 2580.83 312.22 o 6 -9 1 503.49 889.37 152.52 o 7 -9 1 141.77 287.05 157.71 o -12 -8 1 215.18 118.73 112.17 o -11 -8 1 758.82 721.85 125.10 o -10 -8 1 1.77 39.28 94.73 o -9 -8 1 977.28 1025.08 113.75 o -8 -8 1 662.69 811.26 185.62 o -7 -8 1 41.37 37.77 144.25 o -6 -8 1 667.34 597.07 147.45 o -5 -8 1 758.34 874.14 84.94 o -4 -8 1 2938.04 2719.01 123.76 o -3 -8 1 4214.16 4085.18 355.39 o -2 -8 1 2378.56 2214.40 118.34 o -1 -8 1 3319.39 3448.58 135.87 o 0 -8 1 135.90 221.84 64.84 o 1 -8 1 7248.51 7820.11 372.04 o 2 -8 1 93.17 108.89 165.55 o 3 -8 1 58.32 -31.34 175.99 o 4 -8 1 532.22 818.89 218.20 o 5 -8 1 30.56 -202.09 173.57 o 6 -8 1 863.37 1155.46 146.07 o 7 -8 1 725.34 1435.89 162.59 o 8 -8 1 8.63 157.00 139.18 o -13 -7 1 491.48 481.62 156.30 o -12 -7 1 499.70 569.97 175.20 o -11 -7 1 53.24 6.41 101.94 o -10 -7 1 42.10 126.37 165.54 o -9 -7 1 1692.88 1887.64 134.17 o -8 -7 1 2213.64 2240.93 249.52 o -7 -7 1 164.01 45.66 148.66 o -6 -7 1 800.89 606.32 138.21 o -5 -7 1 1.91 7.12 49.04 o -4 -7 1 41.70 -23.18 51.83 o -3 -7 1 30.89 34.62 57.19 o -2 -7 1 64.67 23.81 58.36 o -1 -7 1 102.14 150.13 58.81 o 0 -7 1 1930.28 1826.32 180.82 o 1 -7 1 3619.14 3647.05 121.76 o 2 -7 1 4800.63 4771.45 298.52 o 3 -7 1 637.61 508.28 208.16 o 4 -7 1 2536.38 3275.97 313.82 o 5 -7 1 1083.81 1161.65 232.67 o 6 -7 1 2.49 2.10 254.75 o 7 -7 1 0.38 -29.21 126.51 o 8 -7 1 274.19 414.31 145.81 o 9 -7 1 13.32 217.76 152.22 o -13 -6 1 213.64 390.88 258.96 o -12 -6 1 30.27 -33.76 140.02 o -11 -6 1 47.57 31.73 105.69 o -10 -6 1 786.38 856.34 110.23 o -9 -6 1 1509.05 1764.01 234.45 o -8 -6 1 1053.81 1121.28 103.37 o -7 -6 1 34.02 -1.97 109.29 o -6 -6 1 1355.37 1258.70 61.59 o -5 -6 1 435.84 429.85 52.47 o -4 -6 1 1218.47 1325.92 76.91 o -3 -6 1 10905.85 11493.67 257.34 o -2 -6 1 374.96 376.61 62.13 o -1 -6 1 9846.76 9872.67 225.26 o 0 -6 1 6594.48 6627.11 172.20 o 1 -6 1 19.11 -43.37 47.61 o 2 -6 1 13408.92 14114.91 298.91 o 3 -6 1 73.39 266.80 157.11 o 4 -6 1 136.18 112.11 166.35 o 5 -6 1 519.57 714.43 226.64 o 6 -6 1 282.16 348.41 113.90 o 7 -6 1 359.28 491.23 130.94 o 8 -6 1 709.48 751.65 147.92 o 9 -6 1 238.30 271.62 140.06 o 10 -6 1 70.34 399.40 216.98 o -13 -5 1 51.91 6.30 110.10 o -12 -5 1 54.49 29.37 108.98 o -11 -5 1 281.48 169.17 103.35 o -10 -5 1 51.52 29.10 92.24 o -9 -5 1 1808.08 1857.98 129.78 o -8 -5 1 627.60 710.38 103.07 o -7 -5 1 532.64 519.10 135.40 o -6 -5 1 4093.10 4281.05 189.44 o -5 -5 1 12.55 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