# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 606ph21 [(PPh3)2(Ppyr)2Cu]BF4' _shelx_refln_list_code 4 _shelx_F_calc_maximum 253.04 _exptl_crystal_F_000 860.00 _reflns_d_resolution_high 0.8408 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.8897 _cell_length_b 13.4877 _cell_length_c 15.5473 _cell_angle_alpha 84.972 _cell_angle_beta 109.588 _cell_angle_gamma 101.927 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2899.53 3259.03 54.98 o 3 0 0 16.56 -1.60 7.33 o 4 0 0 1465.02 1554.24 103.89 o 5 0 0 1119.30 1408.46 36.96 o 6 0 0 131.93 181.53 13.42 o 7 0 0 132.23 126.33 12.07 o 8 0 0 24.00 27.23 10.11 o 9 0 0 32.81 52.79 11.24 o 10 0 0 73.95 35.67 13.95 o 11 0 0 76.76 37.94 28.28 o -12 1 0 0.01 -25.87 27.75 o -11 1 0 36.15 21.34 23.46 o -10 1 0 104.46 111.17 15.23 o -9 1 0 3.72 14.93 19.76 o -8 1 0 100.73 121.35 11.39 o -7 1 0 51.48 16.06 18.63 o -6 1 0 3960.78 3514.92 66.52 o -5 1 0 3811.62 4280.47 301.38 o -4 1 0 1574.19 1569.73 141.71 o -3 1 0 3038.77 3140.67 190.13 o -2 1 0 1823.79 2075.17 33.03 o 1 1 0 5541.50 6019.76 92.39 o 2 1 0 1244.07 1182.43 24.51 o 3 1 0 30.01 40.38 9.88 o 4 1 0 74.86 60.03 5.23 o 5 1 0 4.18 12.60 8.15 o 6 1 0 619.89 662.79 29.41 o 7 1 0 629.10 609.31 31.45 o 8 1 0 384.17 379.89 30.70 o 9 1 0 226.57 210.34 18.63 o 10 1 0 30.69 25.04 13.95 o 11 1 0 50.92 85.37 15.91 o -12 2 0 76.16 100.61 15.39 o -11 2 0 115.49 148.20 15.99 o -10 2 0 59.61 77.98 14.03 o -9 2 0 95.74 76.02 11.61 o -8 2 0 284.67 257.41 19.08 o -7 2 0 1137.34 1202.19 39.60 o -6 2 0 544.60 384.41 24.13 o -5 2 0 28.77 25.87 7.16 o -4 2 0 2043.89 2317.63 219.55 o -3 2 0 754.14 806.62 54.83 o -2 2 0 32983.66 33182.30 400.55 o -1 2 0 24.69 4.75 7.32 o 0 2 0 1202.81 1230.82 16.13 o 1 2 0 380.56 185.91 11.84 o 2 2 0 335.91 461.29 23.00 o 3 2 0 1923.73 1897.46 40.42 o 4 2 0 479.00 630.35 68.25 o 5 2 0 132.90 100.38 9.43 o 6 2 0 411.55 491.13 27.83 o 7 2 0 394.76 413.30 29.19 o 8 2 0 0.09 -7.84 22.93 o 9 2 0 4.43 13.20 21.42 o 10 2 0 2.90 32.20 22.32 o 11 2 0 21.41 3.77 25.79 o -12 3 0 46.50 67.20 15.91 o -11 3 0 146.59 141.26 15.84 o -10 3 0 29.54 44.65 13.35 o -9 3 0 5.88 16.44 20.74 o -8 3 0 1265.56 1242.91 45.03 o -7 3 0 1246.18 1346.84 42.31 o -6 3 0 1419.95 1483.35 42.16 o -5 3 0 3465.62 3232.63 60.26 o -4 3 0 5311.78 6397.63 421.86 o -3 3 0 6989.20 7364.36 98.35 o -2 3 0 3595.99 3988.73 221.02 o -1 3 0 51.29 46.23 6.03 o 0 3 0 64030.00 59243.11 1012.88 o 1 3 0 6425.49 6382.10 322.30 o 2 3 0 507.39 431.75 32.92 o 3 3 0 3.88 4.46 10.41 o 4 3 0 111.29 115.69 9.35 o 5 3 0 26.73 31.07 8.22 o 6 3 0 115.44 85.75 11.39 o 7 3 0 2006.44 2055.86 57.02 o 8 3 0 1086.27 1058.96 45.10 o 9 3 0 13.47 -22.48 22.48 o 10 3 0 136.87 128.21 16.52 o 11 3 0 19.90 19.68 23.53 o -12 4 0 16.95 11.92 26.92 o -11 4 0 194.97 200.99 17.72 o -10 4 0 366.94 309.60 22.70 o -9 4 0 731.82 739.64 39.44 o -8 4 0 42.28 25.34 19.99 o -7 4 0 23.88 23.08 15.99 o -6 4 0 281.96 214.12 21.49 o -5 4 0 1182.35 1189.21 35.52 o -4 4 0 649.99 812.62 31.49 o -3 4 0 1202.42 1502.17 88.62 o -2 4 0 1974.02 2031.11 104.15 o -1 4 0 1458.56 1845.09 25.92 o 0 4 0 4200.81 4955.82 146.31 o 1 4 0 852.70 835.17 17.86 o 2 4 0 1927.98 2122.92 71.16 o 3 4 0 1696.45 1713.05 102.83 o 4 4 0 325.37 279.43 21.57 o 5 4 0 418.68 444.15 25.34 o 6 4 0 742.91 668.14 33.49 o 7 4 0 544.81 582.01 36.05 o 8 4 0 45.33 16.29 12.75 o 9 4 0 0.28 17.87 24.13 o 10 4 0 124.31 137.41 16.52 o 11 4 0 6.05 -27.75 27.75 o -12 5 0 27.91 20.36 23.53 o -11 5 0 60.01 46.76 14.86 o -10 5 0 11.95 -3.09 21.34 o -9 5 0 51.16 15.69 20.82 o -8 5 0 145.07 254.92 23.68 o -7 5 0 153.10 134.77 12.37 o -6 5 0 97.07 150.69 13.65 o -5 5 0 28.08 39.97 8.75 o -4 5 0 18.63 3.32 9.43 o -3 5 0 107.18 115.54 7.43 o -2 5 0 2262.63 2239.94 31.57 o -1 5 0 172.98 160.70 9.00 o 0 5 0 3745.79 4391.08 131.68 o 1 5 0 4444.44 4678.78 107.17 o 2 5 0 1570.83 1723.13 90.69 o 3 5 0 94.88 93.60 10.18 o 4 5 0 1094.08 1198.72 38.46 o 5 5 0 417.77 511.49 28.36 o 6 5 0 461.35 430.80 32.20 o 7 5 0 0.74 21.34 22.32 o 8 5 0 214.93 204.69 17.20 o 9 5 0 131.78 150.69 16.22 o 10 5 0 63.39 67.27 15.39 o -11 6 0 43.69 30.85 14.03 o -10 6 0 67.06 53.17 13.73 o -9 6 0 68.41 35.30 25.27 o -8 6 0 204.37 242.85 19.01 o -7 6 0 46.65 46.84 11.31 o -6 6 0 712.22 798.84 34.47 o -5 6 0 741.90 776.97 31.60 o -4 6 0 3128.68 3122.74 61.54 o -3 6 0 2225.32 2514.33 52.27 o -2 6 0 1.75 -8.90 8.98 o -1 6 0 30.87 30.34 5.66 o 0 6 0 133.08 173.53 13.09 o 1 6 0 113.98 152.96 8.82 o 2 6 0 716.12 672.52 29.19 o 3 6 0 1746.87 1635.47 44.80 o 4 6 0 1244.95 1304.23 42.31 o 5 6 0 58.84 83.72 12.29 o 6 6 0 1.48 9.05 21.49 o 7 6 0 612.97 613.69 37.18 o 8 6 0 71.47 71.57 14.78 o 9 6 0 46.34 23.68 25.34 o 10 6 0 0.11 6.03 24.66 o -11 7 0 0.73 -23.98 23.98 o -10 7 0 46.21 55.43 14.03 o -9 7 0 154.10 167.13 14.78 o -8 7 0 18.63 26.32 20.89 o -7 7 0 51.56 32.88 10.71 o -6 7 0 167.11 190.81 16.29 o -5 7 0 254.52 320.38 23.98 o -4 7 0 334.72 419.48 24.74 o -3 7 0 3750.54 3907.48 72.33 o -2 7 0 4638.16 4743.43 80.85 o -1 7 0 892.60 846.96 31.30 o 0 7 0 125.78 165.77 26.47 o 1 7 0 204.07 251.75 21.19 o 2 7 0 32.66 20.66 14.78 o 3 7 0 489.45 459.08 27.30 o 4 7 0 423.54 443.54 30.92 o 5 7 0 136.93 110.87 13.12 o 6 7 0 0.22 -22.48 22.48 o 7 7 0 0.23 12.52 19.99 o 8 7 0 24.66 10.48 25.57 o 9 7 0 6.84 5.81 25.72 o -11 8 0 50.59 27.60 25.72 o -10 8 0 43.05 75.80 12.90 o -9 8 0 44.09 33.49 13.12 o -8 8 0 478.47 517.23 34.69 o -7 8 0 728.39 761.06 37.86 o -6 8 0 915.08 825.09 37.71 o -5 8 0 407.77 392.18 28.28 o -4 8 0 1043.92 1098.48 38.61 o -3 8 0 1497.82 1480.79 43.67 o -2 8 0 37.59 61.17 10.11 o -1 8 0 93.35 101.51 10.94 o 0 8 0 6.52 -20.35 21.38 o 1 8 0 158.75 127.61 12.07 o 2 8 0 23.75 15.91 11.99 o 3 8 0 30.10 38.69 11.46 o 4 8 0 58.10 49.55 13.20 o 5 8 0 746.39 661.81 38.31 o 6 8 0 413.46 447.46 35.22 o 7 8 0 34.77 44.87 13.27 o 8 8 0 99.22 130.17 16.06 o 9 8 0 204.24 204.91 19.68 o -11 9 0 15.67 10.11 25.11 o -10 9 0 78.39 29.87 28.51 o -9 9 0 317.23 359.30 33.71 o -8 9 0 319.36 395.73 31.68 o -7 9 0 18.86 22.70 23.76 o -6 9 0 92.47 92.69 13.58 o -5 9 0 292.67 268.57 19.16 o -4 9 0 9.15 31.15 11.09 o -3 9 0 34.43 59.43 11.09 o -2 9 0 352.61 293.23 25.19 o -1 9 0 518.10 548.75 29.72 o 0 9 0 65.38 51.64 7.65 o 1 9 0 91.54 123.91 12.67 o 2 9 0 57.92 66.67 12.90 o 3 9 0 456.72 434.11 32.05 o 4 9 0 1074.18 995.39 45.03 o 5 9 0 294.16 263.74 21.80 o 6 9 0 183.91 231.39 17.95 o 7 9 0 3.16 -1.66 24.81 o 8 9 0 26.21 -1.81 29.04 o -10 10 0 55.79 76.02 15.23 o -9 10 0 27.11 32.35 23.38 o -8 10 0 150.07 138.62 16.37 o -7 10 0 305.67 286.67 22.10 o -6 10 0 443.51 468.28 35.15 o -5 10 0 34.08 29.56 24.21 o -4 10 0 166.67 171.73 14.78 o -3 10 0 7.04 1.06 19.84 o -2 10 0 1124.51 1173.68 43.59 o -1 10 0 187.64 207.55 17.42 o 0 10 0 1.18 -14.37 14.37 o 1 10 0 1.20 -10.11 19.61 o 2 10 0 116.58 115.32 15.08 o 3 10 0 19.47 -4.15 24.36 o 4 10 0 543.06 591.44 38.69 o 5 10 0 160.98 145.79 16.29 o 6 10 0 147.79 163.89 17.65 o 7 10 0 79.84 97.82 16.22 o -10 11 0 19.29 -12.60 26.92 o -9 11 0 38.92 38.99 14.03 o -8 11 0 81.55 87.41 15.16 o -7 11 0 94.35 102.57 14.56 o -6 11 0 74.98 10.78 25.34 o -5 11 0 79.43 61.54 14.41 o -4 11 0 124.62 119.62 15.08 o -3 11 0 496.79 482.68 31.90 o -2 11 0 8.75 17.95 12.52 o -1 11 0 21.13 10.86 23.08 o 0 11 0 208.97 204.97 13.51 o 1 11 0 394.30 406.06 29.64 o 2 11 0 328.70 315.63 21.87 o 3 11 0 255.57 296.55 22.85 o 4 11 0 334.62 333.20 32.05 o 5 11 0 206.32 217.13 18.25 o 6 11 0 92.67 74.06 16.67 o 7 11 0 3.32 10.71 27.00 o -9 12 0 0.73 20.36 20.97 o -8 12 0 13.69 1.81 23.91 o -7 12 0 0.27 -24.89 24.96 o -6 12 0 5.25 23.76 21.27 o -5 12 0 9.58 -3.17 22.93 o -4 12 0 128.02 104.31 14.78 o -3 12 0 319.88 274.30 21.72 o -2 12 0 1019.60 1082.27 46.68 o -1 12 0 689.25 725.16 40.65 o 0 12 0 395.30 420.15 24.31 o 1 12 0 172.48 124.82 15.99 o 2 12 0 4.00 6.49 24.29 o 3 12 0 19.35 31.15 22.93 o 4 12 0 5.08 -22.40 24.44 o 5 12 0 3.65 -9.96 25.42 o 6 12 0 15.16 36.35 24.36 o -8 13 0 19.75 14.48 14.33 o -7 13 0 213.49 198.43 18.03 o -6 13 0 311.68 377.25 31.15 o -5 13 0 314.01 273.24 22.93 o -4 13 0 146.31 145.03 16.06 o -3 13 0 14.24 19.76 23.76 o -2 13 0 24.69 -25.57 25.57 o -1 13 0 3.20 11.46 24.36 o 0 13 0 155.56 145.94 27.68 o 1 13 0 317.70 349.19 23.68 o 2 13 0 82.34 53.92 15.31 o 3 13 0 16.69 -24.59 26.17 o 4 13 0 31.21 32.13 27.38 o 5 13 0 27.97 8.67 29.11 o -7 14 0 29.49 0.00 27.83 o -6 14 0 1.62 13.88 21.72 o -5 14 0 73.15 50.15 15.08 o -4 14 0 157.16 183.42 17.27 o -3 14 0 10.40 3.54 26.17 o -2 14 0 77.61 55.36 15.23 o -1 14 0 90.06 80.32 15.31 o 0 14 0 89.25 90.56 11.04 o 1 14 0 77.14 62.45 15.31 o 2 14 0 0.71 -13.80 24.51 o 3 14 0 0.90 -20.66 23.91 o -6 15 0 65.42 59.96 16.82 o -5 15 0 140.63 106.72 17.27 o -4 15 0 15.08 -0.08 28.36 o -3 15 0 1.11 19.84 23.15 o -2 15 0 2.54 -24.59 24.59 o -1 15 0 28.91 7.92 27.75 o 0 15 0 55.66 32.95 27.26 o 1 15 0 19.36 -16.59 27.15 o -1 -15 1 55.90 37.33 27.83 o 0 -15 1 13.13 19.89 12.35 o 1 -15 1 1.10 -0.08 25.49 o 2 -15 1 14.04 26.47 14.25 o 3 -15 1 94.49 138.39 17.20 o 4 -15 1 169.36 164.64 17.95 o 5 -15 1 1.69 -26.55 26.55 o -3 -14 1 19.40 18.55 23.98 o -2 -14 1 66.51 51.89 15.99 o -1 -14 1 8.23 9.50 24.13 o 0 -14 1 2.68 -17.74 17.74 o 1 -14 1 9.67 -11.16 27.68 o 2 -14 1 0.30 -0.08 23.23 o 3 -14 1 8.57 -22.25 23.46 o 4 -14 1 53.87 55.21 15.23 o 5 -14 1 260.70 149.48 18.33 o 6 -14 1 259.61 271.36 24.36 o 7 -14 1 163.95 203.03 19.23 o -5 -13 1 47.26 29.04 21.27 o -4 -13 1 16.72 31.90 23.91 o -3 -13 1 3.56 22.70 25.72 o -2 -13 1 3.25 -14.41 24.06 o -1 -13 1 3.78 -28.06 28.06 o 0 -13 1 249.05 243.64 20.66 o 1 -13 1 504.50 540.91 37.11 o 2 -13 1 429.74 398.52 35.90 o 3 -13 1 1.44 -25.04 25.04 o 4 -13 1 229.99 200.39 17.65 o 5 -13 1 43.84 65.61 14.33 o 6 -13 1 0.18 29.94 22.78 o 7 -13 1 65.85 82.66 15.46 o 8 -13 1 35.61 16.67 23.00 o -6 -12 1 25.20 37.48 16.29 o -5 -12 1 73.01 71.12 15.69 o -4 -12 1 107.34 91.33 16.74 o -3 -12 1 10.12 1.58 22.85 o -2 -12 1 320.26 356.06 23.30 o -1 -12 1 215.08 217.28 20.89 o 0 -12 1 40.95 52.87 9.84 o 1 -12 1 57.77 68.41 13.58 o 2 -12 1 47.80 34.84 25.27 o 3 -12 1 48.14 55.13 13.50 o 4 -12 1 39.64 6.11 24.96 o 5 -12 1 57.61 19.61 25.49 o 6 -12 1 102.65 126.63 15.39 o 7 -12 1 161.09 158.83 16.82 o 8 -12 1 10.27 23.30 16.97 o 9 -12 1 3.32 6.18 26.77 o -7 -11 1 60.84 71.80 17.27 o -6 -11 1 120.06 154.91 17.04 o -5 -11 1 142.22 140.05 17.20 o -4 -11 1 4.36 -9.96 25.42 o -3 -11 1 7.74 2.94 25.11 o -2 -11 1 29.38 2.87 21.65 o -1 -11 1 250.49 179.95 16.44 o 0 -11 1 856.38 785.47 62.64 o 1 -11 1 670.23 667.09 37.79 o 2 -11 1 731.30 757.14 39.37 o 3 -11 1 238.03 208.01 19.08 o 4 -11 1 284.25 270.98 21.65 o 5 -11 1 129.41 193.90 15.76 o 6 -11 1 79.08 79.79 14.03 o 7 -11 1 124.83 122.41 16.44 o 8 -11 1 62.12 68.03 15.31 o 9 -11 1 36.74 -17.65 25.64 o -8 -10 1 0.29 10.78 25.49 o -7 -10 1 0.81 -25.34 27.83 o -6 -10 1 110.54 90.58 16.67 o -5 -10 1 273.24 326.72 28.89 o -4 -10 1 691.79 659.17 40.27 o -3 -10 1 865.69 705.78 41.25 o -2 -10 1 150.33 164.34 14.03 o -1 -10 1 121.20 126.78 14.10 o 0 -10 1 221.86 251.79 14.86 o 1 -10 1 444.94 448.52 29.64 o 2 -10 1 17.40 18.25 21.04 o 3 -10 1 158.49 186.51 18.18 o 4 -10 1 166.69 202.20 19.23 o 5 -10 1 210.08 221.28 18.55 o 6 -10 1 0.36 15.84 21.65 o 7 -10 1 152.07 163.66 15.76 o 8 -10 1 329.69 366.24 33.49 o 9 -10 1 67.95 9.20 27.08 o 10 -10 1 5.27 10.11 25.57 o -8 -9 1 22.70 -2.04 27.38 o -7 -9 1 53.00 39.07 15.31 o -6 -9 1 20.12 16.29 23.91 o -5 -9 1 289.70 381.55 31.15 o -4 -9 1 14.11 19.53 16.14 o -3 -9 1 226.65 187.49 18.70 o -2 -9 1 99.77 104.46 13.20 o -1 -9 1 45.66 59.73 11.16 o 0 -9 1 70.21 98.96 9.09 o 1 -9 1 17.32 31.75 10.56 o 2 -9 1 337.94 320.99 25.72 o 3 -9 1 336.01 375.74 26.62 o 4 -9 1 23.44 51.21 11.46 o 5 -9 1 33.94 32.20 12.52 o 6 -9 1 1028.61 942.37 42.91 o 7 -9 1 724.62 797.41 41.78 o 8 -9 1 158.98 167.20 16.06 o 9 -9 1 0.51 -5.28 24.74 o 10 -9 1 0.18 34.47 23.46 o -9 -8 1 0.32 -0.68 16.44 o -8 -8 1 9.43 27.15 14.18 o -7 -8 1 74.87 87.41 14.71 o -6 -8 1 0.60 -24.96 24.96 o -5 -8 1 465.62 430.49 33.26 o -4 -8 1 666.06 720.18 36.65 o -3 -8 1 57.52 57.09 11.84 o -2 -8 1 484.71 642.42 31.90 o -1 -8 1 311.54 284.11 24.06 o 0 -8 1 1241.91 1251.38 68.82 o 1 -8 1 475.24 445.28 27.15 o 2 -8 1 2656.43 2905.76 62.98 o 3 -8 1 2573.73 2647.52 60.79 o 4 -8 1 185.53 145.79 12.07 o 5 -8 1 0.14 13.05 13.27 o 6 -8 1 67.17 58.37 12.90 o 7 -8 1 38.31 28.73 22.40 o 8 -8 1 143.13 147.37 14.93 o 9 -8 1 175.07 175.88 16.14 o 10 -8 1 55.32 66.97 13.88 o 11 -8 1 5.49 1.89 26.25 o -9 -7 1 113.71 129.12 15.99 o -8 -7 1 65.51 65.92 14.63 o -7 -7 1 58.50 111.02 13.88 o -6 -7 1 198.38 188.47 15.84 o -5 -7 1 169.78 170.07 14.48 o -4 -7 1 651.92 659.62 33.34 o -3 -7 1 1388.94 1296.84 43.14 o -2 -7 1 1900.87 2371.11 55.81 o -1 -7 1 605.37 444.82 25.64 o 0 -7 1 635.04 790.18 21.75 o 1 -7 1 15.92 3.92 9.88 o 2 -7 1 1.36 -9.96 14.78 o 3 -7 1 639.53 679.53 30.09 o 4 -7 1 1716.89 1620.01 44.87 o 5 -7 1 665.23 561.88 29.72 o 6 -7 1 166.13 211.70 17.42 o 7 -7 1 211.13 234.78 18.33 o 8 -7 1 462.09 440.90 33.18 o 9 -7 1 199.66 215.62 19.99 o 10 -7 1 27.18 29.72 24.66 o 11 -7 1 0.15 21.49 22.78 o -10 -6 1 36.10 30.09 25.64 o -9 -6 1 1.17 14.48 22.93 o -8 -6 1 41.12 20.66 26.85 o -7 -6 1 13.45 -4.30 21.95 o -6 -6 1 4.22 42.99 11.16 o -5 -6 1 903.48 988.75 39.52 o -4 -6 1 263.63 256.43 22.48 o -3 -6 1 5.92 -10.71 16.82 o -2 -6 1 4385.05 5232.15 86.36 o -1 -6 1 2065.46 2434.41 43.33 o 0 -6 1 60.44 117.58 8.18 o 1 -6 1 11.66 9.98 8.67 o 2 -6 1 1603.09 1395.90 53.70 o 3 -6 1 5963.24 6558.78 99.25 o 4 -6 1 24.24 38.31 8.97 o 5 -6 1 123.99 144.81 14.41 o 6 -6 1 20.70 15.91 16.59 o 7 -6 1 35.16 25.34 20.06 o 8 -6 1 8.49 13.58 18.85 o 9 -6 1 21.72 -12.07 21.19 o 10 -6 1 7.71 28.81 23.08 o 11 -6 1 6.30 -13.35 23.08 o -10 -5 1 27.30 51.06 13.88 o -9 -5 1 0.80 -22.02 23.68 o -8 -5 1 374.02 404.25 30.77 o -7 -5 1 582.84 612.71 36.43 o -6 -5 1 196.82 277.85 26.62 o -5 -5 1 1124.92 1064.85 39.60 o -4 -5 1 677.59 632.62 28.66 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137.64 13.80 o 9 -4 1 1.53 28.73 20.97 o 10 -4 1 12.22 17.87 22.48 o 11 -4 1 97.10 121.43 15.39 o -11 -3 1 39.80 11.39 26.70 o -10 -3 1 6.67 -1.66 25.11 o -9 -3 1 21.88 3.09 23.23 o -8 -3 1 3.43 -20.06 23.30 o -7 -3 1 292.35 242.78 18.78 o -6 -3 1 252.17 174.29 14.41 o -5 -3 1 251.09 310.65 21.12 o -4 -3 1 2018.97 2103.33 81.53 o -3 -3 1 1768.01 1893.74 51.29 o -2 -3 1 3037.16 3017.80 134.13 o -1 -3 1 1784.33 1698.79 100.53 o 0 -3 1 4152.46 4892.47 156.50 o 1 -3 1 3594.53 3355.76 120.52 o 2 -3 1 273.08 309.45 11.61 o 3 -3 1 3614.42 3673.46 89.94 o 4 -3 1 343.97 420.70 23.15 o 5 -3 1 86.23 121.58 11.99 o 6 -3 1 957.07 1176.69 38.16 o 7 -3 1 1.17 8.30 17.72 o 8 -3 1 387.54 447.61 28.81 o 9 -3 1 326.42 299.64 29.72 o 10 -3 1 497.81 546.04 36.80 o 11 -3 1 174.92 180.25 17.65 o -11 -2 1 19.37 1.96 26.77 o -10 -2 1 95.55 65.99 12.82 o -9 -2 1 267.88 275.05 20.97 o -8 -2 1 1713.45 1571.52 52.27 o -7 -2 1 825.40 693.78 33.03 o -6 -2 1 1150.44 1100.97 37.03 o -5 -2 1 101.13 203.78 17.87 o -4 -2 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