Acta Cryst. (2008). E64, m610-m611  [ doi:10.1107/S1600536808008404 ]

Bis(chloroacetato)-²O,O';O-methanol-O-bis(2-methylfuro[3,2-c]pyridine-N)copper(II)

D. Miklos, J. Miklovic, V. Mrázová, J. Moncol and P. Segla

Key indicators

• Single-crystal X-ray study
• T = 173 K
• Mean (C-C) = 0.005 Å
• R factor = 0.044
• wR factor = 0.104
• Data-to-parameter ratio = 13.4

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.92      
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.04      
PLAT153_ALERT_1_C The su's on the Cell Axes   are Equal (x 100000)        300 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H16C   ..  O1      ..       2.63 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H29    ..  O5      ..       2.69 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H19    ..  O5      ..       2.65 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H16A   ..  O9      ..       2.65 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H24    ..  O9      ..       2.67 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H1B    ..  C14     ..       2.87 Ang. 

Alert level G
ABSTM02_ALERT_3_G  When printed, the submitted absorption T values will be
            replaced by the scaled T values. Since the ratio of scaled T's
            is identical to the ratio of reported T values, the scaling
            does not imply a change to the absorption corrections used in
            the study.
            Ratio of Tmax expected/reported      0.922
            Tmax scaled      0.822 Tmin scaled      0.716

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   9 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   7 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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