# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 080324b in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 147.74 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.8401 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 3.6944 _cell_length_b 17.5271 _cell_length_c 7.0520 _cell_angle_alpha 90.000 _cell_angle_beta 94.467 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 27.85 25.27 0.60 o 4 0 0 13.57 16.83 1.82 o 1 1 0 104.11 95.10 1.12 o 2 1 0 173.46 172.33 2.02 o 3 1 0 7.38 7.75 0.86 o 4 1 0 2.92 1.46 0.73 o 0 2 0 39.52 41.53 1.27 o 1 2 0 2828.51 2847.17 20.35 o 2 2 0 293.42 262.77 2.72 o 3 2 0 22.36 22.79 1.11 o 4 2 0 0.47 0.67 0.70 o 1 3 0 1111.18 1045.44 6.57 o 2 3 0 175.17 172.19 2.56 o 3 3 0 22.90 20.54 0.85 o 4 3 0 0.39 -0.42 1.04 o 0 4 0 632.34 804.50 9.14 o 1 4 0 8.31 8.47 0.37 o 2 4 0 222.94 209.64 1.75 o 3 4 0 1.61 1.16 0.47 o 4 4 0 1.12 0.76 1.14 o 1 5 0 547.33 537.82 3.62 o 2 5 0 6.36 5.83 0.47 o 3 5 0 0.42 0.06 0.55 o 4 5 0 45.34 43.81 1.74 o 0 6 0 112.63 136.30 1.82 o 1 6 0 0.25 0.20 0.20 o 2 6 0 121.35 104.76 1.13 o 3 6 0 16.21 17.99 1.20 o 4 6 0 2.44 1.96 0.84 o 1 7 0 87.26 86.89 1.98 o 2 7 0 1.65 1.82 0.30 o 3 7 0 6.71 7.78 0.97 o 4 7 0 3.47 2.98 0.84 o 0 8 0 1045.07 1191.71 22.54 o 1 8 0 574.68 596.07 4.70 o 2 8 0 3.82 3.02 0.37 o 3 8 0 79.91 77.59 5.49 o 4 8 0 0.45 0.49 0.79 o 1 9 0 0.03 0.16 0.25 o 2 9 0 0.35 -0.32 0.37 o 3 9 0 21.06 21.05 1.97 o 0 10 0 1473.37 1673.73 24.76 o 1 10 0 179.07 194.63 2.09 o 2 10 0 21.93 22.09 0.86 o 3 10 0 27.19 29.04 1.37 o 1 11 0 44.57 46.11 0.96 o 2 11 0 54.11 53.91 2.17 o 3 11 0 38.92 36.60 2.92 o 0 12 0 0.28 0.14 0.38 o 1 12 0 30.99 30.46 0.86 o 2 12 0 0.01 0.15 0.45 o 3 12 0 3.03 2.46 1.31 o 1 13 0 108.71 102.54 2.41 o 2 13 0 67.09 66.45 2.79 o 3 13 0 96.10 98.03 2.61 o 0 14 0 36.79 36.13 2.00 o 1 14 0 0.08 -0.03 0.38 o 2 14 0 161.66 156.75 4.80 o 3 14 0 0.01 -0.56 0.78 o 1 15 0 45.77 42.33 1.39 o 2 15 0 3.17 2.20 0.65 o 3 15 0 54.33 52.32 1.94 o 0 16 0 36.42 39.07 2.24 o 1 16 0 84.35 79.77 1.77 o 2 16 0 92.53 92.32 3.14 o 1 17 0 11.02 10.69 0.85 o 2 17 0 1.40 0.72 0.62 o 0 18 0 114.33 126.85 4.35 o 1 18 0 5.50 4.92 1.04 o 2 18 0 101.05 107.93 2.80 o 1 19 0 6.94 7.88 1.08 o 0 20 0 0.00 0.46 0.88 o 1 20 0 3.35 3.05 0.86 o -3 0 1 89.34 87.46 2.91 o 1 0 1 21827.49 19774.62 285.37 o 3 0 1 9.78 11.08 1.36 o -4 1 1 0.14 -0.95 0.64 o -3 1 1 34.98 34.37 1.31 o -2 1 1 58.30 55.05 1.00 o -1 1 1 64.45 66.48 1.73 o 0 1 1 124.67 115.63 2.16 o 1 1 1 589.88 550.62 3.90 o 2 1 1 3.64 3.32 0.38 o 3 1 1 88.37 80.33 1.95 o 4 1 1 0.25 -0.77 0.56 o -4 2 1 0.00 -0.56 0.69 o -3 2 1 3.95 4.64 1.14 o -2 2 1 59.70 56.83 1.16 o -1 2 1 1131.58 1023.48 8.62 o 0 2 1 1441.09 1454.78 16.18 o 1 2 1 7.67 8.83 0.41 o 2 2 1 1276.60 1252.15 10.91 o 3 2 1 36.74 30.99 1.04 o 4 2 1 3.29 3.65 2.22 o -4 3 1 37.71 39.97 2.46 o -3 3 1 0.51 0.31 0.91 o -2 3 1 134.40 133.19 1.67 o -1 3 1 594.11 604.16 5.34 o 0 3 1 1813.19 1713.43 11.90 o 1 3 1 0.38 0.69 0.16 o 2 3 1 130.66 120.53 1.39 o 3 3 1 35.43 34.20 1.07 o 4 3 1 6.68 6.75 3.11 o -4 4 1 16.30 19.82 1.43 o -3 4 1 11.19 11.06 0.91 o -2 4 1 22.39 19.11 0.53 o -1 4 1 823.23 871.15 10.23 o 0 4 1 139.38 122.80 2.62 o 1 4 1 259.46 292.70 2.87 o 2 4 1 5.07 4.51 0.38 o 3 4 1 17.74 17.82 0.91 o 4 4 1 0.20 -0.93 0.82 o -4 5 1 3.17 3.10 1.06 o -3 5 1 174.47 177.15 3.12 o -2 5 1 5.09 5.06 0.32 o -1 5 1 29.88 29.20 0.58 o 0 5 1 595.13 590.92 5.23 o 1 5 1 13.69 14.02 0.36 o 2 5 1 174.48 162.32 1.74 o 3 5 1 0.16 -0.48 0.52 o 4 5 1 0.16 -0.29 2.36 o -4 6 1 0.15 -0.01 0.69 o -3 6 1 0.37 -0.08 0.50 o -2 6 1 92.41 92.67 1.16 o -1 6 1 798.66 803.70 15.34 o 0 6 1 9.08 8.38 0.43 o 1 6 1 85.56 90.70 1.05 o 2 6 1 0.59 0.86 0.30 o 3 6 1 4.05 3.47 0.74 o 4 6 1 1.08 0.67 0.79 o -4 7 1 1.40 0.43 0.76 o -3 7 1 10.80 10.91 1.19 o -2 7 1 43.75 44.63 0.82 o -1 7 1 0.19 -0.02 0.21 o 0 7 1 249.76 266.21 3.13 o 1 7 1 7.38 8.00 0.44 o 2 7 1 8.44 9.11 1.23 o 3 7 1 0.33 0.16 0.64 o 4 7 1 1.50 -0.09 1.01 o -4 8 1 25.29 28.69 3.45 o -3 8 1 10.27 14.21 1.12 o -2 8 1 292.10 295.62 2.84 o -1 8 1 47.58 39.19 0.77 o 0 8 1 501.49 524.84 4.13 o 1 8 1 574.10 565.85 4.54 o 2 8 1 233.88 223.02 2.75 o 3 8 1 0.11 0.21 0.63 o -3 9 1 28.92 29.54 2.26 o -2 9 1 4.31 5.63 0.47 o -1 9 1 0.40 0.32 0.26 o 0 9 1 18.57 21.66 0.55 o 1 9 1 1.02 1.68 0.33 o 2 9 1 2.04 2.59 0.49 o 3 9 1 1.38 -0.15 0.66 o -3 10 1 11.22 13.64 1.17 o -2 10 1 107.24 112.12 1.59 o -1 10 1 4.30 5.62 0.44 o 0 10 1 176.64 199.32 4.28 o 1 10 1 895.24 906.03 7.24 o 2 10 1 72.17 70.64 1.48 o 3 10 1 16.85 16.31 1.31 o -3 11 1 30.31 27.47 2.06 o -2 11 1 93.09 92.94 1.49 o -1 11 1 128.62 139.27 1.72 o 0 11 1 91.51 99.26 2.55 o 1 11 1 0.08 0.46 0.34 o 2 11 1 14.89 17.08 0.93 o 3 11 1 11.95 10.71 1.15 o -3 12 1 34.16 38.39 1.56 o -2 12 1 12.79 13.41 0.70 o -1 12 1 20.02 20.90 0.73 o 0 12 1 40.05 41.86 1.04 o 1 12 1 0.37 0.79 0.36 o 2 12 1 7.28 8.26 0.81 o 3 12 1 1.36 -0.10 1.54 o -3 13 1 44.05 44.08 2.61 o -2 13 1 244.04 243.22 4.01 o -1 13 1 235.48 246.71 3.86 o 0 13 1 93.00 86.51 4.42 o 1 13 1 2.69 2.38 0.46 o 2 13 1 42.41 39.56 1.24 o 3 13 1 11.28 10.57 1.91 o -3 14 1 0.00 0.76 0.76 o -2 14 1 19.04 19.25 0.97 o -1 14 1 309.31 304.40 3.99 o 0 14 1 31.75 34.37 1.40 o 1 14 1 33.97 34.03 0.98 o 2 14 1 8.71 8.71 0.83 o 3 14 1 50.64 52.13 3.73 o -3 15 1 39.65 40.59 1.71 o -2 15 1 142.15 145.28 5.00 o -1 15 1 0.09 0.35 0.44 o 0 15 1 34.76 32.85 1.45 o 1 15 1 5.39 5.88 0.75 o 2 15 1 14.21 14.80 1.24 o -2 16 1 83.68 86.67 1.97 o -1 16 1 163.76 164.76 4.99 o 0 16 1 182.73 180.04 7.29 o 1 16 1 16.84 18.56 1.51 o 2 16 1 21.65 20.96 1.77 o -2 17 1 0.89 0.17 0.68 o -1 17 1 11.00 12.98 1.18 o 0 17 1 18.94 20.08 1.26 o 1 17 1 24.22 23.10 2.32 o 2 17 1 2.86 1.47 0.71 o -2 18 1 4.04 5.23 1.38 o -1 18 1 160.80 159.00 3.53 o 0 18 1 19.03 18.59 1.33 o 1 18 1 63.81 71.01 2.27 o 2 18 1 0.40 -0.94 0.70 o -1 19 1 17.91 18.27 1.42 o 0 19 1 3.96 6.54 1.40 o 1 19 1 0.91 0.88 0.96 o -1 20 1 0.50 1.18 0.73 o 0 20 1 0.03 -0.02 0.62 o 1 20 1 0.05 -1.01 0.74 o -4 0 2 40.94 42.78 2.52 o -2 0 2 343.82 363.01 4.56 o 0 0 2 273.37 280.63 3.31 o 2 0 2 3040.53 2924.15 46.85 o 4 0 2 24.68 21.57 1.36 o -4 1 2 0.02 -0.28 0.68 o -3 1 2 0.74 0.50 0.58 o -2 1 2 241.69 260.26 3.58 o -1 1 2 161.22 158.84 3.35 o 0 1 2 32.92 25.65 0.52 o 1 1 2 0.25 0.48 0.16 o 2 1 2 343.33 319.57 4.25 o 3 1 2 1.51 3.32 0.66 o 4 1 2 24.27 25.07 1.93 o -4 2 2 14.61 17.23 1.40 o -3 2 2 0.36 0.27 0.54 o -2 2 2 27.77 27.41 0.76 o -1 2 2 37.31 41.26 2.52 o 0 2 2 988.79 862.82 6.34 o 1 2 2 101.21 101.82 1.92 o 2 2 2 0.11 -0.03 0.41 o 3 2 2 363.13 354.56 4.72 o 4 2 2 2.47 3.82 0.70 o -4 3 2 21.53 25.09 2.18 o -3 3 2 103.57 113.78 2.47 o -2 3 2 0.24 -0.08 0.27 o -1 3 2 577.82 649.14 7.30 o 0 3 2 673.25 693.68 6.11 o 1 3 2 446.94 425.04 3.01 o 2 3 2 0.04 0.19 0.29 o 3 3 2 3.87 3.81 0.64 o 4 3 2 7.70 6.81 1.36 o -4 4 2 2.75 2.73 1.38 o -3 4 2 82.21 91.30 2.19 o -2 4 2 55.12 58.11 1.73 o -1 4 2 37.14 32.45 0.95 o 0 4 2 716.17 755.32 6.64 o 1 4 2 90.23 85.39 0.95 o 2 4 2 43.02 47.73 0.89 o 3 4 2 4.39 3.69 0.79 o 4 4 2 0.00 -0.03 0.78 o -4 5 2 5.60 7.38 0.99 o -3 5 2 0.39 1.26 0.57 o -2 5 2 437.11 489.70 4.90 o -1 5 2 27.04 28.22 0.68 o 0 5 2 3.17 2.55 0.34 o 1 5 2 205.12 199.13 1.70 o 2 5 2 7.11 8.39 0.62 o 3 5 2 34.89 32.50 2.14 o 4 5 2 1.02 -0.57 1.10 o -4 6 2 6.63 10.33 1.12 o -3 6 2 5.77 6.54 0.98 o -2 6 2 63.31 65.92 1.23 o -1 6 2 219.68 250.66 2.61 o 0 6 2 1242.58 1291.79 12.30 o 1 6 2 8.62 7.19 0.35 o 2 6 2 36.18 37.64 0.83 o 3 6 2 0.66 -0.36 0.63 o -4 7 2 5.67 6.66 1.11 o -3 7 2 7.11 8.10 1.25 o -2 7 2 3.43 3.24 0.38 o -1 7 2 172.00 185.26 1.87 o 0 7 2 37.83 30.54 0.85 o 1 7 2 171.99 162.75 2.30 o 2 7 2 9.37 9.20 0.68 o 3 7 2 0.13 0.46 0.70 o -3 8 2 71.52 74.60 2.90 o -2 8 2 72.59 69.66 1.17 o -1 8 2 374.79 393.09 3.35 o 0 8 2 110.32 101.83 1.55 o 1 8 2 100.53 99.85 2.12 o 2 8 2 128.48 117.71 1.92 o 3 8 2 62.47 57.98 3.32 o -3 9 2 39.11 39.44 1.52 o -2 9 2 35.94 35.66 0.89 o -1 9 2 18.97 21.39 0.64 o 0 9 2 4.90 5.23 0.48 o 1 9 2 34.79 36.22 0.86 o 2 9 2 0.64 1.45 0.52 o 3 9 2 1.33 0.70 0.71 o -3 10 2 32.29 33.76 1.43 o -2 10 2 85.47 82.29 1.36 o -1 10 2 178.82 176.11 3.34 o 0 10 2 4.03 4.22 0.45 o 1 10 2 44.63 44.23 0.97 o 2 10 2 252.76 249.96 4.34 o 3 10 2 19.73 21.53 1.57 o -3 11 2 55.50 59.20 1.88 o -2 11 2 74.51 68.34 1.27 o -1 11 2 144.84 134.73 2.07 o 0 11 2 115.70 123.87 1.54 o 1 11 2 95.84 95.34 1.50 o 2 11 2 0.06 -0.03 0.50 o 3 11 2 4.02 4.64 0.97 o -3 12 2 33.13 37.04 1.27 o -2 12 2 63.62 65.44 1.27 o -1 12 2 19.22 18.85 0.78 o 0 12 2 90.11 98.40 3.47 o 1 12 2 18.32 19.69 0.78 o 2 12 2 3.73 2.94 0.86 o 3 12 2 0.24 -1.10 0.73 o -3 13 2 34.73 36.97 1.30 o -2 13 2 66.44 66.14 1.32 o -1 13 2 365.60 354.70 3.40 o 0 13 2 368.89 372.70 4.18 o 1 13 2 19.26 16.65 1.00 o 2 13 2 1.31 -0.60 0.53 o 3 13 2 6.57 5.42 1.09 o -3 14 2 21.87 20.05 1.02 o -2 14 2 0.79 0.07 0.40 o -1 14 2 106.99 105.28 1.94 o 0 14 2 283.70 286.10 6.57 o 1 14 2 58.56 56.38 1.24 o 2 14 2 25.00 24.23 1.12 o -2 15 2 74.38 73.84 1.75 o -1 15 2 190.98 190.72 3.71 o 0 15 2 4.75 4.26 1.16 o 1 15 2 1.54 1.72 0.49 o 2 15 2 7.08 5.97 0.81 o -2 16 2 20.98 16.95 0.99 o -1 16 2 65.84 65.66 2.09 o 0 16 2 116.09 113.35 4.83 o 1 16 2 186.32 190.51 2.98 o 2 16 2 0.56 -0.73 0.57 o -2 17 2 6.14 5.63 1.36 o -1 17 2 1.31 0.72 0.59 o 0 17 2 60.78 57.74 2.02 o 1 17 2 14.53 14.42 1.55 o 2 17 2 31.90 31.82 2.83 o -2 18 2 51.76 48.61 2.89 o -1 18 2 1.11 1.20 0.73 o 0 18 2 123.91 118.64 5.21 o 1 18 2 22.64 20.26 1.35 o -1 19 2 0.17 0.79 0.71 o 0 19 2 29.88 27.39 1.52 o 1 19 2 0.00 0.34 0.65 o 0 20 2 0.79 0.87 0.77 o -3 0 3 132.78 134.71 3.93 o -1 0 3 472.36 539.51 9.10 o 1 0 3 27.16 28.36 0.73 o 3 0 3 339.31 327.78 4.68 o -4 1 3 39.35 48.69 1.92 o -3 1 3 4.18 5.21 1.08 o -2 1 3 4.56 5.05 0.56 o -1 1 3 682.91 767.67 8.73 o 0 1 3 80.16 74.19 1.03 o 1 1 3 54.45 49.18 0.65 o 2 1 3 5.36 4.72 0.48 o 3 1 3 96.75 96.31 1.60 o -4 2 3 84.63 105.31 2.78 o -3 2 3 49.38 54.82 3.15 o -2 2 3 0.15 0.00 0.38 o -1 2 3 88.91 90.05 1.80 o 0 2 3 3.96 2.86 0.31 o 1 2 3 206.34 187.05 1.68 o 2 2 3 3.45 3.98 0.46 o 3 2 3 1.11 -0.23 0.55 o -4 3 3 0.03 0.64 1.10 o -3 3 3 69.22 81.07 3.92 o -2 3 3 195.59 214.42 9.26 o -1 3 3 0.05 -0.42 0.28 o 0 3 3 758.29 816.42 10.66 o 1 3 3 227.90 222.85 2.97 o 2 3 3 53.01 50.67 0.85 o 3 3 3 0.00 -0.01 0.45 o -4 4 3 1.33 1.02 1.06 o -3 4 3 0.93 0.41 0.51 o -2 4 3 206.76 224.37 13.31 o -1 4 3 121.51 135.87 2.37 o 0 4 3 2.28 1.16 0.31 o 1 4 3 159.33 152.30 1.59 o 2 4 3 23.95 22.74 0.93 o 3 4 3 7.32 6.62 1.15 o -4 5 3 3.03 4.72 0.82 o -3 5 3 13.36 14.63 1.01 o -2 5 3 6.50 6.79 0.72 o -1 5 3 490.11 544.18 4.94 o 0 5 3 27.01 28.72 0.90 o 1 5 3 14.48 14.06 0.49 o 2 5 3 39.18 36.74 1.16 o 3 5 3 2.12 1.31 0.92 o -4 6 3 1.10 1.11 0.85 o -3 6 3 66.74 69.36 1.52 o -2 6 3 33.98 32.37 0.87 o -1 6 3 286.53 314.83 3.17 o 0 6 3 182.10 197.68 2.45 o 1 6 3 467.54 455.68 3.44 o 2 6 3 1.54 1.42 0.40 o 3 6 3 11.87 11.00 1.63 o -3 7 3 4.26 4.19 0.59 o -2 7 3 94.37 88.10 1.36 o -1 7 3 22.77 24.23 0.71 o 0 7 3 206.31 217.22 4.07 o 1 7 3 69.71 65.81 0.97 o 2 7 3 37.42 35.15 1.09 o 3 7 3 5.14 4.52 0.95 o -3 8 3 1.29 1.66 0.50 o -2 8 3 71.21 70.77 1.24 o -1 8 3 170.80 164.82 2.05 o 0 8 3 89.54 83.80 1.49 o 1 8 3 72.16 66.60 1.19 o 2 8 3 5.14 6.22 0.70 o 3 8 3 18.01 21.14 1.80 o -3 9 3 0.08 -0.57 0.40 o -2 9 3 162.62 163.67 2.03 o -1 9 3 18.27 17.09 0.95 o 0 9 3 61.00 63.37 1.33 o 1 9 3 11.76 13.49 0.67 o 2 9 3 19.33 18.88 2.03 o 3 9 3 0.01 -0.38 0.84 o -3 10 3 15.88 17.40 1.02 o -2 10 3 45.56 50.86 1.09 o -1 10 3 200.94 202.48 3.72 o 0 10 3 104.37 95.84 1.70 o 1 10 3 7.47 7.80 0.59 o 2 10 3 1.09 0.28 0.51 o 3 10 3 48.11 49.76 1.91 o -3 11 3 1.10 0.04 0.67 o -2 11 3 106.58 103.14 1.97 o -1 11 3 156.34 150.42 2.31 o 0 11 3 114.20 111.06 2.47 o 1 11 3 42.28 44.30 1.08 o 2 11 3 56.65 55.06 1.49 o 3 11 3 0.65 0.07 0.87 o -3 12 3 46.56 48.65 1.90 o -2 12 3 68.07 72.81 1.67 o -1 12 3 66.01 63.99 1.47 o 0 12 3 9.73 11.89 0.96 o 1 12 3 104.32 108.26 2.45 o 2 12 3 4.29 3.70 0.91 o 3 12 3 3.70 2.72 1.03 o -3 13 3 10.89 9.73 1.12 o -2 13 3 73.05 74.80 1.74 o -1 13 3 67.02 65.18 2.06 o 0 13 3 289.32 274.14 6.70 o 1 13 3 256.56 262.18 2.99 o 2 13 3 0.00 -0.61 0.56 o -2 14 3 31.40 32.29 1.52 o -1 14 3 3.84 4.15 0.87 o 0 14 3 171.53 163.32 6.21 o 1 14 3 120.07 127.02 2.30 o 2 14 3 30.43 31.95 1.27 o -2 15 3 15.08 16.48 1.13 o -1 15 3 88.72 89.23 2.48 o 0 15 3 119.85 119.69 4.35 o 1 15 3 12.33 12.45 1.01 o 2 15 3 6.36 5.04 0.85 o -2 16 3 70.26 78.08 1.90 o -1 16 3 24.40 17.99 2.05 o 0 16 3 21.03 18.71 1.26 o 1 16 3 26.89 27.34 3.11 o 2 16 3 97.89 103.36 5.38 o -2 17 3 0.10 -0.79 0.77 o -1 17 3 38.55 32.96 1.61 o 0 17 3 0.88 0.25 0.70 o 1 17 3 72.41 76.84 2.41 o -1 18 3 63.96 64.05 2.27 o 0 18 3 0.04 0.04 0.79 o 1 18 3 44.87 42.35 1.86 o -1 19 3 3.38 4.28 0.90 o 0 19 3 3.37 5.80 1.00 o -4 0 4 53.51 54.04 2.68 o -2 0 4 317.50 340.51 6.85 o 0 0 4 132.04 144.30 2.48 o 2 0 4 1.02 0.71 0.60 o -4 1 4 51.19 54.31 1.88 o -3 1 4 154.27 134.95 3.75 o -2 1 4 42.75 47.80 3.25 o -1 1 4 20.67 17.98 1.45 o 0 1 4 562.17 601.41 6.26 o 1 1 4 6.82 5.98 0.35 o 2 1 4 10.82 12.05 0.69 o 3 1 4 2.43 2.60 0.56 o -3 2 4 215.61 197.56 4.83 o -2 2 4 100.40 98.79 12.92 o -1 2 4 4.61 6.30 0.67 o 0 2 4 89.19 85.07 2.02 o 1 2 4 0.18 -0.08 0.23 o 2 2 4 25.23 22.90 0.93 o 3 2 4 1.04 0.52 0.65 o -3 3 4 0.34 1.46 0.76 o -2 3 4 158.84 183.10 4.59 o -1 3 4 173.94 193.58 5.92 o 0 3 4 0.08 -0.22 0.29 o 1 3 4 341.86 353.74 2.71 o 2 3 4 41.17 41.33 1.33 o 3 3 4 6.89 8.50 1.74 o -3 4 4 0.54 0.66 0.37 o -2 4 4 0.02 -0.22 0.46 o -1 4 4 205.04 233.14 4.35 o 0 4 4 97.09 100.14 1.67 o 1 4 4 5.04 5.34 0.51 o 2 4 4 14.01 14.08 0.96 o 3 4 4 5.96 5.03 1.01 o -3 5 4 11.19 12.82 1.05 o -2 5 4 6.33 5.15 0.77 o -1 5 4 23.16 23.99 1.08 o 0 5 4 167.01 176.05 3.83 o 1 5 4 7.86 8.47 0.49 o 2 5 4 25.80 23.80 1.18 o 3 5 4 5.80 6.67 2.05 o -3 6 4 3.88 3.21 0.98 o -2 6 4 223.89 220.72 10.32 o -1 6 4 65.31 60.67 3.46 o 0 6 4 279.34 301.20 3.51 o 1 6 4 66.13 64.60 1.04 o 2 6 4 69.45 65.19 1.49 o 3 6 4 0.06 -0.52 1.01 o -3 7 4 8.09 10.49 1.16 o -2 7 4 3.75 1.30 0.61 o -1 7 4 209.47 199.58 3.43 o 0 7 4 108.37 110.73 1.88 o 1 7 4 90.25 90.07 1.24 o 2 7 4 34.24 34.38 1.15 o 3 7 4 2.81 3.82 1.04 o -3 8 4 142.63 139.78 3.05 o -2 8 4 0.26 0.00 0.55 o -1 8 4 3.76 5.66 1.40 o 0 8 4 124.40 119.12 1.99 o 1 8 4 0.24 0.22 0.37 o 2 8 4 24.37 21.90 1.01 o 3 8 4 0.00 -0.44 0.80 o -3 9 4 232.64 237.56 4.28 o -2 9 4 0.00 -0.40 0.43 o -1 9 4 252.13 254.33 6.70 o 0 9 4 2.42 3.15 0.55 o 1 9 4 26.31 26.16 0.87 o 2 9 4 11.04 9.67 0.85 o 3 9 4 6.18 4.88 1.05 o -3 10 4 23.63 19.87 1.33 o -2 10 4 60.76 55.51 1.46 o -1 10 4 13.46 15.63 1.06 o 0 10 4 152.25 152.16 2.38 o 1 10 4 24.10 21.35 0.83 o 2 10 4 1.57 1.27 0.62 o 3 10 4 1.47 1.00 1.32 o -3 11 4 1.32 1.57 1.10 o -2 11 4 12.97 12.72 2.27 o -1 11 4 128.25 115.00 2.69 o 0 11 4 186.21 186.41 2.76 o 1 11 4 50.58 53.23 1.23 o 2 11 4 10.14 11.18 0.97 o -3 12 4 0.68 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