# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' XYZN file = SHELXL INS file, no disorder, for CYMEUK' _shelx_refln_list_code 4 _shelx_F_calc_maximum 197.99 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.8337 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, z+1/2' 'x, -y+1/2, z+1/2' '-x+1/2, -y, z' '-x, -y, -z' 'x-1/2, -y-1/2, -z-1/2' '-x, y-1/2, -z-1/2' 'x-1/2, y, -z' _cell_length_a 8.5314 _cell_length_b 9.5295 _cell_length_c 13.1348 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 296.53 400.17 6.25 o 4 0 0 5565.03 5379.44 268.27 o 6 0 0 12.36 16.20 1.70 o 8 0 0 844.92 880.85 104.22 o 10 0 0 10.17 11.37 0.65 o 2 1 0 33627.22 36813.89 445.25 o 4 1 0 1546.46 1733.95 83.72 o 6 1 0 1124.90 1121.84 90.56 o 8 1 0 15.76 17.01 0.62 o 10 1 0 124.96 110.27 13.48 o 0 2 0 5567.77 4902.63 50.11 o 2 2 0 3510.10 3883.10 112.18 o 4 2 0 9304.98 9540.34 287.57 o 6 2 0 368.09 354.30 15.12 o 8 2 0 350.60 375.46 28.85 o 10 2 0 0.25 -0.75 0.75 o 2 3 0 1625.54 1760.55 28.06 o 4 3 0 163.23 178.56 2.86 o 6 3 0 310.97 350.47 11.14 o 8 3 0 7.87 10.98 0.50 o 0 4 0 9393.37 9089.80 374.25 o 2 4 0 5307.20 5375.02 155.74 o 4 4 0 1205.74 1089.07 96.73 o 6 4 0 19.38 19.37 1.04 o 8 4 0 137.41 115.14 11.19 o 2 5 0 8443.03 7998.66 365.17 o 4 5 0 353.86 365.03 27.75 o 6 5 0 1211.68 1192.28 109.56 o 8 5 0 15.24 16.87 0.47 o 0 6 0 18225.88 18604.90 717.56 o 2 6 0 130.02 131.05 7.30 o 4 6 0 3504.96 3538.86 286.63 o 6 6 0 79.64 70.21 3.98 o 8 6 0 324.97 315.18 31.68 o 2 7 0 4906.29 5059.69 244.97 o 4 7 0 6.12 8.88 1.82 o 6 7 0 282.88 353.98 37.71 o 8 7 0 4.41 5.72 1.00 o 0 8 0 2331.01 2296.50 145.99 o 2 8 0 55.97 55.90 2.82 o 4 8 0 678.92 874.40 87.75 o 6 8 0 1.35 4.03 1.18 o 2 9 0 1.58 24.92 7.19 o 4 9 0 0.10 -1.28 1.28 o 6 9 0 37.20 38.37 1.86 o 0 10 0 666.01 849.76 99.00 o 2 10 0 52.31 61.46 2.80 o 4 10 0 0.74 1.06 0.62 o 2 11 0 358.48 399.58 33.21 o 0 1 1 27.09 38.01 3.41 o 1 1 1 4339.25 4326.61 157.81 o 2 1 1 110.23 81.77 5.12 o 3 1 1 106.77 118.49 1.96 o 4 1 1 7711.65 7654.32 113.28 o 5 1 1 1339.05 1425.43 37.52 o 6 1 1 0.03 0.66 0.79 o 7 1 1 115.23 122.94 4.15 o 8 1 1 310.08 290.23 13.38 o 9 1 1 3.07 5.52 0.76 o 10 1 1 2.98 2.13 0.45 o 1 2 1 1964.57 1797.35 30.58 o 2 2 1 19329.86 19866.31 253.40 o 3 2 1 17.19 21.13 0.86 o 4 2 1 223.09 221.36 4.21 o 5 2 1 964.29 973.30 14.47 o 6 2 1 5006.62 4810.96 138.56 o 7 2 1 286.90 277.19 19.27 o 8 2 1 43.54 39.13 2.35 o 9 2 1 2.89 5.20 1.81 o 10 2 1 22.32 19.57 1.74 o 0 3 1 33957.93 31799.69 952.49 o 1 3 1 473.98 458.91 13.47 o 2 3 1 1763.41 1701.58 13.24 o 3 3 1 1839.48 1794.92 30.01 o 4 3 1 12084.25 11416.85 160.15 o 5 3 1 107.60 96.44 3.79 o 6 3 1 71.13 69.93 4.33 o 7 3 1 174.23 168.67 4.04 o 8 3 1 462.68 464.36 17.53 o 9 3 1 10.43 11.78 0.79 o 1 4 1 982.40 917.28 8.41 o 2 4 1 20579.19 20399.55 637.22 o 3 4 1 629.90 652.35 38.83 o 4 4 1 13.47 17.24 3.39 o 5 4 1 338.96 322.48 7.54 o 6 4 1 1556.83 1524.90 46.09 o 7 4 1 2.54 8.36 2.98 o 8 4 1 7.71 6.11 0.75 o 9 4 1 1.33 0.20 0.71 o 0 5 1 5512.40 4955.17 76.46 o 1 5 1 0.66 12.00 3.15 o 2 5 1 141.17 147.14 2.41 o 3 5 1 132.84 139.35 3.92 o 4 5 1 2022.48 1997.60 67.12 o 5 5 1 56.35 60.17 3.73 o 6 5 1 0.17 2.55 0.89 o 7 5 1 0.06 -1.32 1.32 o 8 5 1 87.99 104.84 3.56 o 9 5 1 0.90 0.83 0.35 o 1 6 1 13.01 18.74 2.29 o 2 6 1 31.10 27.34 1.45 o 3 6 1 3.97 6.94 1.96 o 4 6 1 5.05 7.88 0.94 o 5 6 1 1.64 -1.10 1.67 o 6 6 1 31.43 44.40 1.67 o 7 6 1 4.70 5.77 1.52 o 8 6 1 36.25 34.42 1.47 o 0 7 1 833.96 901.44 64.40 o 1 7 1 2.57 3.33 0.83 o 2 7 1 3.35 15.56 1.84 o 3 7 1 126.13 131.52 4.40 o 4 7 1 689.74 669.53 50.10 o 5 7 1 95.98 108.89 6.18 o 6 7 1 51.68 56.10 2.85 o 7 7 1 7.47 7.54 0.78 o 8 7 1 15.94 9.76 1.04 o 1 8 1 3.74 12.05 1.38 o 2 8 1 1792.20 1954.36 68.44 o 3 8 1 31.49 42.55 2.57 o 4 8 1 16.12 25.87 1.82 o 5 8 1 29.55 26.64 1.93 o 6 8 1 515.85 498.09 30.71 o 7 8 1 20.12 17.43 0.96 o 0 9 1 1639.44 1822.73 110.57 o 1 9 1 5.01 9.28 1.44 o 2 9 1 5.98 4.42 0.73 o 3 9 1 47.78 53.71 2.39 o 4 9 1 1022.16 1114.01 63.26 o 5 9 1 35.48 33.22 1.48 o 6 9 1 0.64 1.29 0.39 o 1 10 1 68.62 71.17 2.48 o 2 10 1 829.38 919.58 24.04 o 3 10 1 0.43 0.74 0.66 o 4 10 1 11.56 10.25 0.43 o 0 11 1 339.40 348.05 19.57 o 1 11 1 7.19 6.21 0.19 o 2 11 1 0.40 0.23 0.29 o 0 0 2 16946.41 14505.39 527.68 o 1 0 2 24217.97 28660.47 631.90 o 2 0 2 2252.55 2453.11 47.25 o 3 0 2 1428.54 1449.16 37.74 o 4 0 2 18884.97 20081.92 430.50 o 5 0 2 72.09 112.51 4.52 o 6 0 2 121.98 141.23 8.87 o 7 0 2 0.79 4.06 0.84 o 8 0 2 248.61 271.18 14.78 o 9 0 2 22.16 22.31 1.59 o 10 0 2 1.14 0.96 0.62 o 1 1 2 2434.04 2369.47 73.07 o 2 1 2 39199.23 46774.24 860.56 o 3 1 2 2053.84 2226.46 23.68 o 4 1 2 43.80 45.37 1.27 o 5 1 2 8.12 10.74 3.07 o 6 1 2 3171.02 3158.41 98.54 o 7 1 2 6.29 3.07 1.66 o 8 1 2 2.36 3.64 1.28 o 9 1 2 17.09 17.70 0.90 o 10 1 2 62.34 52.67 4.58 o 0 2 2 12875.63 12668.37 1242.47 o 1 2 2 140.33 147.76 5.56 o 2 2 2 730.43 729.15 13.69 o 3 2 2 44.22 44.04 2.62 o 4 2 2 1564.99 1684.52 165.96 o 5 2 2 574.95 573.25 16.27 o 6 2 2 124.54 130.82 5.34 o 7 2 2 389.54 378.44 11.90 o 8 2 2 153.16 164.80 6.73 o 9 2 2 0.09 0.70 0.97 o 1 3 2 634.42 612.52 15.69 o 2 3 2 244.51 243.58 5.97 o 3 3 2 103.63 112.16 3.00 o 4 3 2 78.95 84.13 2.24 o 5 3 2 166.75 194.25 5.13 o 6 3 2 44.72 66.69 2.34 o 7 3 2 57.37 58.11 1.54 o 8 3 2 10.74 9.73 0.37 o 9 3 2 0.44 -0.26 0.56 o 0 4 2 6023.44 5699.53 52.52 o 1 4 2 1036.01 984.98 12.48 o 2 4 2 70.45 71.69 2.71 o 3 4 2 118.47 149.82 1.73 o 4 4 2 1741.13 1591.46 38.77 o 5 4 2 192.79 184.97 5.71 o 6 4 2 103.98 104.42 2.93 o 7 4 2 97.82 86.60 3.13 o 8 4 2 40.31 33.95 2.38 o 9 4 2 0.29 -0.10 0.63 o 1 5 2 104.56 102.47 6.83 o 2 5 2 8818.08 8654.91 261.83 o 3 5 2 637.51 608.10 20.11 o 4 5 2 11.97 14.13 0.75 o 5 5 2 199.46 171.89 5.72 o 6 5 2 1103.93 1029.83 42.38 o 7 5 2 72.19 62.69 3.05 o 8 5 2 0.20 0.05 0.91 o 9 5 2 24.88 19.47 1.32 o 0 6 2 8406.26 7890.76 128.10 o 1 6 2 878.63 870.49 31.90 o 2 6 2 25.29 20.26 0.58 o 3 6 2 477.37 474.07 12.78 o 4 6 2 3405.83 3385.49 155.71 o 5 6 2 22.64 24.61 1.52 o 6 6 2 62.36 62.70 3.27 o 7 6 2 66.58 64.62 2.62 o 8 6 2 148.96 133.76 6.14 o 1 7 2 682.35 662.82 22.94 o 2 7 2 4511.40 4422.01 139.68 o 3 7 2 65.38 71.27 5.48 o 4 7 2 9.67 9.37 0.46 o 5 7 2 15.75 22.02 1.06 o 6 7 2 695.44 735.36 41.38 o 7 7 2 2.69 5.09 0.91 o 0 8 2 638.75 597.82 16.70 o 1 8 2 143.94 152.51 5.82 o 2 8 2 6.32 6.48 0.48 o 3 8 2 39.28 50.50 1.80 o 4 8 2 486.77 521.30 25.10 o 5 8 2 16.53 23.94 1.50 o 6 8 2 7.02 5.67 0.25 o 7 8 2 1.01 1.84 0.20 o 1 9 2 33.50 33.64 1.61 o 2 9 2 57.62 59.24 0.94 o 3 9 2 10.99 11.50 0.63 o 4 9 2 28.06 29.57 1.12 o 5 9 2 0.49 2.93 0.84 o 6 9 2 14.07 18.59 0.60 o 0 10 2 99.13 129.05 15.06 o 1 10 2 76.75 88.29 2.91 o 2 10 2 10.67 10.62 0.48 o 3 10 2 0.40 1.78 0.69 o 4 10 2 121.88 117.72 6.28 o 1 11 2 10.79 14.60 0.62 o 2 11 2 234.73 223.86 9.78 o 0 1 3 30102.84 30133.57 1593.13 o 1 1 3 1039.48 1017.52 32.14 o 2 1 3 691.03 731.94 9.31 o 3 1 3 457.14 447.78 13.65 o 4 1 3 720.39 697.51 24.33 o 5 1 3 308.85 292.65 11.99 o 6 1 3 10.84 11.97 1.59 o 7 1 3 289.47 267.40 13.23 o 8 1 3 89.82 93.97 7.93 o 9 1 3 28.50 24.47 1.82 o 10 1 3 0.63 0.13 0.61 o 1 2 3 249.65 225.42 12.60 o 2 2 3 16794.86 17638.45 458.54 o 3 2 3 2436.78 2478.82 44.46 o 4 2 3 35.44 46.45 3.77 o 5 2 3 769.70 764.88 18.82 o 6 2 3 1206.15 1191.63 51.07 o 7 2 3 132.92 128.80 6.75 o 8 2 3 16.74 14.95 1.28 o 9 2 3 5.85 6.23 0.71 o 0 3 3 17833.94 17188.69 992.70 o 1 3 3 9335.41 9283.72 141.81 o 2 3 3 491.06 489.26 12.24 o 3 3 3 2412.32 2365.40 22.96 o 4 3 3 9366.19 9136.15 165.19 o 5 3 3 223.15 217.60 7.08 o 6 3 3 54.91 59.29 1.78 o 7 3 3 244.32 244.64 9.19 o 8 3 3 584.24 575.06 24.40 o 9 3 3 40.68 34.18 2.37 o 1 4 3 4154.06 3929.48 79.75 o 2 4 3 6760.11 6291.55 95.51 o 3 4 3 463.41 442.03 10.68 o 4 4 3 20.37 33.38 4.60 o 5 4 3 2.14 10.54 2.81 o 6 4 3 1956.19 1952.78 66.36 o 7 4 3 78.74 83.11 8.18 o 8 4 3 1.08 1.57 0.64 o 9 4 3 17.06 15.16 0.83 o 0 5 3 5746.25 5190.85 226.33 o 1 5 3 976.52 909.31 21.36 o 2 5 3 102.88 100.21 6.89 o 3 5 3 354.93 360.82 10.35 o 4 5 3 1371.76 1379.58 51.32 o 5 5 3 185.84 186.99 5.43 o 6 5 3 23.38 21.15 1.01 o 7 5 3 89.25 92.19 3.89 o 8 5 3 81.45 94.67 4.75 o 1 6 3 398.82 411.68 18.33 o 2 6 3 177.32 195.96 8.12 o 3 6 3 19.18 17.57 1.23 o 4 6 3 18.16 31.77 12.31 o 5 6 3 50.52 56.72 2.67 o 6 6 3 40.05 27.68 2.63 o 7 6 3 2.96 3.06 1.20 o 8 6 3 0.22 -0.43 0.61 o 0 7 3 365.35 392.37 42.75 o 1 7 3 485.91 520.62 19.07 o 2 7 3 0.19 0.67 1.60 o 3 7 3 0.26 11.48 4.13 o 4 7 3 267.71 246.06 18.58 o 5 7 3 40.58 44.36 2.90 o 6 7 3 0.29 1.50 1.05 o 7 7 3 10.59 6.31 0.79 o 1 8 3 130.32 134.57 5.63 o 2 8 3 1484.37 1583.64 90.31 o 3 8 3 416.07 470.85 26.42 o 4 8 3 5.95 6.63 0.98 o 5 8 3 73.67 67.76 3.90 o 6 8 3 144.32 135.90 12.02 o 7 8 3 15.97 11.27 0.76 o 0 9 3 2085.21 2227.89 193.43 o 1 9 3 256.14 275.77 10.57 o 2 9 3 2.06 5.07 0.65 o 3 9 3 182.53 192.85 8.82 o 4 9 3 426.53 456.99 26.92 o 5 9 3 36.08 37.32 1.89 o 1 10 3 85.43 92.24 3.44 o 2 10 3 511.82 541.61 24.10 o 3 10 3 21.50 20.99 0.69 o 4 10 3 21.09 20.18 1.11 o 0 11 3 164.53 156.07 8.95 o 1 11 3 21.34 19.33 0.81 o 0 0 4 38096.92 38955.89 2023.29 o 1 0 4 2957.11 2813.67 54.98 o 2 0 4 1036.43 1146.80 27.57 o 3 0 4 4032.22 4116.23 100.17 o 4 0 4 6997.56 7653.51 257.60 o 5 0 4 2691.99 2803.51 115.20 o 6 0 4 39.68 43.90 1.97 o 7 0 4 146.10 149.74 7.64 o 8 0 4 940.04 957.89 64.29 o 9 0 4 14.14 12.98 1.74 o 1 1 4 8558.71 7764.05 94.11 o 2 1 4 9591.27 9727.94 157.06 o 3 1 4 2855.61 2914.82 74.09 o 4 1 4 229.73 248.60 12.35 o 5 1 4 1420.41 1383.24 45.55 o 6 1 4 1062.10 1119.66 55.73 o 7 1 4 267.49 238.40 14.34 o 8 1 4 6.69 8.01 0.69 o 9 1 4 45.41 45.58 2.99 o 0 2 4 17828.87 16942.37 156.14 o 1 2 4 846.10 720.64 13.82 o 2 2 4 44.53 59.86 1.80 o 3 2 4 1013.91 1023.84 17.58 o 4 2 4 1365.00 1435.66 33.22 o 5 2 4 258.25 263.25 8.53 o 6 2 4 23.68 26.27 1.70 o 7 2 4 6.87 8.23 1.06 o 8 2 4 14.40 19.21 1.47 o 9 2 4 13.26 13.04 1.13 o 1 3 4 0.37 8.45 2.16 o 2 3 4 220.94 249.53 9.72 o 3 3 4 31.43 23.22 0.48 o 4 3 4 24.94 21.61 0.62 o 5 3 4 45.37 62.32 1.20 o 6 3 4 104.22 90.42 4.06 o 7 3 4 11.47 11.57 1.84 o 8 3 4 10.35 11.86 0.42 o 9 3 4 0.39 0.31 0.31 o 0 4 4 7602.60 7903.05 274.74 o 1 4 4 491.46 493.47 14.29 o 2 4 4 117.86 119.75 5.62 o 3 4 4 896.49 856.36 28.21 o 4 4 4 151.09 138.64 7.72 o 5 4 4 346.17 338.32 13.16 o 6 4 4 6.44 8.05 1.49 o 7 4 4 3.07 9.30 3.59 o 8 4 4 24.46 20.59 1.58 o 9 4 4 3.99 2.86 0.31 o 1 5 4 1802.80 1744.90 27.06 o 2 5 4 5923.11 5841.34 158.99 o 3 5 4 1423.65 1479.86 57.16 o 4 5 4 96.63 95.50 5.43 o 5 5 4 573.56 541.77 27.88 o 6 5 4 14.15 21.80 3.21 o 7 5 4 67.46 60.42 4.31 o 8 5 4 0.92 1.78 0.56 o 0 6 4 7665.96 7140.00 183.28 o 1 6 4 1057.98 1029.66 11.09 o 2 6 4 549.90 552.69 15.67 o 3 6 4 1102.79 1118.34 40.95 o 4 6 4 1726.46 1740.04 76.59 o 5 6 4 549.23 550.57 32.64 o 6 6 4 2.88 2.29 0.62 o 7 6 4 30.13 33.28 2.42 o 8 6 4 79.46 70.29 3.91 o 1 7 4 997.07 974.54 18.11 o 2 7 4 1361.07 1376.26 55.08 o 3 7 4 471.30 481.77 18.76 o 4 7 4 54.32 56.22 3.05 o 5 7 4 260.07 268.29 13.06 o 6 7 4 435.73 435.91 23.50 o 7 7 4 55.71 52.23 3.37 o 0 8 4 619.91 557.05 37.40 o 1 8 4 98.79 92.16 2.38 o 2 8 4 165.11 153.56 7.45 o 3 8 4 68.57 81.38 1.37 o 4 8 4 414.22 422.80 18.12 o 5 8 4 27.61 25.91 1.08 o 6 8 4 1.23 1.31 0.43 o 1 9 4 14.10 10.67 0.33 o 2 9 4 4.90 3.38 1.24 o 3 9 4 1.68 4.05 1.13 o 4 9 4 81.60 72.36 4.36 o 5 9 4 9.18 12.25 0.30 o 0 10 4 108.14 119.07 19.35 o 1 10 4 35.35 45.38 3.40 o 2 10 4 13.28 13.09 1.05 o 3 10 4 35.41 33.74 3.23 o 4 10 4 0.75 1.32 0.69 o 0 1 5 786.64 761.22 61.91 o 1 1 5 2382.41 2062.91 46.24 o 2 1 5 215.85 225.76 3.32 o 3 1 5 2306.79 2327.77 57.97 o 4 1 5 1512.16 1540.56 52.56 o 5 1 5 209.15 200.58 11.10 o 6 1 5 44.25 40.68 2.72 o 7 1 5 4.34 6.43 1.15 o 8 1 5 1.22 7.05 1.50 o 9 1 5 13.11 11.92 1.30 o 1 2 5 10147.03 9506.18 149.13 o 2 2 5 6687.67 6385.28 94.47 o 3 2 5 2207.51 2130.09 80.41 o 4 2 5 102.10 108.37 2.55 o 5 2 5 1026.67 1030.04 30.78 o 6 2 5 998.91 1002.91 38.46 o 7 2 5 401.67 363.32 21.96 o 8 2 5 34.87 30.95 2.15 o 9 2 5 15.16 15.87 0.96 o 0 3 5 786.82 621.91 41.03 o 1 3 5 1734.78 1502.90 49.90 o 2 3 5 643.23 700.10 10.29 o 3 3 5 3069.65 3100.25 82.98 o 4 3 5 4499.33 4693.05 183.18 o 5 3 5 2270.76 2212.63 90.74 o 6 3 5 172.93 156.49 9.17 o 7 3 5 286.39 291.15 12.10 o 8 3 5 137.91 146.50 9.65 o 9 3 5 31.39 24.96 1.93 o 1 4 5 1219.85 1118.10 42.76 o 2 4 5 3846.49 3860.89 125.79 o 3 4 5 2498.76 2592.62 78.24 o 4 4 5 97.19 103.30 3.49 o 5 4 5 2024.38 2089.27 96.65 o 6 4 5 1396.30 1433.39 70.41 o 7 4 5 240.60 225.62 13.14 o 8 4 5 0.50 0.08 0.49 o 9 4 5 20.08 18.05 1.37 o 0 5 5 1501.00 1522.81 68.96 o 1 5 5 533.90 512.54 14.85 o 2 5 5 51.94 56.50 2.37 o 3 5 5 612.22 650.44 23.35 o 4 5 5 324.93 348.29 17.00 o 5 5 5 24.17 29.73 1.33 o 6 5 5 1.38 0.93 1.28 o 7 5 5 18.62 24.29 0.87 o 8 5 5 33.18 35.29 1.76 o 1 6 5 450.65 440.50 11.66 o 2 6 5 339.61 323.46 6.72 o 3 6 5 24.22 26.55 2.35 o 4 6 5 0.03 2.07 0.96 o 5 6 5 35.69 27.18 2.30 o 6 6 5 12.24 14.74 3.88 o 7 6 5 10.44 7.65 0.58 o 8 6 5 10.96 7.18 0.41 o 0 7 5 5.85 15.50 4.77 o 1 7 5 31.72 41.00 2.49 o 2 7 5 343.15 343.75 9.96 o 3 7 5 452.38 438.13 20.35 o 4 7 5 239.22 233.17 14.16 o 5 7 5 122.87 114.66 7.51 o 6 7 5 32.04 24.91 1.39 o 7 7 5 4.77 3.34 0.32 o 1 8 5 831.94 802.78 22.23 o 2 8 5 413.91 412.90 24.77 o 3 8 5 120.10 137.03 8.92 o 4 8 5 18.35 17.31 0.81 o 5 8 5 130.61 114.52 4.70 o 6 8 5 105.48 88.33 6.07 o 0 9 5 332.72 318.67 29.76 o 1 9 5 389.01 377.99 13.00 o 2 9 5 2.08 2.63 0.40 o 3 9 5 211.74 207.66 13.83 o 4 9 5 314.34 277.12 18.75 o 5 9 5 115.96 101.83 6.60 o 1 10 5 154.98 147.04 6.87 o 2 10 5 300.44 280.86 21.96 o 3 10 5 183.02 166.88 16.83 o 0 0 6 6647.48 6782.24 524.04 o 1 0 6 14028.90 13571.48 434.08 o 2 0 6 141.35 130.10 6.97 o 3 0 6 1472.14 1348.90 51.49 o 4 0 6 1536.05 1673.84 91.32 o 5 0 6 1419.18 1396.64 86.42 o 6 0 6 0.19 1.83 0.50 o 7 0 6 1384.85 1415.40 103.45 o 8 0 6 26.18 46.77 5.98 o 9 0 6 71.87 53.44 5.78 o 1 1 6 3352.99 2980.96 34.25 o 2 1 6 4298.37 4047.76 59.38 o 3 1 6 4367.10 4353.84 134.57 o 4 1 6 5.25 8.42 1.52 o 5 1 6 609.57 612.16 20.83 o 6 1 6 336.65 380.07 18.99 o 7 1 6 111.48 98.39 8.68 o 8 1 6 0.29 0.77 0.92 o 9 1 6 59.38 58.86 4.72 o 0 2 6 1437.66 1332.41 41.95 o 1 2 6 6018.90 5966.17 104.54 o 2 2 6 3.22 6.05 0.79 o 3 2 6 1391.48 1379.92 23.31 o 4 2 6 337.03 338.32 13.44 o 5 2 6 29.17 30.66 2.04 o 6 2 6 9.01 9.69 0.62 o 7 2 6 27.44 33.87 2.38 o 8 2 6 39.66 47.37 3.15 o 9 2 6 11.28 9.66 0.87 o 1 3 6 670.59 695.83 13.12 o 2 3 6 7.81 10.68 1.97 o 3 3 6 89.91 92.84 4.51 o 4 3 6 2.58 6.74 0.73 o 5 3 6 102.27 92.35 6.04 o 6 3 6 56.96 60.09 2.42 o 7 3 6 0.18 3.43 1.12 o 8 3 6 3.66 3.77 0.86 o 9 3 6 0.10 -0.20 0.48 o 0 4 6 470.13 675.89 187.51 o 1 4 6 3424.43 3467.33 92.30 o 2 4 6 73.10 61.14 3.34 o 3 4 6 202.32 215.62 9.14 o 4 4 6 107.71 112.56 7.30 o 5 4 6 0.89 1.71 1.65 o 6 4 6 12.09 9.88 1.82 o 7 4 6 27.98 22.93 1.87 o 8 4 6 9.75 9.68 0.55 o 1 5 6 4441.23 4676.08 79.97 o 2 5 6 1014.26 1025.77 38.59 o 3 5 6 1448.79 1556.00 54.67 o 4 5 6 51.09 42.64 2.46 o 5 5 6 2.05 9.26 4.53 o 6 5 6 175.74 192.02 12.52 o 7 5 6 36.01 34.84 2.67 o 8 5 6 5.91 5.64 0.37 o 0 6 6 1558.43 1671.00 131.81 o 1 6 6 4563.81 4500.82 160.30 o 2 6 6 3.63 2.96 1.39 o 3 6 6 478.25 524.86 15.58 o 4 6 6 354.31 361.69 17.71 o 5 6 6 396.14 408.48 21.10 o 6 6 6 5.05 5.22 1.21 o 7 6 6 189.23 167.89 8.84 o 1 7 6 322.14 308.72 11.58 o 2 7 6 880.74 877.51 29.94 o 3 7 6 919.45 876.37 32.34 o 4 7 6 6.46 6.45 0.31 o 5 7 6 243.15 248.26 9.95 o 6 7 6 74.46 73.05 4.26 o 7 7 6 41.16 28.81 1.56 o 0 8 6 155.08 137.15 4.92 o 1 8 6 72.18 61.54 2.04 o 2 8 6 0.52 1.91 1.11 o 3 8 6 464.51 444.29 12.45 o 4 8 6 109.55 106.26 3.59 o 5 8 6 43.02 42.10 1.42 o 6 8 6 0.54 0.19 0.20 o 1 9 6 2.16 2.96 0.48 o 2 9 6 20.73 18.65 0.41 o 3 9 6 66.45 66.52 4.36 o 4 9 6 1.13 0.27 0.54 o 0 10 6 10.39 10.32 2.98 o 1 10 6 111.40 106.77 8.35 o 2 10 6 5.76 4.09 0.59 o 3 10 6 0.28 0.94 0.28 o 0 1 7 163.94 160.91 14.90 o 1 1 7 1943.36 1891.72 70.35 o 2 1 7 77.98 68.75 2.69 o 3 1 7 1442.98 1428.04 27.45 o 4 1 7 112.84 123.05 8.33 o 5 1 7 323.22 317.30 19.64 o 6 1 7 5.10 10.19 1.93 o 7 1 7 4.88 10.19 2.10 o 8 1 7 126.77 130.68 12.66 o 9 1 7 16.21 14.23 1.30 o 1 2 7 3903.30 3737.12 73.82 o 2 2 7 259.87 252.71 30.28 o 3 2 7 2613.74 2551.84 85.97 o 4 2 7 61.65 56.03 4.36 o 5 2 7 892.60 947.11 43.27 o 6 2 7 172.52 186.38 10.79 o 7 2 7 280.82 275.22 20.59 o 8 2 7 0.02 0.02 0.84 o 0 3 7 5618.93 5415.56 230.62 o 1 3 7 2987.16 2759.87 66.03 o 2 3 7 21.47 16.86 0.67 o 3 3 7 3714.82 3896.42 92.77 o 4 3 7 235.99 268.63 14.84 o 5 3 7 1695.54 1693.67 85.57 o 6 3 7 63.17 63.68 3.46 o 7 3 7 317.87 342.38 21.26 o 8 3 7 27.25 30.74 2.41 o 1 4 7 2405.46 2375.73 59.66 o 2 4 7 908.09 899.09 43.66 o 3 4 7 967.55 996.75 46.76 o 4 4 7 21.38 27.08 1.54 o 5 4 7 926.48 1005.68 55.27 o 6 4 7 7.19 4.91 1.03 o 7 4 7 263.23 248.27 16.85 o 8 4 7 10.36 8.31 0.68 o 0 5 7 479.28 490.53 29.42 o 1 5 7 642.74 634.75 11.72 o 2 5 7 81.69 99.85 3.52 o 3 5 7 686.63 787.91 29.84 o 4 5 7 338.00 394.89 22.60 o 5 5 7 111.01 114.12 6.50 o 6 5 7 2.52 1.65 1.48 o 7 5 7 60.30 66.66 3.46 o 8 5 7 11.01 10.33 0.27 o 1 6 7 17.78 20.01 2.30 o 2 6 7 6.21 9.21 1.76 o 3 6 7 10.62 10.21 0.57 o 4 6 7 9.31 13.76 1.55 o 5 6 7 1.01 2.39 0.53 o 6 6 7 51.25 49.03 3.53 o 7 6 7 20.47 14.15 0.96 o 0 7 7 24.68 34.27 6.06 o 1 7 7 45.14 57.75 2.99 o 2 7 7 162.56 138.53 5.04 o 3 7 7 273.33 270.06 10.10 o 4 7 7 1.37 3.16 0.81 o 5 7 7 106.09 97.84 5.74 o 6 7 7 2.60 2.68 0.43 o 1 8 7 411.63 394.00 14.04 o 2 8 7 36.14 31.72 3.21 o 3 8 7 222.75 215.62 8.68 o 4 8 7 38.70 29.60 1.18 o 5 8 7 135.20 117.18 6.31 o 0 9 7 174.24 146.68 17.39 o 1 9 7 390.81 351.52 14.90 o 2 9 7 1.30 2.46 0.63 o 3 9 7 256.42 226.30 16.02 o 4 9 7 18.64 14.26 2.26 o 1 10 7 145.00 120.95 13.51 o 0 0 8 2668.23 2832.98 362.96 o 1 0 8 3872.99 3797.01 247.70 o 2 0 8 85.67 98.53 2.83 o 3 0 8 3610.69 3719.40 127.28 o 4 0 8 26.29 34.32 3.29 o 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1017.93 25.78 o 2 5 8 3.05 43.29 18.65 o 3 5 8 1618.60 1769.55 85.59 o 4 5 8 0.01 0.47 1.47 o 5 5 8 497.43 534.27 34.96 o 6 5 8 53.72 54.27 3.63 o 7 5 8 52.22 40.64 2.85 o 0 6 8 34.25 44.96 9.57 o 1 6 8 1104.18 1220.22 42.23 o 2 6 8 53.60 63.01 4.32 o 3 6 8 841.33 943.63 38.06 o 4 6 8 56.54 66.12 4.93 o 5 6 8 385.66 378.64 21.90 o 6 6 8 0.98 0.96 0.38 o 1 7 8 1297.47 1363.58 39.41 o 2 7 8 92.83 88.65 5.52 o 3 7 8 320.39 332.75 9.52 o 4 7 8 3.81 3.22 1.80 o 5 7 8 201.15 208.82 7.79 o 6 7 8 0.24 2.34 0.57 o 0 8 8 117.81 126.27 13.61 o 1 8 8 106.02 104.04 2.44 o 2 8 8 5.52 6.21 0.56 o 3 8 8 72.10 74.55 2.80 o 4 8 8 17.15 17.73 0.93 o 5 8 8 29.51 23.54 2.09 o 1 9 8 3.94 3.34 0.39 o 2 9 8 14.43 14.03 0.95 o 3 9 8 1.59 1.58 0.29 o 0 1 9 1155.52 1169.29 48.50 o 1 1 9 390.36 355.42 17.24 o 2 1 9 0.97 -1.64 2.12 o 3 1 9 269.42 276.80 11.95 o 4 1 9 94.58 103.43 6.81 o 5 1 9 477.77 482.87 34.61 o 6 1 9 2.17 6.91 1.88 o 7 1 9 198.06 219.25 21.15 o 8 1 9 2.80 2.14 0.44 o 1 2 9 1653.72 1595.92 47.09 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2.07 o 3 7 9 23.07 34.33 2.80 o 4 7 9 1.32 1.20 0.62 o 5 7 9 45.78 39.64 4.76 o 1 8 9 161.85 183.72 17.89 o 2 8 9 7.29 8.35 0.83 o 3 8 9 240.93 211.84 15.48 o 4 8 9 0.06 0.76 0.20 o 0 9 9 40.45 42.96 5.94 o 1 9 9 193.27 167.51 26.25 o 2 9 9 0.01 -0.42 0.42 o 0 0 10 40.00 40.02 2.11 o 1 0 10 6388.61 6478.65 505.63 o 2 0 10 205.19 208.65 13.47 o 3 0 10 1024.01 1131.02 47.12 o 4 0 10 112.56 110.21 5.75 o 5 0 10 171.12 167.89 14.71 o 6 0 10 8.08 8.85 1.32 o 7 0 10 62.35 76.54 8.22 o 1 1 10 1545.43 1573.99 82.18 o 2 1 10 96.80 109.95 7.40 o 3 1 10 1494.67 1472.08 81.13 o 4 1 10 22.24 22.07 0.86 o 5 1 10 95.84 129.32 9.21 o 6 1 10 24.31 20.99 1.86 o 7 1 10 20.24 19.25 2.01 o 0 2 10 57.24 58.08 6.59 o 1 2 10 553.57 516.91 19.00 o 2 2 10 2.14 1.21 1.97 o 3 2 10 273.29 277.93 11.00 o 4 2 10 26.50 25.29 1.87 o 5 2 10 254.01 253.85 16.22 o 6 2 10 2.28 1.09 0.55 o 7 2 10 157.25 158.97 15.63 o 1 3 10 0.20 -0.82 1.30 o 2 3 10 12.03 12.68 0.51 o 3 3 10 69.26 74.83 4.04 o 4 3 10 1.56 0.39 1.65 o 5 3 10 32.92 39.63 2.33 o 6 3 10 0.04 0.35 0.99 o 7 3 10 27.60 24.39 2.09 o 0 4 10 0.82 1.09 3.29 o 1 4 10 714.32 688.66 27.76 o 2 4 10 4.68 4.29 0.82 o 3 4 10 3.32 10.47 1.73 o 4 4 10 106.53 110.24 4.45 o 5 4 10 61.37 60.53 4.26 o 6 4 10 2.40 3.36 0.88 o 7 4 10 32.73 25.98 2.40 o 1 5 10 559.32 558.13 21.24 o 2 5 10 37.90 43.71 5.96 o 3 5 10 424.10 451.50 24.59 o 4 5 10 0.53 1.93 0.63 o 5 5 10 52.05 67.32 3.94 o 6 5 10 35.26 28.17 1.98 o 0 6 10 10.92 23.38 9.95 o 1 6 10 957.89 1040.34 27.99 o 2 6 10 28.49 31.24 2.21 o 3 6 10 426.59 497.10 27.03 o 4 6 10 38.90 44.30 1.74 o 5 6 10 102.38 95.02 10.12 o 1 7 10 339.09 387.25 21.66 o 2 7 10 15.11 19.12 2.51 o 3 7 10 209.26 235.94 33.77 o 4 7 10 10.19 10.60 1.06 o 0 8 10 1.10 -0.26 1.01 o 1 8 10 127.32 143.10 23.10 o 2 8 10 0.34 1.04 0.41 o 3 8 10 116.31 103.96 19.78 o 0 1 11 227.63 236.98 30.51 o 1 1 11 17.97 22.19 2.94 o 2 1 11 43.02 43.84 3.13 o 3 1 11 444.40 517.85 24.58 o 4 1 11 236.80 242.90 16.07 o 5 1 11 161.40 167.28 13.87 o 6 1 11 4.30 6.57 0.89 o 7 1 11 11.18 13.34 1.30 o 1 2 11 802.84 820.36 37.58 o 2 2 11 187.82 190.56 5.06 o 3 2 11 256.93 256.78 15.93 o 4 2 11 23.80 26.54 1.25 o 5 2 11 443.27 527.78 37.94 o 6 2 11 123.15 116.79 10.68 o 7 2 11 154.21 118.19 12.41 o 0 3 11 370.24 389.04 11.24 o 1 3 11 381.46 346.70 18.50 o 2 3 11 99.87 96.65 3.34 o 3 3 11 964.89 1071.67 49.58 o 4 3 11 29.66 35.08 1.63 o 5 3 11 451.36 467.29 31.91 o 6 3 11 14.35 11.86 1.28 o 1 4 11 704.33 690.17 27.74 o 2 4 11 295.38 301.49 18.25 o 3 4 11 463.32 458.98 25.53 o 4 4 11 3.40 5.88 0.52 o 5 4 11 200.87 236.85 16.84 o 6 4 11 6.92 6.00 0.42 o 0 5 11 0.14 6.19 3.07 o 1 5 11 214.31 188.88 11.48 o 2 5 11 15.73 10.18 0.94 o 3 5 11 80.96 92.18 2.80 o 4 5 11 0.36 0.21 0.76 o 5 5 11 50.64 47.53 3.70 o 1 6 11 20.62 16.68 0.43 o 2 6 11 11.86 14.56 1.41 o 3 6 11 5.00 6.80 0.44 o 4 6 11 0.56 0.92 0.32 o 0 7 11 76.40 93.43 10.00 o 1 7 11 4.81 7.27 1.05 o 2 7 11 0.79 0.84 0.22 o 3 7 11 57.67 61.33 11.87 o 1 8 11 67.24 66.18 18.63 o 0 0 12 2479.18 2679.70 376.44 o 1 0 12 698.07 695.94 88.05 o 2 0 12 30.33 35.57 3.86 o 3 0 12 141.66 186.08 20.32 o 4 0 12 20.87 29.73 2.18 o 5 0 12 266.52 269.58 29.70 o 6 0 12 4.41 4.30 0.58 o 1 1 12 717.12 704.07 67.57 o 2 1 12 329.33 353.42 23.45 o 3 1 12 444.28 458.77 46.02 o 4 1 12 23.17 20.18 1.45 o 5 1 12 107.87 129.42 11.25 o 6 1 12 2.96 2.95 0.83 o 0 2 12 19.08 17.60 0.64 o 1 2 12 220.27 224.74 10.85 o 2 2 12 16.56 16.53 1.18 o 3 2 12 129.71 143.30 7.80 o 4 2 12 81.69 81.60 5.01 o 5 2 12 7.31 9.17 0.98 o 6 2 12 16.68 17.37 1.65 o 1 3 12 3.02 0.90 0.79 o 2 3 12 52.95 56.59 2.14 o 3 3 12 4.95 8.01 1.61 o 4 3 12 10.23 11.68 0.87 o 5 3 12 14.35 14.35 0.99 o 6 3 12 11.42 8.87 0.73 o 0 4 12 192.26 184.99 10.46 o 1 4 12 121.71 116.17 4.84 o 2 4 12 70.36 63.12 4.11 o 3 4 12 28.72 34.65 2.08 o 4 4 12 16.75 20.09 1.09 o 5 4 12 8.90 7.74 1.69 o 1 5 12 225.43 231.66 13.93 o 2 5 12 111.60 106.82 8.83 o 3 5 12 204.95 203.51 14.12 o 4 5 12 3.44 4.05 0.81 o 0 6 12 250.67 267.78 11.71 o 1 6 12 233.34 226.32 9.43 o 2 6 12 0.33 0.41 0.36 o 3 6 12 65.34 67.82 5.82 o 1 7 12 146.24 128.03 13.49 o 2 7 12 53.12 50.69 3.11 o 0 1 13 136.88 145.63 20.49 o 1 1 13 232.21 225.84 25.88 o 2 1 13 41.54 42.50 2.72 o 3 1 13 51.72 63.65 6.01 o 4 1 13 50.44 52.30 3.76 o 5 1 13 0.09 0.59 0.64 o 1 2 13 188.45 185.98 15.63 o 2 2 13 157.00 159.92 8.48 o 3 2 13 168.96 153.29 16.21 o 4 2 13 4.36 6.70 0.39 o 5 2 13 15.47 24.15 2.41 o 0 3 13 358.30 368.57 21.39 o 1 3 13 317.97 262.64 12.46 o 2 3 13 0.03 1.37 0.40 o 3 3 13 95.94 111.62 7.71 o 4 3 13 239.28 222.82 16.29 o 5 3 13 74.26 52.07 6.62 o 1 4 13 81.79 69.77 3.06 o 2 4 13 144.26 138.07 6.64 o 3 4 13 75.68 59.34 5.20 o 4 4 13 0.89 0.72 0.56 o 0 5 13 62.99 52.44 2.21 o 1 5 13 76.85 62.96 2.36 o 2 5 13 0.04 0.13 0.68 o 3 5 13 87.20 70.98 4.67 o 1 6 13 13.42 11.67 0.36 o 2 6 13 6.10 6.39 0.58 o 0 0 14 74.64 88.15 17.27 o 1 0 14 97.01 97.47 20.72 o 2 0 14 7.34 5.51 0.59 o 3 0 14 105.25 105.66 17.15 o 4 0 14 259.47 239.56 35.60 o 1 1 14 57.44 60.33 8.00 o 2 1 14 292.19 288.15 33.56 o 3 1 14 66.02 61.25 10.45 o 4 1 14 1.24 2.10 0.21 o 0 2 14 116.87 117.04 12.02 o 1 2 14 96.78 90.57 8.66 o 2 2 14 18.16 18.41 1.15 o 3 2 14 29.78 28.61 2.94 o 4 2 14 8.08 8.54 0.78 o 1 3 14 25.92 21.85 0.90 o 2 3 14 1.12 1.06 0.27 o 3 3 14 0.40 0.71 0.54 o 0 4 14 76.93 67.06 3.62 o 1 4 14 19.39 19.70 1.48 o 2 4 14 8.02 7.39 0.45 o 3 4 14 5.80 4.00 0.90 o 1 5 14 77.10 59.97 5.79 o 0 1 15 145.96 145.72 27.88 o 1 1 15 1.11 0.83 0.39 o 2 1 15 0.22 0.61 0.24 o 3 1 15 5.45 4.20 0.89 o 1 2 15 46.89 37.24 6.54 o 2 2 15 205.28 163.28 24.44 o 0 3 15 147.45 106.71 18.62 o 1 3 15 0.21 0.95 0.22 o