# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ccd3281 in C2 (No. 5; rel. H"aufigkeit 0.9%)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 552.08 _exptl_crystal_F_000 1952.00 _reflns_d_resolution_high 0.8302 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' _cell_length_a 26.2830 _cell_length_b 11.3346 _cell_length_c 19.2190 _cell_angle_alpha 90.000 _cell_angle_beta 121.397 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -11 0 72.20 222.84 499.34 o 3 -11 0 1071.35 934.71 926.45 o 5 -11 0 272.34 -247.60 699.48 o 7 -11 0 10.46 -12.38 742.81 o 15 -11 0 237.59 439.50 744.88 o 0 -10 0 995.99 383.79 491.08 o 2 -10 0 1160.66 1056.45 392.04 o 4 -10 0 1976.12 2036.55 389.98 o 6 -10 0 1785.59 1335.00 534.41 o 8 -10 0 3278.81 3173.47 802.65 o 10 -10 0 543.35 286.81 959.47 o 14 -10 0 67.53 -70.15 511.72 o 16 -10 0 448.76 348.71 643.77 o 18 -10 0 260.95 146.50 703.61 o 1 -9 0 399.78 334.27 317.76 o 3 -9 0 2438.59 2383.20 365.22 o 5 -9 0 391.72 146.50 408.55 o 7 -9 0 327.70 288.87 427.12 o 9 -9 0 558.14 519.97 474.58 o 11 -9 0 898.11 957.41 674.72 o 13 -9 0 587.94 515.84 701.55 o 15 -9 0 360.68 352.84 429.18 o 17 -9 0 252.27 311.57 445.69 o 19 -9 0 91.19 18.57 757.26 o 0 -8 0 9617.79 9761.82 623.14 o 2 -8 0 5407.16 5447.30 356.96 o 4 -8 0 1898.53 1735.30 315.70 o 6 -8 0 137.12 22.70 354.90 o 8 -8 0 3841.16 3493.29 387.91 o 10 -8 0 120.84 202.21 344.58 o 12 -8 0 1596.19 1675.46 412.67 o 14 -8 0 902.33 843.92 344.58 o 16 -8 0 3073.83 3152.83 293.00 o 18 -8 0 3904.08 3804.86 387.91 o 20 -8 0 496.83 208.40 594.25 o 1 -7 0 967.41 860.43 264.11 o 3 -7 0 1769.60 1574.35 301.25 o 5 -7 0 924.06 1000.74 323.95 o 7 -7 0 477.73 614.89 332.20 o 9 -7 0 616.41 782.02 350.77 o 11 -7 0 4071.11 4132.94 222.84 o 13 -7 0 514.27 515.84 187.77 o 15 -7 0 265.01 222.84 177.45 o 17 -7 0 950.87 788.21 262.05 o 19 -7 0 85.12 53.65 270.30 o 21 -7 0 486.48 297.13 447.75 o 23 -7 0 788.72 753.13 699.48 o 0 -6 0 14135.59 15246.26 767.57 o 2 -6 0 132.01 101.11 257.92 o 4 -6 0 5343.45 5249.22 375.53 o 6 -6 0 3261.88 3055.86 278.56 o 8 -6 0 2531.03 2746.35 321.89 o 10 -6 0 636.91 656.15 156.82 o 12 -6 0 5094.70 4995.43 245.54 o 14 -6 0 9138.22 10003.23 402.36 o 16 -6 0 1384.86 1281.35 218.72 o 18 -6 0 1059.91 978.04 276.49 o 20 -6 0 189.85 290.94 274.43 o 22 -6 0 539.15 274.43 489.02 o 24 -6 0 341.35 121.74 598.38 o 1 -5 0 553.21 610.76 220.78 o 3 -5 0 1820.79 1576.42 237.29 o 5 -5 0 872.07 930.58 226.97 o 7 -5 0 139.28 123.80 109.36 o 9 -5 0 93.61 78.41 129.99 o 11 -5 0 3850.93 3501.54 212.53 o 13 -5 0 871.55 897.57 163.01 o 15 -5 0 463.31 278.56 208.40 o 17 -5 0 671.03 732.50 193.96 o 19 -5 0 1310.66 1343.26 309.51 o 21 -5 0 341.02 293.00 293.00 o 23 -5 0 516.34 775.83 466.32 o 25 -5 0 79.69 408.55 614.89 o 0 -4 0 170.29 600.44 181.58 o 2 -4 0 1844.23 1743.55 177.45 o 4 -4 0 9271.82 9937.20 394.10 o 6 -4 0 11652.81 12473.09 354.90 o 8 -4 0 10367.41 11090.63 373.47 o 10 -4 0 627.34 588.06 134.12 o 12 -4 0 2837.39 2872.21 198.08 o 14 -4 0 3753.53 3765.66 224.91 o 16 -4 0 58.61 94.92 146.50 o 18 -4 0 3643.03 3350.92 309.51 o 20 -4 0 337.90 392.04 293.00 o 22 -4 0 84.07 216.65 439.50 o 24 -4 0 57.31 109.36 511.72 o 1 -3 0 162.16 175.39 111.42 o 3 -3 0 1092.80 1056.45 152.69 o 5 -3 0 70.98 88.73 78.41 o 7 -3 0 14.41 -8.25 80.47 o 9 -3 0 1429.02 1493.88 109.36 o 11 -3 0 417.21 439.50 121.74 o 13 -3 0 1584.43 1584.67 171.26 o 15 -3 0 679.81 528.22 181.58 o 17 -3 0 1335.75 1231.83 214.59 o 19 -3 0 2190.15 2090.20 266.18 o 21 -3 0 32.63 26.82 208.40 o 23 -3 0 381.16 812.97 499.34 o 25 -3 0 44.11 148.56 540.60 o 0 -2 0 303963.41 299766.81 10325.12 o 2 -2 0 3230.20 3369.49 107.30 o 4 -2 0 18843.27 19738.22 466.32 o 6 -2 0 33026.96 31837.84 604.57 o 8 -2 0 2553.49 2486.36 121.74 o 10 -2 0 7834.08 8383.48 255.86 o 12 -2 0 4025.28 4087.54 200.15 o 14 -2 0 13613.89 13424.30 460.13 o 16 -2 0 147.60 152.69 169.20 o 18 -2 0 1696.12 1539.28 171.26 o 20 -2 0 881.22 984.23 288.87 o 22 -2 0 34.09 76.34 346.65 o 24 -2 0 283.26 241.41 474.58 o 26 -2 0 145.55 -26.82 577.74 o 3 -1 0 4.57 12.38 33.01 o 5 -1 0 16474.28 15326.73 313.63 o 7 -1 0 1371.31 1423.73 84.60 o 9 -1 0 6772.73 6600.73 222.84 o 11 -1 0 1290.07 1341.19 117.61 o 13 -1 0 334.05 338.39 117.61 o 15 -1 0 140.68 154.75 84.60 o 17 -1 0 1167.80 969.79 231.10 o 19 -1 0 359.58 315.70 210.46 o 21 -1 0 80.50 136.18 297.13 o 23 -1 0 529.51 810.91 497.27 o 25 -1 0 115.72 515.84 569.49 o 4 0 0 419.55 305.38 53.65 o 6 0 0 5896.67 5781.57 210.46 o 8 0 0 2274.07 2168.60 109.36 o 10 0 0 2783.98 2577.15 123.80 o 12 0 0 704.55 751.07 92.85 o 14 0 0 20997.95 21085.61 720.12 o 16 0 0 2920.75 3233.30 284.75 o 18 0 0 4663.56 4749.88 352.84 o 20 0 0 5100.92 5189.38 443.63 o 22 0 0 85.42 259.98 340.46 o 24 0 0 140.37 -253.79 511.72 o 26 0 0 459.84 788.21 608.69 o 3 1 0 4.23 33.01 45.39 o 5 1 0 16509.14 15223.56 317.76 o 7 1 0 1376.16 1452.61 103.17 o 9 1 0 6775.93 6485.18 210.46 o 11 1 0 1305.75 1337.07 129.99 o 13 1 0 331.75 342.52 105.23 o 15 1 0 149.99 150.63 94.92 o 17 1 0 1170.87 1279.29 241.41 o 19 1 0 357.52 383.79 189.83 o 21 1 0 78.84 148.56 307.44 o 23 1 0 528.34 583.93 499.34 o 25 1 0 119.54 -198.08 645.84 o 0 2 0 304789.31 286794.38 6897.85 o 2 2 0 3214.48 3309.65 127.93 o 4 2 0 19078.61 19855.84 464.26 o 6 2 0 33392.75 31643.88 837.73 o 8 2 0 2600.16 2500.81 175.39 o 10 2 0 7828.20 8329.84 278.56 o 12 2 0 4008.72 4044.21 191.89 o 14 2 0 13734.76 13936.02 443.63 o 16 2 0 168.33 191.89 142.37 o 18 2 0 1674.18 1460.87 272.37 o 20 2 0 894.27 829.48 288.87 o 22 2 0 30.57 41.27 297.13 o 24 2 0 287.36 319.82 559.17 o 26 2 0 143.99 136.18 561.24 o 1 3 0 161.58 134.12 59.84 o 3 3 0 1087.42 967.72 123.80 o 5 3 0 71.33 107.30 117.61 o 7 3 0 15.37 18.57 138.25 o 9 3 0 1445.32 1508.33 179.51 o 11 3 0 408.36 472.51 189.83 o 13 3 0 1578.55 1545.47 216.65 o 15 3 0 688.68 536.48 220.78 o 17 3 0 1340.29 1174.06 243.48 o 19 3 0 2206.70 2663.81 456.01 o 21 3 0 30.25 61.90 350.77 o 23 3 0 382.92 379.66 418.86 o 25 3 0 38.80 26.82 577.74 o 0 4 0 195.37 534.41 134.12 o 2 4 0 1950.41 1916.87 86.66 o 4 4 0 9450.58 10197.19 369.34 o 6 4 0 11891.75 12446.26 383.79 o 8 4 0 10362.42 11076.18 443.63 o 10 4 0 620.18 598.38 212.53 o 12 4 0 2756.64 2659.69 266.18 o 14 4 0 3817.33 3586.14 344.58 o 16 4 0 69.93 14.44 278.56 o 18 4 0 3708.85 3493.29 342.52 o 20 4 0 363.62 344.58 427.12 o 22 4 0 80.00 -12.38 509.65 o 24 4 0 55.94 226.97 623.14 o 1 5 0 553.11 517.91 99.04 o 3 5 0 1803.51 1495.95 204.27 o 5 5 0 849.90 693.29 185.70 o 7 5 0 133.06 49.52 183.64 o 9 5 0 98.36 119.68 218.72 o 11 5 0 3847.35 3897.71 338.39 o 13 5 0 867.61 825.35 284.75 o 15 5 0 460.74 379.66 313.63 o 17 5 0 670.56 711.86 280.62 o 19 5 0 1326.49 1238.02 348.71 o 21 5 0 349.36 241.41 614.89 o 23 5 0 525.65 691.23 538.54 o 25 5 0 76.43 251.73 782.02 o 0 6 0 14587.90 14784.07 586.00 o 2 6 0 109.38 68.09 76.34 o 4 6 0 5386.55 5071.77 328.08 o 6 6 0 3241.40 3198.23 247.60 o 8 6 0 2575.20 2657.62 274.43 o 10 6 0 625.75 621.08 290.94 o 12 6 0 5070.05 5389.53 396.17 o 14 6 0 9244.64 10120.84 575.68 o 16 6 0 1401.72 1332.94 348.71 o 18 6 0 1098.42 922.33 410.61 o 20 6 0 207.65 212.53 369.34 o 22 6 0 531.15 264.11 586.00 o 24 6 0 338.23 297.13 709.80 o 1 7 0 971.92 907.88 132.06 o 3 7 0 1749.95 1722.92 249.67 o 5 7 0 923.04 975.98 237.29 o 7 7 0 473.29 332.20 247.60 o 9 7 0 607.87 695.36 319.82 o 11 7 0 4100.33 4219.60 396.17 o 13 7 0 516.79 505.53 371.41 o 15 7 0 251.34 293.00 334.27 o 17 7 0 945.17 817.10 369.34 o 19 7 0 88.18 276.49 480.77 o 21 7 0 497.47 555.05 707.74 o 23 7 0 789.47 763.45 713.93 o 0 8 0 9816.99 9722.61 555.05 o 2 8 0 5428.14 5802.20 402.36 o 4 8 0 1899.61 2055.12 305.38 o 6 8 0 135.93 132.06 284.75 o 8 8 0 3874.54 3491.23 377.60 o 10 8 0 115.33 138.25 317.76 o 12 8 0 1592.69 1885.92 443.63 o 14 8 0 948.24 912.01 410.61 o 16 8 0 3087.54 3375.68 511.72 o 18 8 0 3909.47 4211.34 577.74 o 20 8 0 508.45 414.74 433.31 o 1 9 0 408.88 484.89 140.31 o 3 9 0 2427.60 2430.65 340.46 o 5 9 0 401.03 264.11 332.20 o 7 9 0 326.39 293.00 323.95 o 9 9 0 557.14 334.27 445.69 o 11 9 0 907.95 930.58 371.41 o 13 9 0 594.00 400.29 445.69 o 15 9 0 350.88 445.69 414.74 o 17 9 0 250.27 105.23 528.22 o 19 9 0 90.34 80.47 478.70 o 0 10 0 937.49 1015.18 270.30 o 2 10 0 1088.65 947.09 297.13 o 4 10 0 2062.42 2358.44 332.20 o 6 10 0 1770.21 1661.02 373.47 o 8 10 0 3308.02 3375.68 526.16 o 10 10 0 556.85 278.56 522.03 o 12 10 0 2059.52 2183.05 639.65 o 14 10 0 62.49 697.42 532.35 o 16 10 0 435.31 491.08 563.30 o 18 10 0 251.19 150.63 600.44 o 1 11 0 74.73 99.04 259.98 o 3 11 0 1072.39 1138.98 361.09 o 5 11 0 279.43 435.37 392.04 o 7 11 0 9.08 -280.62 1015.18 o 9 11 0 311.97 581.87 571.55 o 11 11 0 146.05 127.93 691.23 o 13 11 0 28.45 616.95 763.45 o 15 11 0 243.07 177.45 586.00 o 0 12 0 1476.72 1112.16 994.55 o 2 12 0 527.68 753.13 705.67 o 4 12 0 224.78 183.64 445.69 o 6 12 0 474.06 375.53 493.15 o 8 12 0 387.15 666.47 542.67 o 10 12 0 75.16 -326.01 664.41 o 12 12 0 271.97 196.02 546.79 o 1 13 0 1.80 -82.53 1252.47 o 3 13 0 384.27 546.79 1153.43 o 5 13 0 140.79 -493.15 1285.48 o 7 13 0 56.21 -105.23 1326.75 o -7 -11 1 938.38 656.15 870.74 o -5 -11 1 1118.03 736.62 856.30 o -3 -11 1 567.09 670.60 528.22 o -1 -11 1 5117.84 4370.22 926.45 o 1 -11 1 1077.54 1134.85 744.88 o 3 -11 1 921.13 905.82 726.31 o 5 -11 1 356.07 627.27 647.90 o 7 -11 1 179.91 57.77 674.72 o 15 -11 1 69.69 -185.70 676.79 o -18 -10 1 62.29 361.09 685.04 o -16 -10 1 179.40 243.48 728.37 o -10 -10 1 427.81 736.62 1046.13 o -8 -10 1 514.13 278.56 711.86 o -6 -10 1 505.62 472.51 400.29 o -4 -10 1 202.08 146.50 396.17 o -2 -10 1 2117.28 2065.44 400.29 o 0 -10 1 123.69 204.27 336.33 o 2 -10 1 144.56 249.67 354.90 o 4 -10 1 575.82 701.55 323.95 o 6 -10 1 903.08 687.10 468.39 o 8 -10 1 50.12 -216.65 715.99 o 10 -10 1 0.84 177.45 786.14 o 14 -10 1 9.48 -202.21 592.19 o 16 -10 1 245.58 -175.39 629.33 o -21 -9 1 376.60 1081.21 825.35 o -19 -9 1 50.15 -204.27 588.06 o -17 -9 1 306.04 385.85 468.39 o -15 -9 1 935.42 845.98 435.37 o -13 -9 1 322.83 515.84 676.79 o -11 -9 1 1042.73 990.42 538.54 o -9 -9 1 4823.33 4423.87 484.89 o -7 -9 1 2947.36 2812.38 400.29 o -5 -9 1 3508.13 3526.30 410.61 o -3 -9 1 854.80 1037.88 321.89 o -1 -9 1 286.44 379.66 303.32 o 1 -9 1 3694.01 3551.06 367.28 o 3 -9 1 10920.95 10931.75 538.54 o 5 -9 1 4933.26 4914.95 563.30 o 7 -9 1 1565.40 1722.92 425.05 o 9 -9 1 5115.31 4687.98 567.43 o 11 -9 1 7660.69 7374.49 920.26 o 13 -9 1 2013.74 2075.75 466.32 o 15 -9 1 465.03 484.89 462.20 o 17 -9 1 655.15 1035.81 472.51 o 19 -9 1 181.73 641.71 670.60 o -22 -8 1 262.46 150.63 612.82 o -20 -8 1 702.66 530.29 402.36 o -18 -8 1 703.18 658.22 280.62 o -16 -8 1 1055.43 1019.31 204.27 o -14 -8 1 445.40 641.71 406.48 o -12 -8 1 503.12 398.23 427.12 o -10 -8 1 575.96 602.50 311.57 o -8 -8 1 945.59 874.87 383.79 o -6 -8 1 1049.92 1184.38 373.47 o -4 -8 1 474.31 171.26 367.28 o -2 -8 1 1169.42 959.47 297.13 o 0 -8 1 741.15 623.14 243.48 o 2 -8 1 770.28 749.00 266.18 o 4 -8 1 491.67 639.65 336.33 o 6 -8 1 2899.01 2750.48 456.01 o 8 -8 1 556.58 625.20 394.10 o 10 -8 1 152.20 -4.13 383.79 o 12 -8 1 220.79 115.55 286.81 o 14 -8 1 357.01 243.48 198.08 o 16 -8 1 1078.16 990.42 257.92 o 18 -8 1 481.94 255.86 402.36 o 20 -8 1 490.88 493.15 718.05 o -23 -7 1 1596.10 2457.48 761.38 o -21 -7 1 418.92 486.96 379.66 o -19 -7 1 123.37 61.90 237.29 o -17 -7 1 246.41 338.39 241.41 o -15 -7 1 871.50 817.10 216.65 o -13 -7 1 935.35 852.17 175.39 o -11 -7 1 1296.91 1262.78 361.09 o -9 -7 1 6186.55 6545.02 458.07 o -7 -7 1 2572.38 2672.07 373.47 o -5 -7 1 3306.87 3458.21 350.77 o -3 -7 1 5294.05 5558.73 363.15 o -1 -7 1 3411.41 3990.56 297.13 o 1 -7 1 1909.71 1757.99 255.86 o 3 -7 1 5412.90 5608.25 422.99 o 5 -7 1 1753.24 1951.95 375.53 o 7 -7 1 5769.29 5641.26 451.88 o 9 -7 1 18519.19 19449.35 833.60 o 11 -7 1 9156.93 9373.90 394.10 o 13 -7 1 5518.50 5212.08 297.13 o 15 -7 1 1640.36 1401.03 259.98 o 17 -7 1 2397.36 2358.44 342.52 o 19 -7 1 182.28 293.00 313.63 o 21 -7 1 150.22 -152.69 460.13 o -24 -6 1 136.00 468.39 550.92 o -22 -6 1 806.59 897.57 515.84 o -20 -6 1 60.10 229.03 264.11 o -18 -6 1 124.02 -24.76 237.29 o -16 -6 1 883.34 942.96 214.59 o -14 -6 1 1736.95 1644.51 196.02 o -12 -6 1 894.26 953.28 156.82 o -10 -6 1 1882.57 2098.45 187.77 o -8 -6 1 1090.60 1066.76 293.00 o -6 -6 1 665.64 600.44 231.10 o -4 -6 1 356.10 200.15 257.92 o -2 -6 1 363.46 303.32 216.65 o 0 -6 1 167.25 134.12 183.64 o 2 -6 1 1246.48 1124.54 280.62 o 4 -6 1 1001.12 967.72 243.48 o 6 -6 1 3137.89 2965.07 363.15 o 8 -6 1 267.13 191.89 142.37 o 10 -6 1 596.37 550.92 189.83 o 12 -6 1 774.56 720.12 189.83 o 14 -6 1 1761.10 1881.80 202.21 o 16 -6 1 1368.45 1167.87 229.03 o 18 -6 1 179.08 181.58 278.56 o 20 -6 1 275.71 497.27 437.43 o 22 -6 1 531.20 614.89 536.48 o -25 -5 1 262.56 202.21 528.22 o -23 -5 1 277.12 598.38 503.46 o -21 -5 1 847.65 796.46 346.65 o -19 -5 1 2941.44 2606.04 396.17 o -17 -5 1 1789.05 1712.60 214.59 o -15 -5 1 260.49 319.82 173.32 o -13 -5 1 902.01 901.69 146.50 o -11 -5 1 9140.45 9499.77 313.63 o -9 -5 1 2260.49 2226.38 160.94 o -7 -5 1 13804.97 14375.52 379.66 o -5 -5 1 4799.13 5232.71 305.38 o -3 -5 1 5273.17 5350.33 311.57 o -1 -5 1 12072.10 14160.93 501.40 o 1 -5 1 12823.61 14115.53 534.41 o 3 -5 1 2063.40 2459.54 247.60 o 5 -5 1 129.25 101.11 175.39 o 7 -5 1 289.35 262.05 134.12 o 9 -5 1 13935.44 14070.14 412.67 o 11 -5 1 4359.10 4607.51 237.29 o 13 -5 1 2307.04 2290.34 206.34 o 15 -5 1 3928.51 3676.93 257.92 o 17 -5 1 213.29 278.56 202.21 o 19 -5 1 358.92 385.85 350.77 o 21 -5 1 220.49 326.01 420.93 o 23 -5 1 281.80 389.98 559.17 o -26 -4 1 463.20 140.31 678.85 o -24 -4 1 635.91 798.53 418.86 o -22 -4 1 943.72 1167.87 354.90 o -20 -4 1 264.34 414.74 288.87 o -18 -4 1 929.49 852.17 235.22 o -16 -4 1 183.60 226.97 181.58 o -14 -4 1 2177.42 2271.77 187.77 o -12 -4 1 1092.74 1031.69 134.12 o -10 -4 1 2495.75 2471.92 158.88 o -8 -4 1 254.48 323.95 132.06 o -6 -4 1 639.54 782.02 99.04 o -4 -4 1 931.80 728.37 169.20 o -2 -4 1 433.79 319.82 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