# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' kawa481_x in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 227.38 _exptl_crystal_F_000 556.00 _reflns_d_resolution_high 0.7496 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.1969 _cell_length_b 11.2632 _cell_length_c 11.7448 _cell_angle_alpha 71.016 _cell_angle_beta 75.660 _cell_angle_gamma 80.137 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 19010.91 16741.83 557.90 o 2 0 0 2669.12 2847.30 57.60 o 3 0 0 3199.27 3448.23 69.86 o 4 0 0 8959.99 9134.81 182.40 o 5 0 0 9346.29 9516.08 190.61 o 6 0 0 4486.64 4535.36 93.23 o 7 0 0 1230.40 1267.91 29.97 o 8 0 0 424.98 425.29 14.84 o 9 0 0 778.94 781.71 33.58 o 10 0 0 706.76 700.29 33.02 o -10 1 0 129.66 132.96 15.95 o -9 1 0 803.80 782.61 33.91 o -8 1 0 2487.90 2579.45 56.50 o -7 1 0 1124.95 1153.29 27.63 o -6 1 0 260.43 238.15 9.12 o -5 1 0 672.22 660.37 16.32 o -4 1 0 6703.40 6779.71 135.87 o -3 1 0 9819.42 9878.75 196.61 o -2 1 0 3165.37 3255.54 65.41 o -1 1 0 3145.26 3412.65 68.64 o 0 1 0 2896.53 3480.92 98.94 o 1 1 0 6208.90 6578.58 108.47 o 2 1 0 21626.97 20940.56 421.11 o 3 1 0 13144.36 12860.70 255.25 o 4 1 0 1104.73 1133.67 24.97 o 5 1 0 97.66 99.08 10.16 o 6 1 0 1466.92 1566.13 34.93 o 7 1 0 4190.25 4270.98 88.94 o 8 1 0 1647.31 1645.67 38.29 o 9 1 0 263.37 274.60 12.92 o -10 2 0 302.35 312.98 23.36 o -9 2 0 135.69 136.78 15.27 o -8 2 0 279.04 297.37 18.30 o -7 2 0 2569.24 2508.36 54.04 o -6 2 0 6336.12 6449.08 130.84 o -5 2 0 7288.72 7451.80 149.63 o -4 2 0 1490.92 1493.67 31.92 o -3 2 0 510.64 507.36 12.05 o -2 2 0 13507.32 13125.96 261.23 o -1 2 0 51701.55 38283.15 764.71 o 1 2 0 374.84 410.10 7.47 o 2 2 0 220.26 211.44 5.76 o 3 2 0 20153.03 20095.43 402.31 o 4 2 0 15173.92 15430.24 433.70 o 5 2 0 5246.23 5276.93 107.11 o 6 2 0 1610.04 1507.89 88.49 o 7 2 0 285.85 261.71 10.58 o 8 2 0 1264.98 1292.24 31.58 o 9 2 0 1430.25 1380.71 47.39 o 10 2 0 737.02 750.27 32.01 o -10 3 0 444.55 478.05 28.64 o -9 3 0 804.18 854.82 36.72 o -8 3 0 691.19 676.04 29.42 o -7 3 0 85.98 79.84 10.67 o -6 3 0 381.09 370.44 16.73 o -5 3 0 3352.05 3368.79 101.52 o -4 3 0 10936.51 11757.39 234.26 o -3 3 0 8980.12 9078.65 180.88 o -2 3 0 5323.81 5175.03 103.64 o -1 3 0 23.05 29.32 2.05 o 0 3 0 8753.44 8717.51 242.45 o 1 3 0 16866.32 16072.51 449.19 o 2 3 0 14025.63 14186.10 229.84 o 3 3 0 4031.62 4086.94 67.05 o 4 3 0 141.40 125.35 5.67 o 5 3 0 3806.88 3830.60 78.80 o 6 3 0 4650.70 4743.33 97.54 o 7 3 0 3038.17 3103.36 66.10 o 8 3 0 196.65 191.22 9.64 o 9 3 0 76.31 68.61 11.23 o 10 3 0 493.71 506.92 26.17 o -9 4 0 58.49 71.20 13.81 o -8 4 0 1074.21 1082.78 41.55 o -7 4 0 1741.07 1645.74 55.36 o -6 4 0 2768.57 2736.27 84.56 o -5 4 0 834.99 864.43 20.89 o -4 4 0 1061.97 1064.29 32.12 o -3 4 0 11451.82 11747.88 233.67 o -2 4 0 15931.07 15634.71 310.88 o -1 4 0 16999.94 16749.27 258.98 o 0 4 0 50.28 57.38 4.27 o 1 4 0 64.08 53.23 4.49 o 2 4 0 5540.25 5466.95 108.67 o 3 4 0 14682.62 14761.96 239.10 o 4 4 0 9154.44 9193.03 149.34 o 5 4 0 1545.94 1576.17 107.19 o 6 4 0 3.98 10.59 7.13 o 7 4 0 2932.88 2924.38 62.57 o 8 4 0 1077.40 1050.78 38.52 o 9 4 0 991.59 982.50 38.18 o 10 4 0 237.22 211.46 17.74 o -9 5 0 476.07 448.41 26.84 o -8 5 0 34.80 23.13 9.77 o -7 5 0 77.38 88.04 11.68 o -6 5 0 1181.84 1194.30 42.22 o -5 5 0 2339.13 2356.92 73.56 o -4 5 0 5852.64 5902.70 129.54 o -3 5 0 2033.83 1992.25 41.88 o -2 5 0 175.15 232.86 7.19 o -1 5 0 13397.76 13404.39 205.22 o 0 5 0 8182.80 8670.80 242.23 o 1 5 0 12128.08 12059.97 336.11 o 2 5 0 3154.07 3248.26 65.91 o 3 5 0 347.61 362.21 10.07 o 4 5 0 4512.33 4507.51 74.44 o 5 5 0 6309.35 6367.92 128.96 o 6 5 0 5422.41 5531.99 113.15 o 7 5 0 524.33 491.76 22.24 o 8 5 0 49.16 73.33 10.56 o 9 5 0 653.59 694.45 30.77 o 10 5 0 639.06 570.59 28.86 o -9 6 0 453.70 476.82 28.64 o -8 6 0 957.48 901.98 37.84 o -7 6 0 1146.02 1104.68 41.78 o -6 6 0 488.38 478.28 22.91 o -5 6 0 297.51 307.59 17.18 o -4 6 0 2730.56 2889.78 87.82 o -3 6 0 6105.50 6166.66 124.45 o -2 6 0 7632.72 7814.16 156.63 o -1 6 0 781.54 791.04 13.94 o 0 6 0 736.88 766.89 25.04 o 1 6 0 2727.68 2698.31 78.72 o 2 6 0 6911.14 6718.98 134.16 o 3 6 0 4351.47 4399.39 89.13 o 4 6 0 1463.96 1474.92 32.23 o 5 6 0 6.06 9.08 2.72 o 6 6 0 3279.52 3110.89 93.77 o 7 6 0 2413.43 2384.55 75.02 o 8 6 0 1038.41 1058.30 40.09 o 9 6 0 397.64 360.14 22.68 o -8 7 0 51.43 42.11 12.80 o -7 7 0 655.65 644.48 29.87 o -6 7 0 1527.74 1533.77 52.67 o -5 7 0 1601.59 1598.01 53.90 o -4 7 0 934.66 862.90 31.56 o -3 7 0 172.44 165.30 7.50 o -2 7 0 2934.70 3019.22 62.54 o -1 7 0 7477.41 7467.88 115.75 o 0 7 0 6891.94 7227.42 203.60 o 1 7 0 3492.39 3443.52 99.83 o 2 7 0 225.03 224.38 15.44 o 3 7 0 3235.38 3191.85 66.06 o 4 7 0 4063.34 4095.38 83.84 o 5 7 0 3900.91 4068.46 120.27 o 6 7 0 646.27 611.47 25.83 o 7 7 0 12.98 23.47 8.42 o 8 7 0 637.24 637.97 29.31 o 9 7 0 959.30 916.47 38.86 o -8 8 0 399.49 404.39 24.48 o -7 8 0 165.85 165.98 16.40 o -6 8 0 49.76 55.25 10.67 o -5 8 0 1103.51 1121.97 41.55 o -4 8 0 1850.57 1922.44 62.21 o -3 8 0 2068.61 2095.60 65.92 o -2 8 0 952.36 938.82 22.25 o -1 8 0 206.01 188.19 6.60 o 0 8 0 2043.66 2081.78 44.43 o 1 8 0 5953.37 6007.30 171.26 o 2 8 0 4850.47 4629.98 182.93 o 3 8 0 1406.46 1394.49 31.78 o 4 8 0 52.23 63.65 9.10 o 5 8 0 1229.82 1227.65 43.46 o 6 8 0 2805.98 2593.09 81.30 o 7 8 0 1047.76 1030.11 39.42 o 8 8 0 432.71 404.72 23.13 o 9 8 0 11.69 5.39 10.89 o -7 9 0 622.86 603.49 30.77 o -6 9 0 838.58 859.65 36.50 o -5 9 0 433.28 403.94 22.80 o -4 9 0 215.98 205.28 14.94 o -3 9 0 1621.23 1599.58 52.78 o -2 9 0 2725.08 2839.69 86.81 o -1 9 0 1544.21 1514.98 27.35 o 0 9 0 914.83 925.79 22.39 o 1 9 0 92.59 107.02 9.43 o 2 9 0 2161.56 2014.07 44.41 o 3 9 0 4818.51 4709.57 96.87 o 4 9 0 2590.13 2612.96 81.19 o 5 9 0 863.96 856.16 33.46 o 6 9 0 104.75 118.92 13.59 o 7 9 0 263.65 256.04 18.42 o 8 9 0 802.52 748.25 34.36 o -6 10 0 277.50 275.13 19.99 o -5 10 0 852.47 845.72 36.05 o -4 10 0 756.16 706.58 30.43 o -3 10 0 754.80 728.37 29.09 o -2 10 0 11.79 13.14 7.41 o -1 10 0 618.90 606.08 24.37 o 0 10 0 1964.64 1992.80 33.85 o 1 10 0 2726.35 2769.28 83.66 o 2 10 0 733.52 720.96 59.01 o 3 10 0 12.90 10.82 5.32 o 4 10 0 770.24 747.35 30.99 o 5 10 0 2220.31 2257.09 73.56 o 6 10 0 1101.40 1168.13 44.58 o 7 10 0 274.80 248.18 18.64 o 8 10 0 0.02 -0.34 11.57 o -5 11 0 25.51 20.44 12.13 o -4 11 0 790.61 793.16 34.14 o -3 11 0 1695.18 1691.78 57.50 o -2 11 0 1042.39 1130.17 40.76 o -1 11 0 304.33 313.65 17.52 o 0 11 0 36.01 35.94 7.52 o 1 11 0 899.57 868.87 18.59 o 2 11 0 1985.14 2068.60 46.61 o 3 11 0 1946.93 1895.38 61.99 o 4 11 0 591.20 593.16 27.51 o 5 11 0 26.37 28.86 10.11 o 6 11 0 313.92 316.68 22.57 o 7 11 0 624.39 655.49 32.79 o -4 12 0 130.21 124.88 14.60 o -3 12 0 0.61 10.33 9.99 o -2 12 0 434.17 452.00 23.25 o -1 12 0 1097.59 1152.30 41.66 o 0 12 0 1170.37 1204.07 42.11 o 1 12 0 350.72 369.27 14.60 o 2 12 0 6.01 1.70 6.07 o 3 12 0 334.90 343.75 20.33 o 4 12 0 1139.09 1109.29 42.67 o 5 12 0 854.73 781.71 34.81 o 6 12 0 163.44 170.81 17.74 o -3 13 0 406.60 386.87 24.14 o -2 13 0 182.14 195.85 16.28 o -1 13 0 0.27 8.53 8.98 o 0 13 0 475.99 520.73 24.26 o 1 13 0 927.35 952.97 37.96 o 3 13 0 224.08 222.46 17.41 o 4 13 0 4.86 -4.49 9.99 o 5 13 0 168.68 201.13 17.74 o 0 14 0 164.88 135.54 14.94 o -4 -13 1 399.00 413.60 25.04 o -3 -13 1 113.38 119.60 14.49 o -1 -13 1 440.14 408.77 23.58 o 0 -13 1 781.55 829.10 35.71 o 2 -13 1 127.68 151.27 15.27 o -5 -12 1 2.37 -1.01 11.45 o -4 -12 1 444.37 408.65 24.03 o -3 -12 1 1010.08 1065.15 40.76 o -2 -12 1 812.89 863.52 24.34 o -1 -12 1 228.79 226.39 16.84 o 0 -12 1 2.57 15.95 9.10 o 1 -12 1 358.10 382.71 21.00 o 2 -12 1 803.36 836.18 33.91 o 3 -12 1 636.16 698.83 31.56 o 4 -12 1 118.29 124.43 14.71 o -6 -11 1 777.00 802.60 36.72 o -5 -11 1 1061.69 1106.37 43.46 o -4 -11 1 416.41 418.54 23.47 o -3 -11 1 7.08 10.23 11.85 o -2 -11 1 790.20 768.52 26.05 o -1 -11 1 1447.09 1504.42 47.17 o 0 -11 1 1327.31 1386.21 46.49 o 1 -11 1 490.00 494.56 22.35 o 2 -11 1 1.92 -6.29 6.63 o 3 -11 1 410.76 388.33 21.79 o 4 -11 1 929.51 1024.72 41.10 o 5 -11 1 784.76 765.76 35.15 o -7 -10 1 132.98 126.11 15.27 o -6 -10 1 2.89 5.05 9.32 o -5 -10 1 883.80 934.21 37.17 o -4 -10 1 2173.11 2189.60 70.86 o -3 -10 1 2130.76 2159.00 48.39 o -2 -10 1 298.27 302.24 12.23 o -1 -10 1 4.66 6.35 3.63 o 0 -10 1 799.22 752.60 35.77 o 1 -10 1 1775.62 1876.73 59.74 o 2 -10 1 1636.78 1680.10 55.14 o 3 -10 1 482.25 483.33 23.02 o 4 -10 1 9.00 20.44 9.88 o 5 -10 1 267.60 222.69 18.19 o 6 -10 1 435.16 409.22 24.14 o -8 -9 1 240.84 282.77 21.90 o -7 -9 1 754.60 750.38 33.69 o -6 -9 1 1117.21 1025.06 39.64 o -5 -9 1 815.01 822.03 33.80 o -4 -9 1 9.38 34.43 10.44 o -3 -9 1 1236.03 1232.85 29.69 o -2 -9 1 3932.76 4021.07 83.69 o -1 -9 1 3096.29 3174.01 54.61 o 0 -9 1 937.80 898.24 21.88 o 1 -9 1 1.52 12.13 5.95 o 2 -9 1 515.68 502.09 21.56 o 3 -9 1 1931.00 1910.87 61.76 o 4 -9 1 2287.03 2335.92 74.68 o 5 -9 1 670.69 705.68 30.99 o 6 -9 1 0.37 -7.52 10.22 o 7 -9 1 145.71 148.68 15.95 o -8 -8 1 224.44 178.44 17.52 o -7 -8 1 1.57 0.00 9.55 o -6 -8 1 540.44 545.21 25.94 o -5 -8 1 3151.25 3242.40 98.82 o -4 -8 1 2183.90 2264.77 49.37 o -3 -8 1 1104.56 1137.92 27.15 o -2 -8 1 8.68 16.02 4.44 o -1 -8 1 1952.00 1945.08 41.85 o 0 -8 1 5162.87 5241.95 106.63 o 1 -8 1 3929.13 3943.42 62.40 o 2 -8 1 1407.74 1333.66 43.80 o 3 -8 1 7.16 0.45 5.73 o 4 -8 1 1030.51 1020.23 37.17 o 5 -8 1 1663.47 1626.08 55.59 o 6 -8 1 1416.52 1347.70 48.63 o 7 -8 1 347.48 323.42 21.11 o 8 -8 1 2.75 -8.53 9.66 o -9 -7 1 294.27 308.60 22.80 o -8 -7 1 1056.88 1098.95 42.67 o -7 -7 1 1838.58 1861.01 61.99 o -6 -7 1 976.83 940.28 35.26 o -5 -7 1 0.24 8.02 12.30 o -4 -7 1 1094.68 1061.89 38.74 o -3 -7 1 4760.32 4874.49 99.26 o -2 -7 1 5672.64 5589.47 112.96 o -1 -7 1 3082.91 3217.60 66.62 o 0 -7 1 76.82 62.52 4.30 o 1 -7 1 1754.28 1781.17 54.69 o 2 -7 1 4711.25 4597.16 111.51 o 3 -7 1 3073.89 3037.56 91.64 o 4 -7 1 1570.04 1642.93 53.68 o 5 -7 1 5.00 1.57 7.86 o 6 -7 1 277.30 297.82 18.30 o 7 -7 1 833.88 809.34 34.25 o 8 -7 1 752.57 699.73 33.24 o -9 -6 1 223.04 226.51 18.64 o -8 -6 1 17.57 14.26 9.43 o -7 -6 1 460.31 475.47 23.13 o -6 -6 1 3312.31 3359.41 101.29 o -5 -6 1 3050.26 3091.45 64.41 o -4 -6 1 1574.60 1560.12 34.36 o -3 -6 1 43.70 52.94 4.62 o -2 -6 1 2208.11 2238.63 47.09 o -1 -6 1 8762.46 9010.23 179.06 o 0 -6 1 8732.26 8775.96 175.35 o 1 -6 1 5988.47 6025.07 121.11 o 2 -6 1 14.06 16.78 2.78 o 3 -6 1 1902.86 1857.94 39.34 o 4 -6 1 4767.46 5167.19 152.16 o 5 -6 1 2242.92 2302.91 72.77 o 6 -6 1 1131.97 1112.65 40.65 o 7 -6 1 3.10 13.59 8.53 o 8 -6 1 234.19 217.07 17.41 o 9 -6 1 468.88 456.61 26.73 o -9 -5 1 909.10 980.59 39.53 o -8 -5 1 1518.54 1591.94 54.69 o -7 -5 1 1762.10 1793.97 58.84 o -6 -5 1 45.68 43.23 8.31 o -5 -5 1 1754.23 1797.14 31.49 o -4 -5 1 6589.08 6608.70 108.23 o -3 -5 1 5045.36 5323.96 107.04 o -2 -5 1 6283.10 6688.47 133.32 o -1 -5 1 1205.91 1227.93 26.76 o 0 -5 1 3263.77 3308.09 67.17 o 1 -5 1 13064.65 13095.20 260.01 o 2 -5 1 14047.34 14126.16 280.52 o 3 -5 1 4601.74 4786.43 96.54 o 4 -5 1 178.09 142.73 9.88 o 5 -5 1 509.44 496.25 21.45 o 6 -5 1 1265.13 1216.98 42.56 o 7 -5 1 1580.31 1582.06 54.58 o 8 -5 1 688.13 718.26 32.68 o 9 -5 1 51.40 42.79 12.02 o -10 -4 1 175.59 202.47 17.97 o -9 -4 1 30.49 36.50 10.89 o -8 -4 1 477.25 461.66 23.36 o -7 -4 1 1599.19 1611.82 52.89 o -6 -4 1 4442.50 4554.72 93.78 o -5 -4 1 1589.67 1589.45 34.83 o -4 -4 1 8.09 12.66 2.93 o -3 -4 1 4214.36 4394.73 72.29 o -2 -4 1 10692.23 11110.67 219.16 o -1 -4 1 6657.72 6291.97 124.99 o 0 -4 1 5117.78 5066.15 101.39 o 1 -4 1 613.48 597.50 19.32 o 2 -4 1 6262.40 6504.75 129.95 o 3 -4 1 11844.51 12191.11 242.36 o 4 -4 1 6949.48 7286.86 146.07 o 5 -4 1 2520.94 2521.66 77.49 o 6 -4 1 103.67 107.69 9.99 o 7 -4 1 502.87 501.75 24.14 o 8 -4 1 826.06 893.67 36.16 o 9 -4 1 847.20 821.80 36.72 o -10 -3 1 542.61 566.10 28.52 o -9 -3 1 1008.03 1043.14 39.64 o -8 -3 1 966.41 931.07 35.26 o -7 -3 1 67.27 72.90 11.62 o -6 -3 1 2577.44 2673.24 56.82 o -5 -3 1 3689.62 3491.94 307.70 o -4 -3 1 11197.84 11737.06 233.91 o -3 -3 1 10657.18 11356.82 183.75 o -2 -3 1 2425.88 2613.35 43.33 o -1 -3 1 468.95 459.18 16.06 o 0 -3 1 14007.89 13849.38 277.74 o 1 -3 1 17767.38 17274.66 347.13 o 2 -3 1 14661.36 14251.26 395.57 o 3 -3 1 1471.91 1605.85 33.44 o 4 -3 1 1059.39 1100.83 24.03 o 5 -3 1 5439.10 5397.91 109.07 o 6 -3 1 3918.51 3825.79 115.11 o 7 -3 1 1577.83 1613.62 54.91 o 8 -3 1 166.62 173.61 15.16 o 9 -3 1 155.16 163.51 16.73 o 10 -3 1 407.25 428.53 27.18 o -10 -2 1 5.07 11.23 10.56 o -9 -2 1 466.43 435.61 22.80 o -8 -2 1 1424.14 1496.15 50.20 o -7 -2 1 3110.28 3214.24 68.32 o -6 -2 1 972.24 962.18 38.24 o -5 -2 1 1.22 5.67 3.15 o -4 -2 1 3916.78 3941.88 80.28 o -3 -2 1 14606.14 14900.36 241.12 o -2 -2 1 20014.25 19693.51 320.87 o -1 -2 1 10719.09 11118.60 219.47 o 0 -2 1 2899.82 3005.30 60.26 o 1 -2 1 17686.03 17619.38 570.53 o 2 -2 1 7563.99 7977.60 159.64 o 3 -2 1 9316.31 9387.06 186.75 o 4 -2 1 2698.95 2635.39 54.17 o 5 -2 1 561.36 543.53 31.89 o 6 -2 1 960.41 950.72 22.56 o 7 -2 1 2016.52 2009.13 65.25 o 8 -2 1 1903.99 1719.07 58.73 o 9 -2 1 453.67 531.40 27.74 o 10 -2 1 20.14 8.31 11.90 o -9 -1 1 445.46 482.88 23.69 o -8 -1 1 49.01 44.16 6.47 o -7 -1 1 1436.21 1454.10 33.66 o -6 -1 1 1630.21 1621.94 36.09 o -5 -1 1 5438.07 5407.26 109.76 o -4 -1 1 7058.20 7385.45 148.07 o -3 -1 1 2364.91 2583.21 52.92 o -2 -1 1 2118.97 2144.41 35.42 o -1 -1 1 14407.84 14686.16 241.25 o 0 -1 1 42463.06 39103.93 1119.28 o 1 -1 1 10016.70 10017.93 288.83 o 2 -1 1 17644.44 17474.42 598.66 o 3 -1 1 867.22 814.63 17.73 o 4 -1 1 4867.85 4792.18 96.67 o 5 -1 1 11005.42 11467.63 228.98 o 6 -1 1 4427.89 4422.76 90.90 o 7 -1 1 398.76 393.21 12.86 o 8 -1 1 288.76 301.97 19.43 o 9 -1 1 751.41 696.03 31.67 o 10 -1 1 732.79 811.02 36.83 o -9 0 1 971.20 1014.84 27.37 o -8 0 1 2730.68 2725.84 59.61 o -7 0 1 1381.52 1386.31 35.26 o -6 0 1 1.21 44.69 30.99 o -5 0 1 1876.90 1963.59 42.04 o -4 0 1 5783.60 6094.82 122.62 o -3 0 1 11987.06 12110.05 240.57 o -2 0 1 15335.74 15868.04 320.40 o -1 0 1 1474.68 1626.82 33.43 o 0 0 1 6989.31 7364.70 122.44 o 2 0 1 10432.98 10424.82 208.88 o 3 0 1 2834.88 2821.64 57.30 o 4 0 1 166.66 169.44 6.40 o 5 0 1 580.94 577.42 14.73 o 6 0 1 3963.37 3829.90 168.78 o 7 0 1 4238.64 4352.22 90.38 o 8 0 1 1800.54 1802.87 41.16 o 9 0 1 51.50 68.05 12.24 o 10 0 1 148.92 169.01 17.18 o -9 1 1 0.69 6.29 10.44 o -8 1 1 505.64 524.54 16.63 o -7 1 1 2777.19 2800.49 60.04 o -6 1 1 3027.22 2823.48 234.59 o -5 1 1 5059.96 5126.63 104.24 o -4 1 1 1238.25 1322.41 28.70 o -3 1 1 1091.20 1109.16 23.93 o -2 1 1 6513.93 6793.90 135.33 o -1 1 1 27486.13 23925.86 578.79 o 0 1 1 18018.31 17021.65 480.19 o 1 1 1 1569.36 1756.82 36.60 o 2 1 1 87.49 96.07 3.87 o 3 1 1 8246.11 8160.34 162.63 o 4 1 1 11013.44 11114.88 221.50 o 5 1 1 5694.59 5727.78 115.94 o 6 1 1 279.92 279.33 10.50 o 7 1 1 373.07 372.04 12.29 o 8 1 1 2039.40 2050.82 46.08 o 9 1 1 1591.86 1667.95 39.76 o 10 1 1 551.97 593.61 30.10 o -10 2 1 469.32 520.17 28.86 o -9 2 1 731.43 689.51 31.56 o -8 2 1 1073.15 1007.88 38.41 o -7 2 1 18.54 19.49 5.01 o -6 2 1 764.18 780.66 19.63 o -5 2 1 5905.01 6098.37 123.36 o -4 2 1 11776.79 12290.13 244.76 o -3 2 1 3708.87 3806.86 77.05 o -2 2 1 1522.41 1572.89 32.79 o -1 2 1 194.18 175.75 6.74 o 0 2 1 17078.98 16386.37 574.63 o 1 2 1 17673.92 17000.81 343.41 o 2 2 1 10620.42 10613.03 210.75 o 3 2 1 2885.44 2928.35 59.82 o 4 2 1 668.40 628.05 15.16 o 5 2 1 4003.79 4003.73 82.12 o 6 2 1 4524.59 4687.62 96.37 o 7 2 1 3355.45 3345.21 70.76 o 8 2 1 48.39 46.68 6.85 o 9 2 1 109.44 101.05 8.76 o -9 3 1 132.38 139.47 15.61 o -8 3 1 1335.96 1405.98 50.31 o -7 3 1 1352.53 1269.10 78.44 o -6 3 1 2616.65 2680.11 56.89 o -5 3 1 449.50 421.14 40.99 o -4 3 1 874.80 818.76 19.03 o -3 3 1 9148.22 8990.09 179.34 o -2 3 1 12032.13 11417.88 226.91 o -1 3 1 17076.09 16157.97 447.73 o 0 3 1 3912.66 4242.71 77.93 o 1 3 1 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