# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' krop97 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 370.75 _exptl_crystal_F_000 1880.00 _reflns_d_resolution_high 0.8107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 14.8881 _cell_length_b 16.3973 _cell_length_c 18.6471 _cell_angle_alpha 90.000 _cell_angle_beta 105.519 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13217.21 13084.69 6924.33 o 3 0 0 85174.75 98884.88 463.04 o 4 0 0 70001.11 77457.70 496.14 o 5 0 0 7.30 -45.58 247.34 o 6 0 0 1922.69 1805.54 202.28 o 7 0 0 9089.23 9333.96 272.61 o 8 0 0 2558.97 2289.43 214.84 o 9 0 0 9545.64 9551.20 309.94 o 10 0 0 18715.01 18700.62 611.73 o 11 0 0 28883.49 28028.56 512.99 o 12 0 0 91.79 -83.33 292.36 o 13 0 0 28757.51 31378.59 708.00 o 14 0 0 1185.73 1283.35 381.94 o 15 0 0 6.41 191.59 381.97 o 16 0 0 2.54 -146.91 427.74 o 17 0 0 133.18 -181.10 487.19 o 2 1 0 26652.46 31051.87 203.25 o 3 1 0 6026.63 6359.39 149.35 o 4 1 0 4923.43 4560.04 203.04 o 5 1 0 10847.98 11499.60 195.37 o 6 1 0 1153.17 1048.67 147.19 o 7 1 0 188.12 177.88 143.20 o 8 1 0 22.58 98.64 150.32 o 9 1 0 15508.57 15717.08 206.88 o 10 1 0 4937.48 4721.06 193.77 o 11 1 0 1518.69 1450.81 204.81 o 12 1 0 7254.59 6883.27 238.59 o 13 1 0 133.18 310.70 218.45 o 14 1 0 1637.90 1631.90 242.50 o 15 1 0 353.68 226.66 271.89 o 16 1 0 177.40 159.50 293.91 o 17 1 0 52.05 340.50 333.25 o 0 2 0 38360.25 1593.28 130.24 o 1 2 0 5963.33 6673.47 106.26 o 2 2 0 17.83 -18.50 64.23 o 3 2 0 25645.00 28929.39 248.40 o 4 2 0 34153.77 37282.35 294.96 o 5 2 0 352.99 234.59 97.56 o 6 2 0 4223.99 4814.67 159.55 o 7 2 0 2732.34 2402.65 147.88 o 8 2 0 1267.52 1076.92 141.96 o 9 2 0 27402.63 28330.90 393.44 o 10 2 0 1441.22 1236.83 167.91 o 11 2 0 11.92 -9.52 183.45 o 12 2 0 260.66 184.41 198.07 o 13 2 0 3180.46 2931.47 220.02 o 14 2 0 665.43 738.39 233.25 o 15 2 0 869.05 732.81 267.59 o 16 2 0 5.68 4.76 296.92 o 17 2 0 730.46 747.20 334.54 o 1 3 0 34481.63 38335.44 470.87 o 2 3 0 41299.21 47084.04 680.21 o 3 3 0 2251.10 2161.05 95.98 o 4 3 0 26358.55 28159.13 230.67 o 5 3 0 1020.04 924.46 95.92 o 6 3 0 2326.08 2094.70 131.25 o 7 3 0 2103.33 1905.19 136.69 o 8 3 0 5610.83 5136.22 171.91 o 9 3 0 5598.08 5144.58 183.48 o 10 3 0 924.84 756.41 167.32 o 11 3 0 8657.43 8415.42 374.53 o 12 3 0 6175.17 6127.88 233.76 o 13 3 0 1046.43 1157.13 227.30 o 14 3 0 2017.06 1925.58 240.20 o 15 3 0 4732.33 4567.89 271.64 o 16 3 0 491.46 685.19 295.65 o 17 3 0 466.45 441.58 403.99 o 0 4 0 33757.32 37791.59 275.39 o 1 4 0 10989.35 11772.66 251.05 o 2 4 0 2186.70 2023.65 166.66 o 3 4 0 5397.13 5470.53 175.24 o 4 4 0 5226.21 5405.24 109.70 o 5 4 0 42786.63 42502.46 392.89 o 6 4 0 11786.83 11579.66 141.17 o 7 4 0 1103.99 1293.59 127.32 o 8 4 0 19310.90 19053.86 299.45 o 9 4 0 9908.59 9487.63 211.45 o 10 4 0 432.63 227.16 165.38 o 11 4 0 108.73 34.89 186.37 o 12 4 0 58.10 149.88 203.32 o 13 4 0 41.42 330.16 218.26 o 14 4 0 1954.61 1891.43 252.04 o 15 4 0 1371.93 1295.46 270.78 o 16 4 0 6060.68 6909.48 366.80 o 17 4 0 77.13 275.74 404.23 o 1 5 0 37298.14 42065.81 362.30 o 2 5 0 33272.64 36895.18 279.76 o 3 5 0 21516.99 22659.01 253.48 o 4 5 0 9703.24 9710.04 147.20 o 5 5 0 168.61 156.94 88.12 o 6 5 0 22013.01 21940.35 219.16 o 7 5 0 29868.79 31173.45 366.88 o 8 5 0 9953.08 9845.49 297.99 o 9 5 0 896.73 595.71 153.29 o 10 5 0 104.06 114.62 167.20 o 11 5 0 6095.87 6227.88 213.48 o 12 5 0 2945.97 2711.49 261.44 o 13 5 0 184.38 268.10 221.12 o 14 5 0 9.89 -5.84 241.04 o 15 5 0 28.05 262.00 329.77 o 16 5 0 387.66 533.60 371.71 o 17 5 0 1338.34 1563.66 531.11 o 0 6 0 6508.91 6308.99 306.63 o 1 6 0 6189.85 6236.63 132.29 o 2 6 0 3675.15 3216.23 175.37 o 3 6 0 1557.96 1797.32 166.98 o 4 6 0 2343.90 2548.95 118.49 o 5 6 0 3031.88 2754.92 148.06 o 6 6 0 55.88 70.57 110.54 o 7 6 0 2.30 -15.11 108.20 o 8 6 0 9972.05 9599.95 171.61 o 9 6 0 7120.22 6936.33 358.46 o 10 6 0 4075.57 3822.08 179.06 o 11 6 0 9510.48 9252.36 293.70 o 12 6 0 4.89 -56.16 197.82 o 13 6 0 416.84 341.87 231.35 o 14 6 0 371.75 89.55 295.12 o 15 6 0 1318.26 1354.36 551.41 o 16 6 0 420.44 673.06 492.78 o 1 7 0 11439.47 11694.60 328.55 o 2 7 0 2589.83 2955.41 111.24 o 3 7 0 14912.74 14410.16 290.45 o 4 7 0 9704.91 9880.12 236.44 o 5 7 0 241.25 327.53 121.23 o 6 7 0 7958.17 7852.99 160.51 o 7 7 0 22949.47 23472.51 256.21 o 8 7 0 5684.98 5478.93 169.01 o 9 7 0 4674.11 4697.77 273.85 o 10 7 0 15570.11 15841.73 248.04 o 11 7 0 651.65 555.44 178.87 o 12 7 0 160.71 -24.21 207.28 o 13 7 0 12.70 -139.91 292.52 o 14 7 0 4025.33 3526.54 400.15 o 15 7 0 232.75 271.86 465.50 o 16 7 0 2811.93 2964.57 598.08 o 0 8 0 18584.29 19281.51 549.46 o 1 8 0 891.71 954.03 100.77 o 2 8 0 20015.96 21213.29 255.83 o 3 8 0 1212.58 1041.92 163.92 o 4 8 0 72.79 151.17 166.65 o 5 8 0 7025.06 7256.14 207.54 o 6 8 0 4059.76 4097.74 193.61 o 7 8 0 2189.84 1929.21 130.19 o 8 8 0 4064.53 3812.33 156.66 o 9 8 0 145.56 147.74 156.07 o 10 8 0 46.19 151.39 185.61 o 11 8 0 3436.14 2956.25 308.48 o 12 8 0 47.12 -187.50 311.67 o 13 8 0 1990.39 1888.60 327.14 o 14 8 0 933.11 441.87 380.55 o 15 8 0 709.45 1161.32 405.45 o 16 8 0 22.49 514.85 460.20 o 1 9 0 8280.25 7804.16 153.34 o 2 9 0 22780.24 22171.57 517.07 o 3 9 0 12543.25 12126.90 338.78 o 4 9 0 1733.21 1182.80 179.96 o 5 9 0 865.46 542.62 161.01 o 6 9 0 8035.13 7773.89 232.86 o 7 9 0 17615.13 16595.07 230.36 o 8 9 0 3719.36 3233.56 151.65 o 9 9 0 972.04 784.08 168.91 o 10 9 0 261.80 259.40 251.45 o 11 9 0 3010.02 3018.46 296.39 o 12 9 0 343.35 107.91 316.97 o 13 9 0 1.58 -51.17 361.75 o 14 9 0 717.22 754.07 392.20 o 15 9 0 79.21 217.68 425.14 o 0 10 0 16048.13 16249.94 372.75 o 1 10 0 61.17 62.92 111.75 o 2 10 0 3932.70 3705.91 130.60 o 3 10 0 5562.99 4843.40 382.04 o 4 10 0 2005.86 2115.66 236.17 o 5 10 0 33810.18 34747.97 654.69 o 6 10 0 12701.20 13453.71 285.94 o 7 10 0 894.96 820.29 193.19 o 8 10 0 9898.07 9518.61 322.64 o 9 10 0 2292.64 1961.18 221.39 o 10 10 0 549.52 456.17 254.80 o 11 10 0 146.29 168.50 315.54 o 12 10 0 67.38 111.70 327.38 o 13 10 0 1147.76 1002.31 376.87 o 14 10 0 6.04 26.29 386.50 o 15 10 0 732.39 962.30 447.14 o 1 11 0 9759.02 9392.25 242.73 o 2 11 0 12627.27 12074.23 219.76 o 3 11 0 205.27 167.77 122.81 o 4 11 0 5416.24 5198.33 230.01 o 5 11 0 20.74 36.65 117.68 o 6 11 0 2270.15 2096.92 198.38 o 7 11 0 89.94 74.81 215.04 o 8 11 0 3709.51 3670.48 319.94 o 9 11 0 4881.97 5103.26 267.05 o 10 11 0 96.26 28.95 265.62 o 11 11 0 5590.36 6008.90 299.36 o 12 11 0 1588.80 1600.28 351.96 o 13 11 0 142.11 29.54 398.79 o 14 11 0 498.44 553.02 422.14 o 0 12 0 29.28 -21.64 190.40 o 1 12 0 11102.03 11237.57 228.01 o 2 12 0 359.71 291.64 133.00 o 3 12 0 551.35 463.74 136.73 o 4 12 0 542.55 517.53 225.10 o 5 12 0 489.37 388.48 206.82 o 6 12 0 6.11 116.02 206.55 o 7 12 0 932.70 996.83 230.56 o 8 12 0 39.50 149.76 237.20 o 9 12 0 1223.77 1296.02 268.95 o 10 12 0 1835.37 1820.27 281.88 o 11 12 0 139.12 300.20 301.01 o 12 12 0 120.60 105.06 375.93 o 13 12 0 84.26 269.33 414.54 o 14 12 0 1250.33 1420.91 457.65 o 1 13 0 9346.93 9492.81 308.88 o 2 13 0 6862.40 6596.35 247.94 o 3 13 0 133.47 250.15 221.80 o 4 13 0 3144.68 3135.20 203.95 o 5 13 0 805.51 759.24 217.82 o 6 13 0 298.21 164.73 227.40 o 7 13 0 68.26 285.59 240.86 o 8 13 0 294.58 158.86 261.05 o 9 13 0 3432.56 3415.65 272.41 o 10 13 0 4.26 -11.08 296.13 o 11 13 0 2391.00 2415.23 327.81 o 12 13 0 1827.10 1494.15 403.12 o 13 13 0 18.10 261.04 434.20 o 0 14 0 24407.10 24187.67 420.62 o 1 14 0 6026.49 6488.93 268.74 o 2 14 0 2017.98 2008.07 234.12 o 3 14 0 9128.88 9495.49 300.39 o 4 14 0 4294.53 4173.55 305.37 o 5 14 0 683.24 365.48 228.93 o 6 14 0 335.36 417.20 269.42 o 7 14 0 2328.78 2045.39 259.84 o 8 14 0 134.96 46.38 276.95 o 9 14 0 1081.75 1259.70 296.49 o 10 14 0 6768.66 6738.46 325.89 o 11 14 0 2745.05 2845.04 337.77 o 12 14 0 804.44 990.58 380.74 o 1 15 0 395.29 323.31 354.47 o 2 15 0 441.23 362.66 259.97 o 3 15 0 73.10 226.88 221.52 o 4 15 0 186.45 250.59 233.01 o 5 15 0 81.52 30.31 247.54 o 6 15 0 223.16 599.02 269.82 o 7 15 0 848.48 798.55 274.33 o 8 15 0 79.06 234.49 304.49 o 9 15 0 301.18 134.30 324.52 o 10 15 0 240.64 118.68 342.45 o 11 15 0 22.51 282.12 362.77 o 0 16 0 7297.29 6540.70 568.78 o 1 16 0 2499.15 2886.30 361.42 o 2 16 0 0.40 -295.74 376.05 o 3 16 0 2418.30 2485.31 300.82 o 4 16 0 796.46 885.84 256.63 o 5 16 0 4.17 157.27 263.76 o 6 16 0 93.75 180.20 289.91 o 7 16 0 331.94 522.83 292.82 o 8 16 0 82.56 174.65 325.79 o 9 16 0 2397.21 2277.56 346.65 o 10 16 0 3361.52 3322.49 373.15 o 1 17 0 2989.86 2976.32 398.35 o 2 17 0 2846.75 2995.71 313.85 o 3 17 0 492.44 559.04 329.71 o 4 17 0 427.22 563.50 330.16 o 5 17 0 1001.09 1251.13 349.34 o 6 17 0 395.17 696.64 317.32 o 7 17 0 434.95 233.56 342.39 o 8 17 0 1188.07 983.95 362.61 o 9 17 0 2305.13 2267.02 380.05 o 0 18 0 240.68 643.79 654.56 o 1 18 0 322.75 566.26 439.84 o 2 18 0 182.62 183.26 485.32 o 3 18 0 70.30 10.15 358.22 o 4 18 0 891.46 1298.73 370.09 o 5 18 0 4473.76 4872.15 382.80 o 6 18 0 1662.68 2349.96 400.23 o 7 18 0 197.58 376.47 416.88 o 8 18 0 2081.55 2278.84 452.61 o 1 19 0 1364.58 1525.51 480.14 o 2 19 0 1238.81 938.16 494.34 o 3 19 0 1344.56 1690.62 519.30 o 4 19 0 484.06 518.03 557.31 o 5 19 0 251.91 709.55 422.11 o 6 19 0 419.97 351.09 449.02 o 0 20 0 4.68 -351.10 813.58 o 1 20 0 0.15 -308.36 540.73 o 2 20 0 467.22 300.48 556.44 o -17 1 1 205.91 404.32 330.14 o -16 1 1 1132.20 1271.03 296.73 o -15 1 1 2.28 -4.74 258.50 o -14 1 1 14.61 56.32 242.76 o -13 1 1 514.84 457.39 218.54 o -12 1 1 18750.48 19234.24 376.61 o -11 1 1 4271.67 4387.33 202.19 o -10 1 1 151.15 179.25 160.66 o -9 1 1 10772.05 10387.04 168.77 o -8 1 1 51497.45 50566.12 629.34 o -7 1 1 4967.29 4678.87 171.20 o -6 1 1 12567.89 12704.53 176.19 o -5 1 1 60.07 22.69 115.57 o -4 1 1 667.91 618.72 103.33 o -3 1 1 37644.04 42093.12 185.47 o -2 1 1 1546.08 1306.28 416.32 o 1 1 1 122157.13 130769.76 12601.92 o 2 1 1 1054.97 1156.72 67.81 o 3 1 1 15070.00 16172.19 333.01 o 4 1 1 16320.95 17102.99 217.34 o 5 1 1 51093.40 55614.03 733.30 o 6 1 1 64.64 121.93 154.58 o 7 1 1 1170.42 931.90 145.28 o 8 1 1 5161.67 4859.95 178.77 o 9 1 1 7564.04 7223.20 207.55 o 10 1 1 2527.78 2450.17 176.60 o 11 1 1 6471.20 5682.77 217.34 o 12 1 1 17744.99 17674.45 327.38 o 13 1 1 31.49 294.15 222.61 o 14 1 1 5200.15 5564.93 326.17 o 15 1 1 1074.76 1299.79 273.28 o 16 1 1 289.70 168.70 308.78 o 17 1 1 20.31 83.99 341.26 o -17 2 1 69.54 0.63 328.06 o -16 2 1 478.13 569.95 290.48 o -15 2 1 469.51 322.63 263.13 o -14 2 1 300.60 305.22 233.51 o -13 2 1 1430.84 1042.15 214.23 o -12 2 1 8.98 -197.80 197.80 o -11 2 1 5140.37 5246.95 210.54 o -10 2 1 10190.53 9972.74 292.30 o -9 2 1 4037.75 3838.53 169.57 o -8 2 1 24003.38 24948.93 280.90 o -7 2 1 6258.93 6047.63 123.12 o -6 2 1 4979.97 5412.24 115.40 o -5 2 1 5327.39 5249.40 123.15 o -4 2 1 6858.50 7318.45 131.82 o -3 2 1 39530.18 45523.97 810.86 o -2 2 1 18109.64 20479.11 213.35 o -1 2 1 4331.62 4753.56 944.32 o 0 2 1 17982.51 17537.45 5531.92 o 1 2 1 2093.68 2666.55 107.87 o 2 2 1 50.80 10.90 79.41 o 3 2 1 29348.46 32656.19 203.47 o 4 2 1 9386.05 9583.87 187.73 o 5 2 1 12746.18 13486.32 206.01 o 6 2 1 1271.24 1020.48 141.61 o 7 2 1 379.91 368.77 137.70 o 8 2 1 9266.58 9784.13 212.96 o 9 2 1 59.88 173.50 155.35 o 10 2 1 7571.61 6919.78 216.24 o 11 2 1 4725.82 4997.70 214.95 o 12 2 1 1022.27 823.93 205.82 o 13 2 1 4783.06 5016.71 287.48 o 14 2 1 1347.85 1235.44 248.82 o 15 2 1 105.59 48.94 274.22 o 16 2 1 1160.14 1181.88 307.20 o 17 2 1 43.46 36.97 343.39 o -17 3 1 1577.91 2050.26 385.08 o -16 3 1 1909.32 2141.60 284.08 o -15 3 1 347.87 600.46 265.72 o -14 3 1 1246.66 1295.17 246.19 o -13 3 1 338.81 250.29 211.74 o -12 3 1 2519.14 2358.02 192.84 o -11 3 1 6.54 -98.08 184.70 o -10 3 1 1558.92 1212.26 172.10 o -9 3 1 396.52 354.59 152.07 o -8 3 1 16041.71 16770.01 211.93 o -7 3 1 6717.53 5962.10 139.19 o -6 3 1 33.83 -35.40 97.35 o -5 3 1 522.30 399.59 97.57 o -4 3 1 16908.20 18234.55 158.20 o -3 3 1 8589.35 9300.91 101.93 o -2 3 1 11989.99 14031.44 163.22 o -1 3 1 1230.30 1371.89 102.90 o 0 3 1 4725.40 4905.20 108.74 o 1 3 1 1431.93 1689.78 84.29 o 2 3 1 20008.47 21185.74 515.00 o 3 3 1 13012.28 13486.25 275.15 o 4 3 1 1243.21 1211.91 131.47 o 5 3 1 4536.49 4517.74 152.10 o 6 3 1 1228.00 744.22 130.45 o 7 3 1 4804.87 4459.65 158.85 o 8 3 1 3488.86 3140.76 205.13 o 9 3 1 45.49 19.99 157.03 o 10 3 1 10808.50 10547.28 246.09 o 11 3 1 500.95 579.84 180.20 o 12 3 1 2363.12 2171.16 201.85 o 13 3 1 269.20 221.00 224.36 o 14 3 1 1015.95 719.79 246.64 o 15 3 1 196.81 91.70 280.66 o 16 3 1 776.49 634.28 306.92 o 17 3 1 1157.74 1387.74 339.77 o -17 4 1 1.64 322.50 400.46 o -16 4 1 0.09 -7.17 366.27 o -15 4 1 700.68 603.50 262.35 o -14 4 1 2032.23 1726.54 237.80 o -13 4 1 1312.91 1238.65 216.37 o -12 4 1 0.06 -64.94 195.96 o -11 4 1 1106.33 970.79 240.16 o -10 4 1 10153.97 10048.36 325.83 o -9 4 1 3186.69 3037.97 154.95 o -8 4 1 2632.08 2811.30 241.81 o -7 4 1 5094.44 5058.21 120.54 o -6 4 1 670.31 612.06 89.91 o -5 4 1 909.06 1050.24 96.37 o -4 4 1 6.43 -40.62 91.13 o -3 4 1 2179.65 2070.90 94.67 o -2 4 1 12648.76 13763.67 189.73 o -1 4 1 12446.89 12982.48 173.19 o 0 4 1 59138.28 67165.36 505.61 o 1 4 1 21401.27 23470.76 810.15 o 2 4 1 5729.23 6469.12 194.16 o 3 4 1 79843.41 88545.93 1716.45 o 4 4 1 20433.31 21125.63 207.94 o 5 4 1 493.64 407.14 118.20 o 6 4 1 3486.86 3697.82 137.83 o 7 4 1 389.86 314.64 135.14 o 8 4 1 235.03 151.48 148.40 o 9 4 1 3846.97 3745.77 215.66 o 10 4 1 5250.15 4947.25 232.02 o 11 4 1 1618.68 1431.40 185.76 o 12 4 1 1827.41 1494.69 203.49 o 13 4 1 2490.31 2917.62 226.33 o 14 4 1 2633.59 2283.40 254.71 o 15 4 1 386.00 299.82 277.97 o 16 4 1 802.99 1143.95 320.24 o 17 4 1 91.44 125.73 426.70 o -17 5 1 5324.51 5868.62 523.23 o -16 5 1 1947.95 2114.06 368.66 o -15 5 1 1984.04 2311.76 325.32 o -14 5 1 2367.71 2517.98 235.08 o -13 5 1 24.83 83.07 216.93 o -12 5 1 32.19 1.77 193.52 o -11 5 1 1691.17 1461.97 178.13 o -10 5 1 4314.11 4209.82 180.41 o -9 5 1 3431.62 3088.44 137.32 o -8 5 1 2814.78 2634.65 108.76 o -7 5 1 33408.14 34817.73 357.67 o -6 5 1 10653.44 10322.13 145.68 o -5 5 1 14870.60 16347.29 178.96 o -4 5 1 72146.89 81669.27 670.66 o -3 5 1 39264.66 40637.16 298.44 o -2 5 1 3115.23 3264.60 167.22 o -1 5 1 862.65 858.88 95.72 o 0 5 1 769.86 611.53 113.06 o 1 5 1 11.00 -28.34 143.26 o 2 5 1 972.28 758.31 112.07 o 3 5 1 19118.40 20893.39 198.45 o 4 5 1 20733.75 20666.43 204.16 o 5 5 1 1613.30 1603.39 122.82 o 6 5 1 33030.08 34569.18 369.43 o 7 5 1 19997.67 20284.89 342.78 o 8 5 1 2002.43 2066.67 150.73 o 9 5 1 3147.48 3223.91 169.17 o 10 5 1 6618.38 6289.88 205.88 o 11 5 1 81.58 96.46 190.07 o 12 5 1 72.83 115.36 198.80 o 13 5 1 539.02 596.56 228.11 o 14 5 1 371.09 431.46 257.62 o 15 5 1 3944.14 4734.48 454.49 o 16 5 1 18.66 20.99 373.13 o -17 6 1 29.02 -54.81 549.72 o -16 6 1 2750.92 3133.82 530.13 o -15 6 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