Acta Cryst. (2008). E64, m851-m852  [ doi:10.1107/S1600536808015687 ]

Bis(5-chlorosalicylato-O)bis(1,10-phenanthroline-²N,N')cadmium(II)

D. Wen, J. Xie and X. Jiang

Online 7 June 2008

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.007 Å
• R factor = 0.045
• wR factor = 0.087
• Data-to-parameter ratio = 16.7

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT230_ALERT_2_C Hirshfeld Test Diff for    Cl1    --  C5      ..       5.36 su   
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         O1     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C5     
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT850_ALERT_4_C Check Flack Parameter Exact Value 0.00 and su ..       0.19      

Alert level G
REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is
            correct. If it is not, please give the correct count in the
            _publ_section_exptl_refinement section of the submitted CIF.
           From the CIF: _diffrn_reflns_theta_max           27.48
           From the CIF: _reflns_number_total               7696
           Count of symmetry unique reflns         4306
           Completeness (_total/calc)            178.73%
           TEST3: Check Friedels for noncentro structure
           Estimate of Friedel pairs measured      3390
           Fraction of Friedel pairs measured     0.787
           Are heavy atom types Z>Si present        yes
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   3 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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