# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Iodo sulfenamida T(min)=0.4380 T(max)=0.5162 R-3' _shelx_refln_list_code 4 _shelx_F_calc_maximum 464.78 _exptl_crystal_F_000 3240.00 _reflns_d_resolution_high 0.7441 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' _cell_length_a 28.6221 _cell_length_b 28.6221 _cell_length_c 8.4062 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 216021.95 684.15 613.30 o 0 3 0 32505.87 20757.09 1626.46 o -2 4 0 4275.38 7544.78 383.14 o -4 5 0 6249.67 6859.19 176.59 o -1 5 0 1186.10 1396.20 95.35 o -3 6 0 35714.30 48476.60 2094.61 o 0 6 0 51093.98 65427.92 2810.18 o -5 7 0 43612.17 44465.56 2730.03 o -2 7 0 78601.91 109526.73 6683.91 o -7 8 0 25515.13 22898.97 530.72 o -1 8 0 7976.69 6599.67 354.38 o -6 9 0 89889.25 111370.69 3902.21 o 0 9 0 3266.66 4693.26 210.61 o -8 10 0 1490.99 1472.66 100.18 o -5 10 0 12883.90 9263.19 551.32 o -2 10 0 3999.51 4890.83 297.49 o -7 11 0 106.69 1074.68 121.13 o -9 12 0 9931.25 7988.86 328.88 o -6 12 0 17591.13 17579.46 554.46 o -3 12 0 469.85 439.83 196.37 o -8 13 0 239.92 426.39 47.26 o -5 13 0 55615.09 65622.20 3995.17 o -10 14 0 24371.26 22640.60 566.05 o -4 14 0 8798.42 11922.51 278.98 o -9 15 0 4095.73 4198.50 124.67 o -6 15 0 7772.80 6511.43 186.14 o -3 15 0 25411.61 29141.27 726.56 o -14 16 0 37501.36 38340.53 1648.77 o -11 16 0 41151.89 48257.64 2141.99 o -8 16 0 38718.48 43857.69 1538.37 o -5 16 0 426.30 1113.71 51.44 o -2 16 0 11587.46 11122.70 260.94 o -16 17 0 10602.82 11342.52 343.33 o -13 17 0 12952.23 13136.30 386.87 o -10 17 0 79314.02 100285.92 6096.54 o -7 17 0 37950.77 39282.62 1405.58 o -4 17 0 53.41 -5.42 20.84 o -1 17 0 10460.23 11315.35 331.03 o -15 18 0 2098.30 2473.49 111.98 o -12 18 0 5044.73 4527.18 376.81 o -6 18 0 12224.77 11731.41 354.21 o -3 18 0 491.33 291.56 97.65 o 0 18 0 1349.77 1081.00 67.89 o -17 19 0 18294.33 18075.53 456.87 o -14 19 0 30536.16 30903.04 627.93 o -11 19 0 31876.74 31318.71 780.85 o -8 19 0 9193.77 9241.36 387.70 o -5 19 0 28846.50 29542.12 1224.28 o -2 19 0 10389.05 8891.68 379.02 o -19 20 0 15418.95 16282.79 569.36 o -16 20 0 15958.72 16650.35 452.62 o -13 20 0 40500.25 41040.65 942.96 o -10 20 0 4191.23 3795.74 359.39 o -7 20 0 9915.13 9799.97 347.22 o -4 20 0 16377.58 17360.43 802.19 o -1 20 0 19291.01 18632.04 1068.02 o -18 21 0 6721.88 7428.35 223.63 o -15 21 0 29030.13 29890.36 728.32 o -12 21 0 1151.33 1607.79 71.56 o -9 21 0 1286.91 797.37 77.19 o -6 21 0 2425.42 3236.70 169.86 o -3 21 0 53539.43 55360.01 2381.74 o 0 21 0 670.03 674.45 79.73 o -20 22 0 1553.38 1675.09 89.09 o -17 22 0 4984.31 4428.58 131.43 o -14 22 0 7834.20 6405.20 142.36 o -11 22 0 36569.13 36747.37 916.25 o -8 22 0 1781.60 2408.97 140.27 o -5 22 0 3953.38 4089.33 175.74 o -2 22 0 75.71 34.37 50.50 o -22 23 0 4818.53 3861.98 117.85 o -19 23 0 5850.48 6248.52 202.40 o -16 23 0 8680.21 8155.00 244.85 o -13 23 0 21188.92 21243.38 492.04 o -10 23 0 41821.25 41087.14 1023.96 o -7 23 0 10124.74 9058.29 331.00 o -4 23 0 27039.43 28905.24 1020.27 o -1 23 0 3846.66 4080.91 122.83 o -21 24 0 3857.38 3477.03 106.42 o -18 24 0 6772.79 6881.90 165.25 o -15 24 0 675.98 777.79 67.09 o -12 24 0 48234.05 51410.64 1399.17 o -9 24 0 14470.27 13268.57 371.41 o -6 24 0 17517.00 18185.32 646.03 o -3 24 0 449.12 125.83 59.43 o 0 24 0 25996.65 26847.48 747.08 o -23 25 0 15070.97 15662.09 438.82 o -20 25 0 6.88 -33.41 47.71 o -17 25 0 4293.19 4082.56 154.71 o -14 25 0 6375.30 5844.13 171.60 o -11 25 0 37890.97 38642.98 1056.03 o -8 25 0 1160.46 977.89 55.27 o -5 25 0 9151.43 9114.14 360.70 o -2 25 0 1072.88 1073.67 63.05 o -25 26 0 17800.67 17447.72 631.79 o -22 26 0 6310.29 6105.78 197.85 o -19 26 0 4531.64 4715.90 138.96 o -16 26 0 762.70 879.76 44.20 o -13 26 0 27949.30 28410.52 783.65 o -10 26 0 32031.73 32942.92 1009.15 o -7 26 0 2890.80 2712.68 99.85 o -4 26 0 6870.95 5934.79 195.06 o -1 26 0 18320.67 17839.36 640.13 o -24 27 0 17438.11 16550.63 598.18 o -21 27 0 10.16 -53.16 53.16 o -18 27 0 3865.10 3419.52 105.33 o -15 27 0 15073.47 15100.20 420.80 o -12 27 0 27912.59 29694.67 912.38 o -9 27 0 1165.19 782.00 61.37 o -6 27 0 2258.46 1938.23 76.94 o -3 27 0 1937.75 2139.39 93.60 o 0 27 0 32841.42 33329.20 1559.41 o -26 28 0 5673.73 5625.17 282.28 o -23 28 0 5052.82 4352.15 168.84 o -20 28 0 4680.99 5015.56 192.52 o -17 28 0 2394.34 2689.94 87.72 o -14 28 0 17664.42 17585.90 552.73 o -11 28 0 5176.59 4961.59 194.70 o -8 28 0 3183.92 3031.50 120.87 o -5 28 0 692.52 739.16 54.11 o -2 28 0 7457.88 7421.54 358.31 o -28 29 0 2094.59 1971.14 135.85 o -25 29 0 1187.65 996.62 83.50 o -22 29 0 3776.19 3648.39 143.94 o -19 29 0 6389.51 5643.00 211.00 o -16 29 0 6085.66 5400.18 203.83 o -13 29 0 4668.63 4655.51 178.07 o -10 29 0 3844.10 3868.84 152.14 o -7 29 0 1089.40 1446.91 73.89 o -4 29 0 1520.98 1617.60 182.60 o -1 29 0 476.62 461.35 110.21 o -27 30 0 310.75 183.14 57.48 o -24 30 0 2312.46 2156.21 104.07 o -21 30 0 5424.19 5371.56 228.24 o -18 30 0 3510.47 3082.46 145.76 o -15 30 0 122.96 -76.13 76.13 o -12 30 0 10.21 -5.74 66.91 o -9 30 0 12266.89 12891.31 529.31 o -6 30 0 4491.69 4750.48 204.55 o -3 30 0 1010.15 667.81 67.21 o 0 30 0 223.22 238.52 62.20 o -29 31 0 587.60 682.15 96.01 o -26 31 0 121.25 -1.63 97.02 o -23 31 0 2798.22 2771.08 126.44 o -20 31 0 5229.87 5270.48 260.26 o -17 31 0 89.74 117.04 79.59 o -14 31 0 5148.05 5128.40 220.51 o -11 31 0 1461.49 1625.19 86.10 o -8 31 0 3335.37 3237.22 149.84 o -5 31 0 4.11 3.80 48.71 o -2 31 0 1094.39 1022.66 167.97 o -31 32 0 89.22 281.96 68.23 o -28 32 0 2.62 30.80 91.87 o -25 32 0 4529.76 4327.00 323.67 o -22 32 0 416.66 529.67 68.56 o -19 32 0 2304.98 2475.64 148.68 o -16 32 0 3.72 -11.24 67.10 o -13 32 0 5098.21 4861.68 243.03 o -10 32 0 207.37 480.36 57.45 o -7 32 0 21.40 0.39 68.77 o -4 32 0 30.14 94.13 85.35 o -1 32 0 46.17 405.82 79.38 o -30 33 0 1144.50 692.54 120.93 o -27 33 0 1485.12 1430.83 154.33 o -24 33 0 1005.15 1036.14 86.58 o -21 33 0 48.72 118.00 99.64 o -18 33 0 26.79 60.09 65.63 o -15 33 0 2883.67 3180.75 240.14 o -12 33 0 228.61 427.54 71.08 o -9 33 0 602.60 591.11 73.36 o -6 33 0 338.98 66.60 71.47 o -3 33 0 3164.76 3258.30 268.63 o 0 33 0 52.11 133.89 74.81 o -32 34 0 494.83 526.34 162.72 o -29 34 0 676.26 728.25 105.51 o -26 34 0 1574.16 1925.03 282.87 o -23 34 0 696.01 576.23 86.06 o -20 34 0 174.59 118.27 79.57 o -17 34 0 1211.60 1294.90 99.80 o -14 34 0 5019.99 4568.92 344.50 o -11 34 0 880.36 767.28 70.80 o -8 34 0 451.10 566.95 75.97 o -5 34 0 855.57 1167.22 193.12 o -2 34 0 221.13 465.86 86.51 o -31 35 0 124.21 -102.89 102.89 o -28 35 0 2088.64 2001.59 248.93 o -25 35 0 107.63 219.38 84.14 o -22 35 0 2207.34 1944.15 165.17 o -19 35 0 397.48 439.27 92.75 o -16 35 0 3288.68 3829.88 312.57 o -13 35 0 295.70 267.68 108.23 o -10 35 0 1954.43 1927.84 192.37 o -7 35 0 163.98 214.05 165.66 o -4 35 0 1309.84 1817.16 297.31 o -27 36 0 176.58 101.58 122.89 o -24 36 0 705.98 815.55 128.02 o -21 36 0 906.41 1093.81 127.06 o -18 36 0 1250.87 1053.08 114.34 o -15 36 0 160.20 49.45 137.78 o -12 36 0 1028.08 1137.08 157.67 o -9 36 0 1141.25 1567.50 363.16 o -26 37 0 729.98 756.34 209.50 o -23 37 0 5285.27 5573.40 1241.83 o -20 37 0 422.38 471.94 75.82 o -17 37 0 813.29 1059.85 117.49 o -14 37 0 154.69 -15.85 122.13 o -11 37 0 5544.93 5665.42 1260.62 o -22 38 0 3441.95 2753.02 626.95 o -19 38 0 916.52 854.24 230.61 o -16 38 0 12.25 -118.29 118.29 o -1 1 1 2174.42 2867.82 84.13 o -3 2 1 70401.51 109650.51 3847.72 o 0 2 1 38934.92 46406.34 1505.33 o -5 3 1 75328.36 108638.42 6867.25 o -2 3 1 124.11 337.12 22.47 o 1 3 1 42470.60 54426.50 1170.85 o -1 4 1 169.71 358.97 55.42 o 2 4 1 76085.20 101541.13 3074.52 o -3 5 1 8425.18 6260.99 729.49 o 0 5 1 16609.76 19364.49 394.76 o -11 6 1 36006.79 38168.92 1160.94 o -2 6 1 9917.35 5173.46 185.58 o 1 6 1 2560.23 4893.34 162.34 o -13 7 1 2175.28 2815.74 239.09 o -7 7 1 28522.00 38068.73 1038.62 o 2 7 1 35528.39 36632.60 1037.12 o 5 7 1 2504.08 2521.70 154.32 o -12 8 1 16392.93 16584.86 641.30 o -9 8 1 37041.28 41778.96 1472.87 o -6 8 1 40645.45 35369.36 2150.18 o 0 8 1 163.17 634.47 80.74 o 3 8 1 52737.59 57528.74 1325.10 o 6 8 1 28272.54 29571.38 912.83 o -14 9 1 18823.38 17267.23 1074.94 o -11 9 1 39024.70 42396.00 2145.24 o -8 9 1 5689.55 6497.64 136.19 o 1 9 1 454.97 948.53 75.17 o 4 9 1 30754.96 36350.70 781.34 o -19 10 1 53002.09 53224.40 1757.37 o -13 10 1 2039.32 2045.81 479.96 o -10 10 1 675.35 2069.63 123.20 o -7 10 1 33845.89 29976.54 1305.18 o -1 10 1 11767.17 11112.61 294.46 o 2 10 1 39813.61 49181.40 995.01 o 5 10 1 42627.02 49118.13 1057.54 o 8 10 1 17189.32 12914.58 326.32 o -21 11 1 16517.50 15409.16 361.40 o -15 11 1 11816.57 10548.66 476.30 o -12 11 1 5851.56 10420.03 327.20 o -9 11 1 52367.85 74719.00 2266.56 o -3 11 1 20281.11 18248.41 422.49 o 0 11 1 17694.33 23273.44 448.81 o 3 11 1 2459.17 2481.81 121.79 o 6 11 1 38274.19 40816.93 1248.33 o 9 11 1 23894.94 23754.09 515.12 o -23 12 1 3010.96 2874.22 74.80 o -20 12 1 41173.96 41657.93 1136.24 o -17 12 1 28616.86 29618.14 1410.02 o -14 12 1 885.24 1237.72 74.19 o -11 12 1 2181.94 4829.74 182.04 o -8 12 1 14688.51 14337.43 660.05 o -5 12 1 18505.21 17050.05 737.14 o -2 12 1 689.93 1193.80 34.22 o 1 12 1 63.66 565.40 44.78 o 4 12 1 28660.81 37028.16 942.18 o 7 12 1 13276.47 13850.26 347.19 o 10 12 1 277.05 300.58 21.14 o -25 13 1 1046.27 1353.45 52.58 o -22 13 1 3202.08 3008.33 130.52 o -19 13 1 6585.16 7419.26 235.64 o -16 13 1 19.77 94.48 39.29 o -13 13 1 30989.35 36222.50 834.34 o -10 13 1 56546.59 76099.08 2075.51 o -7 13 1 4735.09 6106.35 268.47 o -4 13 1 11570.87 16159.91 331.42 o -1 13 1 21938.38 24142.71 467.59 o 2 13 1 3206.04 2640.28 111.36 o 5 13 1 6513.41 5702.57 330.83 o 8 13 1 2330.32 1697.70 62.86 o 11 13 1 305.50 559.29 49.99 o -27 14 1 932.78 960.52 64.05 o -24 14 1 28432.86 28315.04 867.11 o -21 14 1 8004.41 7659.98 242.85 o -18 14 1 21248.01 20639.68 637.31 o -15 14 1 1696.25 2101.06 87.07 o -12 14 1 30073.92 34091.24 692.36 o -9 14 1 3076.15 3117.66 205.68 o -6 14 1 46150.41 49481.94 1735.85 o -3 14 1 18424.53 16468.35 337.36 o 0 14 1 6598.45 7983.69 180.99 o 3 14 1 64302.48 75325.43 3228.22 o 6 14 1 33426.01 32470.98 812.39 o 9 14 1 36971.26 36870.05 1013.61 o 12 14 1 3582.10 3578.52 120.63 o -29 15 1 4069.01 4428.36 196.00 o -26 15 1 3.91 351.54 58.27 o -23 15 1 6725.01 6386.99 205.50 o -20 15 1 28219.88 27967.11 862.08 o -17 15 1 25239.47 25777.01 792.20 o -14 15 1 2636.29 2464.45 136.89 o -11 15 1 1030.55 1696.00 99.13 o -5 15 1 20676.65 16994.09 426.34 o -2 15 1 20109.04 20399.22 395.25 o 1 15 1 387.88 374.60 42.92 o 4 15 1 50514.18 52837.23 1850.11 o 7 15 1 11602.80 11494.74 375.04 o 10 15 1 13170.55 12582.82 350.25 o 13 15 1 1877.92 2022.31 100.60 o -31 16 1 3392.93 3936.43 171.29 o -28 16 1 166.95 17.25 52.32 o -25 16 1 1228.75 1099.90 66.89 o -22 16 1 6323.87 5912.74 199.42 o -19 16 1 42300.87 44176.52 1348.16 o -16 16 1 10253.72 11502.02 492.26 o -13 16 1 774.68 805.09 102.44 o -10 16 1 17966.56 15275.47 470.74 o -4 16 1 15846.43 14267.12 291.11 o -1 16 1 9903.36 10474.37 223.23 o 2 16 1 19146.79 19867.98 404.82 o 5 16 1 28836.54 28339.29 659.06 o 8 16 1 15989.03 15535.79 391.86 o 11 16 1 1843.12 1830.28 90.30 o 14 16 1 572.59 663.99 50.17 o -33 17 1 3104.05 3377.98 213.52 o -30 17 1 5656.85 5699.10 251.15 o -27 17 1 1074.23 925.88 58.78 o -24 17 1 2696.12 2619.31 134.77 o -21 17 1 45480.33 47478.98 1301.06 o -18 17 1 12124.34 11401.55 359.01 o -15 17 1 15950.93 15492.52 549.62 o -12 17 1 49.65 209.25 33.37 o -6 17 1 33406.37 31865.38 976.51 o -3 17 1 7023.29 7701.18 394.56 o 0 17 1 35796.91 37243.12 856.78 o 3 17 1 36002.35 38724.57 1061.26 o 6 17 1 14030.96 13640.47 379.28 o 9 17 1 1745.79 1704.71 158.36 o 12 17 1 8493.13 7370.91 274.31 o 15 17 1 672.76 856.60 68.77 o -35 18 1 7657.61 7427.26 568.84 o -32 18 1 1703.34 1657.43 88.94 o -29 18 1 413.74 538.47 90.33 o -26 18 1 70.10 -54.96 54.96 o -23 18 1 45571.25 47381.15 1290.93 o -20 18 1 32322.99 33135.22 1176.64 o -17 18 1 262.30 -9.72 67.19 o -14 18 1 37877.14 38643.50 892.19 o -11 18 1 10090.29 10367.84 247.52 o -5 18 1 1024.92 1219.81 83.10 o -2 18 1 49649.96 51992.57 1804.48 o 1 18 1 31.46 270.88 129.50 o 4 18 1 47433.10 52612.52 4686.01 o 7 18 1 191.33 278.52 47.12 o 10 18 1 31431.14 31854.00 925.48 o 13 18 1 1705.01 1237.67 83.58 o 16 18 1 2748.85 2958.03 214.79 o -37 19 1 1153.53 1861.58 335.24 o -34 19 1 7266.93 6991.47 416.97 o -31 19 1 495.54 403.74 47.64 o -28 19 1 1393.56 1243.17 105.62 o -25 19 1 312.52 137.40 88.27 o -22 19 1 22908.27 23152.96 640.94 o -19 19 1 15729.09 16070.31 499.77 o -13 19 1 6202.36 5551.06 143.28 o -10 19 1 39038.43 40993.25 1677.41 o -7 19 1 30294.23 29781.39 812.00 o -4 19 1 39856.26 45087.34 3909.34 o -1 19 1 16260.58 15058.62 378.30 o 2 19 1 6081.04 6199.26 194.84 o 5 19 1 7695.55 7909.85 298.86 o 8 19 1 5475.33 5438.01 158.38 o 11 19 1 16884.88 16291.70 679.19 o 14 19 1 87.52 180.26 84.66 o 17 19 1 348.32 638.48 90.91 o -36 20 1 3040.19 3575.85 338.69 o -33 20 1 921.58 1035.21 74.15 o -30 20 1 902.44 976.73 77.87 o -27 20 1 32180.52 30510.26 1084.29 o -24 20 1 8640.59 7563.32 260.27 o -21 20 1 4324.95 4013.42 134.11 o -18 20 1 5868.04 5167.95 337.07 o -15 20 1 49604.98 50434.32 1773.76 o -12 20 1 1352.34 1861.57 89.05 o -9 20 1 49624.91 53056.73 1878.00 o -6 20 1 2349.19 1986.86 84.86 o 0 20 1 11209.55 9873.58 290.88 o 3 20 1 40914.09 42610.55 1302.16 o 6 20 1 60.41 165.05 56.96 o 9 20 1 12152.05 12193.86 443.99 o 12 20 1 3127.99 3320.44 175.02 o 15 20 1 3151.40 2809.62 224.42 o 18 20 1 360.56 493.93 165.20 o -38 21 1 254.63 631.07 191.19 o -35 21 1 872.75 990.41 101.66 o -32 21 1 4100.35 4301.79 228.29 o -29 21 1 15930.93 16160.33 827.56 o -26 21 1 537.65 605.81 58.58 o -23 21 1 7396.89 5769.24 167.10 o -20 21 1 280.41 201.71 41.77 o -14 21 1 9280.75 7450.55 191.36 o -11 21 1 3300.02 3254.40 114.93 o -8 21 1 2375.89 2279.26 61.93 o -5 21 1 57833.04 55373.17 2391.17 o -2 21 1 10894.06 10190.12 318.43 o 1 21 1 5039.87 5208.53 131.65 o 4 21 1 1812.61 1499.80 109.53 o 7 21 1 2932.79 3323.18 131.72 o 10 21 1 10605.04 10774.95 514.19 o 13 21 1 149.06 18.29 113.29 o 16 21 1 197.99 303.60 102.02 o -37 22 1 61.46 -126.10 126.10 o -34 22 1 159.32 -21.90 68.26 o -31 22 1 7230.79 8507.08 410.71 o -28 22 1 29000.49 28456.48 1173.81 o -25 22 1 304.15 281.27 39.28 o -22 22 1 526.73 360.12 64.07 o -19 22 1 23839.72 23215.09 827.17 o -13 22 1 356.17 315.82 51.90 o -10 22 1 177.38 327.12 48.45 o -7 22 1 15208.95 14754.00 346.22 o -4 22 1 36746.36 35338.95 1535.26 o -1 22 1 30560.27 30763.06 844.04 o 2 22 1 2161.11 2109.89 71.74 o 5 22 1 449.05 591.46 54.53 o 8 22 1 7934.51 8257.87 343.24 o 11 22 1 4980.16 4976.86 300.86 o 14 22 1 714.20 575.17 83.39 o -36 23 1 55.51 233.65 63.69 o -33 23 1 2880.86 2982.83 163.43 o -30 23 1 21255.04 22138.88 1044.49 o -27 23 1 5378.93 4978.37 221.05 o -24 23 1 15.68 -37.56 37.56 o -21 23 1 2310.40 2504.70 90.20 o -18 23 1 42487.91 43329.84 1530.42 o -15 23 1 7881.23 6749.70 158.55 o -12 23 1 89.38 454.40 68.69 o -9 23 1 32.75 51.65 41.51 o -6 23 1 54221.22 56724.05 2444.09 o -3 23 1 42627.18 44642.36 1574.12 o 0 23 1 49.36 52.37 51.44 o 3 23 1 1874.02 1522.00 89.83 o 6 23 1 3598.21 4278.60 189.90 o 9 23 1 5678.26 5352.13 322.74 o 12 23 1 331.37 398.61 85.18 o -35 24 1 63.20 76.86 60.90 o -32 24 1 3391.59 4130.01 218.32 o -29 24 1 584.16 769.92 121.25 o -26 24 1 690.83 567.59 52.51 o -23 24 1 424.55 382.50 40.18 o -20 24 1 16215.70 16255.70 504.11 o -17 24 1 23995.79 23089.51 826.92 o 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