Acta Cryst. (2008). E64, m1187  [ doi:10.1107/S1600536808023799 ]

Triclinic modification of di-n-butylbis(2-hydroxybenzoato-²O¹,O^1')tin(IV)

R. Reisi, M. Misran, K. M. Lo and S. W. Ng

Online 20 August 2008

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.014 Å
• R factor = 0.060
• wR factor = 0.189
• Data-to-parameter ratio = 19.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.62 Ratio
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Sn1    --  O2      ..       5.29 su   
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         O5     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C14     
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang ...         14      
PLAT153_ALERT_1_C The su's on the Cell Axes   are Equal (x 100000)         20 Ang. 
PLAT154_ALERT_1_C The su's on the Cell Angles are Equal  (x 10000)        100 Deg. 
PLAT180_ALERT_4_C Check Cell Rounding: # of Values Ending with 0 =          4      

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          2      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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