Acta Cryst. (2008). E64, m1129-m1130  [ doi:10.1107/S1600536808024458 ]

Bis{[(⁵)-cyclopentadienyl]tris(diethyl phosphito-³P,P',P'')cobaltate(III)-³O,O',O'']oxovanadium(IV)}--oxalate

C. C. McLauchlan and A. E. Anderson

Online 6 August 2008

Key indicators

• Single-crystal X-ray study
• T = 180 K
• Mean (C-C) = 0.006 Å
• R factor = 0.041
• wR factor = 0.110
• Data-to-parameter ratio = 21.2

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       4.29 Ratio

Alert level C
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.92 Ratio
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        O2C     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C34     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C35     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        Co1     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C1B     
PLAT360_ALERT_2_C Short  C(sp3)-C(sp3) Bond  C1A    -   C2A    ...       1.41 Ang. 
PLAT063_ALERT_4_C Crystal Probably too Large for Beam Size .......       0.63 mm   
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #        101     
            O3  -V1  -O2P -P2   -164.00  1.70   1.555   1.555   1.555   1.555  
PLAT720_ALERT_4_C Number of Unusual/Non-Standard Labels ..........         30      

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
  10 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   7 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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