Acta Cryst. (2008). E64, m1316  [ doi:10.1107/S1600536808030043 ]

-3-Thienylmalonato-²O¹:O³-bis[triphenyltin(IV)]

M. Yang, H. Yin, D. Wang, L. Quan and L. Cui

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.015 Å
• R factor = 0.054
• wR factor = 0.131
• Data-to-parameter ratio = 15.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.64 Ratio
PLAT230_ALERT_2_C Hirshfeld Test Diff for    S2     --  C44     ..       6.43 su   
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         S1     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C37     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         S2     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C38     
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C20    -C24           1.37 Ang. 
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C32    -C37           1.36 Ang. 
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C38    -C43           1.37 Ang. 
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C57    -C62           1.37 Ang. 
PLAT331_ALERT_2_C Small Average Phenyl C-C Dist.   C75    -C80           1.37 Ang. 
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang ...         15      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
  12 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  11 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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