# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 310.98 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.8107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 7.6306 _cell_length_b 11.2177 _cell_length_c 15.4431 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10123.02 11399.07 464.68 o 4 0 0 1507.35 1673.25 121.84 o 6 0 0 248.79 21.89 154.21 o 8 0 0 2326.79 2270.90 376.52 o 1 1 0 14247.09 16168.14 397.53 o 2 1 0 56135.14 60482.04 1491.48 o 3 1 0 48534.82 53662.04 1146.63 o 4 1 0 8152.27 9238.22 224.47 o 5 1 0 9253.96 10373.21 355.26 o 6 1 0 152.04 85.61 115.64 o 7 1 0 9105.46 8671.21 509.67 o 8 1 0 358.47 751.13 370.80 o 9 1 0 334.84 439.91 278.53 o 1 2 0 67398.84 68552.77 1825.27 o 2 2 0 11952.47 12061.74 295.39 o 3 2 0 3974.26 4447.43 120.52 o 4 2 0 3169.51 3242.06 103.99 o 5 2 0 631.22 724.95 76.89 o 6 2 0 74.82 151.57 121.54 o 7 2 0 849.50 724.61 176.23 o 8 2 0 863.59 756.26 200.86 o 9 2 0 1871.50 1962.86 292.31 o 1 3 0 3346.40 3380.37 90.87 o 2 3 0 41368.33 42761.43 1041.16 o 3 3 0 787.42 902.08 54.43 o 4 3 0 17036.16 17494.18 401.65 o 5 3 0 633.64 802.19 82.46 o 6 3 0 6713.15 7488.95 449.28 o 7 3 0 2411.26 2861.17 284.10 o 8 3 0 3220.13 3779.62 347.56 o 9 3 0 231.03 119.88 270.09 o 0 4 0 11308.71 11601.16 466.36 o 1 4 0 50908.33 50525.14 1444.36 o 2 4 0 285.57 318.51 33.04 o 3 4 0 1862.01 1874.42 87.20 o 4 4 0 2985.30 3032.00 116.51 o 5 4 0 4568.92 4435.02 232.92 o 6 4 0 12.62 0.00 120.32 o 7 4 0 425.92 358.98 148.95 o 8 4 0 5.29 90.81 169.91 o 9 4 0 3298.14 2894.04 336.73 o 1 5 0 3049.29 3196.85 127.90 o 2 5 0 7992.15 7984.45 181.77 o 3 5 0 1368.37 1345.31 64.86 o 4 5 0 4801.59 4958.62 198.34 o 5 5 0 208.62 159.24 64.28 o 6 5 0 9488.08 9632.82 333.93 o 7 5 0 2526.03 2219.79 318.09 o 8 5 0 3372.71 4064.72 415.63 o 0 6 0 15935.55 15866.89 636.61 o 1 6 0 18423.32 18172.14 671.78 o 2 6 0 4752.98 4880.43 142.47 o 3 6 0 2836.03 2976.81 100.11 o 4 6 0 1268.50 1294.19 86.97 o 5 6 0 51.40 37.00 70.07 o 6 6 0 544.65 417.59 152.31 o 7 6 0 300.64 137.48 157.68 o 8 6 0 1313.80 1950.78 545.62 o 1 7 0 4068.89 3934.07 249.06 o 2 7 0 3848.32 4022.41 138.17 o 3 7 0 9214.91 9303.90 248.39 o 4 7 0 3492.21 3613.29 194.40 o 5 7 0 6099.56 6517.41 261.06 o 6 7 0 354.02 427.27 145.82 o 7 7 0 3009.94 3760.98 413.09 o 8 7 0 68.12 170.87 301.19 o 0 8 0 38394.62 37562.01 1443.17 o 1 8 0 2.07 130.11 81.56 o 2 8 0 12027.23 12265.82 428.27 o 3 8 0 286.25 253.32 91.37 o 4 8 0 173.36 43.70 156.21 o 5 8 0 133.95 116.13 114.43 o 6 8 0 81.88 89.90 145.76 o 7 8 0 10.36 0.00 248.53 o 1 9 0 2752.98 3019.34 229.48 o 2 9 0 3435.41 3461.29 247.93 o 3 9 0 8666.33 8516.32 438.37 o 4 9 0 550.70 855.83 181.02 o 5 9 0 5396.14 5481.46 511.99 o 6 9 0 435.20 544.85 178.07 o 7 9 0 853.54 437.29 271.42 o 0 10 0 5817.50 5397.29 470.40 o 1 10 0 10917.47 10816.63 540.78 o 2 10 0 3749.74 3925.97 278.78 o 3 10 0 273.98 287.75 210.31 o 4 10 0 142.71 204.09 162.77 o 5 10 0 34.20 35.58 164.69 o 6 10 0 10.00 37.84 168.88 o 1 11 0 67.76 165.21 163.15 o 2 11 0 4617.01 5042.99 333.80 o 3 11 0 11.62 12.22 213.43 o 4 11 0 3584.03 4055.56 341.12 o 5 11 0 439.12 612.37 214.26 o 0 12 0 1200.38 1697.73 326.19 o 1 12 0 4933.81 4588.50 341.50 o 2 12 0 0.93 68.02 157.15 o 3 12 0 968.68 1056.74 230.80 o 4 12 0 94.59 41.99 183.76 o 1 13 0 288.20 199.96 176.56 o 2 13 0 78.15 0.00 143.97 o 3 13 0 712.27 844.31 287.64 o 1 0 1 96709.35 103665.19 2067.71 o 2 0 1 11517.48 12820.16 307.57 o 3 0 1 5241.03 5989.49 173.98 o 4 0 1 15395.29 17131.05 454.45 o 5 0 1 322.06 355.03 104.63 o 6 0 1 1220.78 1270.82 175.90 o 7 0 1 1473.07 1255.62 198.28 o 8 0 1 236.44 91.52 163.02 o 9 0 1 3117.58 2956.85 323.07 o -9 1 1 124.04 119.98 189.88 o -8 1 1 2939.61 2981.55 307.40 o -7 1 1 1811.26 2174.24 248.64 o -6 1 1 11061.87 12169.72 596.44 o -5 1 1 3139.95 3448.76 193.88 o -4 1 1 13142.43 14074.20 335.67 o -3 1 1 15868.46 17505.87 390.56 o -2 1 1 90912.77 99120.77 2128.81 o -1 1 1 7069.69 7293.60 211.99 o 0 1 1 2746.00 2655.90 125.50 o 1 1 1 5279.99 5961.12 144.51 o 2 1 1 93205.07 100215.62 2271.36 o 3 1 1 15342.88 16948.23 386.42 o 4 1 1 12226.85 13265.36 296.59 o 5 1 1 3200.74 3499.88 194.36 o 6 1 1 9519.62 10043.29 579.30 o 7 1 1 2026.58 2379.73 251.27 o 8 1 1 3151.42 3368.49 317.97 o 9 1 1 104.03 0.00 179.28 o -9 2 1 1711.48 1672.27 270.62 o -8 2 1 1217.60 1302.87 232.47 o -7 2 1 248.56 195.27 142.80 o -6 2 1 1441.30 1558.88 191.40 o -5 2 1 4524.18 4783.58 183.84 o -4 2 1 956.60 1086.34 63.35 o -3 2 1 14307.96 14476.13 298.69 o -2 2 1 28585.57 29358.10 715.96 o -1 2 1 32146.03 32716.75 989.00 o 0 2 1 94424.96 89129.41 3462.31 o 1 2 1 34665.47 34348.08 765.55 o 2 2 1 29203.22 30705.64 687.52 o 3 2 1 12922.33 13054.75 313.85 o 4 2 1 1777.33 2066.68 69.28 o 5 2 1 4468.00 4999.92 187.52 o 6 2 1 1278.93 1474.00 190.47 o 7 2 1 172.51 13.48 136.40 o 8 2 1 1098.23 1422.12 238.78 o 9 2 1 1643.29 1838.00 282.57 o -9 3 1 490.21 229.16 208.70 o -8 3 1 698.50 412.96 293.25 o -7 3 1 7181.48 7437.05 466.59 o -6 3 1 2951.77 3232.56 252.21 o -5 3 1 11210.31 11698.17 363.44 o -4 3 1 4391.13 4536.37 126.98 o -3 3 1 20933.38 20965.93 497.09 o -2 3 1 5076.84 5285.84 153.93 o -1 3 1 31229.62 31465.33 961.25 o 0 3 1 980.79 1064.57 58.79 o 1 3 1 33463.95 33377.14 732.01 o 2 3 1 7136.65 7052.14 172.86 o 3 3 1 17584.49 18462.42 493.25 o 4 3 1 4312.48 4738.18 134.07 o 5 3 1 10852.94 11546.65 365.52 o 6 3 1 2735.13 3009.61 271.14 o 7 3 1 7102.09 7911.27 474.60 o 8 3 1 775.28 667.02 204.38 o 9 3 1 497.91 459.62 223.85 o -8 4 1 2113.63 1496.04 250.30 o -7 4 1 890.19 776.63 173.08 o -6 4 1 18.38 166.63 163.40 o -5 4 1 4932.17 4940.67 191.09 o -4 4 1 2223.20 2343.33 91.87 o -3 4 1 1169.87 1212.28 55.60 o -2 4 1 24008.09 24570.63 610.05 o -1 4 1 4640.30 4590.04 138.27 o 0 4 1 62570.70 59401.00 1847.22 o 1 4 1 4269.77 4270.96 125.19 o 2 4 1 22060.26 21871.05 499.87 o 3 4 1 1503.83 1533.97 66.63 o 4 4 1 2277.09 2408.83 101.93 o 5 4 1 4411.49 4284.89 191.77 o 6 4 1 18.49 0.00 85.81 o 7 4 1 870.75 1077.00 187.71 o 8 4 1 1932.80 1913.30 261.21 o -8 5 1 759.06 1126.08 233.19 o -7 5 1 5127.38 5252.08 383.57 o -6 5 1 796.22 723.68 105.04 o -5 5 1 6634.56 7036.76 261.69 o -4 5 1 4771.12 4702.06 149.44 o -3 5 1 13229.36 13811.12 333.45 o -2 5 1 5816.57 5838.15 169.16 o -1 5 1 10700.22 10694.55 295.74 o 0 5 1 444.34 517.38 49.13 o 1 5 1 10133.93 9936.80 338.51 o 2 5 1 6301.19 6239.06 160.74 o 3 5 1 14262.51 14077.35 360.62 o 4 5 1 4420.87 4613.91 177.08 o 5 5 1 7110.57 7412.60 296.34 o 6 5 1 759.33 1012.93 158.50 o 7 5 1 5087.42 5461.62 344.09 o 8 5 1 664.98 400.02 184.10 o -8 6 1 850.79 1092.42 247.63 o -7 6 1 463.32 657.61 197.79 o -6 6 1 785.55 836.05 114.62 o -5 6 1 849.00 922.61 107.40 o -4 6 1 1378.26 1370.51 134.37 o -3 6 1 1800.07 1942.53 79.15 o -2 6 1 10729.56 10861.82 289.68 o -1 6 1 17406.87 16288.10 632.48 o 0 6 1 19474.74 18422.64 513.25 o 1 6 1 17986.43 17473.45 544.72 o 2 6 1 12530.11 12761.38 310.56 o 3 6 1 1928.08 1963.80 99.41 o 4 6 1 1282.97 1329.31 108.50 o 5 6 1 778.82 812.84 104.65 o 6 6 1 990.80 906.38 227.50 o 7 6 1 364.11 307.05 168.23 o 8 6 1 867.25 758.86 276.21 o -8 7 1 1309.66 363.63 327.75 o -7 7 1 399.75 283.90 184.17 o -6 7 1 5097.76 5185.12 269.58 o -5 7 1 1261.85 1303.02 109.87 o -4 7 1 5761.53 5833.88 223.28 o -3 7 1 5556.07 5593.20 164.28 o -2 7 1 11298.51 11250.69 306.82 o -1 7 1 206.01 167.95 73.13 o 0 7 1 5411.21 4882.76 174.06 o 1 7 1 179.07 172.31 48.64 o 2 7 1 11118.85 11008.91 330.27 o 3 7 1 5720.68 5833.49 209.93 o 4 7 1 6386.79 6396.98 457.17 o 5 7 1 1169.77 1506.83 180.25 o 6 7 1 5165.02 5158.64 272.01 o 7 7 1 381.15 90.07 231.36 o 8 7 1 1349.00 1935.27 419.74 o -7 8 1 620.87 1213.56 355.97 o -6 8 1 743.30 513.74 139.66 o -5 8 1 83.07 69.34 111.56 o -4 8 1 2073.39 2125.01 213.42 o -3 8 1 4334.01 4209.74 172.63 o -2 8 1 716.72 801.10 108.24 o -1 8 1 20762.67 21145.59 794.24 o 0 8 1 100.73 238.67 82.13 o 1 8 1 21221.36 21006.77 918.39 o 2 8 1 686.91 761.79 126.86 o 3 8 1 4633.89 4879.99 228.30 o 4 8 1 2253.81 2862.64 224.46 o 5 8 1 43.99 75.94 107.26 o 6 8 1 587.04 588.74 251.70 o 7 8 1 640.56 660.38 192.97 o -7 9 1 419.37 126.99 304.97 o -6 9 1 2522.12 2452.69 224.47 o -5 9 1 714.54 831.18 148.91 o -4 9 1 4955.42 5444.96 393.95 o -3 9 1 2047.11 2178.48 293.50 o -2 9 1 5356.22 5471.20 314.94 o -1 9 1 4202.26 4142.03 277.29 o 0 9 1 61.54 156.59 110.07 o 1 9 1 4441.52 4862.03 656.50 o 2 9 1 5081.24 4982.47 311.09 o 3 9 1 1997.97 2122.61 308.69 o 4 9 1 5261.21 5639.60 503.51 o 5 9 1 832.64 504.79 174.87 o 6 9 1 2525.33 2493.40 473.20 o 7 9 1 455.50 435.06 274.83 o -6 10 1 133.84 334.17 202.24 o -5 10 1 422.76 230.16 321.77 o -4 10 1 231.34 76.22 374.74 o -3 10 1 2463.33 2585.14 320.58 o -2 10 1 3104.81 3525.86 369.19 o -1 10 1 4202.63 4418.11 298.59 o 0 10 1 11189.36 11464.31 568.32 o 1 10 1 3931.62 4271.53 296.50 o 2 10 1 3441.29 3825.30 602.78 o 3 10 1 2249.80 2521.01 223.28 o 4 10 1 339.27 218.20 235.42 o 5 10 1 414.33 449.85 187.48 o 6 10 1 78.08 207.75 177.54 o -5 11 1 2253.85 2266.24 280.78 o -4 11 1 283.89 447.13 185.97 o -3 11 1 3017.54 2998.84 363.47 o -2 11 1 917.55 794.22 151.34 o -1 11 1 1512.57 1772.49 208.25 o 0 11 1 718.39 860.25 170.03 o 1 11 1 1647.83 1510.64 202.67 o 2 11 1 1004.56 977.50 190.32 o 3 11 1 2964.55 2888.85 391.30 o 4 11 1 265.99 0.00 226.53 o 5 11 1 2100.05 2341.47 276.40 o -4 12 1 617.30 1061.03 234.21 o -3 12 1 202.76 0.00 242.26 o -2 12 1 3035.01 3460.28 342.46 o -1 12 1 139.32 88.50 134.80 o 0 12 1 3538.11 3352.31 287.26 o 1 12 1 100.47 0.00 202.20 o 2 12 1 3232.86 2893.90 275.86 o 3 12 1 175.84 0.00 237.31 o 4 12 1 538.22 502.82 222.18 o -3 13 1 1088.22 496.98 226.32 o -2 13 1 458.43 585.92 169.42 o -1 13 1 200.77 301.45 159.25 o 0 13 1 80.13 0.00 147.60 o 1 13 1 217.72 266.71 163.58 o 2 13 1 454.83 341.82 181.97 o 3 13 1 1067.80 1779.50 376.74 o 0 0 2 69097.07 60471.91 2530.11 o 1 0 2 734.24 748.56 32.52 o 2 0 2 8229.54 8174.13 193.19 o 3 0 2 16276.46 17424.04 420.47 o 4 0 2 7795.21 8285.23 241.33 o 5 0 2 20526.73 20652.74 782.80 o 6 0 2 20.34 19.42 115.78 o 7 0 2 680.04 585.21 170.47 o 8 0 2 1564.54 1360.11 227.25 o 9 0 2 1.91 28.27 182.30 o -9 1 2 298.77 386.81 193.80 o -8 1 2 1529.02 1590.66 342.41 o -7 1 2 7128.20 7096.58 447.72 o -6 1 2 4540.51 4939.06 338.00 o -5 1 2 9157.79 9635.06 388.94 o -4 1 2 4491.95 4802.65 130.52 o -3 1 2 18349.28 19801.11 447.05 o -2 1 2 21212.93 22633.51 482.85 o -1 1 2 6816.15 7096.31 280.54 o 0 1 2 28138.72 26818.00 1118.93 o 1 1 2 8653.93 8743.80 176.37 o 2 1 2 19557.12 21259.01 444.00 o 3 1 2 18703.56 20119.27 445.00 o 4 1 2 4213.14 4527.92 136.05 o 5 1 2 8217.93 8705.56 383.46 o 6 1 2 5004.71 5216.82 340.91 o 7 1 2 7194.34 7356.82 451.50 o 8 1 2 1417.62 1653.96 245.63 o 9 1 2 285.39 240.05 193.13 o -9 2 2 1192.79 1250.18 251.32 o -8 2 2 749.18 554.66 193.97 o -7 2 2 1149.93 1026.63 189.87 o -6 2 2 2647.64 3033.17 250.26 o -5 2 2 10190.51 10924.12 336.25 o -4 2 2 26318.55 28300.23 580.23 o -3 2 2 8589.96 8957.47 198.87 o -2 2 2 11516.70 11838.31 302.83 o -1 2 2 20775.92 19013.86 733.15 o 0 2 2 53698.35 52904.57 1849.18 o 1 2 2 15204.86 15353.21 307.20 o 2 2 2 13077.78 13770.73 273.48 o 3 2 2 8122.92 8579.29 192.63 o 4 2 2 25807.83 27346.26 575.30 o 5 2 2 9910.71 10579.87 339.61 o 6 2 2 2233.57 2268.47 232.93 o 7 2 2 1159.74 1049.90 200.17 o 8 2 2 497.28 831.29 206.19 o 9 2 2 1230.02 1303.27 161.90 o -9 3 2 233.66 211.60 341.47 o -8 3 2 1297.34 1518.89 403.69 o -7 3 2 2637.41 2820.71 273.34 o -6 3 2 6912.54 7625.34 395.25 o -5 3 2 1288.11 1379.21 79.58 o -4 3 2 13399.95 13956.57 296.22 o -3 3 2 38026.14 39135.57 782.83 o -2 3 2 18259.98 17648.09 458.12 o -1 3 2 7974.22 7660.86 186.24 o 0 3 2 995.62 1006.74 61.60 o 1 3 2 6490.19 6222.81 153.90 o 2 3 2 18981.87 19008.71 377.20 o 3 3 2 37546.43 38881.68 789.17 o 4 3 2 12590.96 13081.78 333.56 o 5 3 2 1265.42 1302.90 93.30 o 6 3 2 6478.58 6642.17 298.42 o 7 3 2 2527.35 2477.83 267.26 o 8 3 2 1259.88 1204.42 232.49 o 9 3 2 173.82 468.79 241.87 o -8 4 2 350.60 223.69 186.38 o -7 4 2 1539.18 1848.42 233.91 o -6 4 2 6581.73 6600.29 354.99 o -5 4 2 299.27 526.72 106.87 o -4 4 2 9424.17 9320.68 256.90 o -3 4 2 3012.12 2925.28 100.78 o -2 4 2 560.17 546.32 43.46 o -1 4 2 60915.95 58256.36 1295.07 o 0 4 2 1.76 9.95 26.75 o 1 4 2 58756.07 56006.17 1742.22 o 2 4 2 650.85 727.45 39.08 o 3 4 2 3143.43 3079.28 83.77 o 4 4 2 10419.12 10576.21 262.19 o 5 4 2 330.84 222.47 225.44 o 6 4 2 5920.22 5486.91 460.59 o 7 4 2 1527.85 1534.06 233.11 o 8 4 2 371.98 535.80 212.45 o -8 5 2 1024.00 937.85 613.78 o -7 5 2 1538.37 1579.08 336.52 o -6 5 2 3623.13 3623.09 217.40 o -5 5 2 2384.31 2408.02 126.76 o -4 5 2 16143.01 16304.40 394.02 o -3 5 2 11680.93 11704.96 273.25 o -2 5 2 15461.65 15217.82 382.28 o -1 5 2 5229.08 5077.20 142.81 o 0 5 2 654.55 630.71 62.85 o 1 5 2 5690.78 5282.79 187.85 o 2 5 2 15743.67 15009.51 385.94 o 3 5 2 11707.11 11939.47 275.76 o 4 5 2 15716.38 15672.17 461.58 o 5 5 2 1996.34 2215.75 175.87 o 6 5 2 3799.37 3713.46 442.77 o 7 5 2 1562.78 1690.47 282.78 o 8 5 2 961.00 894.91 207.22 o -8 6 2 716.17 777.16 258.09 o -7 6 2 521.60 753.87 196.58 o -6 6 2 1929.98 1969.01 160.55 o -5 6 2 6964.27 6588.98 231.44 o -4 6 2 2937.80 3103.72 151.16 o -3 6 2 2701.44 2726.48 104.24 o -2 6 2 11312.97 11081.16 274.99 o -1 6 2 12034.57 11473.94 299.01 o 0 6 2 29339.90 27275.25 806.49 o 1 6 2 13698.78 13099.68 399.37 o 2 6 2 10949.61 10772.05 318.58 o 3 6 2 3245.82 3242.00 112.06 o 4 6 2 3377.50 3297.80 150.33 o 5 6 2 6419.60 6579.45 292.47 o 6 6 2 2059.48 2033.24 173.59 o 7 6 2 588.25 223.27 225.20 o 8 6 2 668.39 1228.73 307.45 o -8 7 2 690.27 458.40 224.61 o -7 7 2 1256.85 1225.16 232.40 o -6 7 2 1624.80 1571.13 190.28 o -5 7 2 6078.35 5631.47 246.47 o -4 7 2 2155.87 2240.74 148.87 o -3 7 2 7792.38 7858.26 228.25 o -2 7 2 7600.93 7706.08 226.49 o -1 7 2 8680.32 8461.90 266.63 o 0 7 2 465.26 364.20 65.52 o 1 7 2 8718.95 8700.41 349.95 o 2 7 2 8125.54 7920.28 283.78 o 3 7 2 8559.51 8700.61 281.47 o 4 7 2 2615.06 3158.43 209.09 o 5 7 2 6307.97 6262.11 332.23 o 6 7 2 1729.35 2209.15 314.31 o 7 7 2 1167.38 1212.41 200.22 o 8 7 2 716.38 716.13 290.11 o -7 8 2 207.55 615.94 289.75 o -6 8 2 61.50 115.45 115.76 o -5 8 2 5169.90 5287.09 369.76 o -4 8 2 1137.03 1334.08 164.73 o -3 8 2 4450.12 4389.52 178.00 o -2 8 2 6562.36 6852.92 304.91 o -1 8 2 961.13 1120.64 120.27 o 0 8 2 11895.51 11530.11 425.70 o 1 8 2 819.28 795.91 129.28 o 2 8 2 7251.38 7159.74 401.96 o 3 8 2 4352.77 4077.12 308.64 o 4 8 2 1256.32 1308.66 253.42 o 5 8 2 5277.89 5056.11 417.69 o 6 8 2 127.75 0.00 164.19 o 7 8 2 259.37 175.86 209.51 o -7 9 2 1253.17 1140.34 377.08 o -6 9 2 517.64 544.25 162.66 o -5 9 2 2822.53 2874.00 249.50 o -4 9 2 747.09 623.90 111.06 o -3 9 2 2324.68 2466.70 232.66 o -2 9 2 5194.67 5066.06 263.90 o -1 9 2 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