# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' _t503' _shelx_refln_list_code 4 _shelx_F_calc_maximum 343.48 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.8300 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.7161 _cell_length_b 13.1040 _cell_length_c 17.1958 _cell_angle_alpha 86.491 _cell_angle_beta 77.568 _cell_angle_gamma 74.103 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8779.24 7617.61 111.10 o 3 0 0 15969.52 14791.10 308.91 o 4 0 0 29507.00 27234.62 348.76 o 5 0 0 417.05 421.49 55.67 o 6 0 0 7198.98 7498.02 157.52 o 7 0 0 4909.10 5033.39 161.05 o 8 0 0 2753.64 3132.73 141.98 o 9 0 0 2012.51 2072.68 153.38 o 10 0 0 3253.35 3793.48 169.67 o 11 0 0 17394.51 18512.50 747.33 o 12 0 0 3557.37 3358.41 295.96 o 13 0 0 227.29 246.39 69.86 o -13 1 0 255.71 -9.14 135.17 o -12 1 0 387.87 242.24 87.95 o -11 1 0 5325.64 6098.09 379.65 o -10 1 0 8554.43 8972.32 392.45 o -9 1 0 450.94 618.04 91.66 o -8 1 0 483.02 538.60 61.95 o -7 1 0 1889.85 1813.61 98.85 o -6 1 0 20254.75 20760.38 324.40 o -5 1 0 35907.81 36388.76 641.00 o -4 1 0 2388.77 2099.02 80.68 o -3 1 0 747.38 762.79 53.84 o -2 1 0 67833.34 66824.32 1564.42 o 2 1 0 23.49 40.23 19.42 o 3 1 0 28707.46 28307.26 260.34 o 4 1 0 17896.92 17675.25 246.33 o 5 1 0 40357.64 38721.64 487.97 o 6 1 0 6441.79 6613.03 166.26 o 7 1 0 1415.83 1492.60 79.59 o 8 1 0 7779.91 8114.02 224.42 o 9 1 0 35859.91 37702.11 1515.29 o 10 1 0 5606.37 6064.38 314.74 o 11 1 0 1519.34 1295.89 115.96 o 12 1 0 537.61 283.73 84.01 o 13 1 0 813.72 505.92 142.49 o -12 2 0 4959.77 4888.94 335.72 o -11 2 0 10.45 93.84 67.71 o -10 2 0 8793.46 9059.53 305.61 o -9 2 0 449.79 297.78 71.02 o -8 2 0 9617.81 9993.00 332.16 o -7 2 0 807.44 954.09 75.22 o -6 2 0 3296.98 3298.32 125.19 o -5 2 0 455.71 488.94 63.37 o -4 2 0 2765.67 2906.92 91.82 o -3 2 0 5198.07 4988.87 116.36 o -2 2 0 10331.96 8948.98 142.15 o -1 2 0 45532.22 45274.44 348.59 o 0 2 0 280.19 407.00 24.15 o 1 2 0 1086.62 1093.99 37.89 o 2 2 0 136.79 143.74 27.43 o 3 2 0 21364.06 21690.71 379.42 o 4 2 0 11056.84 11216.39 162.78 o 5 2 0 25754.90 26802.07 360.10 o 6 2 0 10413.43 10379.95 218.50 o 7 2 0 7739.04 7661.14 183.51 o 8 2 0 7897.16 8244.12 209.13 o 9 2 0 2029.24 2247.85 178.86 o 10 2 0 13509.12 13993.04 421.56 o 11 2 0 266.61 201.72 72.00 o 12 2 0 1204.22 1517.46 297.73 o 13 2 0 2178.80 2219.63 397.37 o -12 3 0 1145.18 1204.07 291.91 o -11 3 0 1673.91 1666.21 187.82 o -10 3 0 5123.31 5559.69 471.93 o -9 3 0 19043.71 21109.15 677.80 o -8 3 0 1389.59 1411.29 123.37 o -7 3 0 4272.06 4356.20 170.63 o -6 3 0 6025.04 5808.37 202.24 o -5 3 0 14751.93 14114.40 266.64 o -4 3 0 8462.03 8149.94 175.17 o -3 3 0 31641.20 31920.46 474.06 o -2 3 0 345.23 326.72 52.12 o -1 3 0 1354.13 1348.06 73.09 o 0 3 0 21215.82 21471.67 266.31 o 1 3 0 2048.11 2164.78 59.95 o 2 3 0 46198.75 48929.98 532.62 o 3 3 0 7860.50 8013.56 116.55 o 4 3 0 150.63 171.03 22.15 o 5 3 0 11671.14 11423.14 189.06 o 6 3 0 36856.50 38231.52 389.12 o 7 3 0 19.12 6.66 40.28 o 8 3 0 16540.94 16926.24 342.08 o 9 3 0 3180.95 2970.40 143.19 o 10 3 0 82.44 69.89 100.35 o 11 3 0 128.51 179.64 48.02 o 12 3 0 1077.03 954.45 183.30 o 13 3 0 1433.58 1803.75 373.49 o -11 4 0 4323.74 5276.95 364.06 o -10 4 0 1727.15 1286.32 252.02 o -9 4 0 2337.79 2483.49 308.17 o -8 4 0 5219.06 4737.10 192.42 o -7 4 0 762.41 1031.22 94.74 o -6 4 0 1622.23 1488.93 121.52 o -5 4 0 15859.37 15314.91 280.54 o -4 4 0 13993.76 13398.82 279.40 o -3 4 0 9825.67 8714.48 187.82 o -2 4 0 132.79 82.17 37.95 o -1 4 0 26993.79 25766.25 389.45 o 0 4 0 61398.61 60701.21 471.68 o 1 4 0 9990.51 9927.71 149.12 o 2 4 0 253.08 297.63 32.92 o 3 4 0 2888.09 2862.75 67.42 o 4 4 0 17260.69 18335.82 376.81 o 5 4 0 2970.88 2884.34 95.78 o 6 4 0 12123.12 12049.58 237.52 o 7 4 0 2895.87 2875.07 103.66 o 8 4 0 2412.51 2286.73 84.37 o 9 4 0 203.70 244.14 48.48 o 10 4 0 1063.35 1013.73 99.65 o 11 4 0 1930.62 1803.52 156.51 o 12 4 0 798.80 875.53 198.89 o 13 4 0 63.83 272.14 157.34 o -11 5 0 1313.24 1342.92 208.23 o -10 5 0 1928.58 1957.93 544.28 o -9 5 0 889.56 752.80 184.62 o -8 5 0 592.92 618.06 107.60 o -7 5 0 2229.05 2128.48 138.00 o -6 5 0 14707.61 15360.67 371.93 o -5 5 0 1913.73 1741.67 152.51 o -4 5 0 3055.98 3086.86 118.11 o -3 5 0 2516.30 2288.57 93.86 o -2 5 0 31602.20 30340.00 370.28 o -1 5 0 6584.51 6563.85 173.56 o 0 5 0 17586.19 17262.17 297.33 o 1 5 0 2572.74 2233.73 73.31 o 2 5 0 899.82 888.21 50.18 o 3 5 0 42.65 53.68 26.77 o 4 5 0 34468.66 34778.82 375.98 o 5 5 0 31655.06 33530.86 342.19 o 6 5 0 2338.55 2189.93 65.29 o 7 5 0 36.06 54.81 24.07 o 8 5 0 12564.30 12458.80 268.50 o 9 5 0 3483.76 3517.88 143.96 o 10 5 0 505.58 474.50 73.31 o 11 5 0 39.77 95.26 58.34 o 12 5 0 8.77 122.40 67.28 o 13 5 0 1503.52 1380.78 299.44 o -10 6 0 110.17 140.54 101.23 o -9 6 0 2428.76 2606.32 315.09 o -8 6 0 1766.10 1900.62 287.65 o -7 6 0 675.09 591.99 119.99 o -6 6 0 1873.92 1906.04 121.20 o -5 6 0 9.99 22.94 56.66 o -4 6 0 1720.33 1638.43 107.02 o -3 6 0 12.14 62.62 42.70 o -2 6 0 9062.49 8804.03 206.92 o -1 6 0 29040.13 28535.26 332.43 o 0 6 0 14546.42 14185.37 233.49 o 1 6 0 7071.12 7149.29 148.30 o 2 6 0 28399.09 29811.76 346.86 o 3 6 0 43448.80 44946.20 562.16 o 4 6 0 205.87 326.85 45.78 o 5 6 0 7924.02 8203.73 172.77 o 6 6 0 2.20 100.71 25.00 o 7 6 0 9806.58 10128.47 301.79 o 8 6 0 13.99 20.45 24.29 o 9 6 0 2927.22 3099.47 167.18 o 10 6 0 1516.41 1509.54 76.77 o 11 6 0 351.30 312.14 103.07 o 12 6 0 1260.54 941.05 192.42 o 13 6 0 7895.86 7845.07 661.99 o -10 7 0 873.94 1207.55 299.19 o -9 7 0 70.25 117.17 77.80 o -8 7 0 4531.11 4746.72 556.38 o -7 7 0 97.51 201.91 74.06 o -6 7 0 1769.19 1863.58 167.32 o -5 7 0 417.81 478.97 75.86 o -4 7 0 10077.60 9901.67 264.98 o -3 7 0 18746.11 17769.98 359.21 o -2 7 0 1146.02 1163.99 128.79 o -1 7 0 125.31 186.53 40.16 o 0 7 0 1319.46 1474.87 76.37 o 1 7 0 2921.59 2861.84 117.46 o 2 7 0 640.44 474.82 53.65 o 3 7 0 17708.96 17467.39 313.59 o 4 7 0 3596.38 3630.17 107.13 o 5 7 0 790.20 947.37 61.87 o 6 7 0 292.94 288.51 36.96 o 7 7 0 2937.40 2757.36 91.64 o 8 7 0 23409.08 23722.54 478.35 o 9 7 0 1353.28 1453.58 134.11 o 10 7 0 819.53 818.82 96.79 o 11 7 0 8667.56 8673.74 354.51 o 12 7 0 7255.41 6849.32 678.85 o 13 7 0 538.06 317.40 163.27 o -9 8 0 1365.39 1374.33 221.22 o -8 8 0 306.35 270.94 92.87 o -7 8 0 1320.16 1311.06 200.62 o -6 8 0 3982.30 3415.85 296.94 o -5 8 0 10470.84 10487.06 372.70 o -4 8 0 286.18 266.21 64.28 o -3 8 0 3411.73 3277.30 143.62 o -2 8 0 1581.68 1427.70 92.04 o -1 8 0 3924.30 3847.00 135.83 o 0 8 0 259.10 261.09 44.37 o 1 8 0 10578.67 10781.13 254.09 o 2 8 0 335.80 336.91 47.21 o 3 8 0 3478.24 3325.17 147.89 o 4 8 0 77.52 112.32 26.78 o 5 8 0 3012.91 3113.72 153.26 o 6 8 0 4512.83 4765.61 147.74 o 7 8 0 795.61 885.17 63.14 o 8 8 0 1363.48 1330.89 90.90 o 9 8 0 458.16 432.63 64.66 o 10 8 0 3443.39 3106.67 185.46 o 11 8 0 138.64 440.83 161.66 o 12 8 0 6042.81 6014.53 618.84 o 13 8 0 902.96 884.66 266.22 o -8 9 0 967.97 672.46 211.48 o -7 9 0 6395.45 6310.89 455.03 o -6 9 0 4128.31 4354.55 397.38 o -5 9 0 316.58 206.30 85.96 o -4 9 0 2616.53 2346.27 149.85 o -3 9 0 4006.78 3925.26 203.85 o -2 9 0 5155.01 4799.25 212.54 o -1 9 0 5287.54 5198.43 187.27 o 0 9 0 17084.49 16808.61 365.30 o 1 9 0 481.54 544.96 89.69 o 2 9 0 3971.45 4123.99 199.20 o 3 9 0 17950.51 18411.12 361.30 o 4 9 0 20936.58 21778.00 432.93 o 5 9 0 790.42 726.79 84.27 o 6 9 0 44.00 129.48 39.34 o 7 9 0 95.15 85.35 26.46 o 8 9 0 7324.58 7284.46 281.96 o 9 9 0 75.11 157.32 48.26 o 10 9 0 2725.21 3087.22 285.49 o 11 9 0 1135.18 1077.63 314.69 o 12 9 0 327.09 216.15 206.11 o -7 10 0 3805.72 3611.82 389.65 o -6 10 0 4750.57 4910.91 433.26 o -5 10 0 785.52 931.80 187.06 o -4 10 0 98.59 193.90 71.41 o -3 10 0 367.09 325.63 102.00 o -2 10 0 15330.61 15900.99 496.66 o -1 10 0 7569.17 7500.77 291.60 o 0 10 0 2706.87 2623.01 159.83 o 1 10 0 1.39 -4.29 57.14 o 2 10 0 21314.06 21482.14 467.32 o 3 10 0 13173.77 13415.83 370.53 o 4 10 0 4439.70 4265.85 185.03 o 5 10 0 7451.48 7055.77 229.82 o 6 10 0 1333.10 1384.56 121.35 o 7 10 0 121.58 61.18 58.48 o 8 10 0 6489.27 6390.30 266.91 o 9 10 0 7907.00 7477.35 401.34 o 10 10 0 363.35 267.90 75.22 o 11 10 0 817.66 487.79 168.99 o 12 10 0 960.04 800.27 212.03 o -6 11 0 1646.00 1337.43 278.36 o -5 11 0 9.48 208.93 95.10 o -4 11 0 1736.70 1760.76 251.48 o -3 11 0 549.19 584.43 150.15 o -2 11 0 66.67 -20.23 79.74 o -1 11 0 950.85 1069.88 135.04 o 0 11 0 832.88 979.32 144.46 o 1 11 0 1517.79 1525.65 144.97 o 2 11 0 2658.73 2441.96 160.90 o 3 11 0 15197.49 16133.29 497.50 o 4 11 0 4141.18 3864.64 171.86 o 5 11 0 1520.07 1653.84 162.99 o 6 11 0 2.54 -24.71 51.39 o 7 11 0 11695.37 11834.14 393.27 o 8 11 0 309.24 267.52 54.43 o 9 11 0 2384.17 2226.08 183.92 o 10 11 0 26.53 -6.12 146.91 o 11 11 0 3224.75 2297.26 375.00 o 12 11 0 2131.92 2223.10 359.14 o -5 12 0 3297.35 3543.25 371.57 o -4 12 0 390.58 446.78 165.77 o -3 12 0 1320.20 1504.21 184.51 o -2 12 0 2504.42 2732.77 319.75 o -1 12 0 596.58 466.13 175.92 o 0 12 0 424.36 306.72 88.11 o 1 12 0 2440.43 2923.39 245.21 o 2 12 0 2569.00 2634.40 217.50 o 3 12 0 965.38 895.75 125.20 o 4 12 0 1560.11 1428.93 140.33 o 5 12 0 4539.28 4645.81 310.75 o 6 12 0 3772.99 3648.52 201.41 o 7 12 0 299.99 206.89 80.07 o 8 12 0 2101.11 1960.06 191.64 o 9 12 0 1578.63 1395.27 137.43 o 10 12 0 2733.30 2829.90 353.22 o 11 12 0 751.94 918.58 285.39 o -4 13 0 199.09 362.66 230.50 o -3 13 0 1769.94 1859.54 315.49 o -2 13 0 115.21 256.89 104.65 o -1 13 0 8498.44 9571.39 590.01 o 0 13 0 2899.26 2859.27 369.98 o 1 13 0 152.40 172.31 81.10 o 2 13 0 107.25 329.39 99.44 o 3 13 0 414.03 235.27 218.76 o 4 13 0 3968.99 3970.27 307.66 o 5 13 0 16.38 60.57 65.90 o 6 13 0 3197.53 2693.61 241.07 o 7 13 0 13.43 156.30 71.77 o 8 13 0 1579.05 1419.40 205.81 o 9 13 0 191.01 -3.71 144.40 o 10 13 0 2079.08 1465.98 252.88 o -2 14 0 3964.42 4130.86 391.51 o -1 14 0 62.69 148.45 136.51 o 0 14 0 3385.49 3581.88 536.91 o 1 14 0 65.81 159.09 82.64 o 2 14 0 4385.63 4734.68 427.03 o 3 14 0 2.32 193.33 48.52 o 4 14 0 3488.40 3457.46 380.48 o 5 14 0 451.65 483.48 141.84 o 6 14 0 375.24 210.51 190.46 o 7 14 0 311.12 166.18 166.38 o 8 14 0 4632.42 4394.12 341.28 o 9 14 0 2068.63 1862.25 344.39 o 0 15 0 827.18 1063.62 234.11 o 1 15 0 350.48 355.23 113.53 o 2 15 0 2567.22 2481.93 275.12 o 3 15 0 5321.97 5816.29 534.70 o 4 15 0 5.54 126.22 93.91 o 5 15 0 84.59 -14.31 132.06 o 6 15 0 1804.87 1440.47 203.33 o 7 15 0 2369.36 2039.39 240.87 o -7 -15 1 1288.20 1174.60 187.93 o -6 -15 1 242.62 218.35 72.37 o -5 -15 1 936.45 866.70 240.38 o -4 -15 1 430.07 283.87 94.29 o -3 -15 1 38.40 139.65 111.77 o -2 -15 1 3172.73 3679.12 603.09 o -1 -15 1 1658.27 1779.90 236.73 o 0 -15 1 97.30 245.97 224.28 o -9 -14 1 1337.23 1105.63 228.69 o -8 -14 1 286.00 106.77 112.19 o -7 -14 1 2312.92 2183.26 432.10 o -6 -14 1 0.01 -38.56 95.06 o -5 -14 1 1196.83 953.70 187.67 o -4 -14 1 257.22 356.81 126.21 o -3 -14 1 4022.26 4234.36 358.96 o -2 -14 1 147.60 115.58 103.83 o -1 -14 1 1734.18 1767.65 234.61 o 0 -14 1 172.27 111.33 153.68 o 1 -14 1 2069.10 1692.43 346.10 o 2 -14 1 1413.54 1438.07 344.59 o -10 -13 1 256.98 282.38 152.53 o -9 -13 1 1204.70 1135.43 232.20 o -8 -13 1 1016.04 1103.66 203.82 o -7 -13 1 96.98 145.79 71.41 o -6 -13 1 291.30 259.11 82.21 o -5 -13 1 7748.21 7183.84 526.27 o -4 -13 1 1724.30 1837.24 452.32 o -3 -13 1 135.05 37.35 74.28 o -2 -13 1 194.43 193.58 84.39 o -1 -13 1 575.25 669.78 140.92 o 0 -13 1 5963.32 6339.02 721.12 o 1 -13 1 31.15 221.20 60.07 o 2 -13 1 1295.34 1373.78 205.77 o 3 -13 1 5.72 192.92 108.44 o 4 -13 1 1670.85 2149.38 243.34 o -11 -12 1 5814.64 6069.12 654.67 o -10 -12 1 4276.26 3896.09 421.86 o -9 -12 1 62.19 51.36 85.75 o -8 -12 1 18.84 -16.50 146.61 o -7 -12 1 3351.61 3267.70 233.88 o -6 -12 1 2587.39 2490.47 185.54 o -5 -12 1 265.59 160.89 48.00 o -4 -12 1 860.66 831.99 171.22 o -3 -12 1 3437.21 3208.04 217.48 o -2 -12 1 3196.87 3033.04 260.80 o -1 -12 1 412.29 470.56 244.20 o 0 -12 1 447.91 350.05 94.20 o 1 -12 1 3689.50 3493.55 344.10 o 2 -12 1 230.91 400.20 112.50 o 3 -12 1 40.28 120.12 107.14 o 4 -12 1 4491.65 4579.89 423.51 o 5 -12 1 2253.81 2099.25 313.54 o -11 -11 1 42.96 -4.52 170.89 o -10 -11 1 1017.42 1130.21 327.23 o -9 -11 1 502.16 426.97 99.15 o -8 -11 1 9386.55 9673.79 327.35 o -7 -11 1 81.42 123.85 56.09 o -6 -11 1 6802.04 6696.47 262.52 o -5 -11 1 0.34 65.23 36.80 o -4 -11 1 1643.54 1856.90 154.53 o -3 -11 1 763.39 905.16 101.37 o -2 -11 1 13718.93 14435.72 459.39 o -1 -11 1 7354.70 7523.88 473.34 o 0 -11 1 361.86 402.28 118.94 o 1 -11 1 498.71 398.31 125.72 o 2 -11 1 3291.99 3489.94 291.45 o 3 -11 1 2162.43 2537.53 381.46 o 4 -11 1 1.29 168.73 61.78 o 5 -11 1 1699.05 1708.09 220.56 o 6 -11 1 238.93 293.41 125.48 o 7 -11 1 1936.98 2147.59 260.22 o -12 -10 1 2844.15 3006.81 437.21 o -11 -10 1 798.52 1421.52 261.51 o -10 -10 1 780.42 632.49 353.12 o -9 -10 1 28.69 33.28 22.04 o -8 -10 1 11688.33 11439.95 364.81 o -7 -10 1 10549.99 10796.26 331.22 o -6 -10 1 27.16 111.63 978.21 o -5 -10 1 1057.07 1147.13 86.90 o -4 -10 1 14387.72 14673.96 311.58 o -3 -10 1 22502.95 23790.83 508.04 o -2 -10 1 542.34 548.74 99.14 o -1 -10 1 2007.88 2084.93 127.27 o 0 -10 1 225.54 274.28 80.29 o 1 -10 1 9588.92 9433.41 369.79 o 2 -10 1 1241.14 1320.15 229.71 o 3 -10 1 9506.70 9356.79 433.27 o 4 -10 1 110.18 168.81 77.18 o 5 -10 1 138.14 245.47 108.43 o 6 -10 1 78.18 199.70 82.11 o 7 -10 1 2379.41 2178.95 374.80 o 8 -10 1 3018.52 2890.76 493.96 o -12 -9 1 92.75 -119.01 159.95 o -11 -9 1 604.67 797.16 208.52 o -10 -9 1 2687.59 2517.12 342.99 o -9 -9 1 3647.50 3845.36 168.34 o -8 -9 1 1143.07 1210.43 94.65 o -7 -9 1 328.23 251.66 49.18 o -6 -9 1 844.99 813.09 99.53 o -5 -9 1 6889.00 6847.07 184.71 o -4 -9 1 2079.11 2114.37 179.69 o -3 -9 1 13127.86 13435.95 286.53 o -2 -9 1 21328.17 22356.65 426.20 o -1 -9 1 1702.46 1597.12 91.35 o 0 -9 1 102.27 48.16 68.07 o 1 -9 1 16273.64 16661.57 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