# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' p1 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 241.95 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7697 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.4367 _cell_length_b 12.4980 _cell_length_c 16.2970 _cell_angle_alpha 92.685 _cell_angle_beta 103.594 _cell_angle_gamma 103.500 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 352.84 376.99 26.09 o 3 0 0 5990.90 8980.54 238.50 o 4 0 0 2348.57 1395.55 97.50 o 5 0 0 127.27 418.58 97.50 o 6 0 0 1174.69 1473.11 78.26 o 7 0 0 8402.44 8015.35 252.67 o 8 0 0 4810.19 4515.51 192.36 o 9 0 0 11.74 34.26 44.72 o 10 0 0 1185.89 1047.33 113.31 o 11 0 0 1158.79 1022.23 108.04 o 12 0 0 241.43 255.61 61.39 o 13 0 0 7.47 -53.47 53.47 o 14 0 0 821.01 400.54 216.08 o 15 0 0 219.36 31.62 237.16 o -15 1 0 583.63 980.26 268.78 o -14 1 0 94.51 -79.54 79.54 o -13 1 0 1242.30 985.08 187.09 o -12 1 0 501.56 663.09 78.00 o -11 1 0 354.77 356.75 54.23 o -10 1 0 199.39 249.19 121.22 o -9 1 0 1757.97 1609.30 100.41 o -8 1 0 3867.36 4301.59 200.27 o -7 1 0 33.95 11.16 31.51 o -6 1 0 2139.56 1878.80 83.79 o -5 1 0 1546.93 2161.76 85.47 o -4 1 0 5606.67 3633.45 117.34 o -3 1 0 6973.13 10014.90 264.59 o 3 1 0 718.06 824.82 65.88 o 4 1 0 693.48 1067.70 53.94 o 5 1 0 6324.55 6305.99 188.17 o 6 1 0 10647.76 10876.54 309.24 o 7 1 0 98.69 85.70 42.73 o 8 1 0 136.15 211.77 63.24 o 9 1 0 273.35 304.85 63.02 o 10 1 0 665.10 840.74 192.36 o 11 1 0 0.15 50.95 51.85 o 12 1 0 1876.00 1759.54 258.24 o 13 1 0 2146.90 2185.61 168.65 o 14 1 0 463.83 600.81 189.73 o -15 2 0 915.14 621.89 179.19 o -14 2 0 532.75 645.70 113.62 o -13 2 0 126.82 234.59 75.78 o -12 2 0 143.65 249.00 57.01 o -11 2 0 236.71 387.20 62.05 o -10 2 0 207.54 290.42 92.23 o -9 2 0 1008.65 957.70 65.85 o -8 2 0 2820.99 2524.99 117.34 o -7 2 0 3486.06 3904.03 141.46 o -6 2 0 149.01 334.28 42.89 o -5 2 0 16.21 -18.27 27.76 o -4 2 0 1122.31 1474.93 68.51 o -3 2 0 3753.16 2400.59 81.99 o -2 2 0 11146.85 8361.22 173.54 o -1 2 0 2523.35 6211.10 167.70 o 0 2 0 98.95 0.00 7.45 o 2 2 0 302.57 1392.36 47.43 o 3 2 0 3428.41 1189.54 86.96 o 4 2 0 11998.89 11771.06 320.49 o 5 2 0 4526.49 4492.33 197.63 o 6 2 0 163.05 218.73 92.23 o 7 2 0 351.13 223.12 48.67 o 8 2 0 8.21 -47.43 47.43 o 9 2 0 875.19 1059.42 93.17 o 10 2 0 157.96 184.89 68.27 o 11 2 0 3161.07 3472.62 153.92 o 12 2 0 2464.90 2480.04 326.75 o 13 2 0 26.10 216.08 137.03 o 14 2 0 31.11 -137.03 137.03 o -15 3 0 812.12 938.10 195.00 o -14 3 0 9.09 -47.08 152.84 o -13 3 0 101.79 124.94 75.78 o -12 3 0 234.31 258.67 60.73 o -11 3 0 469.86 372.14 63.24 o -10 3 0 877.15 1001.34 72.54 o -9 3 0 5167.77 5531.75 197.63 o -8 3 0 3956.77 4041.54 122.65 o -7 3 0 244.63 266.21 147.57 o -6 3 0 622.57 934.33 50.59 o -5 3 0 1008.38 791.97 76.42 o -4 3 0 3118.22 3529.13 123.85 o -3 3 0 1836.03 1884.78 100.13 o -2 3 0 644.59 551.39 26.31 o -1 3 0 22924.57 23443.50 406.20 o 0 3 0 127.63 602.44 26.35 o 1 3 0 2377.92 4244.65 87.52 o 2 3 0 14170.75 9747.56 182.60 o 3 3 0 7825.13 8316.91 190.85 o 4 3 0 25.76 358.31 27.12 o 5 3 0 137.49 207.70 40.99 o 6 3 0 14.29 33.06 39.00 o 7 3 0 226.08 213.44 49.38 o 8 3 0 163.88 58.75 50.21 o 9 3 0 3136.17 3298.22 160.54 o 10 3 0 3194.67 3169.24 179.74 o 11 3 0 20.53 125.90 49.19 o 12 3 0 52.01 70.38 79.05 o 13 3 0 417.87 353.11 147.57 o 14 3 0 79.30 63.24 158.11 o -15 4 0 310.95 969.72 247.70 o -14 4 0 63.17 -8.70 73.42 o -13 4 0 241.93 234.00 87.70 o -12 4 0 49.51 19.01 71.15 o -11 4 0 2281.27 2344.58 118.80 o -10 4 0 1349.60 1135.43 74.09 o -9 4 0 265.31 241.07 60.61 o -8 4 0 69.57 33.27 29.12 o -7 4 0 2.61 30.30 29.12 o -6 4 0 1591.33 1430.91 79.05 o -5 4 0 1311.91 1219.47 52.62 o -4 4 0 10930.07 11061.87 247.63 o -3 4 0 7300.09 7441.55 279.32 o -2 4 0 4131.91 4664.48 116.00 o -1 4 0 221.38 135.13 21.08 o 0 4 0 1146.23 802.93 42.16 o 1 4 0 4123.57 3964.87 83.79 o 2 4 0 1598.06 2988.22 68.87 o 3 4 0 1911.51 997.06 123.85 o 4 4 0 9771.80 12151.39 275.32 o 5 4 0 2677.24 3255.24 142.30 o 6 4 0 71.15 88.04 27.76 o 7 4 0 768.90 837.98 50.80 o 8 4 0 4990.08 4776.35 157.69 o 9 4 0 1108.33 1217.66 74.40 o 10 4 0 160.09 147.16 27.76 o 11 4 0 591.89 485.59 42.73 o 12 4 0 88.72 179.19 63.24 o 13 4 0 2.95 -52.70 131.76 o -15 5 0 0.42 110.67 137.03 o -14 5 0 34.43 104.98 89.59 o -13 5 0 463.84 873.41 104.99 o -12 5 0 1424.44 1487.00 139.66 o -11 5 0 622.16 525.02 73.78 o -10 5 0 90.03 69.95 71.15 o -9 5 0 402.20 370.97 110.67 o -8 5 0 15.85 -24.49 31.51 o -7 5 0 646.43 754.69 57.97 o -6 5 0 868.64 1017.54 56.54 o -5 5 0 10335.42 9364.88 213.44 o -4 5 0 3783.86 3766.82 223.98 o -3 5 0 1399.24 1486.54 137.03 o -2 5 0 614.54 670.55 102.77 o -1 5 0 1050.74 1269.91 55.34 o 0 5 0 1873.52 1252.36 39.00 o 1 5 0 26.25 32.79 16.46 o 2 5 0 5771.47 6884.60 155.99 o 3 5 0 898.09 1283.95 48.45 o 4 5 0 538.40 625.34 34.10 o 5 5 0 284.31 660.86 34.26 o 6 5 0 398.01 373.53 57.97 o 7 5 0 981.98 1097.96 131.76 o 8 5 0 113.31 98.87 47.43 o 9 5 0 860.07 793.09 73.78 o 10 5 0 312.79 432.49 34.10 o 11 5 0 7.53 -47.43 47.43 o 12 5 0 36.46 268.78 189.73 o 13 5 0 240.41 305.67 158.11 o -15 6 0 28.51 -179.19 200.27 o -14 6 0 419.69 247.70 126.49 o -13 6 0 2101.97 2312.89 458.51 o -12 6 0 2.24 -51.82 65.88 o -11 6 0 151.43 153.52 56.96 o -10 6 0 123.75 70.91 39.00 o -9 6 0 80.09 115.34 44.80 o -8 6 0 258.18 271.41 44.69 o -7 6 0 6761.55 6316.83 179.33 o -6 6 0 1401.26 1407.15 63.24 o -5 6 0 253.88 236.79 31.51 o -4 6 0 147.35 262.04 31.51 o -3 6 0 988.08 1082.46 46.47 o -2 6 0 1057.13 1607.42 58.24 o -1 6 0 212.66 254.73 22.36 o 0 6 0 5196.46 5621.71 119.08 o 1 6 0 14536.91 13500.15 251.36 o 2 6 0 355.72 491.75 27.76 o 3 6 0 1848.57 2768.75 82.31 o 4 6 0 494.17 626.52 60.61 o 5 6 0 328.50 303.62 31.62 o 6 6 0 83.53 63.24 23.57 o 7 6 0 631.49 597.42 36.61 o 8 6 0 1482.45 1491.56 113.31 o 9 6 0 491.75 507.92 104.35 o 10 6 0 17.23 -26.35 94.86 o 11 6 0 54.73 21.08 115.94 o 12 6 0 1000.69 743.10 195.00 o -15 7 0 309.45 200.27 147.57 o -14 7 0 472.75 368.92 147.57 o -13 7 0 939.81 1090.94 163.38 o -12 7 0 1344.96 1195.99 181.82 o -11 7 0 241.39 268.27 60.61 o -10 7 0 50.90 114.01 76.42 o -9 7 0 549.28 531.54 57.44 o -8 7 0 2025.44 2537.32 266.15 o -7 7 0 230.10 153.84 37.27 o -6 7 0 1321.84 1249.46 62.05 o -5 7 0 4452.38 4756.02 155.47 o -4 7 0 61.54 66.89 24.01 o -3 7 0 555.52 437.75 32.92 o -2 7 0 1154.27 1192.92 46.75 o -1 7 0 7194.65 6981.13 281.96 o 0 7 0 6224.54 6423.59 137.88 o 1 7 0 3825.00 4122.67 100.41 o 2 7 0 29.35 10.54 39.53 o 3 7 0 24.51 40.66 23.04 o 4 7 0 21.16 45.52 18.30 o 5 7 0 752.24 784.01 46.47 o 6 7 0 2276.16 1933.95 83.79 o 7 7 0 1246.70 1165.30 67.07 o 8 7 0 145.49 163.38 89.59 o 9 7 0 361.19 289.86 89.59 o 10 7 0 45.38 -36.89 105.40 o 11 7 0 577.40 495.40 179.19 o -15 8 0 660.35 621.89 168.65 o -14 8 0 951.13 685.13 158.11 o -13 8 0 491.61 205.54 168.65 o -12 8 0 30.04 -10.66 69.68 o -11 8 0 304.14 250.69 68.27 o -10 8 0 968.92 1043.24 87.52 o -9 8 0 576.37 685.34 115.94 o -8 8 0 4.07 36.61 35.26 o -7 8 0 3122.47 3679.34 135.07 o -6 8 0 1861.69 1935.75 87.36 o -5 8 0 0.30 18.82 34.26 o -4 8 0 49.11 10.54 36.89 o -3 8 0 541.18 502.80 36.71 o -2 8 0 1986.82 1921.56 70.89 o -1 8 0 7.33 44.19 42.16 o 0 8 0 690.64 557.20 36.89 o 1 8 0 47.53 35.45 20.24 o 2 8 0 177.67 144.01 21.44 o 3 8 0 896.66 1018.03 53.94 o 4 8 0 2865.48 2815.60 102.43 o 5 8 0 2298.28 2141.69 247.70 o 6 8 0 265.43 308.23 33.43 o 7 8 0 226.18 184.46 84.32 o 8 8 0 24.68 -57.97 57.97 o 9 8 0 95.28 -31.62 115.94 o 10 8 0 3.29 21.08 126.49 o 11 8 0 838.35 1106.75 184.46 o -14 9 0 48.80 68.51 131.76 o -13 9 0 159.27 173.92 121.22 o -12 9 0 126.58 75.98 78.56 o -11 9 0 765.25 867.14 108.85 o -10 9 0 17.82 -3.71 50.21 o -9 9 0 702.91 905.89 75.89 o -8 9 0 1929.15 2018.91 101.19 o -7 9 0 4.98 44.50 50.07 o -6 9 0 86.83 182.18 52.70 o -5 9 0 58.03 57.97 39.53 o -4 9 0 2240.35 1858.13 82.31 o -3 9 0 134.38 164.19 50.07 o -2 9 0 804.79 949.27 54.42 o -1 9 0 3871.51 3908.40 120.29 o 0 9 0 1563.41 1764.41 65.14 o 1 9 0 7.32 6.02 25.30 o 2 9 0 603.89 552.32 39.00 o 3 9 0 4648.14 5129.63 163.27 o 4 9 0 2880.06 2797.31 108.76 o 5 9 0 16.87 -2.17 30.22 o 6 9 0 652.73 832.70 100.13 o 7 9 0 83.70 163.38 89.59 o 8 9 0 0.15 57.97 79.05 o 9 9 0 274.36 511.21 131.76 o 10 9 0 1175.76 974.99 200.27 o -14 10 0 66.83 216.08 184.46 o -13 10 0 158.44 94.86 115.94 o -12 10 0 189.87 53.22 89.59 o -11 10 0 463.18 318.97 77.20 o -10 10 0 1572.28 2044.21 179.19 o -9 10 0 1237.76 1137.20 91.24 o -8 10 0 0.85 11.02 40.49 o -7 10 0 291.41 315.22 76.42 o -6 10 0 1004.01 691.26 61.40 o -5 10 0 622.94 654.99 51.77 o -4 10 0 143.15 151.87 37.95 o -3 10 0 3814.48 3560.24 118.55 o -2 10 0 2583.75 2909.16 106.35 o -1 10 0 197.40 150.20 33.54 o 0 10 0 204.23 198.56 29.81 o 1 10 0 138.45 265.11 52.70 o 2 10 0 2582.07 2844.20 116.00 o 3 10 0 114.74 21.08 52.70 o 4 10 0 1431.24 1428.23 115.94 o 5 10 0 454.02 558.64 89.59 o 6 10 0 74.35 121.22 84.32 o 7 10 0 218.67 358.38 105.40 o 8 10 0 537.87 511.21 179.19 o 9 10 0 1510.10 1702.28 242.43 o -13 11 0 5.03 147.57 147.57 o -12 11 0 717.80 627.16 137.03 o -11 11 0 1382.54 1398.89 143.15 o -10 11 0 85.02 125.93 68.20 o -9 11 0 12.35 -2.11 55.53 o -8 11 0 1184.66 1102.97 123.85 o -7 11 0 326.36 356.65 51.77 o -6 11 0 267.07 165.67 42.73 o -5 11 0 1682.51 1738.03 93.67 o -4 11 0 1986.06 2447.18 109.51 o -3 11 0 684.08 636.80 52.62 o -2 11 0 256.05 255.86 42.73 o -1 11 0 115.75 121.80 32.92 o 0 11 0 680.09 670.49 65.88 o 1 11 0 219.07 239.00 42.89 o 2 11 0 2456.98 2449.24 124.78 o 3 11 0 2084.30 2039.58 131.76 o 4 11 0 107.38 237.16 73.78 o 5 11 0 1.76 -36.89 68.51 o 6 11 0 33.42 15.81 73.78 o 7 11 0 474.90 553.37 147.57 o 8 11 0 662.36 753.64 184.46 o -13 12 0 782.77 606.08 163.38 o -12 12 0 537.47 664.05 158.11 o -11 12 0 15.86 39.89 88.57 o -10 12 0 481.87 605.94 98.43 o -9 12 0 574.50 735.88 85.71 o -8 12 0 2.42 46.15 68.51 o -7 12 0 563.03 489.44 76.42 o -6 12 0 2713.50 2824.84 130.38 o -5 12 0 1457.18 1671.30 94.97 o -4 12 0 292.38 192.15 42.89 o -3 12 0 44.19 162.83 44.80 o -2 12 0 269.60 244.57 39.00 o -1 12 0 113.11 148.88 48.67 o 0 12 0 75.95 38.65 37.71 o 1 12 0 2958.91 3344.88 142.34 o 2 12 0 774.73 694.21 73.21 o 3 12 0 76.10 89.59 68.51 o 4 12 0 0.54 -57.97 68.51 o 5 12 0 103.01 105.40 89.59 o 6 12 0 345.81 342.56 173.92 o 7 12 0 77.89 100.13 126.49 o -12 13 0 339.75 363.65 126.49 o -11 13 0 344.17 537.56 137.03 o -10 13 0 56.06 147.57 80.06 o -9 13 0 9.88 23.64 59.40 o -8 13 0 658.33 664.25 93.67 o -7 13 0 2510.92 2389.08 170.33 o -6 13 0 141.83 212.68 57.67 o -5 13 0 193.59 199.94 59.28 o -4 13 0 252.63 268.78 50.21 o -3 13 0 9.29 51.08 48.02 o -2 13 0 72.68 118.71 52.70 o -1 13 0 1054.71 1192.04 121.46 o 0 13 0 1669.28 1887.41 221.35 o 1 13 0 770.79 1077.28 90.85 o 2 13 0 21.93 -10.54 56.57 o 3 13 0 65.58 -121.22 121.22 o 4 13 0 821.67 779.99 115.94 o 5 13 0 0.60 -79.05 110.67 o -11 14 0 13.88 -105.40 105.40 o -10 14 0 18.42 263.51 105.40 o -9 14 0 779.80 646.32 98.70 o -8 14 0 42.91 -30.63 58.24 o -7 14 0 58.77 119.11 94.86 o -6 14 0 1170.13 1234.75 126.49 o -5 14 0 88.73 91.70 55.53 o -4 14 0 383.98 426.52 68.51 o -3 14 0 10.33 23.72 40.99 o -2 14 0 1816.47 1490.80 87.52 o -1 14 0 736.12 771.02 78.93 o 0 14 0 143.22 129.65 52.62 o 1 14 0 139.58 231.01 187.09 o 2 14 0 231.41 252.97 121.22 o 3 14 0 134.25 121.22 142.30 o 4 14 0 87.31 -105.40 121.22 o -9 15 0 0.34 68.51 100.13 o -8 15 0 409.28 221.35 89.59 o -7 15 0 713.24 664.05 126.49 o -6 15 0 55.70 31.46 57.44 o -5 15 0 175.32 152.84 65.88 o -4 15 0 160.26 48.75 51.77 o -3 15 0 848.89 620.02 171.28 o -2 15 0 0.16 -36.89 57.97 o -1 15 0 79.13 137.03 89.59 o 0 15 0 339.80 426.89 147.57 o 1 15 0 0.84 121.22 100.13 o 2 15 0 7.43 5.27 142.30 o 2 -16 1 83.57 -36.89 94.86 o 3 -16 1 932.62 890.67 142.30 o 4 -16 1 1323.19 1686.47 216.08 o 5 -16 1 5.61 -21.08 100.13 o -2 -15 1 217.69 432.16 173.92 o -1 -15 1 240.02 242.43 115.94 o 0 -15 1 11.98 36.89 84.32 o 1 -15 1 246.79 226.62 89.59 o 2 -15 1 2028.13 1729.60 118.80 o 3 -15 1 470.63 451.81 91.63 o 4 -15 1 49.60 114.72 102.77 o 5 -15 1 128.46 23.84 266.15 o 6 -15 1 456.19 593.72 98.28 o 7 -15 1 131.78 88.05 76.33 o 8 -15 1 407.06 400.54 158.11 o 9 -15 1 1139.07 1133.10 158.11 o -4 -14 1 396.04 569.18 158.11 o -3 -14 1 22.65 -100.13 158.11 o -2 -14 1 0.19 16.80 59.28 o -1 -14 1 59.34 30.66 60.73 o 0 -14 1 1437.46 1588.74 104.32 o 1 -14 1 438.07 654.41 82.68 o 2 -14 1 269.49 166.19 55.53 o 3 -14 1 362.05 307.55 66.22 o 4 -14 1 13.57 -13.18 48.45 o 5 -14 1 85.72 87.13 55.53 o 6 -14 1 104.96 126.92 108.04 o 7 -14 1 1238.97 1332.11 213.44 o 8 -14 1 1260.13 947.28 123.85 o 9 -14 1 60.33 1.76 104.99 o 10 -14 1 84.12 226.62 152.84 o -6 -13 1 657.55 600.81 158.11 o -5 -13 1 658.85 859.05 158.11 o -4 -13 1 12.24 -68.51 68.51 o -3 -13 1 366.46 447.97 100.13 o -2 -13 1 867.80 799.53 74.09 o -1 -13 1 1095.64 1104.69 92.53 o 0 -13 1 309.16 371.75 105.40 o 1 -13 1 447.78 341.31 192.36 o 2 -13 1 393.17 505.24 63.02 o 3 -13 1 8.14 29.67 68.51 o 4 -13 1 196.33 170.01 50.21 o 5 -13 1 454.07 561.64 70.51 o 6 -13 1 3820.82 3569.96 366.28 o 7 -13 1 329.22 408.97 80.85 o 8 -13 1 0.30 -27.10 63.24 o 9 -13 1 120.91 72.07 80.06 o 10 -13 1 35.42 -110.67 110.67 o 11 -13 1 22.95 -110.67 110.67 o 12 -13 1 329.64 279.32 147.57 o -7 -12 1 1716.12 1665.39 252.97 o -6 -12 1 490.27 906.48 200.27 o -5 -12 1 12.48 94.86 89.59 o -4 -12 1 371.05 247.70 84.32 o -3 -12 1 203.83 84.32 68.51 o -2 -12 1 486.12 378.23 58.24 o -1 -12 1 5.64 -30.81 41.92 o 0 -12 1 1723.60 1786.38 98.16 o 1 -12 1 644.04 530.59 59.40 o 2 -12 1 14.51 -4.58 115.94 o 3 -12 1 0.80 40.26 45.58 o 4 -12 1 1217.13 1068.43 75.78 o 5 -12 1 715.05 741.95 74.71 o 6 -12 1 36.70 -7.10 41.77 o 7 -12 1 404.84 435.23 92.23 o 8 -12 1 105.59 103.32 81.69 o 9 -12 1 58.86 208.59 97.50 o 10 -12 1 141.16 151.60 142.30 o 11 -12 1 954.04 1257.26 151.57 o 12 -12 1 750.86 779.99 179.19 o -8 -11 1 1037.52 1285.93 205.54 o -7 -11 1 88.85 -42.16 100.13 o -6 -11 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