# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' IN+5,5-DIMME-BIPY-2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 253.99 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.7276 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 10.9080 _cell_length_b 11.2087 _cell_length_c 13.3584 _cell_angle_alpha 90.000 _cell_angle_beta 107.211 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11311.54 11523.75 237.24 o 3 0 0 18888.63 18640.35 115.36 o 4 0 0 12505.15 11948.27 122.02 o 5 0 0 12440.71 11841.89 305.84 o 6 0 0 6463.50 6142.64 228.49 o 7 0 0 4987.41 4752.81 74.42 o 8 0 0 78.62 103.75 36.32 o 9 0 0 20280.81 20507.38 653.43 o 10 0 0 1356.97 1267.84 37.43 o 11 0 0 4106.66 4130.11 215.91 o 12 0 0 5448.71 5526.12 134.70 o 13 0 0 2326.19 2458.83 112.07 o 14 0 0 936.83 920.48 53.97 o 1 1 0 31729.53 33195.96 394.60 o 2 1 0 295.16 380.57 65.59 o 3 1 0 4371.96 4133.74 62.17 o 4 1 0 5143.63 4975.44 59.74 o 5 1 0 12044.48 12093.10 147.04 o 6 1 0 281.14 278.78 28.09 o 7 1 0 2668.11 2628.94 33.62 o 8 1 0 7562.21 7408.09 122.26 o 9 1 0 4972.83 4795.25 133.50 o 10 1 0 14901.89 14682.21 289.16 o 11 1 0 198.50 221.87 24.32 o 12 1 0 3622.72 3653.99 84.67 o 13 1 0 2025.02 2067.91 39.55 o 14 1 0 4239.23 4251.37 147.80 o 0 2 0 26634.54 28275.98 149.69 o 1 2 0 310.34 302.06 47.94 o 2 2 0 382.53 312.30 61.99 o 3 2 0 3987.20 3990.70 59.18 o 4 2 0 4259.01 4223.68 49.44 o 5 2 0 2846.12 3196.16 41.94 o 6 2 0 2103.40 1935.77 37.40 o 7 2 0 4.84 34.55 28.09 o 8 2 0 1831.34 1761.01 35.08 o 9 2 0 5380.37 5359.93 109.58 o 10 2 0 1922.47 2051.95 36.47 o 11 2 0 3082.98 3033.28 82.88 o 12 2 0 603.79 602.63 29.95 o 13 2 0 1293.51 1243.78 30.81 o 14 2 0 261.10 301.99 32.13 o 1 3 0 13456.21 14027.06 112.67 o 2 3 0 4779.54 4921.61 74.12 o 3 3 0 152.78 133.87 41.55 o 4 3 0 6.07 39.75 28.97 o 5 3 0 1431.36 1359.54 35.16 o 6 3 0 230.50 206.62 25.49 o 7 3 0 95.90 99.26 33.40 o 8 3 0 92.07 156.52 32.44 o 9 3 0 5.05 9.93 29.96 o 10 3 0 735.67 784.05 26.97 o 11 3 0 194.93 222.24 29.48 o 12 3 0 2.61 43.75 28.23 o 13 3 0 510.83 509.88 32.19 o 0 4 0 4519.43 4644.05 86.61 o 1 4 0 545.15 518.89 29.65 o 2 4 0 1.85 23.90 28.81 o 3 4 0 2.24 -3.89 24.99 o 4 4 0 296.30 328.00 27.09 o 5 4 0 380.25 400.59 26.49 o 6 4 0 1436.05 1477.98 42.89 o 7 4 0 176.94 213.38 32.44 o 8 4 0 70.06 111.32 31.43 o 9 4 0 84.68 67.09 27.81 o 10 4 0 0.30 140.07 32.51 o 11 4 0 10.95 24.32 80.50 o 12 4 0 97.83 147.85 31.93 o 13 4 0 604.98 601.60 34.57 o 1 5 0 12682.68 12551.57 196.91 o 2 5 0 172.54 165.85 30.45 o 3 5 0 12490.58 12975.30 218.46 o 4 5 0 6796.09 6980.52 102.06 o 5 5 0 6201.54 6178.02 121.03 o 6 5 0 3404.15 3335.36 59.99 o 7 5 0 207.85 178.41 27.82 o 8 5 0 5921.66 5942.68 208.30 o 9 5 0 25.93 27.60 22.85 o 10 5 0 1778.31 1809.74 50.04 o 11 5 0 230.76 221.03 26.44 o 12 5 0 721.94 788.66 77.22 o 13 5 0 1367.98 1308.49 90.09 o 0 6 0 25398.04 25250.40 618.48 o 1 6 0 9.72 -23.40 27.11 o 2 6 0 7782.04 7858.18 132.16 o 3 6 0 7562.42 7870.14 126.28 o 4 6 0 9685.75 9514.65 86.99 o 5 6 0 9997.78 9835.97 70.74 o 6 6 0 2869.12 2970.11 43.56 o 7 6 0 3695.91 3592.20 61.61 o 8 6 0 4.13 -30.81 66.55 o 9 6 0 8158.41 8371.29 102.02 o 10 6 0 355.14 337.31 37.42 o 11 6 0 2028.13 2041.53 35.70 o 12 6 0 212.64 261.53 59.53 o 13 6 0 2218.98 2188.53 34.35 o 1 7 0 11449.48 11860.97 188.27 o 2 7 0 7.01 28.13 23.69 o 3 7 0 4336.16 4710.13 72.53 o 4 7 0 1102.62 1086.97 26.50 o 5 7 0 6998.74 6949.97 81.06 o 6 7 0 260.12 287.97 30.50 o 7 7 0 1220.12 1177.03 30.46 o 8 7 0 4757.16 5047.24 147.57 o 9 7 0 1627.66 1697.30 76.11 o 10 7 0 7184.96 7285.59 141.72 o 11 7 0 115.60 114.98 26.47 o 12 7 0 2896.52 2903.96 49.13 o 0 8 0 27088.88 28109.11 998.45 o 1 8 0 2.45 38.02 24.01 o 2 8 0 8296.83 8177.12 143.89 o 3 8 0 2791.39 2809.90 28.05 o 4 8 0 4460.75 4388.59 115.04 o 5 8 0 494.40 559.72 25.94 o 6 8 0 2607.32 2472.82 31.67 o 7 8 0 599.00 570.07 23.98 o 8 8 0 99.37 168.34 33.03 o 9 8 0 8074.73 8141.29 535.44 o 10 8 0 82.43 109.11 22.53 o 11 8 0 2100.36 2135.26 212.95 o 12 8 0 925.71 905.16 47.27 o 1 9 0 13696.79 13696.70 245.24 o 2 9 0 3117.18 3257.09 64.05 o 3 9 0 208.68 264.18 25.36 o 4 9 0 5374.78 5398.77 86.13 o 5 9 0 2133.17 2051.03 30.41 o 6 9 0 782.34 814.23 30.10 o 7 9 0 652.65 616.17 23.51 o 8 9 0 4490.21 4470.18 35.80 o 9 9 0 48.11 181.14 31.74 o 10 9 0 2943.84 2889.20 30.02 o 11 9 0 127.24 172.90 68.54 o 0 10 0 1821.16 1864.99 28.32 o 1 10 0 45.67 72.48 33.88 o 2 10 0 924.36 975.50 78.97 o 3 10 0 824.12 771.34 40.16 o 4 10 0 1.59 -10.80 20.20 o 5 10 0 15.83 -23.27 51.67 o 6 10 0 193.79 204.88 26.01 o 7 10 0 62.08 65.66 27.48 o 8 10 0 725.85 834.84 125.85 o 9 10 0 701.74 734.67 32.87 o 10 10 0 201.63 183.08 22.96 o 1 11 0 19.97 -10.67 40.46 o 2 11 0 236.32 181.71 20.86 o 3 11 0 1126.24 1145.44 24.70 o 4 11 0 847.00 884.73 38.40 o 5 11 0 255.24 312.27 58.71 o 6 11 0 1773.85 1724.93 40.35 o 7 11 0 135.11 169.40 32.69 o 8 11 0 998.91 1030.22 46.98 o 9 11 0 307.38 332.02 49.94 o 0 12 0 31.53 41.05 51.79 o 1 12 0 701.93 709.02 39.23 o 2 12 0 197.89 212.61 17.74 o 3 12 0 212.36 213.68 33.19 o 4 12 0 2529.37 2472.87 77.41 o 5 12 0 568.60 568.21 27.63 o 6 12 0 891.20 818.25 31.27 o 7 12 0 91.78 57.16 22.83 o 8 12 0 106.55 185.63 37.71 o 1 13 0 2225.16 2203.38 25.62 o 2 13 0 7.24 26.10 28.37 o 3 13 0 1431.63 1403.58 30.98 o 4 13 0 1216.01 1290.64 39.13 o 5 13 0 4029.32 4020.52 89.91 o 6 13 0 1685.31 1740.05 52.83 o 7 13 0 446.72 465.28 29.66 o 0 14 0 6605.49 6617.22 215.65 o 1 14 0 219.10 178.59 49.42 o 2 14 0 5118.18 5053.61 90.20 o 3 14 0 1948.98 2034.56 60.45 o 4 14 0 4171.92 3978.00 163.14 o 5 14 0 4707.10 4486.58 74.44 o 1 15 0 4524.67 4299.84 94.54 o 2 15 0 205.87 293.36 34.76 o 3 15 0 3206.34 3061.46 288.54 o -14 1 1 461.10 475.02 52.73 o -13 1 1 9.61 32.68 25.99 o -12 1 1 615.73 698.11 61.96 o -11 1 1 1207.20 1240.25 26.42 o -10 1 1 178.95 217.45 33.57 o -9 1 1 2326.45 2333.38 33.72 o -8 1 1 2.56 10.37 23.54 o -7 1 1 2655.70 2576.04 33.92 o -6 1 1 2228.06 2075.07 29.49 o -5 1 1 11976.61 11718.60 79.04 o -4 1 1 6018.41 5735.80 43.46 o -3 1 1 5562.11 5186.02 55.29 o -2 1 1 1299.00 1296.37 47.61 o -1 1 1 63.66 65.86 61.81 o 0 1 1 4292.82 4822.79 168.09 o 1 1 1 212.02 253.01 74.07 o 2 1 1 11958.09 11940.62 104.89 o 3 1 1 7291.08 7591.77 112.26 o 4 1 1 3467.41 3552.41 43.40 o 5 1 1 4439.39 4684.35 85.62 o 6 1 1 25.79 51.54 26.90 o 7 1 1 3764.59 3627.58 63.99 o 8 1 1 0.42 25.68 27.47 o 9 1 1 997.59 973.55 28.28 o 10 1 1 82.05 93.51 25.69 o 11 1 1 235.16 231.95 28.86 o 12 1 1 1275.91 1288.09 31.71 o 13 1 1 424.84 388.22 29.68 o -14 2 1 2207.94 2248.58 76.15 o -13 2 1 291.10 330.38 29.81 o -12 2 1 1226.87 1248.17 29.21 o -11 2 1 0.03 34.69 28.11 o -10 2 1 4896.34 5016.03 120.97 o -9 2 1 964.93 885.56 31.19 o -8 2 1 5454.66 5543.70 42.55 o -7 2 1 3562.04 3466.28 45.85 o -6 2 1 1077.40 1011.02 33.67 o -5 2 1 6596.74 6187.67 52.11 o -4 2 1 4153.73 4053.63 62.20 o -3 2 1 356.11 358.60 47.69 o -2 2 1 2834.15 2981.81 89.00 o -1 2 1 22216.38 22558.57 685.33 o 0 2 1 542.55 627.25 53.19 o 1 2 1 28780.45 29888.08 491.45 o 2 2 1 1025.35 982.91 56.73 o 3 2 1 12147.18 12165.91 72.31 o 4 2 1 8073.02 8307.91 59.19 o 5 2 1 6243.35 6067.98 45.91 o 6 2 1 104.18 104.74 33.07 o 7 2 1 275.60 341.26 33.03 o 8 2 1 1468.98 1378.32 50.59 o 9 2 1 5360.34 5138.55 58.22 o 10 2 1 3162.91 3235.94 57.98 o 11 2 1 0.48 13.67 27.09 o 12 2 1 2779.34 2843.49 65.23 o 13 2 1 815.95 798.64 36.11 o -14 3 1 385.32 399.35 66.94 o -13 3 1 2604.10 2585.13 68.55 o -12 3 1 441.56 457.95 33.01 o -11 3 1 7001.82 6928.94 199.68 o -10 3 1 1069.81 1033.82 26.97 o -9 3 1 13167.76 13117.66 197.33 o -8 3 1 510.75 540.65 30.79 o -7 3 1 885.83 835.93 39.37 o -6 3 1 11736.67 11212.23 47.40 o -5 3 1 43.92 3.85 31.46 o -4 3 1 1721.77 1614.63 43.27 o -3 3 1 8.88 29.07 29.43 o -2 3 1 2539.05 2553.32 64.94 o -1 3 1 277.46 285.48 38.68 o 0 3 1 34071.23 34477.33 396.46 o 1 3 1 341.07 407.03 38.41 o 2 3 1 16522.50 16952.84 235.78 o 3 3 1 4444.95 4199.31 46.72 o 4 3 1 16310.21 16223.05 274.17 o 5 3 1 38.94 -9.98 30.52 o 6 3 1 4814.45 4873.89 106.74 o 7 3 1 4212.28 4167.44 96.40 o 8 3 1 1907.91 1899.47 32.97 o 9 3 1 5775.43 6074.69 189.68 o 10 3 1 2761.31 2877.16 57.61 o 11 3 1 3684.08 3691.02 129.66 o 12 3 1 1020.80 1007.29 29.29 o 13 3 1 7521.70 7768.38 281.88 o -13 4 1 2271.79 2268.44 33.74 o -12 4 1 913.35 917.01 23.95 o -11 4 1 476.11 502.89 23.89 o -10 4 1 14628.41 14807.25 214.70 o -9 4 1 209.09 171.28 20.49 o -8 4 1 14175.32 14105.42 302.78 o -7 4 1 3661.70 3637.74 97.29 o -6 4 1 6768.97 6603.44 114.96 o -5 4 1 10488.07 10172.04 200.01 o -4 4 1 12746.41 12223.64 388.31 o -3 4 1 5858.96 6178.98 119.45 o -2 4 1 708.71 747.96 38.59 o -1 4 1 64511.26 65024.01 196.18 o 0 4 1 5893.26 6051.86 50.82 o 1 4 1 44057.91 45146.56 670.63 o 2 4 1 6326.23 6456.33 77.62 o 3 4 1 16222.52 15390.99 243.10 o 4 4 1 19226.45 19742.62 147.51 o 5 4 1 9165.16 9507.02 160.71 o 6 4 1 2180.14 2311.01 104.49 o 7 4 1 2.89 110.11 44.48 o 8 4 1 7159.36 7215.73 191.56 o 9 4 1 2030.62 2035.70 37.27 o 10 4 1 8366.21 8106.88 396.61 o 11 4 1 606.53 563.01 33.26 o 12 4 1 4452.91 4512.71 210.55 o 13 4 1 1479.90 1360.41 32.50 o -13 5 1 665.84 647.90 25.17 o -12 5 1 1745.86 1625.25 35.56 o -11 5 1 3463.75 3353.40 34.48 o -10 5 1 244.85 199.90 25.15 o -9 5 1 16222.14 16089.16 311.52 o -8 5 1 8.71 22.90 25.35 o -7 5 1 5720.52 5811.51 160.69 o -6 5 1 7416.72 7186.20 137.79 o -5 5 1 2398.77 2330.73 84.14 o -4 5 1 2412.50 2462.82 37.63 o -3 5 1 881.21 993.98 27.90 o -2 5 1 12892.23 13143.32 253.83 o -1 5 1 1780.80 1822.66 36.65 o 0 5 1 57480.31 61488.85 173.48 o 1 5 1 682.55 885.22 27.42 o 2 5 1 21936.28 23056.99 332.71 o 3 5 1 22917.09 23046.61 474.37 o 4 5 1 15288.29 15640.73 164.76 o 5 5 1 5318.61 5335.00 137.86 o 6 5 1 258.56 297.58 30.41 o 7 5 1 1332.72 1403.99 42.85 o 8 5 1 281.87 339.70 27.30 o 9 5 1 5306.00 5179.42 91.78 o 10 5 1 218.61 221.96 32.87 o 11 5 1 2180.46 2208.75 121.66 o 12 5 1 1964.52 2108.11 71.88 o 13 5 1 1857.75 1850.91 38.32 o -13 6 1 275.19 330.97 33.38 o -12 6 1 200.00 273.22 37.42 o -11 6 1 16.92 12.73 41.52 o -10 6 1 3919.10 3890.26 113.99 o -9 6 1 1012.84 1003.23 35.72 o -8 6 1 1533.38 1519.09 60.11 o -7 6 1 1621.08 1658.05 34.54 o -6 6 1 1.07 10.84 32.15 o -5 6 1 2088.04 2172.50 36.88 o -4 6 1 661.87 582.47 28.35 o -3 6 1 1275.39 1476.98 44.45 o -2 6 1 524.00 596.51 30.17 o -1 6 1 2625.05 2858.89 42.32 o 0 6 1 1145.70 1196.60 42.61 o 1 6 1 2612.97 2652.86 38.06 o 2 6 1 492.00 425.87 23.38 o 3 6 1 3313.99 3222.14 87.30 o 4 6 1 640.27 708.37 27.65 o 5 6 1 4563.05 4477.01 50.49 o 6 6 1 37.18 190.75 36.73 o 7 6 1 1019.53 984.12 49.09 o 8 6 1 600.00 624.37 163.18 o 9 6 1 2885.42 2872.73 33.92 o 10 6 1 1383.89 1409.58 97.11 o 11 6 1 256.22 318.59 32.69 o 12 6 1 3356.85 3396.88 40.48 o -12 7 1 9.29 69.19 42.33 o -11 7 1 24.04 82.22 58.88 o -10 7 1 7.15 11.63 71.36 o -9 7 1 529.83 607.69 37.39 o -8 7 1 252.58 245.43 23.22 o -7 7 1 188.62 167.72 22.49 o -6 7 1 1474.70 1466.24 40.49 o -5 7 1 1.57 16.73 39.87 o -4 7 1 1.50 -12.88 30.43 o -3 7 1 167.61 216.92 22.83 o -2 7 1 631.24 610.50 28.04 o -1 7 1 328.36 382.88 27.24 o 0 7 1 782.23 779.98 29.12 o 1 7 1 41.67 13.34 21.73 o 2 7 1 129.61 186.36 22.05 o 3 7 1 1555.14 1501.91 29.43 o 4 7 1 83.30 37.89 28.53 o 5 7 1 1270.07 1291.69 35.74 o 6 7 1 2157.60 2119.32 60.73 o 7 7 1 2144.11 1928.80 39.40 o 8 7 1 390.34 435.45 42.82 o 9 7 1 0.41 -27.34 31.93 o 10 7 1 412.76 431.17 32.97 o 11 7 1 263.04 287.90 32.80 o 12 7 1 102.96 129.25 34.85 o -12 8 1 679.58 645.87 128.19 o -11 8 1 1085.04 1144.82 29.41 o -10 8 1 192.41 274.03 76.18 o -9 8 1 250.27 287.77 26.15 o -8 8 1 762.23 659.50 23.95 o -7 8 1 2107.94 2009.07 74.35 o -6 8 1 105.04 146.78 42.11 o -5 8 1 316.53 325.94 25.96 o -4 8 1 2098.28 2065.12 45.53 o -3 8 1 2049.06 2206.01 41.47 o -2 8 1 764.44 716.01 28.39 o -1 8 1 481.19 462.06 27.98 o 0 8 1 0.03 -19.38 26.61 o 1 8 1 657.97 580.69 24.74 o 2 8 1 4.71 28.91 23.19 o 3 8 1 113.07 186.76 42.49 o 4 8 1 35.35 45.51 25.53 o 5 8 1 3680.30 3635.37 51.10 o 6 8 1 79.43 91.01 24.55 o 7 8 1 954.85 886.46 69.97 o 8 8 1 1154.69 1130.53 28.63 o 9 8 1 81.55 92.97 35.15 o 10 8 1 448.28 401.02 27.43 o 11 8 1 219.69 241.57 33.45 o -11 9 1 838.40 789.19 33.69 o -10 9 1 370.40 435.71 51.40 o -9 9 1 2584.03 2753.37 32.15 o -8 9 1 106.06 175.27 28.57 o -7 9 1 2875.70 2931.24 69.60 o -6 9 1 910.60 919.45 26.13 o -5 9 1 7338.83 7145.99 116.68 o -4 9 1 4726.51 4765.30 114.93 o -3 9 1 2340.62 2320.37 38.34 o -2 9 1 8092.38 8122.93 206.95 o -1 9 1 20.55 23.59 23.40 o 0 9 1 5073.25 5375.77 104.63 o 1 9 1 314.52 342.64 23.84 o 2 9 1 7133.99 7016.18 129.58 o 3 9 1 5224.94 5342.42 125.13 o 4 9 1 6839.61 6867.13 225.57 o 5 9 1 1933.83 1938.73 66.74 o 6 9 1 2735.87 2699.52 63.18 o 7 9 1 5642.88 5549.06 122.25 o 8 9 1 22.69 0.13 33.62 o 9 9 1 3655.93 3666.24 198.29 o 10 9 1 34.24 150.37 32.04 o 11 9 1 1179.43 1117.06 44.02 o -11 10 1 57.32 38.97 55.50 o -10 10 1 6064.94 6033.51 129.95 o -9 10 1 354.02 426.63 35.28 o -8 10 1 5794.14 5735.36 142.18 o -7 10 1 364.10 370.25 29.87 o -6 10 1 4996.37 4993.22 99.20 o -5 10 1 4906.87 4908.35 93.45 o -4 10 1 7439.34 7416.11 212.92 o -3 10 1 11189.27 10828.59 231.30 o -2 10 1 399.84 401.64 35.31 o -1 10 1 17519.91 17357.39 280.59 o 0 10 1 5.85 12.80 26.29 o 1 10 1 10231.88 10267.88 213.70 o 2 10 1 1555.60 1575.21 84.67 o 3 10 1 6932.85 7055.33 175.93 o 4 10 1 4429.77 4601.36 130.83 o 5 10 1 7444.28 7321.05 184.68 o 6 10 1 2890.90 3018.09 58.53 o 7 10 1 108.13 195.73 53.94 o 8 10 1 6987.96 6988.41 112.85 o 9 10 1 1.16 89.48 59.85 o 10 10 1 1834.90 1853.86 35.68 o -10 11 1 36.08 73.46 67.92 o -9 11 1 5304.13 5361.17 274.76 o -8 11 1 80.78 195.77 52.93 o -7 11 1 1028.85 1041.55 75.99 o -6 11 1 3844.87 3898.69 153.75 o -5 11 1 2469.72 2405.33 24.77 o -4 11 1 1319.43 1413.43 39.73 o -3 11 1 1074.45 1030.33 33.20 o -2 11 1 4421.36 4394.67 117.68 o -1 11 1 0.46 2.24 20.12 o 0 11 1 9044.61 8992.73 194.33 o 1 11 1 622.55 604.65 35.62 o 2 11 1 4276.62 4095.49 140.76 o 3 11 1 1902.68 1843.60 32.30 o 4 11 1 6201.25 6123.41 181.88 o 5 11 1 604.74 674.99 46.51 o 6 11 1 1784.12 1760.26 78.27 o 7 11 1 2898.26 2904.93 66.69 o 8 11 1 400.27 411.85 23.47 o 9 11 1 4434.39 4406.29 190.13 o -9 12 1 133.06 47.04 31.02 o -8 12 1 1344.56 1308.99 25.35 o -7 12 1 846.47 870.13 22.88 o -6 12 1 410.66 453.58 26.61 o -5 12 1 2471.35 2462.03 78.14 o -4 12 1 966.67 988.17 27.41 o -3 12 1 415.16 399.45 19.22 o -2 12 1 71.98 123.46 22.60 o -1 12 1 2720.54 2725.05 61.14 o 0 12 1 238.53 366.06 47.94 o 1 12 1 3573.56 3544.43 147.01 o 2 12 1 223.28 236.67 20.07 o 3 12 1 2010.00 2094.71 102.75 o 4 12 1 454.83 464.38 32.81 o 5 12 1 1905.94 1822.97 65.83 o 6 12 1 26.17 19.08 23.38 o 7 12 1 836.89 867.32 30.78 o 8 12 1 2819.13 2766.65 29.65 o -7 13 1 156.23 248.36 32.21 o -6 13 1 672.05 633.46 31.91 o -5 13 1 1017.54 960.44 60.22 o -4 13 1 115.91 241.69 84.96 o -3 13 1 298.84 274.56 20.86 o -2 13 1 1346.35 1364.11 42.64 o -1 13 1 43.43 98.27 43.85 o 0 13 1 4370.35 4337.93 140.76 o 1 13 1 1.35 29.69 36.88 o 2 13 1 1490.52 1473.10 70.47 o 3 13 1 1730.61 1886.21 72.59 o 4 13 1 1401.22 1416.98 37.85 o 5 13 1 567.28 631.04 66.68 o 6 13 1 152.51 194.95 29.34 o 7 13 1 259.84 286.57 50.55 o -6 14 1 7.51 -47.01 47.01 o -5 14 1 16.60 43.39 30.60 o -4 14 1 2.39 55.73 20.80 o -3 14 1 310.58 354.59 23.35 o -2 14 1 410.35 460.13 21.80 o -1 14 1 64.84 105.77 28.95 o 0 14 1 182.93 239.03 23.21 o 1 14 1 493.11 483.32 29.94 o 2 14 1 385.17 394.63 21.37 o 3 14 1 129.64 176.24 23.74 o 4 14 1 418.82 456.78 36.15 o 5 14 1 75.82 120.41 56.60 o -3 15 1 1298.87 1247.36 64.81 o -2 15 1 1915.38 1763.95 73.65 o -1 15 1 0.46 57.49 21.46 o 0 15 1 1404.19 1334.19 34.79 o 1 15 1 181.62 196.52 25.06 o 2 15 1 687.09 632.87 22.54 o -14 0 2 567.92 544.06 50.39 o -13 0 2 788.97 815.68 34.71 o -12 0 2 676.42 691.75 41.10 o -11 0 2 11530.88 11412.94 228.33 o -10 0 2 1719.51 1666.19 38.44 o -9 0 2 19265.98 18759.95 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