# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_F_calc_maximum 243.49 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.8255 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.8090 _cell_length_b 11.8780 _cell_length_c 20.1780 _cell_angle_alpha 92.656 _cell_angle_beta 94.611 _cell_angle_gamma 90.158 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10426.12 6505.24 620.36 o 3 0 0 1.85 54.43 20.52 o 4 0 0 9005.87 9010.45 209.60 o 5 0 0 6.31 1.54 8.49 o 6 0 0 4583.24 4452.71 159.46 o 7 0 0 0.06 8.94 11.56 o 8 0 0 110.44 198.24 72.73 o 9 0 0 9.90 71.31 24.19 o 10 0 0 86.15 247.03 25.33 o -10 1 0 376.23 460.48 52.44 o -9 1 0 0.01 9.41 21.89 o -8 1 0 250.45 318.13 38.92 o -7 1 0 188.37 237.21 40.26 o -6 1 0 59.48 46.79 32.55 o -5 1 0 518.61 530.76 33.27 o -4 1 0 1482.13 1648.88 19.79 o -3 1 0 410.06 342.37 21.45 o -2 1 0 1719.58 1882.50 125.18 o 2 1 0 3408.15 3097.22 135.26 o 3 1 0 967.70 856.68 43.00 o 4 1 0 1270.55 1342.76 47.00 o 5 1 0 255.05 253.17 27.44 o 6 1 0 130.12 120.74 22.98 o 7 1 0 341.93 345.47 31.41 o 8 1 0 297.73 381.41 46.22 o 9 1 0 0.80 99.06 60.45 o 10 1 0 393.56 423.60 24.61 o -10 2 0 3.04 52.70 71.66 o -9 2 0 22.34 92.81 24.32 o -8 2 0 1632.69 1533.50 110.17 o -7 2 0 50.94 19.38 27.11 o -6 2 0 232.51 243.01 29.29 o -5 2 0 2.37 0.40 27.11 o -4 2 0 1151.90 1076.90 70.94 o -3 2 0 5226.50 5369.60 220.19 o -2 2 0 59285.67 55396.69 2084.96 o 2 2 0 54103.80 55594.07 1605.90 o 3 2 0 4916.01 4741.04 208.41 o 4 2 0 1129.23 952.78 61.88 o 5 2 0 5.13 48.88 22.33 o 6 2 0 416.52 378.85 21.87 o 7 2 0 2.52 36.14 16.88 o 8 2 0 1157.10 1082.36 28.50 o 9 2 0 15.10 26.32 37.12 o 10 2 0 5.43 80.82 48.26 o -10 3 0 11.26 27.09 35.29 o -9 3 0 42.57 157.88 39.14 o -8 3 0 283.22 307.40 35.71 o -7 3 0 261.38 396.21 38.06 o -6 3 0 554.05 489.22 51.94 o -5 3 0 29.22 24.62 9.13 o -4 3 0 2253.53 2467.44 48.83 o -3 3 0 178.14 189.95 15.06 o -2 3 0 9320.64 9505.44 173.85 o -1 3 0 10775.01 10675.84 221.83 o 0 3 0 52.51 372.47 79.24 o 1 3 0 8442.30 8535.59 220.22 o 2 3 0 11743.25 12467.74 158.41 o 3 3 0 253.71 346.36 24.22 o 4 3 0 2377.03 2564.83 54.15 o 5 3 0 28.76 27.94 16.23 o 6 3 0 958.87 868.88 67.83 o 7 3 0 68.76 73.07 18.09 o 8 3 0 511.05 509.66 25.63 o 9 3 0 0.28 19.52 49.11 o 10 3 0 1.57 107.29 44.68 o -9 4 0 3.21 -1.69 29.53 o -8 4 0 246.48 286.45 21.11 o -7 4 0 0.09 8.15 22.26 o -6 4 0 1061.15 1066.74 58.42 o -5 4 0 2.12 3.22 9.52 o -4 4 0 9081.42 9332.83 368.69 o -3 4 0 67.10 106.10 16.16 o -2 4 0 5819.66 5450.31 155.25 o -1 4 0 156.59 129.99 15.49 o 0 4 0 24880.67 24576.59 508.86 o 1 4 0 66.57 62.37 15.35 o 2 4 0 8928.31 8873.67 384.46 o 3 4 0 34.55 57.41 52.26 o 4 4 0 14846.35 15859.85 237.52 o 5 4 0 25.26 40.84 16.60 o 6 4 0 1573.52 1570.61 58.70 o 7 4 0 65.35 104.22 39.12 o 8 4 0 316.58 307.48 22.07 o 9 4 0 18.11 -13.64 25.87 o 10 4 0 169.80 70.40 52.94 o -8 5 0 129.96 98.68 15.44 o -7 5 0 0.82 -10.35 11.38 o -6 5 0 2.16 14.35 27.83 o -5 5 0 25.47 41.61 16.01 o -4 5 0 4915.73 5162.48 121.55 o -3 5 0 4997.95 5087.63 170.17 o -2 5 0 8.21 -6.21 15.70 o -1 5 0 273.22 268.35 9.21 o 0 5 0 88.57 73.85 9.35 o 1 5 0 19.52 52.73 16.34 o 2 5 0 234.07 202.98 10.15 o 3 5 0 6875.93 7293.76 130.58 o 4 5 0 4445.03 4666.40 64.24 o 5 5 0 65.07 134.81 22.20 o 6 5 0 5.74 27.38 20.62 o 7 5 0 42.63 84.43 27.37 o 8 5 0 138.71 210.50 35.33 o 9 5 0 222.11 204.52 64.71 o -9 6 0 0.91 29.51 31.00 o -8 6 0 198.06 206.17 81.31 o -7 6 0 164.63 215.35 33.66 o -6 6 0 2158.79 2227.08 126.27 o -5 6 0 151.77 161.81 24.09 o -4 6 0 1014.73 905.76 18.23 o -3 6 0 21.94 47.89 9.40 o -2 6 0 2118.53 1972.14 24.90 o -1 6 0 2972.17 3095.12 53.03 o 0 6 0 1662.85 1510.25 41.56 o 1 6 0 882.04 804.77 18.66 o 2 6 0 5082.16 5106.66 96.26 o 3 6 0 186.32 215.64 23.65 o 4 6 0 1044.25 1152.56 20.43 o 5 6 0 28.39 77.16 54.15 o 6 6 0 1806.34 1822.53 56.55 o 7 6 0 277.07 371.65 35.91 o 8 6 0 43.97 26.26 35.96 o 9 6 0 20.12 19.16 71.27 o -8 7 0 7.41 -27.16 18.11 o -7 7 0 35.30 29.87 23.26 o -6 7 0 632.96 759.86 38.97 o -5 7 0 716.80 705.71 37.15 o -4 7 0 234.29 201.70 25.10 o -3 7 0 371.43 314.55 16.22 o -2 7 0 122.08 114.32 21.19 o -1 7 0 155.26 163.24 18.57 o 0 7 0 83.20 132.42 24.80 o 1 7 0 1476.61 1520.60 36.60 o 2 7 0 1314.71 1235.29 42.30 o 3 7 0 136.57 115.44 23.56 o 4 7 0 229.79 208.97 22.45 o 5 7 0 644.21 638.04 42.50 o 6 7 0 777.41 818.09 44.55 o 7 7 0 51.72 160.33 14.90 o 8 7 0 30.49 26.33 28.85 o 9 7 0 7.28 7.28 21.17 o -8 8 0 561.32 569.28 42.31 o -7 8 0 242.55 197.60 17.06 o -6 8 0 445.35 476.47 21.04 o -5 8 0 423.64 522.49 23.92 o -4 8 0 689.10 880.48 49.42 o -3 8 0 41.95 116.39 24.09 o -2 8 0 2606.46 2597.72 65.56 o -1 8 0 1594.67 1591.39 40.63 o 0 8 0 1646.64 1604.98 34.07 o 1 8 0 82.39 57.83 26.67 o 2 8 0 4709.44 4734.20 109.97 o 3 8 0 1575.40 1493.13 56.99 o 4 8 0 3195.11 3626.35 139.27 o 5 8 0 2251.98 2399.40 46.14 o 6 8 0 177.12 268.62 35.72 o 7 8 0 3.68 -5.12 26.15 o 8 8 0 673.66 613.86 27.43 o -8 9 0 60.45 61.46 50.77 o -7 9 0 267.18 160.30 22.00 o -6 9 0 109.53 159.24 22.71 o -5 9 0 1061.11 1064.00 47.49 o -4 9 0 31.30 74.59 42.40 o -3 9 0 101.96 140.46 27.08 o -2 9 0 68.66 14.72 12.49 o -1 9 0 627.07 650.54 17.68 o 0 9 0 29.33 14.78 14.28 o 1 9 0 1373.38 1315.17 40.09 o 2 9 0 391.19 389.73 17.85 o 3 9 0 7.26 7.47 15.14 o 4 9 0 516.50 481.47 97.42 o 5 9 0 98.89 143.21 28.72 o 6 9 0 118.17 126.22 15.43 o 7 9 0 59.68 17.46 25.13 o 8 9 0 62.09 -56.06 52.56 o -7 10 0 265.95 205.05 75.61 o -6 10 0 505.57 576.22 49.85 o -5 10 0 0.17 35.10 16.30 o -4 10 0 1625.19 1618.46 67.50 o -3 10 0 3.90 48.29 23.18 o -2 10 0 370.46 488.73 42.73 o -1 10 0 2.94 56.27 32.68 o 0 10 0 1767.67 1936.05 50.40 o 1 10 0 610.33 622.52 33.08 o 2 10 0 1407.15 1394.25 22.44 o 3 10 0 329.11 358.97 19.38 o 4 10 0 109.67 279.26 84.04 o 5 10 0 307.98 350.80 23.27 o 6 10 0 138.79 364.50 101.10 o 7 10 0 315.94 367.42 103.96 o -6 11 0 151.10 96.99 48.81 o -5 11 0 65.83 1.48 27.14 o -4 11 0 107.90 144.58 49.35 o -3 11 0 532.40 616.34 28.73 o -2 11 0 9.01 55.33 15.09 o -1 11 0 108.95 97.47 31.93 o 0 11 0 415.20 423.67 16.50 o 1 11 0 402.51 413.71 22.46 o 2 11 0 54.05 109.44 18.81 o 3 11 0 1473.19 1385.99 53.47 o 4 11 0 297.17 310.71 23.42 o 5 11 0 70.25 121.77 52.41 o 6 11 0 13.22 -9.18 46.15 o -5 12 0 0.72 -44.07 29.38 o -4 12 0 484.02 382.87 70.55 o -3 12 0 7.71 91.11 38.21 o -2 12 0 721.86 745.21 41.08 o -1 12 0 40.95 103.12 54.24 o 0 12 0 526.29 542.82 54.59 o 1 12 0 206.57 288.38 47.66 o 2 12 0 515.69 581.52 17.06 o 3 12 0 248.78 337.60 39.46 o 4 12 0 163.09 103.91 42.10 o 5 12 0 211.33 226.28 34.58 o -4 13 0 24.65 17.02 41.29 o -3 13 0 70.96 75.53 78.66 o -2 13 0 1.29 16.93 52.44 o -1 13 0 584.03 629.19 49.25 o 0 13 0 133.28 196.99 50.09 o 1 13 0 404.71 491.82 28.10 o 2 13 0 2.02 -30.22 20.71 o 3 13 0 29.87 65.53 46.03 o 4 13 0 6.04 9.95 43.32 o -2 14 0 269.61 250.05 45.83 o -1 14 0 69.02 75.31 41.06 o 0 14 0 207.83 213.14 28.68 o 1 14 0 3.00 90.37 30.06 o 2 14 0 38.73 51.78 43.59 o -2 -14 1 184.35 274.92 213.50 o -1 -14 1 1.25 89.97 23.63 o 0 -14 1 330.39 435.50 34.32 o 1 -14 1 2.65 -27.06 21.79 o 2 -14 1 133.99 289.11 45.42 o -4 -13 1 0.03 -31.82 30.27 o -3 -13 1 48.78 62.21 27.24 o -2 -13 1 0.01 -17.80 33.24 o -1 -13 1 371.10 418.59 35.92 o 0 -13 1 10.64 72.87 16.89 o 1 -13 1 315.18 361.07 24.56 o 2 -13 1 4.50 20.05 22.41 o 4 -13 1 0.51 54.56 42.38 o -5 -12 1 37.34 -16.48 63.97 o -4 -12 1 776.27 762.32 43.39 o -3 -12 1 46.75 40.63 22.95 o -2 -12 1 772.31 774.48 16.40 o -1 -12 1 53.09 68.06 21.90 o 0 -12 1 762.78 801.53 28.56 o 1 -12 1 141.11 178.16 25.82 o 2 -12 1 899.80 908.24 25.34 o 3 -12 1 116.06 152.05 24.98 o 4 -12 1 509.78 487.21 65.83 o -6 -11 1 27.47 38.37 39.85 o -5 -11 1 14.16 21.91 36.68 o -4 -11 1 15.43 -1.11 38.68 o -3 -11 1 843.57 811.44 28.71 o -2 -11 1 0.00 14.79 16.71 o -1 -11 1 30.38 80.58 27.38 o 0 -11 1 48.45 38.63 17.51 o 1 -11 1 79.28 141.66 27.54 o 2 -11 1 0.57 37.06 15.55 o 3 -11 1 1250.70 1159.70 35.91 o 4 -11 1 207.94 168.75 34.69 o 5 -11 1 41.73 21.48 17.24 o 6 -11 1 3.04 1.22 33.64 o -7 -10 1 356.62 378.02 49.13 o -6 -10 1 465.35 647.77 41.19 o -5 -10 1 92.67 23.22 64.07 o -4 -10 1 1290.41 1251.73 108.78 o -3 -10 1 97.55 103.32 16.29 o -2 -10 1 578.98 588.70 26.16 o -1 -10 1 34.82 108.29 52.58 o 0 -10 1 1550.31 1673.93 28.81 o 1 -10 1 365.91 419.44 29.36 o 2 -10 1 1147.66 1158.56 26.12 o 3 -10 1 263.01 272.16 28.74 o 4 -10 1 602.24 658.94 42.09 o 5 -10 1 262.78 257.31 36.11 o 6 -10 1 225.26 238.75 39.33 o 7 -10 1 270.23 202.87 25.93 o -8 -9 1 53.93 39.74 44.74 o -7 -9 1 357.68 298.46 18.67 o -6 -9 1 308.61 261.44 36.95 o -5 -9 1 1310.62 1417.39 42.20 o -4 -9 1 145.28 203.90 54.07 o -3 -9 1 97.99 120.04 23.54 o -2 -9 1 16.54 15.27 30.07 o -1 -9 1 709.24 711.19 20.78 o 0 -9 1 3.04 2.26 8.17 o 1 -9 1 1287.53 1224.79 16.99 o 2 -9 1 234.92 247.96 10.69 o 3 -9 1 10.32 61.39 31.08 o 4 -9 1 605.92 708.01 41.40 o 5 -9 1 388.01 396.66 22.98 o 6 -9 1 208.52 179.31 32.12 o 7 -9 1 42.21 5.45 36.31 o -8 -8 1 621.36 741.83 31.05 o -7 -8 1 147.64 120.10 49.06 o -6 -8 1 297.66 422.58 36.84 o -5 -8 1 802.93 796.62 55.66 o -4 -8 1 881.11 1039.25 55.57 o -3 -8 1 47.24 50.84 13.28 o -2 -8 1 2306.09 2264.01 50.77 o -1 -8 1 1363.37 1343.56 27.01 o 0 -8 1 1817.01 1741.21 41.29 o 1 -8 1 125.61 164.80 19.61 o 2 -8 1 4700.52 4800.41 50.99 o 3 -8 1 1410.14 1483.16 30.34 o 4 -8 1 3259.95 3386.48 94.36 o 5 -8 1 1814.97 1808.66 88.67 o 6 -8 1 295.09 347.34 27.28 o 7 -8 1 8.74 -28.32 18.88 o 8 -8 1 611.07 488.44 90.88 o -9 -7 1 1.92 21.95 42.29 o -8 -7 1 7.32 26.88 23.74 o -7 -7 1 80.52 125.49 18.64 o -6 -7 1 613.74 715.90 31.38 o -5 -7 1 1024.02 985.87 27.18 o -4 -7 1 339.19 268.13 28.07 o -3 -7 1 592.56 472.80 28.53 o -2 -7 1 64.15 67.25 10.30 o -1 -7 1 175.22 167.92 12.45 o 0 -7 1 22.97 55.95 24.11 o 1 -7 1 1371.37 1426.45 23.30 o 2 -7 1 1217.81 1177.67 15.74 o 3 -7 1 86.23 65.40 10.26 o 4 -7 1 279.27 365.15 22.80 o 5 -7 1 430.02 474.76 46.22 o 6 -7 1 801.06 901.23 52.70 o 7 -7 1 32.42 27.26 19.44 o 8 -7 1 22.14 25.25 16.72 o -9 -6 1 0.15 44.64 22.68 o -8 -6 1 246.10 394.23 16.70 o -7 -6 1 267.82 301.87 31.27 o -6 -6 1 1948.29 2189.13 50.00 o -5 -6 1 323.60 333.78 37.79 o -4 -6 1 925.25 1010.99 30.93 o -3 -6 1 132.20 183.58 25.83 o -2 -6 1 1361.86 1192.58 12.93 o -1 -6 1 2394.64 2485.83 27.20 o 0 -6 1 3568.85 3218.30 53.71 o 1 -6 1 512.85 417.81 18.24 o 2 -6 1 5704.11 5900.96 75.30 o 3 -6 1 259.88 255.58 23.23 o 4 -6 1 1246.18 1224.76 31.04 o 5 -6 1 73.08 98.68 23.66 o 6 -6 1 1696.75 1791.71 155.28 o 7 -6 1 267.17 295.91 20.33 o 8 -6 1 51.25 -20.95 45.39 o -9 -5 1 94.58 124.02 33.54 o -8 -5 1 119.88 117.75 30.00 o -7 -5 1 11.17 65.83 23.24 o -6 -5 1 11.26 13.46 24.82 o -5 -5 1 209.51 222.88 20.61 o -4 -5 1 4690.85 5066.84 79.11 o -3 -5 1 4764.04 5103.30 68.31 o -2 -5 1 342.15 274.40 17.33 o -1 -5 1 626.03 598.62 15.25 o 0 -5 1 196.94 175.15 13.76 o 1 -5 1 63.54 114.41 12.26 o 2 -5 1 679.09 683.34 21.80 o 3 -5 1 4435.51 4347.04 77.81 o 4 -5 1 3758.55 3873.91 269.47 o 5 -5 1 353.12 410.78 44.55 o 6 -5 1 17.67 30.28 21.86 o 7 -5 1 19.45 44.79 43.48 o 8 -5 1 238.23 283.93 49.47 o 9 -5 1 84.51 144.59 31.75 o -10 -4 1 324.10 368.63 78.80 o -9 -4 1 7.08 -56.70 38.35 o -8 -4 1 95.37 91.25 38.72 o -7 -4 1 10.22 -7.14 36.79 o -6 -4 1 678.88 809.89 53.59 o -5 -4 1 53.10 64.70 21.19 o -4 -4 1 4033.08 4239.35 58.70 o -3 -4 1 415.38 381.38 11.28 o -2 -4 1 2637.30 2275.29 136.84 o -1 -4 1 986.22 1091.83 32.58 o 0 -4 1 14013.94 14000.79 307.32 o 1 -4 1 409.51 289.40 18.11 o 2 -4 1 7602.90 7580.23 114.76 o 3 -4 1 446.94 463.75 13.17 o 4 -4 1 16050.41 16490.27 268.21 o 5 -4 1 1.32 -20.40 14.47 o 6 -4 1 1454.24 1434.96 85.88 o 7 -4 1 155.21 213.67 33.05 o 8 -4 1 333.34 238.88 31.76 o 9 -4 1 29.11 -1.61 19.63 o -10 -3 1 40.62 -46.61 31.07 o -9 -3 1 58.73 62.49 24.11 o -8 -3 1 73.49 9.61 10.90 o -7 -3 1 10.25 -9.12 10.34 o -6 -3 1 523.44 501.71 32.29 o -5 -3 1 724.58 570.47 44.38 o -4 -3 1 1799.58 1726.91 89.19 o -3 -3 1 93.65 120.44 14.02 o -2 -3 1 3983.99 4194.60 224.41 o -1 -3 1 10706.75 10545.95 385.15 o 0 -3 1 1536.59 1675.29 52.92 o 1 -3 1 1618.88 1493.91 29.58 o 2 -3 1 11256.82 11428.96 164.52 o 3 -3 1 1329.01 1282.50 62.12 o 4 -3 1 241.84 348.88 19.72 o 5 -3 1 106.22 179.89 44.37 o 6 -3 1 2182.65 2321.71 104.46 o 7 -3 1 54.33 11.73 19.15 o 8 -3 1 590.65 693.65 47.71 o 9 -3 1 10.07 -24.84 16.56 o 10 -3 1 12.54 8.03 64.92 o -9 -2 1 202.87 187.40 19.76 o -8 -2 1 2115.54 2090.55 82.76 o -7 -2 1 14.53 40.99 9.70 o -6 -2 1 149.15 157.98 20.35 o -5 -2 1 1.19 4.93 9.30 o -4 -2 1 5299.68 4819.67 197.95 o -3 -2 1 54.91 32.44 10.39 o -2 -2 1 41482.61 41446.16 2564.66 o 2 -2 1 26354.17 26538.56 882.41 o 3 -2 1 145.17 75.51 32.19 o 4 -2 1 3010.61 3119.92 82.40 o 5 -2 1 147.67 166.66 27.73 o 6 -2 1 579.87 527.98 14.55 o 7 -2 1 41.14 83.35 43.30 o 8 -2 1 266.03 190.04 16.62 o 9 -2 1 141.16 216.74 40.97 o 10 -2 1 16.54 56.13 38.74 o -10 -1 1 34.28 42.71 21.37 o -9 -1 1 18.27 12.98 29.43 o -8 -1 1 35.06 28.91 14.44 o -7 -1 1 271.81 310.14 36.14 o -6 -1 1 172.75 213.87 17.31 o -5 -1 1 244.82 229.69 17.39 o -4 -1 1 1338.76 1285.58 58.10 o -3 -1 1 404.25 332.16 19.57 o -2 -1 1 1506.86 1510.29 77.45 o 2 -1 1 7143.44 6634.23 389.81 o 3 -1 1 144.23 83.95 11.56 o 4 -1 1 2369.71 2376.17 101.54 o 5 -1 1 727.72 636.84 27.14 o 6 -1 1 1537.83 1490.04 94.01 o 7 -1 1 173.18 170.00 20.87 o 8 -1 1 548.17 559.06 46.66 o 9 -1 1 54.77 38.25 25.39 o 10 -1 1 185.00 290.56 23.64 o -10 0 1 448.07 424.63 49.09 o -9 0 1 0.00 28.03 19.70 o -8 0 1 168.03 154.50 22.68 o -7 0 1 0.25 9.81 36.84 o -6 0 1 4916.31 4870.94 250.59 o -5 0 1 0.00 7.34 11.21 o -4 0 1 7483.47 7352.07 492.73 o -3 0 1 3.64 7.80 10.96 o 2 0 1 1408.73 1411.41 64.28 o 3 0 1 1.20 8.39 11.10 o 4 0 1 2174.82 2228.83 74.41 o 5 0 1 2.18 -19.14 12.76 o 6 0 1 3142.16 3004.14 94.07 o 7 0 1 8.83 17.78 32.27 o 8 0 1 30.86 30.62 26.92 o 9 0 1 2.72 2.71 15.47 o 10 0 1 182.55 333.34 54.83 o -10 1 1 1.54 68.89 22.69 o -9 1 1 130.56 173.09 20.89 o -8 1 1 73.13 90.28 34.68 o -7 1 1 164.42 211.39 32.18 o -6 1 1 335.41 358.58 20.90 o -5 1 1 456.91 425.22 30.21 o -4 1 1 834.21 853.76 45.05 o -3 1 1 549.81 452.12 16.91 o -2 1 1 3440.08 3157.77 210.93 o 2 1 1 4100.63 4135.59 135.05 o 3 1 1 94.86 84.72 21.24 o 4 1 1 2690.72 2782.11 88.60 o 5 1 1 397.17 373.81 18.30 o 6 1 1 1840.24 1836.30 73.48 o 7 1 1 174.82 168.38 15.37 o 8 1 1 382.02 437.61 18.62 o 9 1 1 64.14 14.14 15.16 o 10 1 1 146.26 126.84 40.80 o -10 2 1 8.93 30.48 62.88 o -9 2 1 200.56 251.90 26.04 o -8 2 1 2028.39 2000.19 100.30 o -7 2 1 17.56 20.58 28.04 o -6 2 1 400.05 432.14 13.35 o -5 2 1 3.24 -23.90 18.75 o -4 2 1 7329.12 7765.64 117.89 o -3 2 1 59.95 15.97 13.44 o -2 2 1 30620.58 31666.54 590.28 o 2 2 1 21457.28 22852.95 893.34 o 3 2 1 16.60 32.37 9.01 o 4 2 1 3276.89 3030.66 228.26 o 5 2 1 405.50 332.97 23.04 o 6 2 1 357.33 316.02 25.04 o 7 2 1 197.13 236.72 18.13 o 8 2 1 192.39 123.31 18.13 o 9 2 1 165.14 210.70 30.91 o -10 3 1 57.04 44.54 91.72 o -9 3 1 58.76 156.60 47.65 o -8 3 1 2.41 -23.67 16.68 o -7 3 1 4.02 179.51 46.89 o -6 3 1 535.74 645.14 46.79 o -5 3 1 1272.48 1292.37 31.00 o -4 3 1 2707.61 2741.08 87.94 o -3 3 1 115.36 133.42 17.53 o -2 3 1 795.79 792.88 49.75 o -1 3 1 5862.49 5639.70 119.18 o 0 3 1 5168.48 4870.83 70.88 o 1 3 1 512.99 564.41 36.23 o 2 3 1 10834.51 10897.07 247.59 o 3 3 1 1330.76 1252.95 53.00 o 4 3 1 678.33 724.69 52.58 o 5 3 1 712.57 613.14 43.58 o 6 3 1 2856.08 2812.45 117.96 o 7 3 1 53.39 22.08 8.41 o 8 3 1 333.31 337.49 34.03 o 9 3 1 39.98 26.99 17.78 o 10 3 1 25.10 -8.46 48.94 o -9 4 1 52.92 65.19 83.09 o -8 4 1 34.65 14.46 36.04 o -7 4 1 124.47 88.32 19.14 o -6 4 1 835.73 740.55 76.19 o -5 4 1 251.69 232.01 16.09 o -4 4 1 1542.76 1620.70 86.90 o -3 4 1 344.76 277.10 20.58 o -2 4 1 365.27 364.19 16.61 o -1 4 1 452.21 493.79 21.75 o 0 4 1 4834.54 4578.94 122.89 o 1 4 1 448.85 337.85 10.54 o 2 4 1 3012.89 2990.20 55.74 o 3 4 1 877.58 935.69 25.77 o 4 4 1 9125.69 9826.57 129.86 o 5 4 1 20.94 7.05 17.27 o 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