# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' nvr in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 264.28 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.8092 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 12.3370 _cell_length_b 10.0540 _cell_length_c 11.0640 _cell_angle_alpha 90.000 _cell_angle_beta 102.420 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2776.47 2995.76 43.02 o 6 0 0 9134.00 9322.01 132.77 o 8 0 0 10499.01 10943.15 192.20 o 10 0 0 625.21 604.80 18.06 o 12 0 0 78.48 66.48 5.56 o 14 0 0 655.50 610.79 20.74 o 1 1 0 90.62 75.94 1.17 o 3 1 0 363.21 274.16 3.46 o 5 1 0 3625.24 3751.67 38.49 o 7 1 0 105.17 88.84 2.53 o 9 1 0 591.12 577.01 9.31 o 11 1 0 139.63 142.46 5.45 o 13 1 0 0.03 1.93 1.56 o 0 2 0 35507.39 29774.93 1276.25 o 2 2 0 6877.58 7028.97 131.88 o 4 2 0 425.36 555.14 5.70 o 6 2 0 308.68 278.94 4.04 o 8 2 0 1724.54 1666.56 50.04 o 10 2 0 148.74 129.93 6.58 o 12 2 0 123.90 118.53 7.03 o 14 2 0 154.39 149.94 6.43 o 1 3 0 702.84 560.28 6.29 o 3 3 0 324.18 338.99 4.33 o 5 3 0 949.27 1013.42 12.01 o 7 3 0 353.24 361.01 6.38 o 9 3 0 145.90 135.01 3.78 o 11 3 0 166.16 146.10 4.29 o 13 3 0 1.41 3.53 1.72 o 0 4 0 2298.97 2643.33 38.52 o 2 4 0 382.68 323.36 4.32 o 4 4 0 3522.28 3756.83 38.63 o 6 4 0 695.44 661.98 8.13 o 8 4 0 342.77 311.07 6.13 o 10 4 0 525.10 541.80 9.59 o 12 4 0 334.56 351.97 7.64 o 14 4 0 56.89 70.02 6.38 o 1 5 0 66.64 51.14 1.91 o 3 5 0 1072.25 1095.81 12.23 o 5 5 0 89.30 89.03 2.04 o 7 5 0 11.21 16.88 2.19 o 9 5 0 0.31 0.35 1.29 o 11 5 0 27.54 23.93 2.08 o 13 5 0 36.49 40.42 2.64 o 0 6 0 1395.59 1620.83 24.67 o 2 6 0 106.30 111.99 2.21 o 4 6 0 2799.22 2945.00 42.97 o 6 6 0 2527.58 2607.40 32.92 o 8 6 0 107.07 100.29 3.36 o 10 6 0 178.06 164.98 4.75 o 12 6 0 178.74 179.33 8.99 o 1 7 0 28.86 33.60 1.52 o 3 7 0 34.07 45.90 1.85 o 5 7 0 179.17 175.60 6.91 o 7 7 0 151.39 140.48 7.45 o 9 7 0 0.03 2.07 1.94 o 11 7 0 445.82 484.33 11.93 o 0 8 0 6608.52 5714.92 116.25 o 2 8 0 1084.89 1092.33 18.47 o 4 8 0 8685.09 9192.85 185.55 o 6 8 0 4.80 5.71 2.48 o 8 8 0 125.97 143.95 8.05 o 10 8 0 745.82 719.37 22.28 o 1 9 0 527.15 520.83 15.67 o 3 9 0 104.46 97.34 6.16 o 5 9 0 449.46 439.67 14.87 o 7 9 0 260.30 254.66 11.33 o 9 9 0 586.32 619.82 20.44 o 0 10 0 33.12 26.93 3.83 o 2 10 0 849.58 934.25 24.98 o 4 10 0 1847.39 2002.31 47.00 o 6 10 0 0.29 0.89 2.04 o 8 10 0 21.93 25.73 4.12 o 1 11 0 74.07 86.35 6.21 o 3 11 0 105.78 114.33 7.30 o 5 11 0 6.03 8.69 2.88 o 2 12 0 194.14 226.10 10.88 o -15 1 1 186.67 174.73 7.24 o -13 1 1 156.63 165.22 6.39 o -11 1 1 174.53 175.66 5.97 o -9 1 1 142.91 135.98 4.24 o -7 1 1 460.23 583.80 7.24 o -5 1 1 716.75 595.26 6.94 o -3 1 1 32062.08 29650.88 540.37 o -1 1 1 42.83 56.79 1.05 o 1 1 1 486.36 395.22 6.35 o 3 1 1 69845.06 63419.71 2858.63 o 5 1 1 7096.28 7160.61 72.47 o 7 1 1 9969.11 11132.99 112.27 o 9 1 1 411.41 403.71 7.52 o 11 1 1 5657.98 5866.58 89.33 o 13 1 1 0.68 1.34 1.53 o -14 2 1 60.55 55.86 5.09 o -12 2 1 137.65 126.74 5.31 o -10 2 1 632.58 619.19 13.23 o -8 2 1 451.52 481.82 7.91 o -6 2 1 546.74 489.94 7.48 o -4 2 1 856.85 933.90 12.17 o -2 2 1 189.98 133.38 1.91 o 0 2 1 50.24 37.99 1.37 o 2 2 1 6082.64 5930.63 88.14 o 4 2 1 3916.59 4104.36 37.34 o 6 2 1 89.77 71.17 2.09 o 8 2 1 200.25 203.41 3.71 o 10 2 1 72.30 67.62 3.71 o 12 2 1 550.49 524.20 16.04 o 14 2 1 14.44 8.69 5.86 o -13 3 1 27.40 31.69 2.96 o -11 3 1 58.55 54.47 2.62 o -9 3 1 821.12 829.54 12.48 o -7 3 1 1757.57 1716.50 22.23 o -5 3 1 1823.45 1690.47 21.35 o -3 3 1 222.54 257.41 3.42 o -1 3 1 1735.50 1639.22 17.05 o 1 3 1 13489.78 13479.98 256.69 o 3 3 1 9.28 3.63 0.45 o 5 3 1 7.90 3.06 0.51 o 7 3 1 2194.44 2214.01 21.20 o 9 3 1 420.57 406.95 7.59 o 11 3 1 88.85 95.95 3.53 o 13 3 1 91.11 94.18 4.95 o -14 4 1 177.68 153.02 6.54 o -12 4 1 66.31 62.64 3.01 o -10 4 1 420.51 427.48 8.01 o -8 4 1 284.45 231.16 12.05 o -6 4 1 76.32 97.62 2.77 o -4 4 1 2423.36 2563.17 31.32 o -2 4 1 338.36 357.56 4.51 o 0 4 1 467.85 506.00 7.01 o 2 4 1 2443.79 2606.03 27.03 o 4 4 1 2165.10 2395.80 25.28 o 6 4 1 571.63 568.61 7.34 o 8 4 1 63.92 58.09 2.47 o 10 4 1 59.06 54.78 2.64 o 12 4 1 2.11 5.15 1.30 o -13 5 1 38.14 50.68 2.94 o -11 5 1 519.95 517.66 11.32 o -9 5 1 1519.46 1583.98 25.28 o -7 5 1 1183.04 1157.24 16.10 o -5 5 1 194.36 162.04 3.58 o -3 5 1 2091.45 2078.43 26.22 o -1 5 1 885.96 858.26 9.66 o 1 5 1 1921.75 2117.07 22.25 o 3 5 1 3.43 10.40 0.78 o 5 5 1 2379.83 2564.19 27.30 o 7 5 1 1293.43 1307.65 18.07 o 9 5 1 135.98 122.72 3.85 o 11 5 1 7.74 10.11 1.52 o 13 5 1 179.88 194.34 5.76 o -12 6 1 16.28 13.81 1.79 o -10 6 1 0.98 2.93 1.17 o -8 6 1 252.05 263.11 9.80 o -6 6 1 155.75 144.24 4.59 o -4 6 1 53.02 52.34 1.80 o -2 6 1 14.53 18.55 0.96 o 0 6 1 308.90 352.60 7.39 o 2 6 1 194.22 216.50 3.40 o 4 6 1 113.12 116.19 6.46 o 6 6 1 20.53 19.95 1.90 o 8 6 1 212.19 199.81 6.36 o 10 6 1 7.12 10.47 2.01 o 12 6 1 41.90 40.57 3.45 o -11 7 1 233.10 219.41 8.10 o -9 7 1 285.95 254.65 7.43 o -7 7 1 1350.28 1270.61 46.22 o -5 7 1 622.95 592.68 11.49 o -3 7 1 29.57 27.44 1.95 o -1 7 1 1206.05 1284.68 16.77 o 1 7 1 457.06 470.97 10.92 o 3 7 1 515.47 544.93 10.48 o 5 7 1 305.61 300.11 7.43 o 7 7 1 3453.86 3608.84 55.40 o 9 7 1 214.86 213.22 7.01 o 11 7 1 199.17 208.62 7.34 o -10 8 1 11.70 3.38 2.63 o -8 8 1 8.37 7.10 2.63 o -6 8 1 461.39 458.89 15.02 o -4 8 1 174.58 148.59 7.36 o -2 8 1 30.83 27.84 2.26 o 0 8 1 2.00 -0.22 1.04 o 2 8 1 200.89 176.53 5.13 o 4 8 1 14.35 17.99 2.19 o 6 8 1 437.62 427.89 9.91 o 8 8 1 33.50 41.36 3.01 o 10 8 1 297.11 314.40 11.61 o -9 9 1 1.13 0.50 2.33 o -7 9 1 552.14 533.01 17.45 o -5 9 1 685.43 730.55 21.14 o -3 9 1 111.26 108.42 6.41 o -1 9 1 1323.86 1346.24 22.45 o 1 9 1 4231.64 4571.14 95.24 o 3 9 1 420.35 384.37 13.23 o 5 9 1 19.15 21.96 3.78 o 7 9 1 3386.36 3778.57 82.94 o 9 9 1 168.97 146.79 9.04 o -8 10 1 320.93 319.99 13.62 o -6 10 1 81.81 77.26 6.11 o -4 10 1 1024.14 1048.66 27.97 o -2 10 1 23.15 20.17 3.73 o 0 10 1 13.15 9.62 1.81 o 2 10 1 161.17 170.84 8.40 o 4 10 1 23.27 20.67 3.78 o 6 10 1 5.00 17.93 3.68 o 8 10 1 14.80 15.75 3.83 o -7 11 1 11.40 7.10 2.93 o -5 11 1 5.96 3.63 2.53 o -3 11 1 570.89 662.44 20.44 o -1 11 1 850.36 907.28 24.92 o 1 11 1 148.14 155.73 8.20 o 3 11 1 270.16 314.35 12.77 o 5 11 1 279.67 310.13 13.27 o -2 12 1 123.89 125.36 8.00 o 2 12 1 1.11 5.12 2.93 o -14 0 2 105.11 98.73 7.30 o -12 0 2 649.33 625.31 19.50 o -10 0 2 772.50 752.07 20.75 o -8 0 2 1763.37 1636.99 25.31 o -6 0 2 1256.95 1298.85 20.01 o -4 0 2 11257.40 10199.13 332.61 o -2 0 2 7243.07 7142.72 102.20 o 0 0 2 13424.17 13775.43 199.50 o 2 0 2 7534.94 7806.52 184.46 o 4 0 2 1865.30 2324.10 34.56 o 6 0 2 5161.73 5073.53 73.83 o 8 0 2 8971.06 9429.95 135.60 o 10 0 2 478.21 470.26 10.14 o 12 0 2 118.47 99.92 6.96 o 14 0 2 1469.41 1473.75 40.08 o -15 1 2 0.11 -0.34 1.58 o -13 1 2 161.82 141.25 10.01 o -11 1 2 45.70 41.46 2.99 o -9 1 2 297.19 283.84 5.45 o -7 1 2 1653.50 1622.69 17.58 o -5 1 2 168.17 188.80 2.75 o -3 1 2 2099.75 1857.85 19.26 o -1 1 2 1759.14 1962.19 20.14 o 1 1 2 366.18 246.34 3.16 o 3 1 2 1988.30 2129.37 22.34 o 5 1 2 1909.97 1933.05 20.84 o 7 1 2 397.90 397.91 5.82 o 9 1 2 532.77 506.82 7.34 o 11 1 2 64.06 55.80 7.40 o 13 1 2 239.42 228.15 8.18 o -14 2 2 44.02 41.10 3.47 o -12 2 2 1135.32 1201.99 22.41 o -10 2 2 490.59 480.82 8.31 o -8 2 2 403.62 386.55 6.66 o -6 2 2 10.16 4.56 1.33 o -4 2 2 5618.01 4984.00 58.83 o -2 2 2 11303.63 10954.95 160.67 o 0 2 2 1384.71 1637.48 19.80 o 2 2 2 3.75 9.38 1.01 o 4 2 2 3585.83 3332.76 30.73 o 6 2 2 3846.98 3877.67 40.39 o 8 2 2 426.84 404.77 6.09 o 10 2 2 4.80 4.64 1.47 o 12 2 2 130.90 127.61 5.59 o 14 2 2 385.92 377.32 14.81 o -13 3 2 51.10 51.81 3.71 o -11 3 2 128.86 126.27 3.85 o -9 3 2 277.97 271.42 5.62 o -7 3 2 754.60 754.88 10.99 o -5 3 2 13.54 8.57 0.91 o -3 3 2 6891.66 8051.94 81.01 o -1 3 2 433.33 420.95 5.95 o 1 3 2 4323.66 4745.99 48.27 o 3 3 2 2096.31 2268.74 27.28 o 5 3 2 1755.65 1835.48 17.71 o 7 3 2 623.51 665.48 10.30 o 9 3 2 166.03 150.80 4.20 o 11 3 2 148.58 133.85 4.32 o 13 3 2 60.00 68.76 7.28 o -14 4 2 147.56 151.35 6.39 o -12 4 2 291.45 324.68 7.11 o -10 4 2 228.95 238.53 5.49 o -8 4 2 1356.20 1275.68 17.54 o -6 4 2 3429.68 3366.36 41.09 o -4 4 2 876.85 763.44 8.78 o -2 4 2 126.99 69.36 3.29 o 0 4 2 413.78 382.32 5.73 o 2 4 2 1151.48 1159.84 12.76 o 4 4 2 1500.38 1559.43 19.53 o 6 4 2 95.40 92.73 2.28 o 8 4 2 55.59 51.26 2.89 o 10 4 2 534.51 520.73 9.56 o 12 4 2 145.93 144.34 4.76 o -13 5 2 567.08 554.20 18.60 o -11 5 2 104.13 102.93 5.08 o -9 5 2 902.82 930.35 13.93 o -7 5 2 2139.45 2291.08 35.94 o -5 5 2 733.14 771.82 11.01 o -3 5 2 4055.79 4649.79 47.48 o -1 5 2 7.85 11.09 0.98 o 1 5 2 1673.59 1930.57 23.87 o 3 5 2 157.10 143.83 2.61 o 5 5 2 241.06 218.77 3.73 o 7 5 2 20.04 22.45 2.41 o 9 5 2 0.89 0.88 0.93 o 11 5 2 0.00 1.58 1.41 o -12 6 2 15.87 16.06 1.87 o -10 6 2 286.13 272.09 7.28 o -8 6 2 2954.02 2991.76 38.91 o -6 6 2 2636.80 2686.29 33.64 o -4 6 2 539.35 455.53 26.89 o -2 6 2 503.90 579.93 8.44 o 0 6 2 209.84 218.85 4.52 o 2 6 2 4601.07 4982.08 58.98 o 4 6 2 101.20 97.56 4.30 o 6 6 2 143.33 153.55 5.12 o 8 6 2 376.68 347.76 9.05 o 10 6 2 622.09 592.00 14.80 o 12 6 2 58.62 60.70 4.07 o -11 7 2 21.29 24.78 3.30 o -9 7 2 222.08 263.59 7.39 o -7 7 2 13.31 9.02 1.56 o -5 7 2 72.43 71.00 7.70 o -3 7 2 1454.71 1408.59 18.31 o -1 7 2 61.74 45.44 1.89 o 1 7 2 164.16 156.87 4.17 o 3 7 2 115.99 98.37 2.90 o 5 7 2 22.09 22.31 2.08 o 7 7 2 65.10 61.21 3.46 o 9 7 2 121.37 120.07 5.09 o 11 7 2 11.45 10.68 3.23 o -10 8 2 177.27 154.15 8.65 o -8 8 2 1251.45 1314.89 33.26 o -6 8 2 362.06 320.00 11.88 o -4 8 2 17.73 11.13 2.63 o -2 8 2 1198.70 1226.16 17.13 o 0 8 2 210.30 198.40 7.28 o 2 8 2 40.30 37.21 2.50 o 4 8 2 2457.37 2555.39 40.12 o 6 8 2 147.21 153.29 11.85 o 8 8 2 226.27 238.47 7.40 o 10 8 2 704.82 740.23 16.14 o -9 9 2 312.91 325.95 13.37 o -7 9 2 299.80 299.76 12.23 o -5 9 2 252.79 259.69 10.69 o -3 9 2 188.48 196.25 8.75 o -1 9 2 2582.15 2662.42 40.83 o 1 9 2 47.67 49.93 3.09 o 3 9 2 1263.19 1257.24 31.52 o 5 9 2 39.25 37.76 4.37 o 7 9 2 257.53 241.04 11.23 o 9 9 2 0.47 -0.50 2.29 o -8 10 2 227.89 219.76 10.88 o -6 10 2 214.00 199.33 9.84 o -4 10 2 11.68 7.60 2.68 o -2 10 2 273.78 272.62 10.88 o 0 10 2 881.66 934.84 17.29 o 2 10 2 493.50 535.75 17.00 o 4 10 2 225.69 252.26 11.03 o 6 10 2 61.30 66.48 6.01 o 8 10 2 90.37 87.10 7.20 o -7 11 2 9.40 1.19 2.53 o -5 11 2 0.98 -0.15 2.09 o -3 11 2 151.18 170.74 8.99 o -1 11 2 253.12 287.21 11.53 o 1 11 2 0.48 2.29 2.33 o 3 11 2 10.80 20.87 3.78 o 5 11 2 70.78 97.48 7.35 o -2 12 2 92.67 104.59 7.25 o 2 12 2 445.85 457.21 16.41 o -15 1 3 27.07 20.18 2.89 o -13 1 3 499.96 503.48 14.72 o -11 1 3 375.73 386.26 9.79 o -9 1 3 8.63 8.34 1.01 o -7 1 3 473.04 425.27 5.76 o -5 1 3 16.59 25.02 1.25 o -3 1 3 476.44 509.41 5.91 o -1 1 3 18703.69 17791.44 196.58 o 1 1 3 12135.61 12352.27 170.43 o 3 1 3 1250.11 1274.79 14.13 o 5 1 3 185.98 169.24 3.17 o 7 1 3 3565.89 3443.00 36.51 o 9 1 3 1914.60 1899.95 21.69 o 11 1 3 430.94 426.20 8.45 o 13 1 3 26.04 19.63 2.76 o -14 2 3 0.10 0.77 1.49 o -12 2 3 19.85 16.93 2.32 o -10 2 3 2.40 2.64 0.94 o -8 2 3 23.60 17.69 2.41 o -6 2 3 17.81 18.51 1.26 o -4 2 3 3545.84 3732.20 51.21 o -2 2 3 4232.06 4982.96 50.39 o 0 2 3 698.94 643.40 7.38 o 2 2 3 798.13 996.17 9.93 o 4 2 3 1826.49 2039.77 19.53 o 6 2 3 819.09 840.85 10.40 o 8 2 3 72.70 64.74 2.18 o 10 2 3 13.06 13.41 2.67 o 12 2 3 1.96 2.95 1.60 o -13 3 3 141.66 150.96 6.08 o -11 3 3 326.40 318.96 6.63 o -9 3 3 1389.51 1382.30 18.86 o -7 3 3 469.85 430.47 7.10 o -5 3 3 110.69 78.70 2.53 o -3 3 3 4355.64 4129.85 42.11 o -1 3 3 1587.88 1384.56 14.80 o 1 3 3 1428.01 1412.06 15.23 o 3 3 3 2473.70 2585.53 27.20 o 5 3 3 5.67 6.37 0.98 o 7 3 3 538.95 509.79 6.35 o 9 3 3 1104.56 1131.53 16.72 o 11 3 3 35.01 29.75 2.27 o 13 3 3 8.40 18.06 2.75 o -14 4 3 46.77 47.57 4.07 o -12 4 3 126.10 125.32 5.31 o -10 4 3 1208.51 1249.65 21.45 o -8 4 3 387.85 387.38 6.92 o -6 4 3 6815.80 7503.76 88.71 o -4 4 3 5.93 9.46 1.39 o -2 4 3 4706.05 5197.59 52.86 o 0 4 3 5898.54 6841.87 79.59 o 2 4 3 161.17 186.68 3.01 o 4 4 3 8685.14 9595.63 96.91 o 6 4 3 581.16 629.49 8.35 o 8 4 3 490.31 517.82 9.14 o 10 4 3 23.72 20.67 1.94 o 12 4 3 101.73 112.13 4.25 o -13 5 3 10.89 15.87 2.48 o -11 5 3 736.26 716.79 11.96 o -9 5 3 661.02 664.96 10.77 o -7 5 3 823.93 794.50 11.77 o -5 5 3 3269.41 3163.52 38.73 o -3 5 3 1698.78 1734.82 18.63 o -1 5 3 336.85 277.40 4.83 o 1 5 3 139.39 92.14 2.51 o 3 5 3 974.23 1013.10 13.82 o 5 5 3 2396.94 2465.12 32.81 o 7 5 3 46.99 49.04 4.32 o 9 5 3 234.86 246.37 7.50 o 11 5 3 97.34 99.84 4.98 o -12 6 3 1.26 0.99 1.18 o -10 6 3 442.03 461.12 8.65 o -8 6 3 94.90 109.92 4.05 o -6 6 3 126.20 152.19 5.87 o -4 6 3 205.08 158.29 6.21 o -2 6 3 1167.12 1264.16 16.52 o 0 6 3 13.93 18.62 1.32 o 2 6 3 167.82 195.66 4.36 o 4 6 3 310.00 325.61 7.82 o 6 6 3 54.70 56.75 3.14 o 8 6 3 54.77 62.27 4.89 o 10 6 3 21.57 18.68 3.43 o -11 7 3 11.44 11.20 1.97 o -9 7 3 181.23 182.13 5.95 o -7 7 3 1336.45 1332.98 22.84 o -5 7 3 2420.62 2279.88 147.44 o -3 7 3 257.31 247.96 4.80 o -1 7 3 5.36 3.84 0.86 o 1 7 3 756.67 752.59 11.09 o 3 7 3 1412.54 1436.31 19.22 o 5 7 3 449.40 428.99 9.82 o 7 7 3 78.78 76.47 4.72 o 9 7 3 0.80 0.25 1.17 o 11 7 3 11.09 14.09 2.39 o -10 8 3 42.84 39.15 4.67 o -8 8 3 63.11 49.91 4.50 o -6 8 3 483.75 503.64 10.82 o -4 8 3 1226.76 1160.49 20.01 o -2 8 3 28.33 21.17 1.64 o 0 8 3 61.28 70.16 4.84 o 2 8 3 133.62 140.33 7.31 o 4 8 3 97.84 98.13 10.96 o 6 8 3 298.60 291.45 8.13 o 8 8 3 43.54 42.98 3.20 o 10 8 3 371.16 398.63 26.87 o -9 9 3 100.15 82.13 6.56 o -7 9 3 95.89 78.95 5.96 o -5 9 3 485.42 476.64 15.56 o -3 9 3 1052.11 964.20 25.19 o -1 9 3 20.93 18.22 2.17 o 1 9 3 62.87 74.08 3.66 o 3 9 3 1831.10 1950.15 25.75 o 5 9 3 203.71 226.44 6.96 o 7 9 3 15.97 21.14 2.50 o 9 9 3 184.86 196.95 7.21 o -8 10 3 10.85 9.74 3.28 o -6 10 3 20.51 16.99 3.48 o -4 10 3 474.70 442.35 15.16 o -2 10 3 143.85 120.40 7.25 o 0 10 3 2.53 0.92 1.40 o 2 10 3 254.36 287.25 7.81 o 4 10 3 7.41 4.87 2.53 o 6 10 3 158.23 143.16 8.70 o -5 11 3 49.82 29.51 4.47 o -3 11 3 370.86 381.36 14.17 o -1 11 3 458.42 507.15 16.56 o 1 11 3 2.24 6.26 2.88 o 3 11 3 44.75 31.75 4.42 o 5 11 3 770.11 812.81 24.92 o -2 12 3 11.02 33.68 4.72 o 0 12 3 347.99 429.30 15.36 o -14 0 4 606.31 667.74 21.58 o -12 0 4 66.14 40.24 4.42 o -10 0 4 82.06 90.13 5.66 o -8 0 4 3680.69 3632.20 71.13 o -6 0 4 81.82 91.55 2.75 o -4 0 4 176.99 226.80 4.66 o -2 0 4 9198.54 9425.39 108.52 o 0 0 4 823.92 919.97 14.56 o 2 0 4 247.20 353.76 25.88 o 4 0 4 8179.77 8557.06 122.64 o 6 0 4 717.11 681.64 12.71 o 8 0 4 130.45 123.32 4.44 o 10 0 4 1436.14 1482.98 25.49 o 12 0 4 437.98 435.49 16.36 o -15 1 4 7.43 8.65 2.36 o -13 1 4 48.56 42.54 3.34 o -11 1 4 22.98 20.21 2.26 o -9 1 4 24.62 20.72 1.57 o -7 1 4 26.54 23.16 1.09 o -5 1 4 1449.39 1486.96 16.02 o -3 1 4 20.66 16.76 0.73 o -1 1 4 431.33 419.04 4.69 o 1 1 4 1087.04 1104.58 10.97 o 3 1 4 2517.25 2695.44 32.76 o 5 1 4 372.73 378.92 5.65 o 7 1 4 312.19 286.90 4.99 o 9 1 4 27.39 26.37 1.84 o 11 1 4 10.75 9.28 1.46 o 13 1 4 0.13 -1.86 1.86 o -14 2 4 342.56 359.48 10.66 o -12 2 4 1.17 0.01 1.28 o -10 2 4 293.15 296.49 5.94 o -8 2 4 1164.14 1165.41 15.91 o -6 2 4 909.56 844.82 9.71 o -4 2 4 566.10 471.38 5.09 o -2 2 4 290.19 256.47 3.56 o 0 2 4 1467.07 1388.53 15.03 o 2 2 4 1166.77 1022.60 10.39 o 4 2 4 862.13 886.04 9.47 o 6 2 4 1294.79 1240.81 17.81 o 8 2 4 356.21 322.02 5.56 o 10 2 4 247.80 238.06 5.87 o 12 2 4 357.12 387.30 8.46 o -13 3 4 20.27 16.54 3.88 o -11 3 4 108.49 95.79 4.34 o -9 3 4 51.73 54.86 2.33 o -7 3 4 5.37 6.33 1.70 o -5 3 4 415.68 431.36 5.48 o -3 3 4 7137.83 8094.06 81.55 o -1 3 4 2232.44 2244.10 23.53 o 1 3 4 4813.22 5379.06 54.87 o 3 3 4 1604.11 1686.74 16.50 o 5 3 4 406.15 396.83 6.86 o 7 3 4 40.11 42.94 1.57 o 9 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