# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 336.88 _exptl_crystal_F_000 1260.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.9375 _cell_length_b 14.7406 _cell_length_c 14.8043 _cell_angle_alpha 103.368 _cell_angle_beta 111.716 _cell_angle_gamma 92.582 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 113488.51 -10.04 6.69 o 2 0 0 8242.75 8219.46 260.86 o 3 0 0 0.34 28.35 33.47 o 4 0 0 2480.98 2317.04 110.65 o 5 0 0 95.54 114.85 17.06 o 6 0 0 895.88 1096.24 146.94 o 7 0 0 23.06 43.42 29.84 o 8 0 0 599.61 606.37 40.96 o 9 0 0 1216.00 1544.09 118.32 o 10 0 0 2549.42 2515.12 99.67 o 11 0 0 0.25 -11.34 26.50 o 12 0 0 2726.92 2670.97 151.68 o 13 0 0 1207.12 1094.39 163.42 o 14 0 0 9.87 -96.18 96.18 o 15 0 0 1649.94 1753.96 217.76 o -15 1 0 1535.16 1663.88 211.65 o -14 1 0 264.98 248.67 123.84 o -13 1 0 4006.89 3810.82 278.30 o -12 1 0 7845.98 7060.04 285.05 o -11 1 0 1991.01 2044.16 330.18 o -10 1 0 7.69 27.79 24.92 o -9 1 0 93.19 80.16 24.88 o -8 1 0 0.86 40.55 27.96 o -7 1 0 2613.74 2680.50 176.21 o -6 1 0 7008.15 6882.04 346.81 o -5 1 0 6728.94 6636.32 327.52 o -4 1 0 267.30 393.97 57.98 o -3 1 0 14228.17 14633.32 651.79 o -2 1 0 414.25 494.27 19.40 o 0 1 0 74668.02 -0.03 1.33 o 1 1 0 54087.54 13066.70 571.46 o 2 1 0 4702.55 3423.89 183.79 o 3 1 0 5663.78 5756.28 138.66 o 4 1 0 26486.55 25531.32 696.13 o 5 1 0 22913.33 22122.89 474.01 o 6 1 0 6727.19 6605.94 156.45 o 7 1 0 2360.66 2347.10 63.81 o 8 1 0 873.69 877.04 57.33 o 9 1 0 4670.32 4628.69 259.87 o 10 1 0 3707.97 3886.26 116.85 o 11 1 0 14.10 29.88 30.36 o 12 1 0 785.83 763.92 75.65 o 13 1 0 1361.37 1195.14 126.60 o 14 1 0 153.08 65.90 52.67 o 15 1 0 130.85 -7.88 102.77 o -15 2 0 323.68 479.91 136.44 o -14 2 0 778.41 696.97 143.63 o -13 2 0 8497.81 8182.76 472.33 o -12 2 0 19644.55 18352.39 896.03 o -11 2 0 8281.27 7943.04 308.83 o -10 2 0 987.19 889.75 69.36 o -9 2 0 89.68 85.36 24.02 o -8 2 0 273.19 374.28 33.44 o -7 2 0 270.77 287.33 47.60 o -6 2 0 3076.74 3636.08 146.30 o -5 2 0 3573.10 3761.59 119.68 o -4 2 0 3935.48 4003.98 93.78 o -3 2 0 16016.69 16357.22 325.81 o -1 2 0 5979.25 5534.71 216.50 o 1 2 0 2573.21 2682.33 57.87 o 2 2 0 19540.42 20116.06 318.38 o 3 2 0 10367.44 7959.00 427.24 o 4 2 0 62537.63 61234.62 1102.61 o 5 2 0 84069.11 84994.99 1663.73 o 6 2 0 8984.04 8650.78 215.42 o 7 2 0 482.93 460.25 27.43 o 8 2 0 324.39 389.73 28.57 o 9 2 0 1118.41 1057.15 45.42 o 10 2 0 216.81 284.30 29.54 o 11 2 0 113.75 132.97 46.00 o 12 2 0 1434.63 1313.63 73.79 o 13 2 0 3750.28 3655.16 181.57 o 14 2 0 2409.93 2158.09 135.29 o 15 2 0 51.37 56.16 52.69 o -15 3 0 461.94 565.36 144.91 o -14 3 0 2111.61 1780.73 205.94 o -13 3 0 11002.22 10615.68 576.78 o -12 3 0 16665.11 15333.15 768.84 o -11 3 0 10516.64 10203.35 314.26 o -10 3 0 1052.80 1074.50 56.97 o -9 3 0 1282.50 1317.55 61.99 o -8 3 0 4802.13 4542.14 167.29 o -7 3 0 2335.64 2149.42 80.93 o -6 3 0 4001.15 4663.15 110.24 o -5 3 0 1164.92 1240.58 39.25 o -4 3 0 2466.28 2499.35 53.50 o -3 3 0 5132.92 4870.46 237.15 o -2 3 0 13286.37 13545.55 208.37 o -1 3 0 2250.26 2179.23 46.34 o 0 3 0 16253.01 17297.54 326.26 o 1 3 0 3.84 6.91 12.11 o 2 3 0 613.27 596.05 23.74 o 3 3 0 3861.12 3511.12 77.83 o 4 3 0 43489.83 36243.09 1683.57 o 6 3 0 11719.85 11616.01 240.03 o 7 3 0 1395.61 1457.26 61.39 o 8 3 0 2589.67 2646.87 84.83 o 9 3 0 1661.94 1768.59 63.28 o 10 3 0 902.09 853.31 44.90 o 11 3 0 48.11 34.49 43.58 o 12 3 0 2068.15 2186.18 101.10 o 13 3 0 7265.36 7097.65 241.56 o 14 3 0 4998.99 4685.29 170.38 o -15 4 0 200.23 259.00 126.70 o -14 4 0 41.50 58.18 102.18 o -13 4 0 1416.02 1502.93 184.28 o -12 4 0 2451.29 2333.03 97.29 o -11 4 0 2184.61 2090.68 88.82 o -10 4 0 167.43 272.47 86.29 o -9 4 0 13427.95 13712.08 345.73 o -8 4 0 38223.26 38418.35 824.16 o -7 4 0 20757.16 20413.18 444.99 o -6 4 0 3318.10 3068.51 83.17 o -5 4 0 4.36 8.61 11.34 o -4 4 0 848.60 926.61 32.27 o -3 4 0 11698.28 12210.10 212.34 o -2 4 0 5946.92 5734.65 100.01 o -1 4 0 3471.66 3610.71 72.92 o 0 4 0 434.23 598.48 25.05 o 1 4 0 18648.78 18813.52 331.38 o 2 4 0 2376.76 2334.86 55.08 o 3 4 0 360.74 371.71 21.81 o 4 4 0 10235.08 10131.87 223.79 o 5 4 0 9979.86 9449.63 182.89 o 6 4 0 5065.13 5097.28 189.59 o 7 4 0 135.72 98.67 21.09 o 8 4 0 9523.88 9673.15 226.02 o 9 4 0 14445.78 14060.04 321.15 o 10 4 0 5245.91 5040.32 173.31 o 11 4 0 2223.51 2227.93 101.55 o 12 4 0 1478.82 1348.50 95.54 o 13 4 0 474.45 596.91 62.54 o 14 4 0 774.42 910.25 99.07 o -15 5 0 30.27 -33.86 111.14 o -14 5 0 526.73 371.13 126.70 o -13 5 0 96.32 151.27 49.32 o -12 5 0 937.57 814.81 101.20 o -11 5 0 7.86 -0.87 29.30 o -10 5 0 1052.34 1215.41 48.83 o -9 5 0 15342.27 15305.76 341.45 o -8 5 0 41350.11 41311.84 886.50 o -7 5 0 25021.59 24961.59 542.08 o -6 5 0 2131.71 1882.05 58.20 o -5 5 0 849.23 1103.09 38.05 o -4 5 0 2164.99 2022.98 76.13 o -3 5 0 779.80 869.12 34.38 o -2 5 0 217.96 329.83 21.73 o -1 5 0 64.14 83.11 15.58 o 0 5 0 15.68 23.51 13.61 o 1 5 0 3072.57 2784.86 71.96 o 2 5 0 22424.63 22016.44 406.58 o 3 5 0 5024.62 4928.61 103.57 o 4 5 0 208.24 272.29 21.98 o 5 5 0 3078.61 2742.77 128.08 o 6 5 0 2578.93 2413.36 62.12 o 7 5 0 674.95 776.12 41.34 o 9 5 0 5585.08 5401.84 183.45 o 10 5 0 5632.17 5312.92 183.70 o 11 5 0 1012.20 1001.67 74.69 o 12 5 0 341.88 369.71 55.52 o 13 5 0 10.12 -15.79 43.22 o 14 5 0 0.01 6.78 54.11 o -15 6 0 110.84 118.92 116.85 o -14 6 0 993.68 1137.16 116.11 o -13 6 0 796.28 887.82 97.51 o -12 6 0 26.82 -2.77 35.30 o -11 6 0 6.72 -48.82 32.54 o -10 6 0 123.25 88.87 29.68 o -9 6 0 3490.56 3538.87 98.65 o -8 6 0 19350.47 19032.80 438.10 o -7 6 0 11425.66 10880.20 229.18 o -6 6 0 3554.37 3391.45 89.94 o -5 6 0 682.89 757.06 55.71 o -4 6 0 33134.84 35869.03 721.56 o -3 6 0 28942.23 30272.35 678.49 o -2 6 0 5679.63 5353.86 110.49 o -1 6 0 2880.98 2608.33 70.40 o 0 6 0 2166.62 1939.14 71.07 o 1 6 0 2014.43 1675.98 59.14 o 2 6 0 9225.53 8973.70 176.44 o 3 6 0 8958.28 8704.76 183.94 o 4 6 0 196.78 197.63 30.64 o 5 6 0 3591.48 3276.86 90.34 o 6 6 0 5112.17 4821.93 126.24 o 7 6 0 255.09 254.61 27.58 o 8 6 0 2522.35 2462.81 97.41 o 9 6 0 2469.34 2634.57 113.20 o 10 6 0 663.50 623.28 63.62 o 11 6 0 26.90 -64.80 86.16 o 12 6 0 688.96 750.19 70.43 o 13 6 0 510.45 728.12 72.67 o -15 7 0 6.37 -102.57 72.55 o -14 7 0 275.67 236.47 62.39 o -13 7 0 191.29 180.51 57.32 o -12 7 0 17.31 62.91 42.16 o -11 7 0 493.48 490.44 74.65 o -10 7 0 783.36 875.51 77.28 o -9 7 0 103.26 117.49 28.43 o -8 7 0 2582.29 2508.47 79.41 o -7 7 0 8617.80 8939.47 209.27 o -6 7 0 1250.96 1410.05 47.88 o -5 7 0 1731.35 1795.59 60.01 o -4 7 0 38544.66 41018.19 913.75 o -3 7 0 34609.80 35034.77 709.40 o -2 7 0 30224.35 31127.98 632.41 o -1 7 0 2074.19 1914.37 74.18 o 0 7 0 757.12 1115.40 81.08 o 1 7 0 249.11 299.21 35.36 o 2 7 0 2870.56 3202.48 82.24 o 3 7 0 1.23 -24.10 16.07 o 4 7 0 2421.40 2219.11 61.53 o 5 7 0 12798.10 12864.07 312.87 o 6 7 0 6323.68 6642.56 141.77 o 7 7 0 5695.85 5700.91 136.53 o 8 7 0 749.48 832.45 109.36 o 9 7 0 167.24 198.53 63.45 o 10 7 0 1195.02 1268.43 88.45 o 11 7 0 48.81 36.97 46.78 o 12 7 0 1554.86 1697.25 100.73 o 13 7 0 3450.83 3446.80 150.62 o -14 8 0 975.64 1069.76 85.41 o -13 8 0 921.98 843.71 91.15 o -12 8 0 2304.65 2410.67 145.51 o -11 8 0 2348.17 2351.99 221.59 o -10 8 0 3917.61 3668.11 142.33 o -9 8 0 395.71 511.58 58.48 o -8 8 0 36.23 5.74 24.99 o -7 8 0 2071.38 2285.72 67.12 o -6 8 0 724.23 679.56 39.58 o -5 8 0 17.82 18.06 20.25 o -4 8 0 10726.06 11246.77 243.01 o -3 8 0 21191.70 21195.62 438.83 o -2 8 0 7926.25 7959.01 220.24 o -1 8 0 588.24 620.71 45.67 o 0 8 0 6967.10 6925.79 195.34 o 1 8 0 6034.51 5712.14 167.17 o 2 8 0 3318.70 3383.82 103.13 o 3 8 0 6988.53 6908.62 170.07 o 4 8 0 8310.40 7798.93 189.38 o 5 8 0 12000.37 11712.78 303.68 o 6 8 0 5971.11 5736.79 140.36 o 7 8 0 5248.16 5275.88 182.97 o 8 8 0 344.34 379.79 53.03 o 9 8 0 436.49 431.90 60.76 o 10 8 0 3097.31 3121.08 136.46 o 11 8 0 645.10 748.68 76.76 o 12 8 0 167.64 195.72 60.10 o -14 9 0 1775.59 1731.91 112.64 o -13 9 0 1002.55 1102.81 93.03 o -11 9 0 1682.91 1640.94 156.62 o -10 9 0 855.04 1113.49 133.49 o -9 9 0 1900.86 1960.88 177.30 o -8 9 0 493.45 616.05 107.01 o -7 9 0 2935.55 3091.12 97.99 o -6 9 0 2944.50 3645.90 125.76 o -5 9 0 1416.58 1594.36 57.78 o -4 9 0 436.82 485.38 34.30 o -3 9 0 5384.24 5305.81 159.38 o -2 9 0 9247.11 9658.38 264.10 o -1 9 0 246.29 447.02 58.78 o 0 9 0 7630.68 7505.75 213.69 o 1 9 0 20331.49 19771.22 508.35 o 2 9 0 16201.55 15203.12 343.42 o 3 9 0 5565.33 5319.68 139.81 o 4 9 0 2505.75 2548.62 84.29 o 5 9 0 1877.48 1953.38 74.40 o 6 9 0 1041.09 1037.85 79.37 o 7 9 0 462.24 559.05 59.76 o 8 9 0 134.11 264.13 52.07 o 9 9 0 6098.57 6146.03 217.49 o 10 9 0 9669.97 9744.08 316.41 o 11 9 0 4655.08 4479.54 180.06 o 12 9 0 1291.99 1323.90 100.09 o -14 10 0 2794.64 2687.74 192.50 o -13 10 0 62.78 10.49 128.42 o -12 10 0 687.78 766.67 128.57 o -11 10 0 371.85 423.66 74.14 o -10 10 0 278.98 352.58 71.01 o -9 10 0 1536.87 1567.98 117.97 o -8 10 0 1525.47 1721.19 122.56 o -7 10 0 9100.84 9127.49 366.87 o -6 10 0 13261.00 13218.56 288.05 o -5 10 0 6109.37 6418.94 154.67 o -4 10 0 4.04 -32.32 38.38 o -3 10 0 2267.49 2267.55 92.26 o -2 10 0 8929.62 8995.98 252.70 o 0 10 0 652.69 763.56 56.27 o 1 10 0 7059.88 6551.03 163.50 o 2 10 0 6799.52 6820.53 172.12 o 3 10 0 3168.85 3011.49 159.04 o 4 10 0 461.87 479.35 43.23 o 5 10 0 154.88 142.64 40.07 o 6 10 0 694.19 804.68 101.89 o 7 10 0 115.49 334.28 57.89 o 8 10 0 1408.99 1689.46 100.87 o 9 10 0 5639.79 5533.17 204.03 o 10 10 0 8918.77 8813.74 293.59 o 11 10 0 5795.49 5974.89 231.43 o -13 11 0 61.17 45.37 59.22 o -12 11 0 3508.20 3554.92 185.56 o -11 11 0 5722.33 5485.37 249.85 o -10 11 0 3283.47 3063.08 168.61 o -9 11 0 2587.78 2342.06 145.17 o -8 11 0 6133.90 5862.16 260.25 o -7 11 0 3141.19 2942.36 197.82 o -6 11 0 11967.78 11677.88 319.09 o -5 11 0 4234.56 4378.27 145.96 o -4 11 0 401.69 506.75 62.41 o -3 11 0 1548.68 1698.73 83.11 o -2 11 0 5151.40 5464.58 171.51 o -1 11 0 4493.68 5108.63 163.31 o 0 11 0 2294.36 2717.85 142.76 o 1 11 0 55.68 85.03 26.39 o 2 11 0 1194.73 1100.59 56.48 o 3 11 0 3642.85 3334.20 103.36 o 4 11 0 385.21 355.02 41.17 o 5 11 0 1918.61 1961.56 77.18 o 6 11 0 2760.84 2634.82 119.68 o 7 11 0 865.21 957.50 77.76 o 8 11 0 753.27 778.82 75.58 o 9 11 0 1315.50 1332.74 95.66 o 10 11 0 3149.63 3032.24 143.32 o 11 11 0 2601.99 2490.46 159.74 o -13 12 0 0.50 7.66 62.18 o -12 12 0 1523.32 1720.77 134.34 o -11 12 0 4136.41 4236.63 213.29 o -10 12 0 4879.74 5173.56 244.90 o -9 12 0 103.45 228.83 71.47 o -8 12 0 14.66 16.85 66.35 o -7 12 0 448.01 480.71 82.17 o -6 12 0 363.79 309.52 76.33 o -5 12 0 39.27 13.95 34.86 o -4 12 0 883.54 967.68 81.49 o -3 12 0 7694.51 7690.92 228.24 o -2 12 0 15065.37 15167.44 409.14 o -1 12 0 9810.46 11050.62 310.24 o 0 12 0 3456.98 4299.19 149.69 o 1 12 0 22.37 107.47 27.07 o 2 12 0 2848.97 2743.02 91.87 o 3 12 0 803.99 822.43 52.56 o 4 12 0 1063.66 1185.88 62.12 o 5 12 0 527.80 645.31 77.04 o 6 12 0 2233.41 2288.71 112.10 o 7 12 0 0.32 -62.91 41.94 o 8 12 0 74.72 -22.92 46.12 o 9 12 0 102.80 69.35 51.58 o 10 12 0 287.52 290.74 68.96 o -12 13 0 241.33 255.12 77.51 o -11 13 0 631.66 818.11 103.62 o -10 13 0 643.12 915.80 105.89 o -9 13 0 19.98 158.35 98.39 o -8 13 0 3174.64 3116.88 182.47 o -7 13 0 3610.25 3644.87 225.38 o -6 13 0 2104.21 2324.12 212.29 o -5 13 0 134.73 179.73 71.97 o -4 13 0 413.07 510.25 55.39 o -3 13 0 5165.56 5131.04 170.45 o -2 13 0 6457.32 6752.96 210.69 o -1 13 0 12972.56 13388.13 371.86 o 0 13 0 4251.95 5589.60 183.45 o 1 13 0 782.06 944.46 70.53 o 2 13 0 2856.09 2766.21 115.57 o 3 13 0 2101.76 1896.60 98.44 o 4 13 0 565.24 640.22 94.09 o 5 13 0 88.26 50.69 103.27 o 6 13 0 62.58 49.82 66.54 o 7 13 0 157.45 167.99 76.00 o 8 13 0 491.69 589.54 101.04 o 9 13 0 665.46 696.67 107.46 o -11 14 0 673.70 976.13 121.18 o -10 14 0 1473.91 1605.42 141.01 o -9 14 0 225.78 104.27 75.84 o -8 14 0 1404.07 1495.62 137.21 o -7 14 0 5986.66 6101.43 288.19 o -6 14 0 6159.77 5909.48 280.93 o -5 14 0 2178.51 2572.98 170.11 o -4 14 0 51.84 2.27 44.03 o -3 14 0 1145.47 1299.05 81.86 o -2 14 0 2219.79 2334.18 107.47 o -1 14 0 2663.47 2839.15 118.62 o 0 14 0 31.32 77.93 43.63 o 1 14 0 1761.40 1911.71 99.73 o 2 14 0 9370.14 9162.53 403.86 o 3 14 0 11358.94 11229.04 347.99 o 4 14 0 3370.80 3372.07 224.25 o 5 14 0 197.57 231.35 77.76 o 6 14 0 85.53 141.48 69.39 o 7 14 0 110.22 84.10 107.89 o 8 14 0 565.43 554.91 107.53 o -10 15 0 1969.32 2099.69 163.87 o -9 15 0 282.46 349.36 93.90 o -8 15 0 67.32 61.78 128.32 o -7 15 0 415.17 382.62 95.08 o -6 15 0 1469.53 1292.80 213.42 o -5 15 0 330.40 244.18 86.70 o -4 15 0 464.37 486.89 101.38 o -3 15 0 1055.87 1138.33 81.73 o -2 15 0 648.59 709.10 68.66 o -1 15 0 407.68 453.74 60.90 o 0 15 0 7.00 24.65 45.16 o 1 15 0 3069.75 3002.96 128.53 o 2 15 0 8211.17 7967.87 251.83 o 3 15 0 8277.91 7628.58 342.13 o 4 15 0 3304.39 3073.86 222.73 o 5 15 0 53.87 -16.80 67.06 o 6 15 0 2461.37 2370.25 189.80 o 7 15 0 2568.77 2591.09 182.27 o -9 16 0 4562.54 4788.35 254.28 o -8 16 0 1370.25 1426.86 145.22 o -7 16 0 112.57 175.51 86.38 o -6 16 0 995.25 896.05 117.87 o -5 16 0 98.03 -49.32 119.12 o -4 16 0 809.02 692.09 117.79 o -3 16 0 1857.45 1731.02 153.11 o -2 16 0 1135.23 1109.66 83.10 o -1 16 0 156.88 160.01 52.55 o 0 16 0 22.77 14.41 45.02 o 1 16 0 817.12 754.63 74.35 o 2 16 0 3218.86 3160.14 188.55 o 3 16 0 2759.94 2393.12 169.06 o 4 16 0 945.43 948.61 119.00 o 5 16 0 407.91 177.84 89.39 o -8 17 0 2533.77 2742.42 254.82 o -7 17 0 115.58 71.10 89.13 o -6 17 0 939.98 1151.17 137.96 o -5 17 0 677.05 659.42 116.18 o -4 17 0 63.39 -104.69 69.80 o -3 17 0 73.40 58.40 81.01 o -2 17 0 60.29 11.45 78.55 o -1 17 0 140.53 86.97 50.58 o 0 17 0 311.52 269.39 60.73 o 1 17 0 150.81 41.56 68.06 o 2 17 0 7.54 15.07 70.72 o 3 17 0 457.29 460.07 94.91 o 4 17 0 197.59 143.88 119.76 o -6 18 0 4637.62 4843.27 272.11 o -5 18 0 3424.46 3261.05 215.41 o -4 18 0 3297.57 3106.78 208.40 o -3 18 0 1057.74 1057.23 136.76 o -2 18 0 121.82 206.15 90.76 o -1 18 0 335.65 176.33 95.42 o 0 18 0 2529.16 2258.56 126.84 o 1 18 0 1520.99 1381.65 143.91 o -2 -18 1 1892.65 1654.94 205.84 o -1 -18 1 1246.94 1206.61 133.26 o 0 -18 1 2.26 -42.88 53.91 o 1 -18 1 2062.10 2044.06 179.41 o 2 -18 1 1142.91 1081.84 133.57 o 3 -18 1 1.21 126.60 87.73 o 4 -18 1 384.33 195.47 97.49 o 5 -18 1 1182.87 1305.92 149.64 o 6 -18 1 1398.16 1383.99 154.56 o -4 -17 1 95.62 92.38 111.14 o -3 -17 1 2.21 50.64 103.81 o -2 -17 1 141.09 224.58 80.63 o -1 -17 1 583.18 498.94 83.87 o 0 -17 1 1454.71 1322.53 116.46 o 1 -17 1 4044.59 3982.84 159.15 o 2 -17 1 5469.66 5560.77 287.18 o 3 -17 1 1425.02 1393.33 145.49 o 4 -17 1 56.83 86.54 81.74 o 5 -17 1 1531.98 1666.28 155.75 o 6 -17 1 717.51 607.62 145.99 o 7 -17 1 96.42 217.57 93.82 o 8 -17 1 1696.11 1832.63 168.29 o -6 -16 1 1683.98 1895.12 165.51 o -5 -16 1 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