# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' JAK_D36_p-1 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 183.87 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7971 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 5.5061 _cell_length_b 7.4731 _cell_length_c 25.0391 _cell_angle_alpha 83.464 _cell_angle_beta 85.196 _cell_angle_gamma 79.439 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1737.28 1747.50 23.86 o 3 0 0 1581.06 1550.55 26.53 o 4 0 0 456.02 463.21 15.31 o 5 0 0 763.88 756.03 29.65 o 6 0 0 239.58 277.01 20.92 o -6 1 0 344.75 366.60 26.06 o -5 1 0 5.12 -0.92 4.79 o -4 1 0 24.27 24.16 5.69 o -3 1 0 2127.15 2139.34 40.04 o -2 1 0 398.58 387.00 11.24 o -1 1 0 1035.39 1047.57 33.28 o 1 1 0 526.96 524.52 18.74 o 2 1 0 2904.60 2921.69 40.79 o 3 1 0 840.24 789.26 18.48 o 4 1 0 21.45 23.54 4.26 o 5 1 0 331.81 332.66 16.93 o 6 1 0 329.53 305.46 25.56 o -6 2 0 409.48 437.49 33.23 o -5 2 0 27.67 26.66 12.75 o -4 2 0 1530.64 1561.14 53.58 o -3 2 0 1964.40 1983.83 43.56 o -2 2 0 0.85 3.02 4.29 o -1 2 0 5963.37 6131.36 74.34 o 0 2 0 1358.15 1352.70 17.97 o 1 2 0 91.20 94.98 3.43 o 3 2 0 1544.41 1517.50 28.42 o 4 2 0 92.06 92.91 7.28 o 5 2 0 1498.45 1548.36 37.73 o 6 2 0 1561.03 1602.32 48.62 o -5 3 0 2.22 8.26 9.51 o -4 3 0 951.68 1003.74 34.12 o -3 3 0 602.77 626.62 23.54 o -2 3 0 55.97 50.45 7.61 o -1 3 0 1533.38 1490.65 29.86 o 0 3 0 1148.16 1119.61 17.60 o 1 3 0 2402.64 2382.17 29.38 o 2 3 0 834.31 808.32 30.53 o 4 3 0 29.82 37.30 16.64 o 5 3 0 915.22 892.80 75.98 o 6 3 0 3.02 5.93 12.95 o -5 4 0 3.99 -3.57 6.86 o -4 4 0 471.91 533.31 28.34 o -3 4 0 633.31 650.83 25.77 o -2 4 0 56.40 26.62 9.32 o -1 4 0 801.26 813.54 23.32 o 0 4 0 1095.74 1094.15 35.70 o 1 4 0 422.90 425.84 10.54 o 2 4 0 2212.84 2386.32 39.84 o 3 4 0 9.66 13.45 13.56 o 5 4 0 858.94 679.34 58.56 o 6 4 0 25.34 17.71 19.96 o -5 5 0 65.89 63.62 11.51 o -4 5 0 493.85 549.20 39.52 o -3 5 0 243.76 278.15 22.53 o -2 5 0 398.26 398.26 19.61 o -1 5 0 1852.90 1873.97 42.42 o 0 5 0 275.53 322.37 15.10 o 1 5 0 468.71 488.77 17.51 o 2 5 0 1115.00 1132.95 22.86 o 3 5 0 24.59 22.90 5.21 o 4 5 0 430.66 406.34 45.71 o -4 6 0 226.52 223.51 22.82 o -3 6 0 5.95 13.67 8.31 o -2 6 0 295.01 286.42 22.50 o -1 6 0 1263.83 1253.12 38.46 o 0 6 0 5.51 2.54 5.33 o 1 6 0 897.70 944.26 34.40 o 2 6 0 725.56 713.60 21.99 o 3 6 0 7.28 5.37 7.44 o 4 6 0 306.61 299.53 18.77 o 5 6 0 187.48 231.53 35.05 o -3 7 0 13.52 28.85 11.37 o -2 7 0 51.20 55.39 10.50 o -1 7 0 325.44 353.20 24.23 o 0 7 0 1.42 4.05 7.06 o 1 7 0 900.30 939.74 37.26 o 2 7 0 318.31 302.83 31.38 o 3 7 0 157.67 108.85 20.38 o 4 7 0 211.69 202.51 17.03 o 5 7 0 174.11 203.68 48.71 o -2 8 0 1161.44 1053.77 49.95 o -1 8 0 278.95 289.21 26.22 o 0 8 0 42.09 46.84 8.58 o 1 8 0 466.14 418.79 28.65 o 2 8 0 117.58 123.78 22.31 o 3 8 0 414.79 415.94 32.85 o 4 8 0 128.49 44.22 23.70 o 0 9 0 121.53 122.10 42.11 o 1 9 0 261.16 311.70 48.71 o 2 9 0 27.99 32.44 22.86 o -2 -9 1 164.79 141.50 24.05 o -1 -9 1 74.59 49.91 24.99 o 0 -9 1 2.13 13.10 28.35 o -4 -8 1 1068.22 1037.61 50.31 o -3 -8 1 2.54 -8.96 18.13 o -2 -8 1 463.44 452.16 38.23 o -1 -8 1 268.22 229.75 36.19 o 0 -8 1 55.22 64.88 9.44 o 1 -8 1 738.63 718.47 41.35 o 2 -8 1 115.13 171.09 24.96 o -4 -7 1 138.33 156.46 17.29 o -3 -7 1 16.20 14.43 8.07 o -2 -7 1 370.36 371.96 32.85 o -1 -7 1 184.94 164.27 27.70 o 0 -7 1 241.48 271.44 19.65 o 1 -7 1 567.05 536.71 30.29 o 2 -7 1 13.33 22.60 11.10 o 3 -7 1 332.47 329.69 31.08 o -5 -6 1 375.84 413.82 50.87 o -4 -6 1 75.02 59.18 11.81 o -3 -6 1 825.30 846.94 41.72 o -2 -6 1 1178.86 1194.40 34.75 o -1 -6 1 33.75 28.30 5.95 o 0 -6 1 399.85 387.74 21.40 o 1 -6 1 1111.80 1121.25 35.99 o 2 -6 1 76.62 70.53 12.21 o 3 -6 1 410.58 453.45 29.71 o 4 -6 1 99.68 107.36 17.28 o -4 -5 1 2.58 1.73 15.21 o -3 -5 1 1200.28 1165.35 27.24 o -2 -5 1 941.91 994.47 16.61 o -1 -5 1 120.47 126.51 8.56 o 0 -5 1 1255.51 1322.92 32.92 o 1 -5 1 933.32 894.40 27.09 o 2 -5 1 3.14 4.78 5.09 o 3 -5 1 967.79 1070.62 39.50 o 4 -5 1 173.67 197.47 19.63 o 5 -5 1 95.09 126.59 24.65 o -6 -4 1 218.09 169.51 30.57 o -5 -4 1 666.07 705.09 40.57 o -4 -4 1 2.50 16.43 15.04 o -3 -4 1 667.96 661.95 14.79 o -2 -4 1 718.86 583.84 15.48 o -1 -4 1 157.52 166.07 6.90 o 0 -4 1 2514.02 2427.75 42.18 o 1 -4 1 300.11 272.05 13.97 o 2 -4 1 561.93 577.42 22.53 o 3 -4 1 963.45 935.42 31.69 o 4 -4 1 198.10 216.81 20.31 o 5 -4 1 258.00 262.64 24.56 o -6 -3 1 157.09 165.41 13.87 o -5 -3 1 555.04 574.94 24.03 o -4 -3 1 139.16 116.35 16.65 o -3 -3 1 2442.15 2285.70 122.81 o -2 -3 1 126.17 126.46 6.84 o -1 -3 1 789.10 785.32 12.98 o 0 -3 1 1257.57 1240.26 19.02 o 1 -3 1 144.82 130.28 9.60 o 2 -3 1 1842.80 1791.16 40.56 o 3 -3 1 778.89 736.69 25.73 o 4 -3 1 5.76 13.48 7.06 o 5 -3 1 417.02 435.26 24.64 o -6 -2 1 589.22 581.56 25.55 o -5 -2 1 315.85 327.97 14.53 o -4 -2 1 354.20 363.54 12.63 o -3 -2 1 3166.22 3155.18 57.39 o -2 -2 1 292.81 316.39 13.15 o -1 -2 1 3461.34 3374.57 43.75 o 0 -2 1 438.87 437.37 8.65 o 1 -2 1 741.77 794.71 15.64 o 2 -2 1 490.92 432.27 14.66 o 3 -2 1 1359.43 1337.23 33.80 o 4 -2 1 959.63 1032.02 35.62 o 5 -2 1 649.44 669.86 30.38 o 6 -2 1 184.02 222.73 24.29 o -6 -1 1 479.63 430.16 20.59 o -5 -1 1 125.19 117.08 11.49 o -4 -1 1 707.17 740.92 20.47 o -3 -1 1 732.25 718.55 15.41 o -2 -1 1 113.36 119.16 6.01 o -1 -1 1 9161.33 8503.96 121.90 o 1 -1 1 267.67 265.17 7.02 o 2 -1 1 1788.22 1773.62 28.67 o 3 -1 1 1014.55 1061.71 25.09 o 4 -1 1 30.82 18.93 6.77 o 5 -1 1 1894.20 1873.48 46.15 o 6 -1 1 64.69 25.73 12.94 o -6 0 1 906.54 907.12 35.12 o -5 0 1 127.54 137.02 14.50 o -4 0 1 2030.49 1999.83 41.84 o -3 0 1 1381.70 1343.92 24.08 o -2 0 1 130.39 134.70 5.37 o -1 0 1 5657.95 5969.82 147.99 o 1 0 1 115.84 87.72 9.85 o 2 0 1 4886.15 4972.88 53.57 o 3 0 1 192.13 208.84 8.53 o 4 0 1 471.37 490.71 15.76 o 5 0 1 753.95 748.89 29.47 o 6 0 1 28.97 40.53 8.23 o -6 1 1 336.14 376.75 31.63 o -5 1 1 1031.42 937.14 29.77 o -4 1 1 145.92 149.08 12.31 o -3 1 1 939.37 954.69 23.39 o -2 1 1 309.47 315.54 10.17 o -1 1 1 1685.43 1654.70 40.79 o 1 1 1 422.82 415.55 15.81 o 2 1 1 4342.10 4310.93 58.59 o 3 1 1 63.16 57.56 4.79 o 4 1 1 380.12 382.05 13.85 o 5 1 1 430.68 436.52 19.48 o 6 1 1 40.73 24.82 10.29 o -6 2 1 210.00 204.85 23.59 o -5 2 1 135.79 143.54 13.32 o -4 2 1 1374.20 1464.28 39.95 o -3 2 1 443.35 426.69 17.70 o -2 2 1 859.31 884.47 25.58 o -1 2 1 6410.13 6526.34 76.33 o 0 2 1 3456.02 3445.49 39.18 o 1 2 1 7504.57 7525.21 97.42 o 3 2 1 0.33 2.27 3.07 o 4 2 1 1282.83 1271.87 22.40 o 5 2 1 1311.09 1382.33 40.41 o 6 2 1 26.70 31.09 9.29 o -5 3 1 411.12 388.33 23.43 o -4 3 1 996.13 986.85 33.60 o -3 3 1 26.70 28.80 6.65 o -2 3 1 929.53 908.70 26.37 o -1 3 1 1272.28 1206.27 25.87 o 0 3 1 132.15 135.51 5.95 o 1 3 1 113.73 135.20 4.27 o 2 3 1 437.79 407.56 10.71 o 5 3 1 209.58 150.09 86.40 o 6 3 1 39.68 30.19 35.78 o -5 4 1 326.32 345.49 26.25 o -4 4 1 1823.90 1772.06 53.48 o -3 4 1 0.02 -2.41 4.52 o -1 4 1 163.22 150.93 11.21 o 0 4 1 23.58 14.16 4.58 o 1 4 1 1658.10 1630.24 22.90 o 2 4 1 1113.86 1110.21 21.93 o 6 4 1 67.54 59.07 15.79 o -5 5 1 485.69 472.06 30.49 o -4 5 1 314.94 322.45 25.67 o -3 5 1 10.60 10.28 6.91 o -2 5 1 1061.71 1033.22 31.43 o -1 5 1 881.76 893.61 36.68 o 0 5 1 106.65 85.36 8.57 o 1 5 1 1050.68 1049.80 23.65 o 2 5 1 301.12 285.18 12.62 o 3 5 1 329.45 318.46 11.72 o 4 5 1 860.82 850.65 64.67 o -4 6 1 98.08 98.34 16.00 o -3 6 1 351.65 390.55 28.83 o -2 6 1 678.23 718.69 31.36 o -1 6 1 242.29 269.96 18.83 o 0 6 1 315.37 332.94 21.54 o 1 6 1 1282.96 1315.29 38.48 o 2 6 1 1.31 -0.26 2.33 o 3 6 1 460.10 472.54 28.67 o 4 6 1 252.85 249.46 16.15 o -3 7 1 112.43 138.88 28.63 o -2 7 1 330.23 344.80 25.82 o -1 7 1 6.79 20.28 7.01 o 0 7 1 374.89 373.99 20.33 o 1 7 1 783.93 775.53 32.74 o 2 7 1 29.23 30.43 15.62 o 3 7 1 1014.97 1034.52 50.46 o 4 7 1 166.69 161.18 41.96 o 5 7 1 4.49 -7.39 17.77 o -2 8 1 31.35 38.44 10.81 o -1 8 1 24.61 -5.62 6.69 o 0 8 1 379.62 413.52 26.45 o 1 8 1 167.19 158.44 19.08 o 2 8 1 89.02 86.12 19.21 o 3 8 1 760.87 787.10 46.74 o 4 8 1 179.89 137.00 47.05 o 0 9 1 277.28 324.41 57.40 o 1 9 1 125.28 172.93 37.66 o 2 9 1 48.52 4.26 18.02 o -2 -9 2 126.63 136.17 25.00 o -1 -9 2 73.68 50.34 26.97 o 0 -9 2 137.25 103.64 39.32 o -4 -8 2 318.27 299.16 38.62 o -3 -8 2 282.74 312.92 28.79 o -2 -8 2 321.83 303.07 34.37 o -1 -8 2 1.66 -3.50 10.77 o 0 -8 2 291.83 330.90 23.43 o 1 -8 2 91.67 94.35 13.00 o 2 -8 2 37.02 44.71 11.55 o -5 -7 2 180.94 114.40 82.41 o -4 -7 2 0.98 -3.84 7.54 o -3 -7 2 138.90 139.50 40.78 o -2 -7 2 59.56 50.25 13.24 o -1 -7 2 88.27 70.44 15.51 o 0 -7 2 508.91 453.27 25.81 o 1 -7 2 13.72 12.46 12.16 o 2 -7 2 368.74 396.64 31.54 o 3 -7 2 484.42 465.80 36.47 o -5 -6 2 99.44 168.91 35.65 o -4 -6 2 9.17 15.51 5.47 o -3 -6 2 1427.34 1390.71 58.32 o -2 -6 2 478.93 478.54 20.67 o -1 -6 2 446.06 424.40 22.97 o 0 -6 2 645.60 678.70 28.89 o 1 -6 2 49.72 56.49 10.35 o 2 -6 2 939.90 915.94 36.25 o 3 -6 2 571.82 548.21 30.13 o 4 -6 2 15.21 7.22 7.82 o -6 -5 2 293.33 245.05 50.83 o -5 -5 2 8.73 28.35 19.17 o -4 -5 2 291.45 287.95 16.65 o -3 -5 2 119.39 147.89 9.12 o -2 -5 2 130.06 124.94 7.29 o -1 -5 2 1337.88 1339.82 32.70 o 0 -5 2 1350.21 1357.81 40.46 o 1 -5 2 4.31 4.04 4.49 o 2 -5 2 296.08 320.56 18.40 o 3 -5 2 331.90 369.89 25.41 o 4 -5 2 22.73 22.70 10.21 o 5 -5 2 448.32 452.25 33.52 o -6 -4 2 266.58 221.43 54.61 o -5 -4 2 47.00 93.23 29.72 o -4 -4 2 386.84 368.83 28.13 o -3 -4 2 641.18 626.68 17.11 o -2 -4 2 59.03 50.42 5.27 o -1 -4 2 1455.11 1479.97 23.56 o 0 -4 2 1537.56 1544.39 34.41 o 1 -4 2 141.66 160.18 11.69 o 2 -4 2 1634.61 1722.28 79.06 o 3 -4 2 359.62 393.59 24.30 o 4 -4 2 17.34 41.84 12.61 o 5 -4 2 461.35 454.54 33.26 o -6 -3 2 179.93 164.99 13.97 o -5 -3 2 0.53 -3.56 6.08 o -4 -3 2 457.02 447.55 11.06 o -3 -3 2 1340.34 1309.42 25.76 o -2 -3 2 300.61 291.35 9.37 o -1 -3 2 3578.30 3598.63 42.63 o 0 -3 2 213.05 220.43 9.03 o 1 -3 2 808.90 819.45 29.27 o 2 -3 2 3107.67 3152.03 57.90 o 3 -3 2 742.58 827.34 27.70 o 4 -3 2 451.09 422.07 22.51 o 5 -3 2 571.33 598.46 29.29 o -6 -2 2 297.71 296.55 17.74 o -5 -2 2 109.81 112.18 12.94 o -4 -2 2 1196.57 1231.21 25.12 o -3 -2 2 1476.62 1524.27 34.33 o -2 -2 2 531.16 616.11 12.09 o -1 -2 2 5633.61 5480.83 69.08 o 0 -2 2 3.80 2.55 2.22 o 1 -2 2 1320.10 1304.34 21.13 o 2 -2 2 531.98 495.19 17.33 o 3 -2 2 16.11 5.50 4.55 o 4 -2 2 392.74 373.04 19.20 o 5 -2 2 690.37 719.27 27.84 o 6 -2 2 3.39 0.21 10.29 o -6 -1 2 497.64 474.66 21.93 o -5 -1 2 123.29 125.79 12.24 o -4 -1 2 1247.85 1251.80 28.96 o -3 -1 2 3.53 2.92 2.17 o -2 -1 2 1513.73 1498.79 22.37 o -1 -1 2 10875.79 10659.28 136.11 o 0 -1 2 6.40 -0.87 0.87 o 1 -1 2 3829.89 3849.83 44.13 o 2 -1 2 1250.83 1232.22 27.34 o 3 -1 2 1.54 0.97 3.58 o 4 -1 2 1062.45 1070.94 30.57 o 5 -1 2 1030.15 1058.57 32.17 o 6 -1 2 62.41 35.75 14.51 o -6 0 2 471.63 413.14 31.03 o -5 0 2 1417.36 1443.62 47.52 o -4 0 2 2013.70 2042.09 38.67 o -3 0 2 83.54 87.18 6.16 o -2 0 2 3710.76 3732.51 43.76 o -1 0 2 1774.27 1848.19 40.42 o 1 0 2 1154.14 645.74 26.83 o 2 0 2 3484.66 3582.98 40.00 o 3 0 2 385.10 376.00 11.09 o 4 0 2 5314.00 5206.84 80.00 o 5 0 2 451.80 467.53 22.62 o 6 0 2 75.23 70.51 12.34 o -6 1 2 0.16 -6.70 6.70 o -5 1 2 276.38 299.44 22.31 o -4 1 2 82.43 86.05 9.50 o -3 1 2 20.06 24.72 5.47 o -2 1 2 1993.91 1962.36 30.07 o -1 1 2 20.82 18.42 3.03 o 0 1 2 84.77 75.04 4.27 o 1 1 2 1756.67 1688.04 58.95 o 2 1 2 1295.06 1309.85 22.83 o 3 1 2 298.64 310.04 9.62 o 4 1 2 1167.35 1163.60 27.15 o 5 1 2 461.39 426.00 25.81 o 6 1 2 605.01 567.20 31.33 o -6 2 2 0.34 3.01 8.99 o -5 2 2 1086.62 1095.67 35.33 o -4 2 2 281.26 289.62 17.60 o -3 2 2 266.28 281.01 15.16 o -2 2 2 1857.43 1828.73 34.20 o -1 2 2 1477.23 1452.92 24.55 o 0 2 2 33808.75 34134.74 360.64 o 1 2 2 16440.71 16248.51 181.38 o 3 2 2 1149.32 1164.15 45.64 o 4 2 2 1821.30 1856.46 33.78 o 5 2 2 8.89 -0.06 5.20 o 6 2 2 187.70 187.46 14.90 o -5 3 2 14.36 12.30 8.70 o -4 3 2 643.33 633.98 26.55 o -3 3 2 276.34 290.87 17.27 o -2 3 2 2226.16 2178.68 45.88 o -1 3 2 53.32 58.62 6.40 o 0 3 2 256.99 256.07 7.61 o 1 3 2 1762.08 1675.39 20.54 o 2 3 2 83.47 99.00 9.25 o 5 3 2 62.04 39.51 15.55 o 6 3 2 248.66 234.99 40.31 o -5 4 2 376.40 397.90 34.80 o -4 4 2 4.08 20.41 6.98 o -3 4 2 585.90 607.23 24.76 o -2 4 2 1464.60 1432.68 63.20 o -1 4 2 320.37 364.66 15.83 o 0 4 2 2482.42 2485.53 40.91 o 1 4 2 733.84 732.76 13.31 o 2 4 2 13.97 13.39 2.77 o 6 4 2 1040.39 1014.30 69.86 o -5 5 2 461.20 489.58 43.70 o -4 5 2 4.61 6.40 7.55 o -3 5 2 492.69 533.69 27.97 o -2 5 2 677.59 693.55 24.89 o -1 5 2 3.47 -1.02 4.21 o 0 5 2 858.75 821.70 24.28 o 1 5 2 44.80 46.15 5.54 o 2 5 2 107.89 93.97 7.15 o 3 5 2 656.55 679.87 32.11 o -4 6 2 1.50 4.16 8.56 o -3 6 2 840.30 854.89 36.71 o -2 6 2 308.53 320.30 23.42 o -1 6 2 108.74 107.97 13.65 o 0 6 2 691.45 688.48 24.86 o 1 6 2 389.27 399.67 18.52 o 2 6 2 262.48 274.63 19.60 o 3 6 2 648.87 630.51 33.22 o 4 6 2 3.73 0.03 14.16 o -3 7 2 605.66 625.62 33.77 o -2 7 2 191.58 189.94 18.44 o -1 7 2 440.09 497.13 25.51 o 0 7 2 720.75 730.65 27.27 o 1 7 2 77.37 70.65 8.70 o 2 7 2 131.65 116.01 17.94 o 3 7 2 494.45 527.42 33.97 o 4 7 2 1.51 -4.71 4.71 o 5 7 2 211.74 164.55 60.84 o -2 8 2 3.78 8.07 12.79 o -1 8 2 387.11 409.02 25.11 o 0 8 2 462.22 473.66 37.95 o 1 8 2 12.40 8.72 6.93 o 2 8 2 640.68 620.75 43.71 o 3 8 2 297.67 233.28 36.63 o 4 8 2 10.86 -15.80 15.80 o 0 9 2 143.90 162.41 45.82 o 1 9 2 5.71 12.00 15.43 o 2 9 2 279.21 270.76 34.77 o -2 -9 3 3.86 5.65 14.08 o -1 -9 3 470.15 483.93 60.43 o 0 -9 3 630.22 655.31 75.54 o -4 -8 3 307.03 282.45 43.67 o -3 -8 3 343.07 415.81 34.10 o -2 -8 3 4.13 11.37 8.82 o -1 -8 3 146.73 151.02 26.84 o 0 -8 3 723.94 741.46 34.97 o 1 -8 3 43.10 36.95 8.26 o 2 -8 3 258.40 225.02 23.45 o -5 -7 3 52.40 34.48 31.12 o -4 -7 3 103.09 77.50 22.60 o -3 -7 3 245.12 282.34 29.79 o -2 -7 3 105.92 74.19 33.32 o -1 -7 3 519.05 558.21 24.86 o 0 -7 3 327.59 323.38 21.88 o 1 -7 3 282.69 265.91 23.73 o 2 -7 3 615.00 624.82 42.48 o 3 -7 3 158.49 140.80 25.10 o -5 -6 3 68.49 28.80 24.15 o -4 -6 3 1861.92 2032.27 71.19 o -3 -6 3 403.28 420.60 26.09 o -2 -6 3 3.06 7.83 3.26 o -1 -6 3 1012.76 1012.70 33.57 o 0 -6 3 294.20 299.55 20.05 o 1 -6 3 600.70 619.34 29.83 o 2 -6 3 818.56 790.18 38.08 o 3 -6 3 144.96 162.54 21.13 o 4 -6 3 265.20 303.78 31.06 o -6 -5 3 125.32 120.13 46.91 o -5 -5 3 176.73 142.79 34.17 o -4 -5 3 881.84 957.53 37.95 o -3 -5 3 316.70 301.79 13.76 o -2 -5 3 143.74 144.32 7.72 o -1 -5 3 1311.32 1330.35 32.70 o 0 -5 3 428.77 408.14 20.78 o 1 -5 3 1006.67 1005.81 62.52 o 2 -5 3 530.19 548.38 22.16 o 3 -5 3 52.89 49.56 11.08 o 4 -5 3 457.48 414.46 30.44 o -6 -4 3 49.09 66.84 21.09 o -5 -4 3 202.11 192.08 24.31 o -4 -4 3 739.09 791.36 22.72 o -3 -4 3 16.34 18.83 4.29 o -2 -4 3 1739.95 1730.22 27.03 o -1 -4 3 1540.92 1563.72 26.99 o 0 -4 3 70.10 75.34 8.10 o 1 -4 3 1201.45 1155.19 30.30 o 2 -4 3 1431.11 1425.00 37.64 o 3 -4 3 71.81 64.44 12.56 o 4 -4 3 372.94 401.28 25.70 o 5 -4 3 111.34 80.62 21.48 o -6 -3 3 8.79 6.80 7.33 o -5 -3 3 426.55 418.95 19.83 o -4 -3 3 310.09 312.28 9.49 o -3 -3 3 67.91 47.73 5.44 o -2 -3 3 1482.20 1523.40 25.92 o -1 -3 3 2088.18 2093.33 28.45 o 0 -3 3 358.34 351.97 10.69 o 1 -3 3 2735.57 2744.03 56.22 o 2 -3 3 1512.07 1557.29 35.65 o 3 -3 3 184.12 229.42 15.39 o 4 -3 3 1062.24 1119.18 36.65 o 5 -3 3 115.52 122.13 14.10 o -6 -2 3 14.93 25.48 5.86 o -5 -2 3 754.43 781.71 24.95 o -4 -2 3 911.43 942.40 28.05 o -3 -2 3 0.99 3.79 3.05 o -2 -2 3 450.38 376.48 9.57 o -1 -2 3 1744.60 1749.33 23.90 o 0 -2 3 543.71 525.64 12.22 o 1 -2 3 4721.49 4725.29 57.43 o 2 -2 3 5.96 1.45 3.58 o 3 -2 3 553.78 531.29 20.15 o 4 -2 3 803.56 756.76 29.71 o 5 -2 3 83.92 83.18 12.78 o 6 -2 3 263.19 318.05 35.79 o -6 -1 3 10.84 9.91 8.92 o -5 -1 3 505.91 533.04 22.30 o -4 -1 3 606.35 625.10 18.45 o -3 -1 3 867.98 887.56 16.84 o -2 -1 3 3731.31 3767.06 53.27 o -1 -1 3 225.05 235.38 6.90 o 1 -1 3 4148.00 4198.34 52.89 o 2 -1 3 4.33 -2.32 2.80 o 3 -1 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27.16 o 3 3 26 335.72 328.39 50.41 o 4 3 26 47.29 20.09 25.56 o -2 4 26 2.36 -8.41 11.88 o -1 4 26 215.14 203.80 21.57 o 0 4 26 2008.27 2013.02 67.26 o 1 4 26 121.58 106.39 13.41 o 2 4 26 255.69 194.08 39.92 o 3 4 26 152.57 120.80 29.83 o -1 5 26 217.84 213.09 23.51 o 0 5 26 2.74 18.17 8.36 o 1 5 26 202.31 187.59 27.90 o 2 5 26 576.71 545.36 40.29 o 3 5 26 55.54 83.66 34.35 o 1 6 26 126.81 151.72 44.69 o -1 -3 27 3.26 -4.91 14.09 o 0 -3 27 226.31 219.26 25.36 o 1 -3 27 396.44 421.20 35.81 o -2 -2 27 281.55 298.30 32.99 o -1 -2 27 21.13 8.07 7.99 o 0 -2 27 255.63 323.84 25.63 o 1 -2 27 190.20 210.29 24.62 o 2 -2 27 26.48 22.97 31.65 o -2 -1 27 25.30 30.79 9.29 o -1 -1 27 160.56 188.32 26.25 o 0 -1 27 509.34 542.12 33.37 o 1 -1 27 68.36 58.55 10.13 o 2 -1 27 287.90 280.71 24.47 o 3 -1 27 229.53 228.49 25.50 o -2 0 27 0.26 -10.70 15.85 o -1 0 27 166.99 144.28 21.94 o 0 0 27 380.66 498.81 38.43 o 1 0 27 4.50 13.59 7.43 o 2 0 27 490.82 509.28 33.34 o 3 0 27 199.85 181.94 22.72 o -2 1 27 1.39 19.36 7.18 o -1 1 27 287.34 308.06 33.17 o 0 1 27 194.30 170.46 24.99 o 1 1 27 29.15 24.93 10.78 o 2 1 27 620.34 672.18 44.39 o 3 1 27 45.23 46.84 17.08 o -2 2 27 2.16 11.46 8.94 o -1 2 27 342.53 337.30 35.24 o 0 2 27 64.51 82.23 15.79 o 1 2 27 78.21 99.70 16.93 o 2 2 27 176.81 186.94 24.18 o 3 2 27 27.38 22.64 22.31 o -2 3 27 117.14 78.93 16.69 o -1 3 27 10.61 -4.76 6.87 o 0 3 27 1.12 2.70 7.23 o 1 3 27 225.92 233.59 28.45 o 2 3 27 329.97 359.97 60.59 o 3 3 27 9.74 37.81 20.58 o -1 4 27 342.06 363.30 30.90 o 0 4 27 69.93 67.30 11.75 o 1 4 27 5.52 -3.52 9.50 o 2 4 27 161.82 195.35 41.23 o 3 4 27 0.04 -18.36 18.53 o 0 5 27 1.41 6.26 8.54 o 1 5 27 201.45 160.21 26.94 o 2 5 27 229.82 230.41 31.37 o 0 -3 28 85.04 61.76 12.76 o -2 -2 28 23.84 0.07 24.78 o -1 -2 28 174.13 138.51 17.04 o 0 -2 28 65.45 73.67 10.86 o 1 -2 28 2.53 26.82 12.19 o 2 -2 28 487.85 549.01 52.13 o -2 -1 28 56.90 28.50 11.37 o -1 -1 28 380.49 427.99 39.65 o 0 -1 28 115.73 119.93 17.37 o 1 -1 28 84.30 109.42 24.67 o 2 -1 28 88.74 97.35 14.45 o -2 0 28 146.23 155.26 36.48 o -1 0 28 323.99 329.79 34.29 o 0 0 28 17.35 16.83 8.80 o 1 0 28 149.69 194.21 29.82 o 2 0 28 280.11 276.46 27.38 o 3 0 28 19.12 19.31 8.44 o -2 1 28 158.02 172.60 22.30 o -1 1 28 380.11 388.81 37.47 o 0 1 28 3.92 23.53 8.91 o 1 1 28 361.61 382.67 36.64 o 2 1 28 326.98 374.30 30.06 o 3 1 28 38.99 54.48 20.31 o -2 2 28 248.48 204.86 24.22 o -1 2 28 229.11 236.22 25.03 o 0 2 28 46.16 34.29 30.85 o 1 2 28 398.70 414.71 34.01 o 2 2 28 42.59 30.35 20.14 o 3 2 28 217.23 241.30 33.86 o -1 3 28 181.75 159.00 19.60 o 0 3 28 172.85 150.50 21.33 o 1 3 28 436.07 441.75 34.00 o 2 3 28 48.02 39.47 10.20 o 3 3 28 177.55 190.02 47.62 o -1 4 28 6.19 11.76 12.73 o 0 4 28 141.85 116.90 16.47 o 1 4 28 59.55 98.30 14.96 o 2 4 28 1.84 4.31 23.79 o 1 5 28 97.77 128.81 25.46 o -1 -2 29 131.97 108.81 18.19 o 0 -2 29 2.88 7.58 7.67 o 1 -2 29 699.61 786.50 45.56 o -1 -1 29 148.29 118.37 33.20 o 0 -1 29 5.34 8.54 9.85 o 1 -1 29 580.88 726.60 38.54 o 2 -1 29 44.82 35.28 16.39 o -2 0 29 345.39 358.87 37.68 o -1 0 29 141.33 137.26 23.58 o 0 0 29 69.97 75.84 15.29 o 1 0 29 344.02 331.28 32.88 o 2 0 29 209.50 276.55 28.45 o -2 1 29 165.06 139.18 24.45 o -1 1 29 68.62 68.28 16.26 o 0 1 29 171.51 191.82 27.01 o 1 1 29 437.16 437.80 35.92 o 2 1 29 5.47 13.00 7.68 o 3 1 29 134.30 146.37 36.01 o -1 2 29 0.59 11.71 7.84 o 0 2 29 197.06 265.96 31.34 o 1 2 29 332.17 363.96 46.61 o 2 2 29 19.22 24.66 8.56 o 3 2 29 259.61 269.62 57.08 o -1 3 29 4.61 10.20 10.74 o 0 3 29 304.45 330.47 34.68 o 1 3 29 203.48 213.90 34.86 o 2 3 29 48.70 43.14 30.78 o 0 4 29 259.20 228.89 27.71 o 1 4 29 14.39 10.75 10.33 o 2 4 29 98.65 110.81 38.72 o 0 -1 30 102.61 104.53 25.70 o 1 -1 30 35.42 65.07 12.62 o -1 0 30 0.82 7.74 13.18 o 0 0 30 154.56 114.47 20.31 o 1 0 30 170.93 164.92 21.66 o 2 0 30 69.86 72.23 11.54 o -1 1 30 55.02 49.50 15.25 o 0 1 30 226.41 227.46 35.28 o 1 1 30 94.51 72.68 21.74 o 2 1 30 56.27 125.06 21.37 o -1 2 30 182.20 170.94 25.00 o 0 2 30 160.66 130.38 22.58 o 1 2 30 25.87 16.33 9.04 o 2 2 30 200.85 170.51 24.35 o 0 3 30 174.36 157.46 37.06 o 1 3 30 0.14 -0.59 17.60 o 2 3 30 233.04 187.19 48.54 o 0 0 31 82.63 70.75 24.51 o 0 1 31 86.46 40.99 15.46 o 1 1 31 86.66 93.39 19.39 o 1 2 31 86.45 51.85 11.77 o