Acta Cryst. (2008). E64, m1565  [ doi:10.1107/S1600536808037616 ]

Tetra-n-butylammonium bis(2,2-dicyanoethylene-1,1-dithiolato)palladium(II)

N. Kanganga, K. R. Mann and D. E. Janzen

Key indicators

• Single-crystal X-ray study
• T = 173 K
• Mean (C-C) = 0.003 Å
• R factor = 0.024
• wR factor = 0.063
• Data-to-parameter ratio = 17.5

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT230_ALERT_2_B Hirshfeld Test Diff for    C2     --  C4      ..       7.01 su   
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Pd1    --  S1      ..      11.93 su   

Alert level C
            Value of measurement temperature given =   173.000
            Value of melting point given =     0.000
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Pd1    --  S2      ..       9.61 su   
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C2     -   C3     ...       1.42 Ang. 
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C2     -   C4     ...       1.43 Ang. 

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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