Acta Cryst. (2009). E65, m111-m112  [ doi:10.1107/S1600536808042773 ]

1,3-Bis(thiophen-2-ylmethyl)-3,4,5,6-tetrahydropyrimidinium trichlorido(⁶-p-cymene)ruthenate(II)

H. Arslan, D. VanDerveer, I. Özdemir, N. Gürbüz, Y. Gök and B. Çetinkaya

Online 20 December 2008

Key indicators

• Single-crystal X-ray study
• T = 153 K
• Mean (C-C) = 0.005 Å
• R factor = 0.032
• wR factor = 0.076
• Data-to-parameter ratio = 15.8

checkCIF/PLATON results

No syntax errors found






Alert level C
            Value of measurement temperature given =   153.000
            Value of melting point given =     0.000
PLAT154_ALERT_1_C The su's on the Cell Angles are Equal  (x 10000)       3000 Deg. 

Alert level G
PLAT333_ALERT_2_G Check Large Av C6-Ring C-C Dist. C15    -C20           1.42 Ang. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   1 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check


checkCIF publication errors

Alert level A
PUBL024_ALERT_1_A The number of authors is greater than 5.
              Please specify the role of each of the co-authors
              for your paper.

   1 ALERT level A = Data missing that is essential or data in wrong format
   0 ALERT level G = General alerts. Data that may be required is missing

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