# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' dmt143 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 228.79 _exptl_crystal_F_000 931.90 _reflns_d_resolution_high 0.7980 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.1102 _cell_length_b 13.2229 _cell_length_c 13.4273 _cell_angle_alpha 97.746 _cell_angle_beta 102.616 _cell_angle_gamma 93.333 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1999.56 1700.53 152.80 o 2 0 0 10253.03 9918.81 161.21 o 3 0 0 14325.52 14435.93 233.31 o 4 0 0 7449.30 7363.72 123.70 o 5 0 0 5541.55 5794.21 122.05 o 6 0 0 54.48 110.34 13.36 o 7 0 0 894.30 903.06 30.19 o 8 0 0 11.36 23.06 16.29 o 9 0 0 756.15 737.45 41.54 o 10 0 0 74.76 55.26 48.31 o 11 0 0 48.58 -0.55 47.76 o 12 0 0 176.28 144.20 48.68 o 13 0 0 447.38 416.85 61.12 o 14 0 0 1586.28 1398.23 95.34 o -14 1 0 257.76 269.36 59.47 o -13 1 0 92.06 88.20 40.81 o -12 1 0 867.24 702.32 61.12 o -11 1 0 48.32 -12.81 29.10 o -10 1 0 93.86 81.98 37.33 o -9 1 0 0.06 13.36 29.83 o -8 1 0 303.24 307.06 22.32 o -7 1 0 1944.67 2033.57 50.51 o -6 1 0 8143.65 8612.63 166.52 o -5 1 0 11893.97 12086.52 227.27 o -4 1 0 1196.80 1235.19 32.21 o -3 1 0 4563.77 4569.09 90.03 o -2 1 0 1170.59 1148.26 27.27 o -1 1 0 38889.69 37353.10 1000.96 o 0 1 0 687.58 379.71 143.83 o 1 1 0 20303.26 20245.88 434.60 o 2 1 0 4403.08 4350.96 73.93 o 3 1 0 118.00 111.44 9.70 o 4 1 0 2142.43 2184.91 42.82 o 5 1 0 9.40 23.42 10.61 o 6 1 0 904.21 912.39 25.80 o 7 1 0 231.04 264.24 21.23 o 8 1 0 7.11 54.53 29.28 o 9 1 0 102.29 80.33 36.05 o 10 1 0 47.00 51.97 38.61 o 11 1 0 2422.65 2387.11 123.52 o 12 1 0 4.88 60.75 56.73 o 13 1 0 2817.53 2664.52 147.67 o -14 2 0 139.86 199.46 50.14 o -13 2 0 35.57 36.78 38.61 o -12 2 0 97.24 122.79 41.72 o -11 2 0 268.94 300.10 51.60 o -10 2 0 118.42 113.82 35.13 o -9 2 0 67.75 96.44 22.32 o -8 2 0 253.07 255.27 24.52 o -7 2 0 73.36 36.78 14.82 o -6 2 0 505.48 464.43 57.82 o -5 2 0 164.35 166.89 13.54 o -4 2 0 4910.48 4451.24 89.30 o -3 2 0 3009.97 2996.47 62.22 o -2 2 0 381.48 370.56 40.26 o -1 2 0 175.01 196.17 14.09 o 0 2 0 9438.86 9166.90 149.14 o 1 2 0 17.57 14.46 6.59 o 2 2 0 1763.45 1744.45 34.04 o 3 2 0 1315.92 1209.02 32.57 o 4 2 0 2096.89 2216.20 43.37 o 5 2 0 2799.10 2717.41 52.15 o 6 2 0 425.74 516.40 19.40 o 7 2 0 165.61 110.16 18.85 o 8 2 0 1194.27 1211.21 43.55 o 9 2 0 874.41 859.14 82.89 o 10 2 0 5110.24 5130.69 141.27 o 11 2 0 1288.96 1116.24 77.95 o 12 2 0 3471.21 3370.68 155.91 o 13 2 0 67.13 -15.55 53.43 o 14 2 0 651.51 821.81 115.83 o -14 3 0 14.22 90.76 55.63 o -13 3 0 307.51 282.90 62.22 o -12 3 0 916.28 843.04 69.54 o -11 3 0 151.91 122.60 41.90 o -10 3 0 531.89 520.06 54.53 o -9 3 0 158.06 152.25 23.42 o -8 3 0 58.71 59.65 28.73 o -7 3 0 6562.68 6574.30 131.20 o -6 3 0 3290.81 3368.49 73.01 o -5 3 0 2594.13 2401.38 58.01 o -4 3 0 2710.35 2776.51 74.48 o -3 3 0 6366.33 5729.25 136.51 o -2 3 0 1749.85 1706.02 72.10 o -1 3 0 3.26 10.06 9.15 o 0 3 0 383.09 347.50 12.44 o 1 3 0 8707.71 8787.75 144.56 o 2 3 0 3446.45 3375.81 60.39 o 3 3 0 121.51 131.57 10.61 o 4 3 0 351.78 463.33 15.74 o 5 3 0 137.50 178.96 10.06 o 6 3 0 2423.79 2599.38 52.70 o 7 3 0 2.89 13.18 15.19 o 8 3 0 2.41 -10.25 21.23 o 9 3 0 2022.39 1941.71 69.90 o 10 3 0 110.45 99.00 32.57 o 11 3 0 3233.35 3372.33 148.59 o 12 3 0 415.41 329.38 52.88 o 13 3 0 1322.92 1490.09 107.42 o 14 3 0 145.25 158.10 79.42 o -14 4 0 0.67 14.27 44.65 o -13 4 0 11.73 36.78 43.00 o -12 4 0 43.38 20.13 34.59 o -11 4 0 404.63 405.51 35.32 o -10 4 0 22.40 49.77 22.87 o -9 4 0 792.57 796.56 42.09 o -8 4 0 2745.95 2811.10 82.89 o -7 4 0 549.19 502.86 31.84 o -6 4 0 12738.65 12199.97 281.44 o -5 4 0 145.75 158.29 24.34 o -4 4 0 2917.82 2875.51 77.59 o -3 4 0 24.54 18.12 15.01 o -2 4 0 5585.47 5323.37 127.91 o -1 4 0 1163.85 1161.44 26.35 o 0 4 0 6355.03 6438.33 108.51 o 1 4 0 2659.28 2542.65 47.94 o 2 4 0 264.82 315.84 13.91 o 3 4 0 103.32 82.35 11.16 o 4 4 0 654.05 692.62 20.31 o 5 4 0 1988.13 2024.06 52.34 o 6 4 0 1255.26 1127.77 38.06 o 7 4 0 1074.07 1005.35 37.88 o 8 4 0 1878.74 1863.39 54.35 o 9 4 0 348.48 370.56 32.21 o 10 4 0 3283.98 3437.66 90.03 o 11 4 0 719.16 709.27 64.60 o 12 4 0 1917.49 1991.48 114.37 o 13 4 0 483.94 449.42 61.85 o -14 5 0 567.79 510.36 73.56 o -13 5 0 192.84 176.95 48.31 o -12 5 0 748.04 686.58 65.69 o -11 5 0 759.74 773.13 45.75 o -10 5 0 143.44 127.18 28.73 o -9 5 0 2299.60 2292.50 75.58 o -8 5 0 5864.53 5616.71 202.94 o -7 5 0 9342.39 9264.07 221.42 o -6 5 0 171.04 201.84 27.45 o -5 5 0 6472.68 6211.61 152.43 o -4 5 0 3671.54 3708.12 129.56 o -3 5 0 179.80 110.34 19.58 o -2 5 0 10335.84 10821.14 178.78 o -1 5 0 257.65 276.68 13.54 o 0 5 0 4114.67 3911.60 70.09 o 1 5 0 11.25 28.18 10.06 o 2 5 0 1987.39 1915.54 45.02 o 3 5 0 16.28 30.19 10.61 o 4 5 0 610.89 604.42 20.49 o 5 5 0 6145.99 6213.44 129.74 o 6 5 0 408.40 372.20 24.34 o 7 5 0 5132.51 4937.81 110.89 o 8 5 0 143.94 151.88 25.80 o 9 5 0 4869.85 5070.85 116.56 o 10 5 0 9.94 -12.63 26.17 o 11 5 0 2964.07 2867.28 100.10 o 12 5 0 570.20 524.45 77.95 o 13 5 0 108.06 34.95 53.98 o -14 6 0 70.94 29.83 73.75 o -13 6 0 2995.80 3157.32 159.57 o -12 6 0 657.67 745.32 54.17 o -11 6 0 850.05 831.69 111.26 o -10 6 0 2551.67 2571.93 88.57 o -9 6 0 23.61 11.35 25.44 o -8 6 0 3037.73 3064.91 92.23 o -7 6 0 2011.21 2163.68 74.29 o -6 6 0 3066.05 3263.27 92.04 o -5 6 0 712.65 685.30 35.50 o -4 6 0 288.41 385.74 37.15 o -3 6 0 6734.33 7481.38 152.07 o -2 6 0 675.39 729.95 21.59 o -1 6 0 820.49 847.25 23.97 o 0 6 0 1806.55 1847.65 38.98 o 1 6 0 922.87 866.28 24.34 o 2 6 0 10231.40 10569.34 176.22 o 3 6 0 467.61 449.61 19.21 o 4 6 0 3076.81 3187.51 62.03 o 5 6 0 27.07 29.83 16.10 o 6 6 0 4343.68 4299.73 97.35 o 7 6 0 90.47 45.02 21.04 o 8 6 0 940.23 937.28 43.37 o 9 6 0 34.19 27.27 21.78 o 10 6 0 755.31 755.75 45.56 o 11 6 0 1629.40 1451.30 76.86 o 12 6 0 9.58 14.64 33.12 o 13 6 0 17.64 154.81 71.92 o -13 7 0 836.04 790.15 91.50 o -12 7 0 1114.36 1070.31 59.29 o -11 7 0 718.42 703.78 47.21 o -10 7 0 182.66 163.41 39.53 o -9 7 0 2317.24 2301.47 77.22 o -8 7 0 16.17 -6.59 34.77 o -7 7 0 1742.16 1812.52 79.05 o -6 7 0 1325.41 1302.53 50.69 o -5 7 0 112.24 89.85 18.48 o -4 7 0 10350.65 10949.60 183.91 o -3 7 0 104.26 80.33 12.44 o -2 7 0 279.12 219.41 15.37 o -1 7 0 923.15 959.05 27.08 o 0 7 0 2316.90 2151.60 44.83 o 1 7 0 1957.73 1935.31 41.90 o 2 7 0 690.83 644.68 22.14 o 3 7 0 2197.44 2039.06 44.47 o 4 7 0 67.02 83.08 21.04 o 5 7 0 6510.26 6285.72 133.77 o 6 7 0 2.73 -15.92 15.92 o 7 7 0 689.32 689.51 35.87 o 8 7 0 493.65 462.78 33.49 o 9 7 0 40.85 28.36 24.70 o 10 7 0 165.18 137.61 61.67 o 11 7 0 9.46 -28.00 28.00 o 12 7 0 489.97 524.27 128.46 o -13 8 0 897.85 894.09 55.45 o -12 8 0 1441.97 1523.40 67.52 o -11 8 0 6.65 -21.78 21.78 o -10 8 0 2979.77 2963.71 95.89 o -9 8 0 49.05 58.01 27.27 o -8 8 0 1116.96 1151.74 131.20 o -7 8 0 36.81 66.97 51.24 o -6 8 0 1145.06 1054.94 85.27 o -5 8 0 426.35 471.57 29.46 o -4 8 0 582.33 638.27 31.84 o -3 8 0 2834.35 2954.38 59.11 o -2 8 0 90.04 108.15 20.68 o -1 8 0 1265.60 1205.36 31.47 o 0 8 0 3074.82 3238.01 62.95 o 1 8 0 1374.15 1403.17 34.95 o 2 8 0 2709.71 2488.30 52.15 o 3 8 0 0.86 4.39 13.91 o 4 8 0 2370.17 2479.89 65.51 o 5 8 0 1.44 10.80 18.67 o 6 8 0 2472.83 2665.80 70.63 o 7 8 0 2308.62 2448.05 68.44 o 8 8 0 447.73 454.18 35.87 o 9 8 0 1140.90 1144.79 51.97 o 10 8 0 8.24 -27.45 32.02 o 11 8 0 321.92 307.97 71.92 o 12 8 0 131.00 24.70 82.89 o -13 9 0 899.09 762.16 56.36 o -12 9 0 151.15 150.60 35.68 o -11 9 0 604.35 546.04 44.83 o -10 9 0 2064.56 1974.83 150.78 o -9 9 0 23.61 48.13 31.84 o -8 9 0 37.57 -16.65 20.86 o -7 9 0 24.57 35.50 25.98 o -6 9 0 82.41 134.50 45.56 o -5 9 0 1336.62 1467.40 57.09 o -4 9 0 99.93 101.38 21.04 o -3 9 0 70.04 53.07 19.21 o -2 9 0 912.71 866.09 33.85 o -1 9 0 2564.94 2597.91 63.68 o 0 9 0 1224.05 1137.83 44.28 o 1 9 0 4855.28 4737.07 88.38 o 2 9 0 45.97 34.40 19.58 o 3 9 0 12065.32 12016.80 238.44 o 4 9 0 2248.61 2280.79 63.50 o 5 9 0 2791.72 2755.29 73.01 o 6 9 0 1741.54 1797.51 55.81 o 7 9 0 138.76 163.96 28.18 o 8 9 0 474.48 431.31 47.94 o 9 9 0 127.42 93.69 30.01 o 10 9 0 27.47 39.34 43.92 o 11 9 0 4.20 -30.01 30.01 o -12 10 0 683.24 544.21 46.48 o -11 10 0 1377.50 1324.48 64.78 o -10 10 0 75.78 94.61 36.23 o -9 10 0 549.24 586.85 63.68 o -8 10 0 1111.84 1153.75 58.56 o -7 10 0 542.00 504.69 59.65 o -6 10 0 577.67 609.72 39.16 o -5 10 0 211.33 238.80 34.95 o -4 10 0 1953.63 1956.90 55.08 o -3 10 0 1163.91 1147.53 41.54 o -2 10 0 4486.51 4373.10 97.90 o -1 10 0 1550.55 1630.63 48.13 o 0 10 0 6022.08 6076.38 128.09 o 1 10 0 284.67 289.31 27.45 o 2 10 0 10331.97 10538.05 208.79 o 3 10 0 364.90 384.28 36.96 o 4 10 0 1112.46 1182.12 57.46 o 5 10 0 3763.54 3667.86 113.64 o 6 10 0 3.02 1.83 23.61 o 7 10 0 395.96 381.53 68.62 o 8 10 0 168.64 231.67 36.78 o 9 10 0 492.50 663.52 96.07 o 10 10 0 84.20 75.39 45.93 o -11 11 0 43.49 -19.76 34.22 o -10 11 0 897.56 931.60 64.78 o -9 11 0 185.28 172.93 50.14 o -8 11 0 26.33 42.27 30.93 o -7 11 0 331.08 275.95 42.27 o -6 11 0 3275.36 3165.18 120.22 o -5 11 0 335.69 351.34 49.77 o -4 11 0 1735.35 1571.52 129.56 o -3 11 0 2123.39 2111.89 60.94 o -2 11 0 1188.47 1184.50 51.60 o -1 11 0 1577.34 1680.77 51.42 o 0 11 0 280.58 276.86 31.47 o 1 11 0 437.83 458.76 32.57 o 2 11 0 208.13 258.02 35.32 o 3 11 0 2041.80 2229.92 81.61 o 4 11 0 498.73 523.72 42.45 o 5 11 0 195.19 188.66 36.42 o 6 11 0 624.58 616.86 47.76 o 7 11 0 101.45 -7.50 57.64 o 8 11 0 100.38 139.07 35.68 o 9 11 0 358.29 365.25 47.94 o 10 11 0 347.12 452.54 99.55 o -11 12 0 71.91 62.77 44.65 o -10 12 0 0.06 47.58 54.17 o -9 12 0 937.58 939.66 55.63 o -8 12 0 246.57 255.45 36.42 o -7 12 0 673.58 608.26 45.75 o -6 12 0 80.73 8.78 25.07 o -5 12 0 455.38 476.32 38.79 o -4 12 0 1236.14 1224.02 59.29 o -3 12 0 599.98 544.95 35.50 o -2 12 0 1090.71 1111.30 44.83 o -1 12 0 45.68 9.70 21.96 o 0 12 0 510.45 514.75 37.88 o 1 12 0 1065.43 1020.54 45.56 o 2 12 0 393.83 340.73 82.35 o 3 12 0 22.27 8.05 32.39 o 4 12 0 37.81 1.65 24.89 o 5 12 0 253.59 234.59 40.44 o 6 12 0 7.64 31.29 31.47 o 7 12 0 26.47 44.65 33.30 o 8 12 0 4.22 32.39 41.72 o 9 12 0 201.69 94.61 37.88 o -10 13 0 452.38 497.92 68.62 o -9 13 0 54.43 74.48 32.57 o -8 13 0 1282.24 1309.11 81.25 o -7 13 0 178.26 220.32 36.23 o -6 13 0 1767.44 1859.73 74.29 o -5 13 0 2396.61 2317.39 85.82 o -4 13 0 56.20 21.78 27.08 o -3 13 0 1522.08 1621.29 73.20 o -2 13 0 958.36 967.29 44.28 o -1 13 0 4550.50 4839.73 113.45 o 0 13 0 115.96 120.22 27.63 o 1 13 0 0.99 34.59 39.16 o 2 13 0 424.84 483.46 42.45 o 3 13 0 33.52 34.04 27.81 o 4 13 0 81.23 128.64 32.02 o 5 13 0 494.67 536.71 51.97 o 6 13 0 419.49 349.51 45.56 o 7 13 0 662.30 650.90 55.26 o -8 14 0 368.55 364.70 46.66 o -7 14 0 1114.26 1024.56 58.92 o -6 14 0 1463.41 1650.02 76.86 o -5 14 0 744.45 681.09 52.88 o -4 14 0 4027.28 4055.43 242.83 o -3 14 0 243.74 194.70 32.02 o -2 14 0 756.47 831.69 43.37 o -1 14 0 824.11 793.26 65.69 o 0 14 0 7.56 -4.94 34.40 o 1 14 0 1314.68 1258.42 68.62 o 2 14 0 1534.85 1455.87 68.07 o 3 14 0 18.37 -6.59 28.73 o 4 14 0 253.21 233.31 53.80 o 5 14 0 603.95 516.58 113.27 o 6 14 0 802.84 648.33 57.28 o -7 15 0 718.66 753.19 59.65 o -6 15 0 160.82 204.40 50.14 o -5 15 0 697.59 564.16 50.87 o -4 15 0 654.11 627.29 46.85 o -3 15 0 120.64 133.95 46.66 o -2 15 0 789.60 868.11 53.98 o -1 15 0 76.62 54.35 28.55 o 0 15 0 526.30 538.72 56.73 o 1 15 0 1197.12 1061.53 112.91 o 2 15 0 45.94 -18.30 59.65 o 3 15 0 623.57 547.14 49.04 o 4 15 0 1154.86 1041.58 133.22 o -4 16 0 28.39 56.36 57.09 o -3 16 0 276.11 321.70 43.73 o -2 16 0 117.03 140.72 81.98 o -1 16 0 549.20 644.49 86.19 o 0 16 0 624.33 587.58 67.16 o 1 16 0 283.51 216.29 158.84 o -2 -16 1 1525.01 1563.47 79.42 o -1 -16 1 30.53 -40.26 40.26 o 0 -16 1 32.91 -42.45 42.45 o 1 -16 1 1.87 55.81 57.82 o 2 -16 1 285.78 264.24 36.42 o 3 -16 1 105.11 156.27 58.74 o 4 -16 1 1138.37 1091.54 81.98 o -5 -15 1 1865.34 2094.14 93.87 o -4 -15 1 36.71 43.37 34.22 o -3 -15 1 787.95 812.66 113.45 o -2 -15 1 632.57 595.27 49.96 o -1 -15 1 421.39 416.30 54.71 o 0 -15 1 39.01 45.93 46.11 o 1 -15 1 797.32 835.17 46.11 o 2 -15 1 6.27 -9.52 29.10 o 3 -15 1 721.03 748.98 49.41 o 4 -15 1 647.61 651.26 48.86 o 5 -15 1 122.54 49.04 97.72 o 6 -15 1 1187.04 1217.25 68.44 o 7 -15 1 508.38 541.10 55.63 o -6 -14 1 1686.53 1764.94 82.53 o -5 -14 1 42.18 71.00 62.03 o -4 -14 1 360.63 451.25 64.23 o -3 -14 1 53.12 77.59 70.63 o -2 -14 1 581.84 590.14 105.95 o -1 -14 1 67.56 100.10 52.34 o 0 -14 1 46.44 42.64 47.58 o 1 -14 1 709.17 725.37 41.72 o 2 -14 1 648.10 722.26 42.64 o 3 -14 1 461.91 539.27 46.30 o 4 -14 1 43.50 89.12 36.42 o 5 -14 1 3357.19 3461.63 125.90 o 6 -14 1 1206.02 1232.07 69.72 o 7 -14 1 1372.40 1310.94 144.56 o 8 -14 1 1983.53 2103.84 84.72 o -8 -13 1 39.68 -31.84 33.49 o -7 -13 1 431.73 456.74 47.03 o -6 -13 1 139.16 98.81 36.05 o -5 -13 1 126.79 155.54 54.53 o -4 -13 1 450.58 421.61 44.47 o -3 -13 1 8.27 0.37 26.53 o -2 -13 1 65.47 39.53 31.66 o -1 -13 1 495.64 512.19 37.88 o 0 -13 1 1602.22 1678.75 55.63 o 1 -13 1 134.34 119.31 24.70 o 2 -13 1 825.97 887.14 39.16 o 3 -13 1 64.98 68.99 28.55 o 4 -13 1 586.75 613.02 55.81 o 5 -13 1 2363.78 2234.13 84.72 o 6 -13 1 467.73 435.88 59.65 o 7 -13 1 989.10 1037.01 88.57 o 8 -13 1 0.49 25.44 29.64 o 9 -13 1 2944.86 3153.84 106.87 o -9 -12 1 188.85 181.71 64.23 o -8 -12 1 160.40 112.36 35.87 o -7 -12 1 83.34 91.86 48.49 o -6 -12 1 409.73 359.76 42.82 o -5 -12 1 114.32 77.22 41.54 o -4 -12 1 107.27 184.27 36.78 o -3 -12 1 201.81 204.58 43.73 o -2 -12 1 66.18 36.23 29.10 o -1 -12 1 1115.12 1111.12 44.10 o 0 -12 1 43.31 37.33 19.58 o 1 -12 1 1021.48 995.65 39.89 o 2 -12 1 58.79 39.71 18.67 o 3 -12 1 406.13 417.58 30.38 o 4 -12 1 2841.73 2828.30 92.96 o 5 -12 1 17.48 11.89 47.39 o 6 -12 1 2347.93 2440.36 92.96 o 7 -12 1 38.77 -22.51 22.51 o 8 -12 1 1211.33 1163.82 56.73 o 9 -12 1 260.40 275.22 39.16 o 10 -12 1 243.97 280.34 46.11 o -10 -11 1 743.78 762.70 66.61 o 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