# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 225.96 _exptl_crystal_F_000 652.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.3582 _cell_length_b 9.8181 _cell_length_c 15.2913 _cell_angle_alpha 73.641 _cell_angle_beta 82.482 _cell_angle_gamma 88.059 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2159.42 2204.81 71.17 o 2 0 0 4617.08 4651.02 148.67 o 3 0 0 2436.35 2505.10 94.86 o 4 0 0 240.96 173.56 31.23 o 5 0 0 842.86 965.55 57.09 o 6 0 0 2.38 19.92 54.53 o 7 0 0 26.13 66.66 34.83 o 8 0 0 7.87 -47.69 40.05 o 9 0 0 80.34 85.87 47.28 o 10 0 0 443.85 441.08 69.43 o 11 0 0 1027.33 1108.22 179.90 o 12 0 0 12.65 -16.71 115.10 o -11 1 0 220.48 361.16 242.37 o -10 1 0 18.02 54.77 72.09 o -9 1 0 178.49 169.67 51.54 o -8 1 0 832.59 951.75 71.29 o -7 1 0 423.26 383.60 50.03 o -6 1 0 1271.73 1320.54 75.28 o -5 1 0 843.59 925.60 64.39 o -4 1 0 3763.70 3318.60 124.49 o -3 1 0 135.31 101.93 33.52 o -2 1 0 5908.32 6069.44 240.16 o -1 1 0 6.91 6.79 19.21 o 1 1 0 3050.67 2984.80 65.24 o 2 1 0 13859.17 14982.73 381.49 o 3 1 0 318.98 341.76 33.57 o 4 1 0 37.70 5.64 25.18 o 5 1 0 1907.69 1903.46 85.02 o 6 1 0 1562.13 1706.61 75.97 o 7 1 0 3091.03 3067.84 112.15 o 8 1 0 52.85 -23.52 40.75 o 9 1 0 608.76 763.37 69.36 o 10 1 0 675.42 728.19 175.46 o 11 1 0 1.42 94.37 119.47 o 12 1 0 166.87 404.86 146.94 o -11 2 0 212.96 429.96 133.31 o -10 2 0 845.24 914.28 107.85 o -9 2 0 249.74 242.41 61.96 o -8 2 0 196.22 132.92 49.03 o -7 2 0 4.67 -35.44 40.00 o -6 2 0 3434.79 3065.05 129.29 o -5 2 0 14.66 1.42 37.32 o -4 2 0 23.24 26.52 37.58 o -3 2 0 303.18 358.90 43.81 o -2 2 0 751.68 803.63 52.63 o -1 2 0 324.49 423.79 49.33 o 0 2 0 2317.43 2295.49 94.92 o 1 2 0 221.11 212.27 31.40 o 2 2 0 262.06 281.66 23.16 o 3 2 0 507.93 501.50 41.43 o 4 2 0 453.23 424.30 34.08 o 5 2 0 2854.00 2567.82 89.22 o 6 2 0 732.14 891.60 56.89 o 7 2 0 329.65 383.73 47.26 o 8 2 0 421.44 412.97 53.53 o 9 2 0 1907.25 1976.43 147.14 o 10 2 0 8.83 -72.92 69.34 o 11 2 0 600.02 735.25 168.43 o -11 3 0 73.15 15.07 108.42 o -10 3 0 1.49 -125.05 83.37 o -9 3 0 153.92 36.55 57.87 o -8 3 0 956.00 1126.41 88.70 o -7 3 0 33.45 89.21 53.27 o -6 3 0 134.34 146.97 65.56 o -5 3 0 367.25 316.02 52.03 o -4 3 0 11460.76 11181.90 360.56 o -3 3 0 466.55 396.97 49.12 o -2 3 0 1925.38 1781.33 103.24 o -1 3 0 766.55 808.34 58.62 o 0 3 0 128.87 99.80 32.15 o 1 3 0 501.92 397.32 47.44 o 2 3 0 753.44 792.60 44.15 o 3 3 0 209.19 235.59 39.08 o 4 3 0 3423.62 3295.60 126.50 o 5 3 0 668.51 642.93 43.73 o 6 3 0 126.68 141.27 36.25 o 7 3 0 2256.38 2146.59 98.53 o 8 3 0 112.57 51.81 65.91 o 9 3 0 227.70 300.11 81.49 o 10 3 0 36.41 -51.14 68.36 o 11 3 0 15.22 66.16 83.55 o -11 4 0 257.39 199.09 119.88 o -10 4 0 6.22 52.51 99.93 o -9 4 0 1261.93 1261.00 142.02 o -8 4 0 255.19 231.44 78.67 o -7 4 0 1331.20 1294.30 164.83 o -6 4 0 2372.60 2237.52 135.09 o -5 4 0 39.98 1.53 55.03 o -4 4 0 35.49 -59.54 49.90 o -3 4 0 4191.92 4250.70 198.91 o -2 4 0 1320.92 1341.88 70.25 o -1 4 0 283.75 179.76 43.81 o 0 4 0 2492.46 2604.02 117.14 o 1 4 0 248.45 346.84 90.77 o 2 4 0 115.94 138.57 42.96 o 3 4 0 4814.21 3886.51 135.92 o 4 4 0 401.65 361.87 39.01 o 5 4 0 3187.80 2701.87 109.39 o 6 4 0 53.31 19.01 55.67 o 7 4 0 306.90 271.00 73.90 o 8 4 0 401.57 538.15 91.79 o 9 4 0 59.59 21.21 111.68 o 10 4 0 4.77 -63.02 73.04 o 11 4 0 201.58 43.52 87.66 o -11 5 0 261.44 197.49 126.11 o -10 5 0 666.63 437.26 135.42 o -9 5 0 26.48 -13.63 98.28 o -8 5 0 1354.80 1254.52 97.01 o -7 5 0 308.77 407.19 79.09 o -6 5 0 287.34 296.29 74.42 o -5 5 0 1419.77 1680.57 123.59 o -4 5 0 124.20 138.63 64.08 o -3 5 0 1622.16 1486.69 111.81 o -2 5 0 1801.58 1573.47 95.33 o -1 5 0 888.07 841.29 70.87 o 0 5 0 44.95 113.32 35.12 o 1 5 0 475.43 619.27 80.75 o 2 5 0 1.94 11.09 73.16 o 3 5 0 1129.81 1112.25 85.87 o 4 5 0 2123.23 2054.77 122.54 o 5 5 0 1167.57 1058.93 97.04 o 6 5 0 907.94 909.62 96.16 o 7 5 0 295.46 428.62 82.66 o 8 5 0 177.90 40.21 69.29 o 9 5 0 610.89 570.78 103.62 o 10 5 0 78.59 230.65 94.39 o -10 6 0 149.36 212.41 126.21 o -9 6 0 665.59 771.56 159.59 o -8 6 0 16.16 -38.57 56.02 o -7 6 0 913.59 1104.87 199.70 o -6 6 0 1.37 -23.51 64.60 o -5 6 0 257.40 170.32 75.87 o -4 6 0 88.51 61.00 41.50 o -3 6 0 748.44 922.95 78.97 o -2 6 0 42.56 58.52 63.23 o -1 6 0 318.79 327.47 58.28 o 0 6 0 5390.16 4893.07 191.40 o 1 6 0 0.40 -34.60 24.33 o 2 6 0 2481.09 2130.16 121.07 o 3 6 0 725.13 573.21 50.77 o 4 6 0 3494.02 3561.16 179.99 o 5 6 0 128.14 97.99 62.37 o 6 6 0 157.74 139.03 67.68 o 7 6 0 310.03 315.47 82.39 o 8 6 0 203.51 297.89 87.51 o 9 6 0 1138.63 1229.11 230.85 o 10 6 0 96.27 90.97 123.02 o -9 7 0 205.52 51.22 114.33 o -8 7 0 19.22 -48.78 60.39 o -7 7 0 11.48 -94.04 67.86 o -6 7 0 8.20 55.37 73.41 o -5 7 0 377.56 351.12 122.35 o -4 7 0 2314.47 2116.05 198.47 o -3 7 0 706.01 844.00 80.94 o -2 7 0 5849.91 5720.39 247.64 o -1 7 0 1069.88 1149.45 93.36 o 0 7 0 1968.45 2111.18 179.97 o 1 7 0 4082.21 3898.57 179.25 o 2 7 0 792.31 719.55 77.76 o 3 7 0 1293.69 1324.97 105.63 o 4 7 0 0.34 -8.32 57.54 o 5 7 0 81.57 61.10 65.69 o 6 7 0 292.11 231.61 78.76 o 7 7 0 1628.72 1453.08 171.78 o 8 7 0 1.77 122.67 85.07 o 9 7 0 630.11 672.99 115.32 o -9 8 0 13.40 -67.17 119.42 o -8 8 0 84.60 228.97 130.22 o -7 8 0 46.71 -159.31 106.20 o -6 8 0 1853.91 1691.65 213.08 o -5 8 0 136.55 108.57 118.14 o -4 8 0 722.91 513.43 148.58 o -3 8 0 18.52 60.15 56.21 o -2 8 0 681.12 643.55 78.92 o -1 8 0 394.48 359.91 69.08 o 0 8 0 1084.44 1043.13 77.45 o 1 8 0 17.46 -0.34 46.45 o 2 8 0 919.20 921.05 91.70 o 3 8 0 2.72 -31.41 64.65 o 4 8 0 113.28 186.28 70.60 o 5 8 0 111.17 70.58 68.16 o 6 8 0 37.84 51.76 78.05 o 7 8 0 230.25 232.62 85.91 o 8 8 0 668.35 791.44 120.00 o 9 8 0 5.05 -118.81 124.49 o -8 9 0 119.83 377.19 158.25 o -7 9 0 141.55 222.23 135.78 o -6 9 0 64.34 153.37 126.52 o -5 9 0 72.85 261.88 135.57 o -4 9 0 103.51 70.10 128.16 o -3 9 0 133.81 413.35 146.53 o -2 9 0 665.33 890.88 169.00 o -1 9 0 1.84 -65.18 57.66 o 0 9 0 1661.37 1616.57 149.10 o 1 9 0 0.69 1.89 54.69 o 2 9 0 349.05 409.68 83.63 o 3 9 0 210.73 359.68 88.87 o 4 9 0 97.15 68.72 93.78 o 5 9 0 48.23 -8.11 72.63 o 6 9 0 413.60 432.84 191.04 o 7 9 0 91.49 113.75 143.34 o 8 9 0 84.67 90.87 102.91 o -6 10 0 930.73 788.22 185.46 o -5 10 0 13.48 146.47 144.73 o -4 10 0 321.68 430.78 165.19 o -3 10 0 43.76 100.80 137.17 o -2 10 0 884.54 894.48 180.47 o -1 10 0 12.57 -18.05 122.51 o 0 10 0 147.51 174.17 145.70 o 1 10 0 7.05 53.44 60.66 o 2 10 0 2.92 128.57 58.46 o 3 10 0 522.03 533.45 117.85 o 4 10 0 14.29 80.33 88.31 o 5 10 0 819.51 1069.05 127.45 o 6 10 0 44.64 54.11 81.91 o -5 11 0 124.67 187.36 154.65 o -4 11 0 56.55 -83.01 141.18 o -3 11 0 9.59 48.14 146.78 o -2 11 0 15.08 -44.33 123.28 o -1 11 0 291.28 123.18 148.94 o 0 11 0 12.83 -186.69 124.46 o 1 11 0 898.63 834.63 115.41 o 2 11 0 411.82 304.06 73.33 o 3 11 0 1301.04 1048.83 101.99 o 4 11 0 566.33 622.49 138.83 o 5 11 0 76.19 61.63 164.19 o -2 12 0 18.34 100.34 144.78 o -1 12 0 346.74 565.07 186.95 o 0 12 0 26.05 168.54 155.83 o 1 12 0 132.76 57.55 151.67 o 2 12 0 338.96 423.27 181.96 o 0 -12 1 9.46 -121.48 150.90 o 1 -12 1 117.17 157.07 155.99 o -4 -11 1 339.63 244.03 93.86 o -3 -11 1 311.56 182.42 75.78 o -2 -11 1 268.25 42.73 80.88 o -1 -11 1 8.49 60.16 79.20 o 0 -11 1 127.33 -74.83 133.82 o 1 -11 1 6.11 -57.65 122.51 o 2 -11 1 294.80 291.51 150.28 o 3 -11 1 23.57 -72.93 128.22 o 4 -11 1 568.67 632.91 127.85 o -6 -10 1 114.69 114.56 94.37 o -5 -10 1 37.47 -68.58 83.16 o -4 -10 1 52.48 197.27 83.51 o -3 -10 1 1181.91 1270.89 122.08 o -2 -10 1 39.72 -43.43 54.84 o -1 -10 1 94.12 112.23 60.33 o 0 -10 1 368.71 323.02 113.69 o 1 -10 1 111.05 187.16 107.44 o 2 -10 1 235.51 88.20 128.37 o 4 -10 1 118.15 274.64 148.94 o 5 -10 1 972.82 1059.88 337.23 o 6 -10 1 127.98 129.42 247.82 o -7 -9 1 481.15 446.41 104.18 o -6 -9 1 127.04 43.45 79.75 o -5 -9 1 223.81 71.55 78.42 o -4 -9 1 553.36 570.74 105.59 o -3 -9 1 38.02 -68.71 62.08 o -2 -9 1 93.95 9.43 59.02 o -1 -9 1 871.76 855.66 99.13 o 0 -9 1 1090.57 1054.12 106.86 o 1 -9 1 243.02 193.64 68.97 o 2 -9 1 72.24 -14.32 58.56 o 3 -9 1 67.88 96.84 129.71 o 4 -9 1 870.69 990.65 181.70 o 5 -9 1 22.57 101.73 126.62 o 6 -9 1 1008.13 811.99 247.74 o 7 -9 1 0.61 -78.59 128.94 o 8 -9 1 61.26 44.95 135.62 o -8 -8 1 0.55 -70.03 76.99 o -7 -8 1 6.86 -20.79 70.87 o -6 -8 1 82.77 105.19 79.60 o -5 -8 1 106.91 163.09 77.08 o -4 -8 1 9.83 3.03 62.35 o -3 -8 1 301.48 229.19 71.36 o -2 -8 1 2274.92 2232.40 140.69 o -1 -8 1 2017.70 1927.46 171.42 o 0 -8 1 3445.40 3303.59 141.23 o 1 -8 1 234.03 155.04 123.72 o 2 -8 1 1532.00 1562.81 116.93 o 3 -8 1 29.60 66.66 65.70 o 4 -8 1 351.32 190.24 123.64 o 5 -8 1 103.43 -74.57 111.30 o 6 -8 1 28.61 -153.01 105.43 o 7 -8 1 32.65 138.99 90.88 o 8 -8 1 73.97 292.74 147.71 o 9 -8 1 41.40 -32.71 128.47 o -9 -7 1 249.72 303.46 98.29 o -8 -7 1 1052.22 1370.51 138.59 o -7 -7 1 1.60 -96.10 64.07 o -6 -7 1 198.51 191.33 77.98 o -5 -7 1 17.85 -26.39 63.22 o -4 -7 1 1260.61 1175.73 169.26 o -3 -7 1 44.07 -5.10 55.64 o -2 -7 1 2443.13 2416.97 139.42 o -1 -7 1 672.84 492.25 84.53 o 0 -7 1 331.15 286.25 51.29 o 1 -7 1 1928.04 1766.21 192.74 o 2 -7 1 888.61 957.17 87.73 o 3 -7 1 784.55 932.74 87.97 o 4 -7 1 491.88 487.38 73.51 o 5 -7 1 373.66 311.67 123.33 o 6 -7 1 244.08 396.73 126.93 o 7 -7 1 521.54 383.80 79.35 o 8 -7 1 1.35 46.34 113.20 o 9 -7 1 805.05 916.85 181.40 o -10 -6 1 139.13 239.26 101.52 o -9 -6 1 75.57 57.67 87.46 o -8 -6 1 4250.42 3970.79 224.96 o -7 -6 1 828.32 798.49 102.07 o -6 -6 1 370.11 356.97 107.85 o -5 -6 1 420.43 346.70 74.85 o -4 -6 1 922.05 885.72 91.28 o -3 -6 1 340.39 246.75 60.79 o -2 -6 1 83.65 62.19 49.32 o -1 -6 1 4330.99 4250.86 189.85 o 0 -6 1 453.60 444.34 57.37 o 1 -6 1 261.69 254.42 57.50 o 2 -6 1 2293.11 2186.59 124.18 o 3 -6 1 3368.71 3143.03 168.02 o 4 -6 1 59.83 11.24 91.73 o 5 -6 1 519.80 623.22 189.83 o 6 -6 1 223.37 211.53 77.48 o 7 -6 1 8.86 7.73 54.84 o 8 -6 1 1172.41 1078.14 174.71 o 9 -6 1 303.49 494.09 146.63 o 10 -6 1 759.34 980.88 187.36 o -10 -5 1 23.37 103.50 87.72 o -9 -5 1 2.84 -49.28 71.96 o -8 -5 1 2.43 45.56 68.03 o -7 -5 1 124.59 126.81 70.01 o -6 -5 1 138.55 43.28 60.89 o -5 -5 1 3207.68 3098.41 232.83 o -4 -5 1 88.20 59.80 52.77 o -3 -5 1 9960.98 10024.82 388.52 o -2 -5 1 1526.72 1358.85 91.23 o -1 -5 1 4437.68 4516.73 278.91 o 0 -5 1 715.36 792.03 91.13 o 1 -5 1 34.17 69.99 48.86 o 2 -5 1 553.04 717.06 67.88 o 3 -5 1 124.42 112.20 44.67 o 4 -5 1 899.46 1145.66 101.36 o 5 -5 1 1080.64 1000.22 97.28 o 6 -5 1 313.19 399.89 76.91 o 7 -5 1 401.82 269.69 61.99 o 8 -5 1 146.60 228.12 62.89 o 9 -5 1 762.05 839.09 159.07 o 10 -5 1 2.68 54.31 109.80 o 11 -5 1 6.72 113.04 123.54 o -11 -4 1 36.92 79.92 87.50 o -10 -4 1 153.71 240.15 88.70 o -9 -4 1 212.06 232.01 86.41 o -8 -4 1 128.69 36.77 67.37 o -7 -4 1 1699.40 1552.43 123.64 o -6 -4 1 1115.55 1120.47 101.13 o -5 -4 1 42.98 20.60 51.33 o -4 -4 1 773.15 591.78 68.81 o -3 -4 1 428.29 352.11 55.29 o -2 -4 1 34.86 49.73 40.67 o -1 -4 1 1272.97 1125.80 75.88 o 0 -4 1 552.95 692.56 81.36 o 1 -4 1 1402.95 1424.22 87.53 o 2 -4 1 281.55 413.35 43.97 o 3 -4 1 1094.17 864.84 71.45 o 4 -4 1 2722.24 2226.79 114.81 o 5 -4 1 3813.03 3915.44 154.91 o 6 -4 1 38.48 13.29 47.50 o 7 -4 1 302.81 243.04 53.00 o 8 -4 1 106.72 174.11 51.16 o 9 -4 1 96.56 -45.62 95.10 o 10 -4 1 114.25 210.56 121.89 o 11 -4 1 7.49 -44.28 106.51 o -11 -3 1 342.43 449.78 105.85 o -10 -3 1 363.95 237.37 86.37 o -9 -3 1 415.59 353.27 87.45 o -8 -3 1 696.43 578.47 91.75 o -7 -3 1 126.52 159.82 64.86 o -6 -3 1 113.32 164.30 35.41 o -5 -3 1 4293.62 4051.82 167.85 o -4 -3 1 18.47 213.56 32.32 o -3 -3 1 159.61 70.12 41.32 o -2 -3 1 3.44 -5.06 34.46 o -1 -3 1 1227.91 1090.37 69.58 o 0 -3 1 932.68 668.05 244.35 o 1 -3 1 686.73 780.21 49.39 o 2 -3 1 222.19 624.28 73.33 o 3 -3 1 1306.40 1466.23 78.51 o 4 -3 1 591.90 592.69 55.31 o 5 -3 1 5.31 30.70 47.62 o 6 -3 1 3384.18 3094.00 113.24 o 7 -3 1 1309.58 1421.96 79.72 o 8 -3 1 139.85 166.91 51.36 o 9 -3 1 0.99 36.09 70.94 o 10 -3 1 524.05 390.51 131.92 o 11 -3 1 0.73 -16.25 106.20 o -11 -2 1 487.04 533.40 108.42 o -10 -2 1 179.76 255.97 148.48 o -9 -2 1 1574.57 1793.14 139.07 o -8 -2 1 111.86 139.77 52.44 o -7 -2 1 475.64 527.85 50.18 o -6 -2 1 4.73 -44.32 29.55 o -5 -2 1 1087.35 1071.57 53.26 o -4 -2 1 12.23 -1.40 24.16 o -3 -2 1 109.34 97.29 20.57 o -2 -2 1 1904.67 1900.84 94.51 o -1 -2 1 2043.68 2069.87 95.39 o 0 -2 1 4341.63 4542.82 143.36 o 1 -2 1 334.13 371.74 47.21 o 2 -2 1 4557.37 4612.62 156.32 o 3 -2 1 4822.11 5048.88 171.51 o 4 -2 1 1863.43 1468.83 76.91 o 5 -2 1 1598.80 1507.88 68.63 o 6 -2 1 1270.38 1379.26 71.75 o 7 -2 1 581.42 611.44 57.53 o 8 -2 1 66.35 51.30 45.22 o 9 -2 1 529.20 675.27 67.87 o 10 -2 1 104.77 81.32 86.53 o 11 -2 1 88.00 130.38 119.58 o -11 -1 1 194.87 253.54 81.09 o -10 -1 1 110.62 149.21 58.37 o -9 -1 1 243.52 272.60 97.79 o -8 -1 1 65.77 23.76 47.62 o -7 -1 1 123.67 123.14 40.48 o -6 -1 1 26.54 24.83 31.60 o -5 -1 1 1242.76 1479.73 64.03 o -4 -1 1 2434.84 2222.63 93.58 o -3 -1 1 1852.84 1685.51 59.49 o -2 -1 1 9142.24 8459.76 256.24 o -1 -1 1 188.11 158.39 26.11 o 0 -1 1 8975.83 9657.93 296.61 o 1 -1 1 7578.74 8308.32 264.25 o 2 -1 1 2702.86 2713.21 95.75 o 3 -1 1 450.67 497.52 43.49 o 4 -1 1 33.51 56.62 33.87 o 5 -1 1 810.54 1038.54 56.63 o 6 -1 1 83.33 129.84 39.12 o 7 -1 1 379.01 338.96 48.10 o 8 -1 1 76.61 85.64 65.17 o 9 -1 1 562.93 540.03 71.41 o 10 -1 1 93.80 50.27 62.09 o 11 -1 1 8.15 8.14 150.20 o 12 -1 1 606.33 787.92 168.28 o -11 0 1 329.00 497.85 142.26 o -10 0 1 273.96 249.35 82.05 o -9 0 1 190.99 195.09 57.05 o -8 0 1 1469.90 1612.26 83.94 o -7 0 1 0.15 -31.05 34.46 o -6 0 1 2673.08 2635.02 96.26 o -5 0 1 0.67 -44.26 29.51 o -4 0 1 3097.60 2721.28 92.03 o -3 0 1 186.19 172.70 32.86 o -2 0 1 154.29 135.86 39.57 o -1 0 1 3106.28 3290.43 103.36 o 0 0 1 1573.76 -2.58 1.72 o 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