Acta Cryst. (2009). E65, m224  [ doi:10.1107/S1600536809002359 ]

Tetrachlorido(1,10-phenanthroline-²N,N')platinum(IV) acetonitrile hemisolvate

N.-H. Kim, I.-C. Hwang and K. Ha

Online 23 January 2009

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.012 Å
• R factor = 0.035
• wR factor = 0.104
• Data-to-parameter ratio = 15.7

checkCIF/PLATON results

No syntax errors found






Alert level C
            Value of measurement temperature given =   293.000
            Value of melting point given =     0.000
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang ...         12      
PLAT152_ALERT_1_C Supplied and Calc Volume s.u. Inconsistent .....          ?
PLAT234_ALERT_4_C Large Hirshfeld Difference N2     --  C11     ..       0.11  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C4     --  C12     ..       0.11  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C14    --  C15     ..       0.14  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C16    --  C17     ..       0.12  Ang.
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        C26     

Alert level G
PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 =          3      
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   3 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   6 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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