# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 08mz462_0m in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 237.27 _exptl_crystal_F_000 1042.00 _reflns_d_resolution_high 0.7501 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.3268 _cell_length_b 14.7014 _cell_length_c 15.4318 _cell_angle_alpha 101.379 _cell_angle_beta 104.946 _cell_angle_gamma 107.678 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11848.86 12303.68 223.00 o 2 0 0 195.28 260.53 20.83 o 3 0 0 12181.43 11931.44 225.18 o 4 0 0 1126.53 1137.00 46.95 o 5 0 0 2741.21 2678.60 75.96 o 6 0 0 2032.01 2217.89 73.73 o 7 0 0 2827.02 3204.53 95.60 o 8 0 0 3927.16 3926.99 145.05 o 9 0 0 61.49 -0.90 65.01 o 10 0 0 114.11 -12.49 77.91 o 11 0 0 0.36 -22.81 160.89 o 12 0 0 9.46 -94.07 94.07 o 13 0 0 55.74 108.81 123.09 o -13 1 0 25.13 -43.74 112.95 o -12 1 0 93.58 -94.71 110.45 o -11 1 0 3.45 -97.01 143.88 o -10 1 0 62.79 -51.62 69.83 o -9 1 0 1485.88 1526.39 100.96 o -8 1 0 1687.82 1823.91 75.43 o -7 1 0 7.11 11.84 34.78 o -6 1 0 6985.70 7555.34 188.89 o -5 1 0 126.71 157.30 31.18 o -4 1 0 4846.40 4653.76 103.24 o -3 1 0 10332.36 11032.96 277.72 o -2 1 0 4183.61 4615.61 111.48 o -1 1 0 40666.32 37544.65 671.39 o 0 1 0 12601.28 13006.42 445.97 o 1 1 0 14115.95 15387.74 276.94 o 2 1 0 1796.62 1746.94 48.47 o 3 1 0 572.44 552.80 39.39 o 4 1 0 1680.98 1510.76 54.49 o 5 1 0 1462.44 1804.64 136.05 o 6 1 0 9.56 7.16 32.16 o 7 1 0 3909.51 4326.38 143.23 o 8 1 0 757.13 679.97 140.60 o 9 1 0 252.64 245.89 85.07 o 10 1 0 63.34 100.27 82.10 o 11 1 0 73.61 -30.21 141.79 o 12 1 0 197.67 38.94 110.66 o 13 1 0 115.85 129.15 132.34 o -14 2 0 2.62 74.63 185.67 o -13 2 0 10.38 -157.01 157.61 o -12 2 0 64.25 -15.08 120.30 o -11 2 0 10.94 -69.22 74.58 o -10 2 0 39.90 -66.85 92.83 o -9 2 0 2531.90 2566.57 92.18 o -8 2 0 587.66 612.08 52.87 o -7 2 0 7962.26 8178.15 178.20 o -6 2 0 354.57 421.89 39.76 o -4 2 0 155.71 173.45 56.35 o -3 2 0 35.07 84.19 22.18 o -2 2 0 1304.71 1297.40 42.38 o -1 2 0 6948.40 6816.64 127.29 o 0 2 0 23354.50 26143.55 465.91 o 1 2 0 5106.33 4858.79 164.70 o 2 2 0 1335.35 1341.32 46.09 o 3 2 0 881.48 787.81 38.98 o 4 2 0 169.83 149.85 53.73 o 5 2 0 9.24 -38.75 40.92 o 6 2 0 9359.03 10222.62 255.86 o 7 2 0 429.80 486.49 67.23 o 8 2 0 76.98 19.38 68.36 o 9 2 0 3.43 -68.20 68.20 o 10 2 0 58.96 -87.16 87.16 o 11 2 0 526.82 431.38 147.76 o 12 2 0 151.01 81.78 120.62 o -14 3 0 15.57 -54.33 176.71 o -13 3 0 8.54 -149.25 149.25 o -12 3 0 21.44 -81.62 81.62 o -11 3 0 15.73 -71.66 71.66 o -10 3 0 114.18 106.11 91.34 o -9 3 0 187.59 114.26 50.85 o -8 3 0 678.23 704.89 54.86 o -7 3 0 1453.14 1587.53 65.37 o -6 3 0 131.38 112.74 36.85 o -4 3 0 758.90 681.07 39.97 o -3 3 0 1014.62 1021.29 40.31 o -2 3 0 6409.68 5786.22 114.84 o -1 3 0 3715.04 3645.52 77.76 o 0 3 0 16912.01 18886.91 567.08 o 1 3 0 34.63 68.04 28.71 o 2 3 0 4277.56 3941.52 102.85 o 3 3 0 741.54 666.07 34.56 o 4 3 0 96.68 228.57 44.73 o 5 3 0 1080.81 1290.07 54.86 o 6 3 0 552.87 664.20 65.68 o 7 3 0 569.59 671.38 75.94 o 8 3 0 1107.11 1188.24 119.10 o 9 3 0 24.99 -73.82 73.82 o 10 3 0 340.85 246.54 148.06 o 11 3 0 84.64 -77.89 102.10 o 12 3 0 150.21 198.04 130.21 o -14 4 0 76.28 -60.30 155.82 o -13 4 0 59.02 -62.09 141.49 o -12 4 0 4.64 -117.61 117.61 o -11 4 0 102.93 101.42 73.58 o -10 4 0 2.75 -52.75 52.75 o -9 4 0 881.72 888.88 64.19 o -8 4 0 679.07 596.44 52.24 o -7 4 0 25.00 -36.27 36.27 o -6 4 0 3575.45 3506.77 92.47 o -5 4 0 2629.21 2778.59 130.75 o -4 4 0 35.47 49.87 24.15 o -3 4 0 1941.57 1758.16 53.54 o -2 4 0 1333.69 1193.81 43.79 o -1 4 0 6971.99 6983.72 137.67 o 0 4 0 153.55 208.19 36.13 o 1 4 0 389.69 344.67 30.81 o 2 4 0 183.29 159.42 41.08 o 3 4 0 343.36 425.17 50.63 o 4 4 0 3636.10 3510.35 231.35 o 5 4 0 151.30 238.80 62.69 o 6 4 0 975.93 1072.25 79.74 o 7 4 0 1625.47 1597.52 98.60 o 8 4 0 208.96 82.75 72.78 o 9 4 0 772.35 831.00 105.53 o 10 4 0 118.73 96.20 100.39 o 11 4 0 284.86 218.96 116.32 o 12 4 0 180.85 -36.72 134.18 o -14 5 0 21.24 -35.22 150.45 o -13 5 0 26.01 -131.34 131.34 o -12 5 0 82.84 -43.58 120.60 o -11 5 0 220.31 186.66 75.13 o -10 5 0 239.31 181.56 52.49 o -9 5 0 660.90 781.97 61.87 o -8 5 0 145.05 121.26 40.44 o -7 5 0 1240.14 1081.98 91.00 o -6 5 0 594.70 556.03 42.90 o -5 5 0 163.58 1321.18 107.46 o -4 5 0 264.09 340.42 33.76 o -3 5 0 678.17 631.30 47.22 o -2 5 0 1308.43 1197.60 47.28 o -1 5 0 6416.41 6398.05 156.08 o 0 5 0 183.48 363.62 32.57 o 1 5 0 914.67 877.34 46.08 o 2 5 0 634.90 695.81 43.44 o 3 5 0 2444.76 2180.18 87.64 o 4 5 0 552.19 612.09 45.77 o 5 5 0 164.64 121.09 38.86 o 6 5 0 1867.51 1771.85 95.03 o 7 5 0 280.93 302.51 72.51 o 8 5 0 787.64 778.23 96.73 o 9 5 0 86.32 7.01 87.27 o 10 5 0 44.19 18.26 99.35 o 11 5 0 257.01 229.54 146.27 o -14 6 0 33.42 447.76 156.42 o -13 6 0 4.38 10.75 130.15 o -12 6 0 91.10 148.66 121.79 o -11 6 0 6.59 28.12 65.94 o -10 6 0 213.60 181.34 52.77 o -9 6 0 51.85 27.18 45.56 o -8 6 0 82.92 106.64 39.19 o -7 6 0 56.72 45.81 32.05 o -6 6 0 578.05 688.65 46.51 o -5 6 0 140.34 128.33 32.50 o -4 6 0 1474.05 1507.44 57.70 o -3 6 0 7650.53 7324.68 151.79 o -2 6 0 2823.83 2817.83 98.51 o -1 6 0 2.86 -8.01 28.02 o 0 6 0 4123.93 4129.29 168.67 o 1 6 0 794.65 826.72 47.52 o 2 6 0 12309.59 12457.18 249.21 o 3 6 0 5340.65 5148.76 153.28 o 4 6 0 2093.97 2113.97 72.31 o 5 6 0 4443.93 4177.10 185.99 o 6 6 0 55.06 -1.28 58.37 o 7 6 0 40.21 -48.90 65.84 o 8 6 0 765.05 833.27 106.06 o 9 6 0 206.70 97.51 98.69 o 10 6 0 1122.07 1242.87 138.88 o 11 6 0 66.29 9.70 131.37 o -14 7 0 124.27 481.79 137.91 o -13 7 0 31.82 153.43 122.39 o -12 7 0 87.12 250.74 114.03 o -11 7 0 6.68 67.06 68.84 o -10 7 0 344.08 253.28 68.28 o -9 7 0 198.14 324.24 59.26 o -8 7 0 72.22 153.80 78.89 o -7 7 0 30.73 -35.26 38.78 o -6 7 0 838.29 774.79 50.78 o -5 7 0 577.78 640.79 46.47 o -4 7 0 1788.68 1746.16 63.39 o -3 7 0 2574.65 2461.62 83.55 o -2 7 0 1661.17 1677.28 62.96 o -1 7 0 6714.48 6763.18 146.03 o 0 7 0 713.58 788.67 57.70 o 1 7 0 6814.46 6479.85 144.61 o 2 7 0 14372.40 13667.86 269.68 o 3 7 0 18.81 -0.34 34.06 o 4 7 0 3863.32 3696.16 104.25 o 5 7 0 471.26 533.95 99.70 o 6 7 0 35.64 118.80 91.94 o 7 7 0 1054.30 1184.60 107.62 o 8 7 0 6.41 -85.48 85.48 o 9 7 0 1222.96 1234.98 132.70 o 10 7 0 321.43 282.38 123.07 o -12 8 0 124.34 399.40 99.70 o -11 8 0 9.23 -42.39 111.04 o -10 8 0 53.00 -102.09 102.09 o -9 8 0 15.59 -91.34 91.34 o -8 8 0 584.25 605.19 57.21 o -7 8 0 149.39 104.81 40.96 o -6 8 0 588.57 763.21 53.62 o -5 8 0 1351.37 1266.85 60.29 o -4 8 0 1073.30 1076.36 55.58 o -3 8 0 12.36 -19.50 33.69 o -2 8 0 2332.38 2336.72 76.24 o -1 8 0 485.16 565.11 46.71 o 0 8 0 1324.52 1321.35 113.66 o 1 8 0 4564.57 4404.87 136.60 o 2 8 0 111.12 107.11 39.86 o 3 8 0 1651.37 1555.93 70.31 o 4 8 0 285.26 290.44 77.46 o 5 8 0 17.65 -24.46 60.30 o 6 8 0 9.17 -42.98 94.92 o 7 8 0 2.58 -79.57 79.57 o 8 8 0 883.06 1036.70 120.32 o 9 8 0 261.74 292.60 114.61 o 10 8 0 176.61 132.28 122.95 o -12 9 0 19.56 -101.49 121.79 o -11 9 0 6.48 -81.67 81.67 o -10 9 0 193.70 227.08 85.14 o -9 9 0 375.67 183.58 77.33 o -8 9 0 0.17 -85.67 85.67 o -7 9 0 285.51 208.12 49.54 o -6 9 0 74.76 48.19 38.77 o -5 9 0 962.80 1271.03 61.76 o -4 9 0 843.12 853.28 52.55 o -3 9 0 417.98 413.75 45.03 o -2 9 0 822.03 828.45 54.96 o -1 9 0 98.74 70.03 38.92 o 0 9 0 3191.97 3270.36 98.94 o 1 9 0 2.55 -27.79 39.20 o 2 9 0 2203.07 2099.18 82.37 o 3 9 0 1088.50 1106.69 68.22 o 4 9 0 1.70 -7.09 61.63 o 5 9 0 112.55 126.83 69.65 o 6 9 0 32.91 -22.69 108.66 o 7 9 0 644.53 548.21 105.53 o 8 9 0 509.08 500.77 120.30 o 9 9 0 34.36 71.72 115.30 o -14 10 0 309.86 514.62 219.10 o -13 10 0 128.30 285.37 188.06 o -12 10 0 212.41 364.39 109.70 o -11 10 0 42.11 59.13 93.22 o -10 10 0 612.15 674.73 150.74 o -9 10 0 134.70 90.72 109.85 o -8 10 0 141.58 144.07 76.24 o -7 10 0 1.18 -12.23 46.22 o -6 10 0 114.25 81.50 57.63 o -5 10 0 2.00 -38.92 38.92 o -4 10 0 75.21 129.64 42.69 o -3 10 0 961.89 1085.32 64.76 o -2 10 0 65.83 -0.66 41.38 o -1 10 0 297.43 372.72 51.33 o 0 10 0 623.27 830.18 90.14 o 1 10 0 2747.04 2831.13 99.28 o 2 10 0 417.27 418.07 78.42 o 3 10 0 11.92 11.87 51.05 o 4 10 0 1502.87 1462.53 103.96 o 5 10 0 76.01 124.61 78.09 o 6 10 0 114.21 242.39 127.16 o 7 10 0 542.12 515.17 114.23 o 8 10 0 91.07 42.98 134.92 o -14 11 0 64.67 -91.94 220.89 o -13 11 0 114.61 168.82 126.08 o -12 11 0 48.47 -96.33 104.74 o -11 11 0 180.91 201.09 104.38 o -10 11 0 43.10 -89.44 89.44 o -9 11 0 44.11 -80.38 80.38 o -8 11 0 34.28 -72.07 73.62 o -7 11 0 0.15 -43.48 68.37 o -6 11 0 96.89 121.40 49.52 o -5 11 0 4.50 52.01 45.08 o -4 11 0 1257.53 1277.44 74.62 o -3 11 0 487.77 541.06 59.63 o -2 11 0 53.36 4.22 47.05 o -1 11 0 654.25 682.12 85.05 o 0 11 0 2583.66 2606.10 100.40 o 1 11 0 1296.23 1294.73 80.22 o 2 11 0 3.50 -56.76 56.76 o 3 11 0 708.63 772.40 75.78 o 4 11 0 5.07 -71.22 71.22 o 5 11 0 5.79 49.55 130.15 o 6 11 0 54.27 219.70 128.95 o 7 11 0 156.85 65.07 134.33 o -13 12 0 264.84 279.06 140.14 o -12 12 0 20.46 104.48 121.06 o -11 12 0 3.65 87.24 112.03 o -10 12 0 0.77 -97.27 97.27 o -9 12 0 137.74 -48.49 89.03 o -8 12 0 103.21 -52.38 82.91 o -7 12 0 43.09 48.33 77.82 o -6 12 0 363.69 331.96 55.59 o -5 12 0 198.08 178.37 57.18 o -4 12 0 0.25 -18.84 52.26 o -3 12 0 367.84 290.23 80.37 o -2 12 0 3577.87 3675.58 152.35 o -1 12 0 587.48 700.11 74.21 o 0 12 0 418.83 424.81 67.81 o 1 12 0 108.02 7.28 59.34 o 2 12 0 254.32 240.82 69.88 o 3 12 0 352.36 395.82 128.95 o 4 12 0 25.72 47.76 115.22 o 6 12 0 6.24 17.91 134.33 o 7 12 0 599.37 510.44 170.15 o -13 13 0 23.25 87.30 145.23 o -12 13 0 471.07 533.65 136.99 o -11 13 0 7.39 -83.96 120.46 o -10 13 0 1.82 -109.28 109.28 o -9 13 0 17.10 -62.69 98.36 o -8 13 0 0.45 -84.65 90.91 o -7 13 0 31.73 -78.25 81.39 o -6 13 0 15.93 -75.99 75.99 o -5 13 0 696.24 645.30 89.51 o -4 13 0 596.77 700.89 74.53 o -3 13 0 149.49 103.26 66.55 o -2 13 0 147.86 97.49 66.05 o -1 13 0 25.85 -62.25 62.25 o 0 13 0 0.22 -40.50 65.06 o 1 13 0 328.42 295.91 91.68 o 2 13 0 797.82 813.13 111.56 o 3 13 0 5.79 103.28 128.95 o 4 13 0 581.53 711.04 152.83 o 6 13 0 368.95 348.65 154.03 o -13 14 0 393.06 573.87 169.51 o -12 14 0 257.66 379.43 146.74 o -11 14 0 148.58 2.51 130.45 o -10 14 0 154.45 66.52 137.01 o -9 14 0 153.42 46.55 114.12 o -8 14 0 153.69 21.33 102.45 o -7 14 0 408.28 409.49 106.07 o -6 14 0 65.78 -2.81 92.26 o -5 14 0 165.45 31.94 96.12 o -4 14 0 16.57 -80.51 80.51 o -3 14 0 52.15 47.21 70.78 o -2 14 0 35.63 23.58 83.11 o -1 14 0 4.10 -108.36 108.36 o 0 14 0 51.13 -64.86 88.40 o 1 14 0 358.79 232.24 97.28 o 2 14 0 9.96 28.66 122.39 o 3 14 0 346.51 336.12 143.88 o 4 14 0 31.30 -20.90 121.79 o -12 15 0 9.07 52.37 149.53 o -11 15 0 216.96 318.71 149.48 o -10 15 0 240.90 70.38 132.88 o -9 15 0 4.45 -111.78 116.70 o -8 15 0 11.38 -109.37 109.37 o -7 15 0 14.75 -126.97 160.60 o -6 15 0 0.88 -94.72 107.02 o -5 15 0 2.80 -155.22 155.22 o -4 15 0 53.73 -75.03 103.88 o -3 15 0 179.34 53.71 91.22 o -2 15 0 14.56 -81.71 81.71 o -1 15 0 10.53 -89.07 89.07 o 0 15 0 62.25 -94.92 94.92 o 1 15 0 33.05 -89.99 95.20 o 2 15 0 70.09 -53.73 121.19 o 3 15 0 52.01 194.62 141.49 o -12 16 0 258.21 243.87 174.10 o -11 16 0 356.63 349.34 163.13 o -10 16 0 0.26 -144.08 144.08 o -9 16 0 45.51 -144.48 178.51 o -8 16 0 25.50 -164.18 166.57 o -7 16 0 129.06 151.04 188.06 o -6 16 0 107.30 -60.89 175.52 o -5 16 0 3.54 -166.57 166.57 o -4 16 0 0.51 -135.52 162.98 o -3 16 0 9.98 -95.42 95.42 o -2 16 0 154.63 19.40 104.47 o -1 16 0 44.23 -126.27 126.27 o 0 16 0 28.12 -73.08 100.80 o 1 16 0 89.46 -18.51 134.92 o 2 16 0 37.77 44.78 145.07 o -11 17 0 11.03 -90.15 189.85 o -10 17 0 237.56 201.79 210.74 o -9 17 0 34.78 -194.62 194.62 o -8 17 0 64.02 240.00 198.21 o -7 17 0 84.95 -133.73 185.07 o -6 17 0 19.87 38.81 188.06 o -5 17 0 267.17 363.58 200.59 o -4 17 0 321.27 344.47 189.25 o -3 17 0 62.06 -160.00 160.60 o -2 17 0 90.05 -19.81 111.34 o -1 17 0 10.23 -110.29 110.29 o 0 17 0 31.02 -143.28 143.28 o 1 17 0 3.87 -2.99 158.21 o -9 18 0 74.74 -165.37 201.79 o -8 18 0 25.11 -167.76 187.46 o -7 18 0 5.35 -31.04 188.65 o -6 18 0 134.26 -15.52 187.46 o -5 18 0 171.08 343.28 197.01 o -4 18 0 23.64 44.78 173.73 o -3 18 0 3.23 -177.91 177.91 o -2 18 0 0.48 -183.28 188.65 o -1 18 0 17.23 -151.94 151.94 o -7 19 0 54.24 8.96 198.21 o -6 19 0 30.77 2.39 187.46 o -5 19 0 1.06 -75.82 196.42 o -4 19 0 47.58 10.15 208.36 o 3 -19 1 121.22 -1.79 207.16 o 4 -19 1 141.47 -71.64 197.01 o 5 -19 1 6.24 -118.21 188.65 o 6 -19 1 313.06 402.98 202.39 o 7 -19 1 71.06 -121.79 192.24 o 0 -18 1 172.71 97.31 175.52 o 1 -18 1 13.00 -180.89 180.89 o 2 -18 1 72.71 -118.80 180.30 o 3 -18 1 155.70 -22.09 182.09 o 4 -18 1 40.87 93.73 173.73 o 5 -18 1 121.90 -165.37 165.37 o 6 -18 1 108.75 80.00 189.85 o 7 -18 1 8.65 -134.33 181.49 o 8 -18 1 124.01 -77.01 193.43 o 9 -18 1 8.33 -195.22 195.22 o -1 -17 1 152.15 242.98 164.77 o 0 -17 1 20.21 -63.88 144.48 o 1 -17 1 7.97 -104.02 108.24 o 2 -17 1 259.05 4.18 171.94 o 3 -17 1 101.57 80.60 174.92 o 4 -17 1 266.14 425.67 190.45 o 5 -17 1 473.89 687.75 211.34 o 6 -17 1 12.80 -172.54 172.54 o 7 -17 1 635.71 679.40 213.73 o 8 -17 1 21.42 -158.80 176.71 o 9 -17 1 55.98 -189.85 189.85 o 10 -17 1 77.62 -20.52 209.25 o 11 -17 1 14.90 -153.20 153.20 o -2 -16 1 22.25 124.77 148.66 o -1 -16 1 130.87 31.04 136.12 o 0 -16 1 0.18 -93.52 93.52 o 1 -16 1 676.99 717.15 120.87 o 2 -16 1 119.06 -63.84 96.93 o 3 -16 1 652.24 583.28 188.65 o 4 -16 1 1078.23 1236.40 219.10 o 5 -16 1 8.80 -170.15 170.15 o 6 -16 1 1078.01 1220.15 166.86 o 7 -16 1 276.08 309.55 126.28 o 8 -16 1 79.33 -68.70 120.56 o 9 -16 1 234.26 266.43 168.65 o 10 -16 1 2.99 -94.09 139.03 o 11 -16 1 86.37 101.07 153.34 o -2 -15 1 303.22 461.49 147.46 o -1 -15 1 58.02 -60.63 188.65 o 0 -15 1 572.17 870.95 169.55 o 1 -15 1 93.36 68.05 92.10 o 2 -15 1 453.28 524.21 109.86 o 3 -15 1 351.95 324.13 83.09 o 4 -15 1 49.54 16.12 101.91 o 5 -15 1 838.57 819.95 118.62 o 6 -15 1 1557.55 1718.95 135.11 o 7 -15 1 31.07 -49.32 102.09 o 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