Acta Cryst. (2009). E65, m191  [ doi:10.1107/S1600536809000890 ]

(3,5,7-Tribromotropolonato-²O,O')tris(triphenylphosphine-P)silver(I)

G. Steyl and T. N. Hill

Online 14 January 2009

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.008 Å
• R factor = 0.046
• wR factor = 0.165
• Data-to-parameter ratio = 18.3

checkCIF/PLATON results

No syntax errors found




Alert level C
            Value of measurement temperature given =   100.000
            Value of melting point given =     0.000
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.77 Ratio
PLAT432_ALERT_2_C Short Inter X...Y Contact  Br5    ..  C224    ..       3.27 Ang. 
PLAT234_ALERT_4_C Large Hirshfeld Difference O2     --  C2      ..       0.11  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C121   --  C122    ..       0.10  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C133   --  C134    ..       0.13  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C214   --  C215    ..       0.11  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C324   --  C325    ..       0.12  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C334   --  C335    ..       0.10  Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C335   --  C336    ..       0.11  Ang.

Alert level G
PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 =          3      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   9 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   8 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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