Acta Cryst. (2009). E65, m158-m159  [ doi:10.1107/S1600536808042980 ]

[Bis(diphenylphosphino)methane-²P,P']dichloridopalladium(II)

M. Shahid, Imtiaz-ud-Din, M. Mazhar, M. Zeller and A. D. Hunter

Online 8 January 2009

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.004 Å
• Disorder in main residue
• R factor = 0.035
• wR factor = 0.078
• Data-to-parameter ratio = 18.6

checkCIF/PLATON results

No syntax errors found




Alert level C
            Value of measurement temperature given =   100.000
            Value of melting point given =     0.000
PLAT083_ALERT_2_C SHELXL Second Parameter in WGHT unusually Large.       8.00      
PLAT301_ALERT_3_C Main Residue  Disorder .........................      12.00 Perc.
PLAT764_ALERT_4_C Overcomplete CIF Bond List Detected (Rep/Expd) .       1.19 Ratio

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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