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Acta Cryst. (2009). E65, m273  [ doi:10.1107/S1600536809004279 ]


Z. Hong

Online 13 February 2009

Key indicators

checkCIF/PLATON results

No syntax errors found

Alert level C Value of measurement temperature given = 298.000 Value of melting point given = 0.000 PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ni1 -- N1 .. 5.72 su PLAT420_ALERT_2_C D-H Without Acceptor N1 - H1 ... ? PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ? PLAT062_ALERT_4_C Rescale T(min) & T(max) by ..................... 0.98
Alert level G FORMU01_ALERT_1_G There is a discrepancy between the atom counts in the _chemical_formula_sum and _chemical_formula_moiety. This is usually due to the moiety formula being in the wrong format. Atom count from _chemical_formula_sum: C14 H10 Cl2 N2 Ni1 O2 Atom count from _chemical_formula_moiety: PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 1
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 4 ALERT level C = Check and explain 2 ALERT level G = General alerts; check 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

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