# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' cad4 in C 2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 805.52 _exptl_crystal_F_000 3024.00 _reflns_d_resolution_high 0.7577 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 31.4371 _cell_length_b 14.1778 _cell_length_c 16.0344 _cell_angle_alpha 90.000 _cell_angle_beta 99.605 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 21697.52 22010.61 325.90 o 8 0 0 55489.29 48269.63 723.39 o 10 0 0 17554.01 15590.81 111.61 o 12 0 0 6983.75 5945.44 207.17 o 14 0 0 22600.61 22356.74 206.09 o 16 0 0 771.21 780.26 40.77 o 18 0 0 3939.79 4050.93 83.02 o 20 0 0 24562.81 23581.03 213.35 o 22 0 0 13186.23 12517.10 149.11 o 24 0 0 2964.45 2813.92 86.04 o 26 0 0 16478.32 16179.21 375.53 o 28 0 0 961.30 1110.32 93.38 o 30 0 0 500.90 685.05 62.09 o 32 0 0 1001.07 899.23 99.87 o 34 0 0 18.86 75.09 218.76 o 36 0 0 1675.08 1640.53 104.90 o 38 0 0 7.49 -107.74 113.45 o 40 0 0 880.95 896.68 104.07 o 3 1 0 12232.48 12400.36 78.38 o 5 1 0 1301.73 1419.65 28.31 o 7 1 0 15625.25 15394.65 165.43 o 9 1 0 225.56 221.61 32.16 o 11 1 0 1754.05 1660.41 42.63 o 13 1 0 1173.55 1160.31 67.25 o 15 1 0 1986.38 1837.78 73.28 o 17 1 0 28.76 -44.51 50.39 o 19 1 0 3250.10 3208.12 74.56 o 21 1 0 1437.40 1112.29 57.47 o 23 1 0 613.21 633.22 55.30 o 25 1 0 6216.44 6316.32 122.11 o 27 1 0 4526.89 4213.10 232.37 o 29 1 0 710.16 764.36 72.97 o 31 1 0 97.86 77.97 69.20 o 33 1 0 477.11 407.91 68.20 o 35 1 0 388.86 225.34 89.94 o 37 1 0 20.73 -84.14 110.23 o 39 1 0 689.61 636.47 100.18 o 0 2 0 84.85 196.97 25.97 o 2 2 0 1207.30 1229.71 25.91 o 4 2 0 17908.36 17943.89 117.63 o 6 2 0 3059.10 3879.56 85.81 o 8 2 0 45408.23 39267.86 818.47 o 10 2 0 3180.76 3968.62 135.59 o 12 2 0 53163.50 54903.57 392.85 o 14 2 0 8648.92 8877.49 97.08 o 16 2 0 7073.74 7027.71 147.65 o 18 2 0 5531.47 6638.49 98.06 o 20 2 0 566.28 455.03 82.71 o 22 2 0 653.25 538.41 52.47 o 24 2 0 9662.51 9069.91 486.38 o 26 2 0 4315.26 3839.67 104.29 o 28 2 0 3653.13 3354.38 106.66 o 30 2 0 619.48 611.09 66.65 o 32 2 0 2725.67 2520.27 144.09 o 34 2 0 50.40 37.31 78.99 o 36 2 0 1197.36 1417.86 98.25 o 38 2 0 61.55 153.11 85.65 o 40 2 0 114.77 15.34 117.71 o 1 3 0 19094.93 16118.13 102.54 o 3 3 0 44839.22 45292.04 1527.33 o 5 3 0 19631.56 19171.62 788.17 o 9 3 0 850.49 1574.36 41.51 o 11 3 0 3018.28 2786.27 54.88 o 13 3 0 10363.13 9673.55 238.09 o 15 3 0 344.60 351.12 36.16 o 17 3 0 65.26 -50.59 50.59 o 21 3 0 1696.33 1477.92 65.59 o 23 3 0 5382.80 4716.20 104.51 o 25 3 0 413.23 522.34 60.94 o 27 3 0 137.32 47.42 79.77 o 29 3 0 1138.07 1211.61 131.10 o 31 3 0 1.27 19.10 83.90 o 33 3 0 461.30 660.91 183.05 o 35 3 0 320.94 361.97 104.82 o 37 3 0 102.98 87.93 90.17 o 39 3 0 260.77 200.75 97.15 o 0 4 0 2715.15 2290.30 59.68 o 2 4 0 2456.40 2479.33 68.18 o 4 4 0 1512.06 1638.90 81.79 o 6 4 0 1819.97 1677.92 53.03 o 10 4 0 1.29 31.44 64.47 o 12 4 0 107.38 28.42 35.35 o 14 4 0 13039.50 13564.95 289.57 o 16 4 0 5.05 -18.08 46.52 o 18 4 0 3352.62 3049.30 75.10 o 20 4 0 9133.88 8198.54 119.92 o 22 4 0 4740.24 4666.13 180.73 o 24 4 0 10100.67 9540.43 147.58 o 26 4 0 16572.59 15715.48 194.36 o 28 4 0 328.63 195.24 124.61 o 30 4 0 331.09 298.20 65.69 o 32 4 0 116.33 24.57 100.55 o 34 4 0 15.04 -105.69 105.69 o 36 4 0 9.28 -112.15 112.15 o 38 4 0 244.17 360.33 97.40 o 1 5 0 23092.79 21901.60 170.68 o 3 5 0 1113.91 987.64 36.51 o 5 5 0 607.68 419.15 62.92 o 7 5 0 2611.87 2687.10 54.09 o 9 5 0 7564.67 7217.86 217.06 o 11 5 0 4529.47 4681.36 145.79 o 13 5 0 1865.99 1773.33 56.96 o 15 5 0 4800.63 4116.10 181.20 o 17 5 0 3223.33 3327.87 79.15 o 19 5 0 6043.03 5960.28 173.77 o 21 5 0 6.60 -64.32 64.32 o 23 5 0 3408.33 3074.61 93.68 o 25 5 0 478.12 486.67 62.63 o 27 5 0 2299.74 2327.23 91.15 o 29 5 0 545.18 572.03 70.52 o 31 5 0 2043.45 2035.89 97.61 o 33 5 0 46.43 111.83 94.33 o 35 5 0 1457.81 1657.83 104.61 o 37 5 0 101.00 180.85 166.66 o 39 5 0 146.01 196.51 83.59 o 0 6 0 415.30 677.78 55.04 o 2 6 0 17.83 84.96 50.86 o 4 6 0 2804.71 2197.02 102.97 o 6 6 0 21956.29 20211.42 934.43 o 8 6 0 18465.88 19097.63 938.14 o 10 6 0 4867.75 4596.69 190.78 o 12 6 0 320.96 404.59 110.08 o 14 6 0 3637.05 4036.95 80.99 o 16 6 0 11.98 -20.83 81.94 o 18 6 0 4832.26 4282.03 265.76 o 20 6 0 363.48 408.59 94.15 o 22 6 0 481.76 458.19 58.30 o 24 6 0 5802.37 5607.79 124.27 o 26 6 0 60.97 61.62 84.37 o 28 6 0 25.28 50.51 66.75 o 30 6 0 117.68 151.64 73.10 o 32 6 0 231.82 131.32 87.49 o 34 6 0 317.99 464.49 77.34 o 36 6 0 32.33 51.57 108.99 o 38 6 0 271.36 399.81 84.72 o 1 7 0 550.91 483.44 72.20 o 3 7 0 4.11 -41.84 44.38 o 5 7 0 5529.39 5319.01 153.37 o 7 7 0 770.50 719.86 44.05 o 9 7 0 4465.24 3897.80 77.24 o 11 7 0 525.39 518.22 45.01 o 13 7 0 461.64 437.27 79.16 o 15 7 0 2601.87 2661.86 128.48 o 17 7 0 19437.28 17596.02 953.13 o 19 7 0 4933.44 4630.68 105.27 o 21 7 0 3967.92 3604.66 102.88 o 23 7 0 3307.67 2985.26 96.37 o 25 7 0 4.78 30.53 83.70 o 27 7 0 181.38 154.32 190.47 o 29 7 0 20.01 -6.42 83.12 o 31 7 0 16.08 17.43 110.70 o 33 7 0 16.86 27.80 96.95 o 35 7 0 0.71 -42.46 113.26 o 37 7 0 622.55 631.38 117.34 o 0 8 0 6950.58 7064.16 135.74 o 2 8 0 1655.74 1610.18 54.06 o 4 8 0 12.41 13.77 40.09 o 6 8 0 18.42 85.00 35.20 o 8 8 0 7128.04 7322.10 422.53 o 10 8 0 11775.91 11422.72 524.42 o 12 8 0 22462.50 22404.35 464.74 o 14 8 0 4870.57 4766.86 162.95 o 16 8 0 1531.81 1388.47 67.52 o 18 8 0 26.97 113.83 59.17 o 20 8 0 5167.94 5328.06 456.24 o 22 8 0 636.38 578.33 101.57 o 24 8 0 151.78 199.51 62.29 o 26 8 0 4490.44 4749.69 125.06 o 28 8 0 146.59 60.39 76.98 o 30 8 0 2525.77 2667.90 201.91 o 32 8 0 994.55 913.98 272.88 o 34 8 0 2844.27 3153.04 133.95 o 36 8 0 801.17 779.43 110.85 o 1 9 0 334.50 367.61 64.47 o 3 9 0 3059.22 3301.75 77.16 o 5 9 0 26032.97 23862.84 538.95 o 7 9 0 18659.48 17520.05 627.54 o 9 9 0 15284.13 14450.01 485.30 o 11 9 0 10207.86 9425.95 347.39 o 13 9 0 1566.60 1371.04 214.13 o 15 9 0 3413.22 3385.35 227.27 o 17 9 0 1847.52 1932.58 79.47 o 19 9 0 210.00 159.17 80.70 o 21 9 0 212.15 289.09 56.87 o 23 9 0 292.55 260.99 155.69 o 25 9 0 161.87 118.37 76.99 o 27 9 0 775.35 690.14 80.61 o 29 9 0 1371.48 1436.21 217.68 o 31 9 0 795.79 842.84 183.82 o 33 9 0 236.42 359.50 80.88 o 35 9 0 209.43 116.17 99.32 o 0 10 0 299.94 235.31 62.46 o 2 10 0 10.39 -35.62 87.51 o 4 10 0 1.06 -43.84 60.43 o 6 10 0 1332.02 1183.30 89.52 o 8 10 0 73.16 -8.61 84.72 o 10 10 0 9040.21 8315.74 217.37 o 12 10 0 757.10 531.50 62.75 o 14 10 0 33.08 -57.64 65.56 o 16 10 0 342.18 295.95 120.75 o 18 10 0 451.18 525.67 61.21 o 20 10 0 433.91 565.49 67.49 o 22 10 0 659.75 809.37 73.65 o 24 10 0 509.11 672.41 179.49 o 26 10 0 47.04 86.69 84.43 o 28 10 0 46.29 -23.17 98.54 o 30 10 0 330.04 294.25 81.55 o 32 10 0 27.68 73.63 108.73 o 34 10 0 64.17 -105.65 197.74 o 1 11 0 849.54 777.08 62.42 o 3 11 0 282.75 313.43 50.22 o 5 11 0 2.01 -68.43 68.43 o 7 11 0 54.65 143.78 53.12 o 9 11 0 1969.19 1926.63 81.52 o 11 11 0 1332.36 1175.65 168.67 o 13 11 0 45.29 27.42 130.02 o 15 11 0 3138.19 2797.81 99.10 o 17 11 0 729.13 749.12 71.04 o 19 11 0 266.71 283.85 102.19 o 21 11 0 3025.49 2788.43 247.06 o 23 11 0 1052.54 870.33 109.61 o 25 11 0 266.32 98.53 103.12 o 27 11 0 6.53 -46.82 101.63 o 29 11 0 199.83 195.09 219.69 o 31 11 0 45.06 223.94 107.14 o 33 11 0 56.56 84.33 96.03 o 0 12 0 7634.15 6535.41 178.10 o 2 12 0 536.79 427.22 61.66 o 4 12 0 1149.98 920.98 72.70 o 6 12 0 10804.12 10290.50 401.66 o 8 12 0 3496.11 3254.71 99.69 o 10 12 0 2521.66 2653.05 95.21 o 12 12 0 7973.27 7337.57 366.10 o 14 12 0 8250.19 7820.73 163.57 o 16 12 0 428.82 268.80 69.40 o 18 12 0 621.42 525.21 84.26 o 20 12 0 1.71 -108.22 108.22 o 22 12 0 414.09 482.71 72.41 o 24 12 0 41.57 63.94 104.02 o 26 12 0 104.20 104.46 104.58 o 28 12 0 25.98 25.16 109.39 o 30 12 0 81.43 226.00 79.04 o 1 13 0 81.93 167.59 60.33 o 3 13 0 714.27 828.11 70.93 o 5 13 0 1.52 103.25 63.54 o 7 13 0 6.86 -80.50 86.56 o 9 13 0 0.20 98.54 57.36 o 11 13 0 58.03 42.55 89.27 o 13 13 0 4515.18 4449.44 164.96 o 15 13 0 1745.29 1657.50 208.87 o 17 13 0 1515.47 1505.49 89.84 o 19 13 0 2299.72 2445.58 209.64 o 21 13 0 2676.32 2712.73 116.86 o 23 13 0 976.77 1102.13 91.02 o 25 13 0 66.62 157.26 119.51 o 27 13 0 35.89 97.06 110.08 o 29 13 0 310.95 176.23 94.55 o 0 14 0 381.05 434.75 94.93 o 2 14 0 131.26 166.30 122.29 o 4 14 0 365.64 331.91 64.66 o 6 14 0 317.18 160.17 157.08 o 8 14 0 305.65 320.03 65.59 o 10 14 0 2998.70 2571.13 108.21 o 12 14 0 795.61 711.73 81.66 o 14 14 0 706.51 680.27 154.29 o 16 14 0 1236.56 1138.75 91.73 o 18 14 0 834.76 775.57 82.65 o 20 14 0 300.33 333.24 74.71 o 22 14 0 23.29 65.73 106.12 o 24 14 0 5.60 -62.80 109.99 o 26 14 0 219.22 61.32 120.26 o 1 15 0 663.80 762.93 78.34 o 3 15 0 1000.42 986.48 82.20 o 5 15 0 188.50 212.93 71.33 o 7 15 0 0.39 5.14 83.02 o 9 15 0 216.93 84.97 84.17 o 11 15 0 117.67 30.54 85.77 o 13 15 0 43.85 11.18 85.33 o 15 15 0 8.42 92.01 76.82 o 17 15 0 160.40 6.26 104.89 o 19 15 0 59.68 99.33 86.41 o 21 15 0 27.23 46.16 106.00 o 23 15 0 72.96 266.32 82.63 o 0 16 0 1215.98 1712.39 136.67 o 2 16 0 119.42 251.70 168.36 o 4 16 0 1.39 -29.64 175.01 o 6 16 0 222.26 64.31 89.48 o 8 16 0 54.23 -115.88 171.46 o 10 16 0 2.56 -17.26 99.18 o 12 16 0 210.06 429.40 127.08 o 14 16 0 110.58 114.08 85.95 o 16 16 0 47.42 -122.29 122.29 o 18 16 0 231.50 410.07 80.75 o 20 16 0 90.14 218.24 88.43 o 1 17 0 38.18 -100.21 105.52 o 3 17 0 441.69 520.88 81.21 o 5 17 0 1598.57 1434.71 108.55 o 7 17 0 604.35 578.95 89.09 o 9 17 0 28.90 -36.01 110.29 o 11 17 0 198.37 -19.53 90.87 o 13 17 0 255.48 412.05 85.04 o 15 17 0 4.51 13.72 91.12 o 17 17 0 21.78 143.06 88.60 o 0 18 0 71.48 38.34 157.70 o 2 18 0 566.78 744.41 88.80 o 4 18 0 52.41 33.07 115.64 o 6 18 0 148.09 279.59 223.71 o 8 18 0 116.06 150.17 100.08 o 10 18 0 130.55 127.59 105.55 o -41 1 1 0.71 -84.89 170.53 o -39 1 1 234.78 20.36 190.47 o -37 1 1 53.12 112.83 79.55 o -35 1 1 474.81 613.21 98.02 o -33 1 1 16.38 46.17 73.50 o -31 1 1 1579.28 1554.83 86.33 o -29 1 1 2.15 -31.00 79.20 o -27 1 1 700.65 705.81 68.87 o -25 1 1 11237.17 10895.47 154.09 o -23 1 1 1585.48 1314.09 67.42 o -21 1 1 14955.77 13692.65 149.97 o -19 1 1 12624.28 12065.84 131.29 o -17 1 1 9476.33 7787.21 179.65 o -15 1 1 728.02 743.69 131.26 o -13 1 1 12337.72 12626.65 111.93 o -11 1 1 5612.58 4890.83 151.98 o -9 1 1 14007.54 11443.08 161.87 o -7 1 1 129.67 355.96 27.83 o -5 1 1 22151.03 25096.98 133.14 o -3 1 1 5795.50 5564.92 44.22 o 1 1 1 142284.33 128078.13 4292.27 o 3 1 1 2217.01 2183.62 32.16 o 5 1 1 61664.94 57600.80 209.57 o 7 1 1 10371.28 10894.48 76.63 o 11 1 1 1516.71 1709.53 49.47 o 13 1 1 15871.64 17935.69 129.32 o 15 1 1 50963.51 47228.66 317.44 o 17 1 1 62.90 41.00 50.50 o 19 1 1 4435.06 4002.05 94.46 o 21 1 1 203.92 139.50 45.01 o 23 1 1 9.11 -55.10 67.12 o 25 1 1 3.78 -29.42 123.99 o 27 1 1 3304.10 3247.37 128.78 o 29 1 1 2317.12 2026.02 89.90 o 31 1 1 74.28 90.73 84.10 o 33 1 1 311.63 364.44 71.03 o 35 1 1 89.20 110.45 79.61 o 37 1 1 564.26 771.46 89.93 o 39 1 1 84.90 -102.50 132.38 o -40 2 1 20.90 102.72 94.48 o -38 2 1 198.49 175.75 81.07 o -36 2 1 139.15 343.42 196.97 o -34 2 1 148.22 213.82 128.01 o -32 2 1 132.54 168.55 62.75 o -30 2 1 242.48 257.43 61.96 o -28 2 1 3667.33 3529.18 148.57 o -26 2 1 694.44 620.46 79.16 o -24 2 1 5788.37 5419.67 111.13 o -22 2 1 1955.34 2058.10 72.26 o -20 2 1 59.96 121.78 49.01 o -18 2 1 3622.55 3326.43 75.43 o -16 2 1 6367.34 6492.17 91.06 o -14 2 1 2591.27 2345.13 56.07 o -12 2 1 5660.35 5441.70 71.70 o -10 2 1 14379.02 13382.64 98.93 o -8 2 1 27449.73 24297.24 423.00 o -6 2 1 21560.16 19419.20 118.71 o -4 2 1 77641.34 73341.30 857.28 o -2 2 1 206.66 262.78 27.06 o 0 2 1 31075.16 29762.26 1465.03 o 2 2 1 1248.06 2114.97 71.74 o 4 2 1 48364.48 44339.12 1311.97 o 6 2 1 37431.88 35485.70 488.70 o 8 2 1 51081.28 47410.70 396.56 o 10 2 1 3046.69 2592.36 63.08 o 12 2 1 3997.96 3643.21 121.05 o 14 2 1 8553.66 9006.04 99.70 o 16 2 1 484.10 461.53 40.55 o 18 2 1 5607.10 5121.84 88.96 o 20 2 1 144.97 302.14 70.04 o 22 2 1 9089.07 8985.25 131.15 o 24 2 1 789.39 867.90 66.13 o 26 2 1 1303.94 1298.88 74.04 o 28 2 1 1919.16 1746.84 85.27 o 30 2 1 759.44 647.83 73.44 o 32 2 1 1029.50 920.01 84.07 o 34 2 1 263.13 226.23 73.84 o 36 2 1 0.01 59.51 81.15 o 38 2 1 38.04 -88.86 109.17 o 40 2 1 938.38 1053.98 107.24 o -39 3 1 936.93 930.41 103.72 o -37 3 1 370.75 274.98 97.52 o -35 3 1 434.45 497.42 80.62 o -33 3 1 152.90 333.17 194.65 o -31 3 1 689.24 588.36 70.37 o -29 3 1 6.47 -29.07 170.68 o -27 3 1 5847.69 5790.70 128.85 o -25 3 1 9617.31 8887.88 208.25 o -23 3 1 6623.41 6215.04 241.03 o -21 3 1 2002.63 2004.20 69.62 o -19 3 1 2218.89 2036.81 64.82 o -17 3 1 145.35 227.63 36.29 o -15 3 1 7165.64 6850.69 155.84 o -13 3 1 4479.90 5197.52 120.59 o -11 3 1 36817.43 34473.42 241.59 o -9 3 1 18427.37 17243.33 460.87 o -7 3 1 8212.14 7356.23 70.62 o -5 3 1 6038.87 6261.42 124.15 o -3 3 1 49.86 133.77 22.18 o -1 3 1 3891.52 3068.83 41.54 o 1 3 1 74924.17 68057.48 2894.03 o 3 3 1 90545.84 85773.26 3769.40 o 5 3 1 30125.14 30431.57 1090.27 o 7 3 1 48378.50 41539.03 843.05 o 9 3 1 45.07 69.50 46.54 o 11 3 1 8589.17 9118.22 129.87 o 13 3 1 5932.47 5760.98 219.07 o 15 3 1 3608.81 4469.96 77.82 o 17 3 1 787.88 854.21 88.43 o 19 3 1 11945.02 11606.12 135.77 o 21 3 1 11123.36 10116.49 137.19 o 23 3 1 22816.96 21383.98 407.07 o 25 3 1 7611.10 7623.46 135.88 o 27 3 1 3841.98 3750.85 152.13 o 29 3 1 7399.35 6799.16 181.20 o 31 3 1 741.09 690.75 73.28 o 33 3 1 670.86 776.43 78.30 o 35 3 1 3.43 57.67 77.45 o 37 3 1 182.34 304.37 134.04 o 39 3 1 214.63 310.52 84.40 o -40 4 1 237.24 3.50 174.24 o -38 4 1 352.90 333.77 145.64 o -36 4 1 516.71 695.35 97.71 o -34 4 1 201.23 212.33 86.83 o -32 4 1 117.04 -48.66 103.28 o -30 4 1 633.46 663.88 122.60 o -28 4 1 296.77 233.94 63.08 o -26 4 1 46.43 -39.34 79.11 o -24 4 1 751.70 755.74 94.93 o -22 4 1 2534.49 2469.34 185.99 o -20 4 1 474.80 612.80 127.24 o -18 4 1 1273.35 1273.92 55.81 o -16 4 1 927.03 898.10 69.11 o -14 4 1 9201.82 8586.99 103.50 o -12 4 1 1826.87 1893.55 52.14 o -10 4 1 124.76 134.61 28.84 o -8 4 1 5070.69 4540.59 162.18 o -6 4 1 3252.67 3625.38 93.69 o -2 4 1 1154.48 1190.17 33.77 o 2 4 1 23505.69 21999.58 546.06 o 4 4 1 24553.17 24066.45 515.60 o 6 4 1 1654.50 2043.06 45.47 o 8 4 1 133.57 166.38 40.35 o 10 4 1 39379.59 40195.46 711.49 o 12 4 1 750.74 755.90 39.98 o 14 4 1 12436.44 11660.21 345.38 o 16 4 1 6774.99 6059.41 151.82 o 18 4 1 35.74 39.73 74.06 o 20 4 1 1497.22 1527.21 64.92 o 22 4 1 10799.08 10420.18 201.60 o 24 4 1 3393.78 3272.15 101.71 o 26 4 1 944.17 1305.68 78.03 o 28 4 1 2099.50 2194.61 95.00 o 30 4 1 1742.08 1536.83 92.20 o 32 4 1 1863.83 1908.36 99.79 o 34 4 1 569.06 684.26 101.11 o 36 4 1 1813.40 1995.20 113.76 o 38 4 1 30.66 38.50 121.58 o -39 5 1 28.83 93.95 95.63 o -37 5 1 30.56 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