# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' A in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 743.77 _exptl_crystal_F_000 1240.00 _reflns_d_resolution_high 0.7699 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 8.0678 _cell_length_b 19.4461 _cell_length_c 15.1075 _cell_angle_alpha 90.000 _cell_angle_beta 99.354 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14365.53 13740.29 165.40 o 4 0 0 9521.92 9569.34 176.01 o 6 0 0 2922.72 3058.76 105.92 o 8 0 0 38.41 71.20 20.48 o 1 1 0 48185.21 22755.09 99.07 o 3 1 0 3464.80 3355.50 47.00 o 5 1 0 413.84 427.37 29.08 o 7 1 0 404.92 394.87 29.15 o 9 1 0 208.89 234.65 48.36 o 0 2 0 12.38 0.77 1.21 o 2 2 0 137448.48 134336.52 2880.56 o 4 2 0 2134.33 2045.69 46.14 o 6 2 0 183.47 205.39 15.27 o 8 2 0 53.75 107.70 19.00 o 10 2 0 23.17 8.30 14.94 o 1 3 0 20039.48 19675.04 90.56 o 3 3 0 3568.18 3753.41 59.97 o 5 3 0 1107.16 1040.35 42.37 o 7 3 0 1787.01 1844.16 98.38 o 9 3 0 761.90 556.37 77.04 o 0 4 0 3155.05 3398.28 55.00 o 2 4 0 2695.22 2511.69 17.72 o 4 4 0 56.36 32.49 4.25 o 6 4 0 6668.08 6702.34 102.28 o 8 4 0 845.38 695.09 73.25 o 10 4 0 677.08 503.57 299.99 o 1 5 0 14219.12 13239.92 112.16 o 3 5 0 574.91 679.17 23.46 o 5 5 0 767.95 861.90 29.44 o 7 5 0 3060.75 3286.03 148.45 o 9 5 0 883.52 632.63 86.69 o 0 6 0 72.14 65.26 9.03 o 2 6 0 2727.98 2869.34 47.28 o 4 6 0 922.21 912.33 34.67 o 6 6 0 5993.83 6199.28 133.04 o 8 6 0 121.50 97.14 24.63 o 10 6 0 7.78 24.91 12.52 o 1 7 0 30155.48 28796.86 171.65 o 3 7 0 270.57 211.12 12.06 o 5 7 0 115.45 106.07 19.41 o 7 7 0 51.53 94.33 27.71 o 9 7 0 48.90 46.81 18.27 o 0 8 0 261792.16 270533.03 7921.30 o 2 8 0 6696.84 6617.41 143.78 o 4 8 0 240.84 174.53 20.05 o 6 8 0 2146.48 2194.97 48.68 o 8 8 0 92.95 95.73 45.80 o 1 9 0 20521.84 19775.65 337.29 o 3 9 0 4954.44 4781.44 152.72 o 5 9 0 938.47 945.93 48.45 o 7 9 0 1337.61 1418.53 128.62 o 9 9 0 107.03 82.67 23.26 o 0 10 0 147.53 171.00 17.87 o 2 10 0 37303.96 38867.40 458.75 o 4 10 0 1110.07 1165.15 56.08 o 6 10 0 67.19 58.63 14.58 o 8 10 0 16.05 26.64 9.82 o 1 11 0 9384.07 10034.69 173.03 o 3 11 0 4515.84 4511.91 86.49 o 5 11 0 1213.82 1187.38 71.21 o 7 11 0 251.50 225.72 34.94 o 9 11 0 117.97 125.09 48.15 o 0 12 0 4363.74 4204.40 206.24 o 2 12 0 1033.27 1036.07 30.28 o 4 12 0 79.85 50.31 8.62 o 6 12 0 2751.26 3043.85 96.47 o 8 12 0 167.69 158.00 28.11 o 1 13 0 700.87 679.29 21.80 o 3 13 0 197.17 199.24 12.13 o 5 13 0 1047.30 1163.18 41.13 o 7 13 0 1645.34 1657.50 109.37 o 0 14 0 161.24 163.15 21.95 o 2 14 0 4970.28 5164.06 66.71 o 4 14 0 138.12 171.05 38.27 o 6 14 0 5501.02 6027.98 261.59 o 8 14 0 91.06 86.36 25.44 o 1 15 0 3890.42 3852.76 76.76 o 3 15 0 14.81 18.33 14.89 o 5 15 0 275.55 234.85 27.66 o 7 15 0 228.51 248.44 25.26 o 0 16 0 7338.87 8193.13 208.30 o 2 16 0 1435.34 1523.94 44.47 o 4 16 0 5879.59 6095.36 155.52 o 6 16 0 808.79 752.88 75.50 o 1 17 0 4047.08 4177.05 65.00 o 3 17 0 1478.85 1477.90 56.02 o 5 17 0 946.33 771.32 49.87 o 7 17 0 656.42 565.60 69.74 o 0 18 0 112.88 131.54 29.27 o 2 18 0 2135.72 2355.09 53.42 o 4 18 0 240.42 213.84 37.57 o 6 18 0 0.29 6.73 29.89 o 1 19 0 2195.15 2296.78 68.66 o 3 19 0 1261.71 1366.09 68.85 o 5 19 0 666.74 665.07 113.44 o 0 20 0 93.91 79.45 32.03 o 2 20 0 181.61 140.40 25.91 o 4 20 0 532.07 482.17 60.48 o 6 20 0 567.58 409.50 64.95 o 1 21 0 86.47 71.86 31.22 o 3 21 0 340.02 306.57 52.49 o 5 21 0 555.91 572.25 104.02 o 0 22 0 90.11 42.64 15.50 o 2 22 0 516.61 556.85 39.53 o 4 22 0 9.84 35.03 16.11 o 1 23 0 23.80 54.51 10.93 o 3 23 0 19.22 41.83 19.27 o 0 24 0 22.37 36.10 22.21 o 2 24 0 210.47 306.33 38.26 o 1 25 0 453.18 301.48 115.04 o -9 1 1 7.47 31.91 17.31 o -7 1 1 4219.41 4307.66 135.09 o -5 1 1 6.58 24.13 6.06 o -3 1 1 6227.67 5524.02 90.37 o -1 1 1 48071.54 44034.50 102.48 o 1 1 1 5378.75 5229.84 27.59 o 3 1 1 17374.67 17403.66 79.12 o 5 1 1 4893.15 4783.42 61.16 o 7 1 1 1389.20 1447.46 39.77 o 9 1 1 475.09 552.05 51.47 o -10 2 1 61.18 39.30 21.03 o -8 2 1 269.77 304.32 36.63 o -6 2 1 4862.84 5079.75 140.85 o -4 2 1 3995.39 4719.93 32.52 o -2 2 1 29127.80 29045.71 344.96 o 2 2 1 15873.46 15367.23 86.79 o 4 2 1 13876.36 14809.63 230.08 o 6 2 1 5230.62 5611.44 153.98 o 8 2 1 91.24 152.80 28.97 o -9 3 1 378.84 351.77 55.22 o -7 3 1 3067.78 3217.12 119.12 o -5 3 1 7.36 23.42 11.35 o -3 3 1 333.18 601.73 19.20 o -1 3 1 22613.91 21441.75 125.19 o 1 3 1 582.12 463.81 12.64 o 5 3 1 20.39 32.17 7.77 o 7 3 1 370.36 368.84 39.26 o 9 3 1 1093.59 1047.79 201.47 o -10 4 1 23.95 31.44 10.48 o -8 4 1 19.32 57.29 17.22 o -6 4 1 376.13 422.35 27.52 o -4 4 1 1000.14 972.97 28.99 o -2 4 1 1915.53 2345.36 108.71 o 0 4 1 227.82 161.22 5.27 o 2 4 1 96.46 72.32 4.75 o 4 4 1 571.48 582.23 36.93 o 6 4 1 322.29 326.96 30.76 o 8 4 1 89.76 64.56 12.18 o 10 4 1 31.61 6.64 17.16 o -9 5 1 12.02 32.85 23.25 o -7 5 1 741.34 832.23 80.69 o -5 5 1 1742.16 1695.03 27.97 o -3 5 1 2416.61 2586.26 107.10 o -1 5 1 987.78 873.15 22.87 o 1 5 1 493.82 473.16 13.23 o 3 5 1 3220.85 2863.86 59.15 o 5 5 1 2602.70 2576.64 60.45 o 7 5 1 133.01 178.46 20.45 o 9 5 1 227.06 186.98 38.60 o -10 6 1 25.24 43.79 12.23 o -8 6 1 638.76 649.38 65.30 o -6 6 1 7614.85 7550.06 321.74 o -4 6 1 1197.56 927.77 52.21 o -2 6 1 3183.81 2805.41 56.56 o 0 6 1 21532.73 19983.24 101.51 o 2 6 1 8286.49 8316.28 134.85 o 4 6 1 5458.82 4667.93 109.41 o 6 6 1 2477.36 2436.35 74.62 o 8 6 1 753.50 628.47 42.01 o -9 7 1 4.08 45.39 14.49 o -7 7 1 3556.74 3803.35 85.33 o -5 7 1 29.75 62.40 11.71 o -3 7 1 12921.15 12612.82 874.24 o -1 7 1 18194.76 17706.12 90.67 o 1 7 1 7140.45 6772.30 72.58 o 3 7 1 8848.50 8444.89 156.87 o 5 7 1 6053.70 6165.23 151.56 o 7 7 1 726.06 704.34 77.44 o 9 7 1 406.64 324.45 89.67 o -8 8 1 5.41 47.60 16.60 o -6 8 1 241.18 251.08 24.17 o -4 8 1 3604.84 3550.87 115.01 o -2 8 1 173.21 170.68 11.33 o 0 8 1 5762.30 5214.37 89.55 o 2 8 1 107.73 144.00 12.31 o 4 8 1 3.22 24.21 13.52 o 6 8 1 883.45 984.27 45.00 o 8 8 1 7.28 45.87 25.81 o -9 9 1 48.81 64.47 20.21 o -7 9 1 816.10 1011.20 52.70 o -5 9 1 2.67 22.64 11.67 o -3 9 1 2590.90 2263.38 74.68 o -1 9 1 37368.14 35960.13 315.53 o 1 9 1 914.66 816.74 32.71 o 3 9 1 9120.26 9497.67 175.08 o 5 9 1 2601.39 2338.36 129.42 o 7 9 1 733.22 821.56 71.39 o 9 9 1 58.55 68.63 40.96 o -8 10 1 184.65 265.29 34.37 o -6 10 1 1605.38 1742.33 52.16 o -4 10 1 1604.46 1820.11 45.68 o -2 10 1 23196.13 23914.76 162.34 o 0 10 1 32315.31 32140.24 447.89 o 2 10 1 6625.82 6468.96 56.81 o 4 10 1 8969.97 9510.39 309.75 o 6 10 1 2769.03 3104.04 84.20 o 8 10 1 2.80 9.95 6.52 o -9 11 1 167.37 94.63 32.68 o -7 11 1 2014.29 2175.89 170.87 o -5 11 1 30.87 62.40 12.68 o -3 11 1 1479.37 1531.79 55.68 o -1 11 1 12069.42 12032.35 197.73 o 1 11 1 44.64 84.07 12.62 o 3 11 1 8617.16 8416.67 197.12 o 5 11 1 378.70 434.29 34.60 o 7 11 1 282.38 257.55 38.53 o 9 11 1 819.48 733.18 162.17 o -8 12 1 0.36 32.32 12.60 o -6 12 1 768.50 832.04 89.00 o -4 12 1 843.06 696.52 111.10 o -2 12 1 3883.29 3828.30 81.88 o 0 12 1 500.38 548.67 17.91 o 2 12 1 1684.34 1657.24 38.67 o 4 12 1 1864.64 1744.26 81.85 o 6 12 1 517.96 575.32 54.92 o 8 12 1 197.19 98.65 28.54 o -7 13 1 84.74 86.50 19.58 o -5 13 1 1698.95 1793.53 143.56 o -3 13 1 2145.61 2114.62 45.67 o -1 13 1 172.68 116.35 8.64 o 1 13 1 32.83 34.89 18.64 o 3 13 1 15.63 43.62 10.27 o 5 13 1 3079.52 3262.82 91.79 o 7 13 1 565.82 586.68 72.79 o -8 14 1 435.48 532.14 57.39 o -6 14 1 2662.45 2661.03 127.21 o -4 14 1 1.66 43.44 10.44 o -2 14 1 579.09 626.19 22.88 o 0 14 1 1791.14 1809.88 56.07 o 2 14 1 318.44 301.45 17.56 o 4 14 1 1444.00 1498.67 36.59 o 6 14 1 236.35 288.57 41.77 o 8 14 1 566.66 488.56 70.21 o -7 15 1 1351.98 1512.60 138.27 o -5 15 1 5.24 16.02 17.58 o -3 15 1 5303.04 5384.56 79.84 o -1 15 1 4060.66 4119.46 61.63 o 1 15 1 2079.70 2065.60 64.57 o 3 15 1 1364.21 1396.85 28.47 o 5 15 1 3013.58 3257.05 216.90 o 7 15 1 110.65 94.76 25.54 o -8 16 1 57.17 68.63 18.47 o -6 16 1 370.56 357.93 38.40 o -4 16 1 2307.07 2317.90 68.11 o -2 16 1 22.32 43.04 11.20 o 0 16 1 2489.45 2475.80 38.49 o 2 16 1 44.35 48.15 10.73 o 4 16 1 4.28 23.86 12.34 o 6 16 1 733.04 697.49 55.93 o -7 17 1 7.83 56.20 15.15 o -5 17 1 107.32 61.32 15.94 o -3 17 1 919.53 987.51 91.03 o -1 17 1 8072.17 8442.85 143.48 o 1 17 1 54.12 56.63 16.98 o 3 17 1 1700.66 1779.95 49.50 o 5 17 1 827.75 825.85 77.74 o 7 17 1 44.55 50.44 21.59 o -6 18 1 462.82 394.82 39.41 o -4 18 1 5.48 11.83 9.87 o -2 18 1 6953.46 7637.22 187.59 o 0 18 1 6551.17 6883.77 97.16 o 2 18 1 963.87 991.05 38.11 o 4 18 1 2425.21 2612.38 135.25 o 6 18 1 350.38 257.67 36.91 o -5 19 1 343.67 278.87 43.22 o -3 19 1 164.74 110.18 21.86 o -1 19 1 2802.24 3052.03 68.28 o 1 19 1 5.08 33.53 18.65 o 3 19 1 1584.68 1590.49 79.24 o 5 19 1 33.94 54.17 22.85 o -6 20 1 85.40 48.82 28.12 o -4 20 1 96.10 66.55 50.09 o -2 20 1 1043.25 1046.42 83.29 o 0 20 1 641.49 689.71 30.78 o 2 20 1 1296.33 1247.26 101.98 o 4 20 1 563.82 457.14 60.80 o 6 20 1 76.60 31.87 20.54 o -5 21 1 207.95 165.40 34.75 o -3 21 1 470.89 537.39 38.68 o -1 21 1 50.37 86.50 25.08 o 1 21 1 7.23 59.96 19.51 o 3 21 1 28.42 40.54 15.98 o 5 21 1 786.22 719.04 104.75 o -4 22 1 29.16 85.88 21.71 o -2 22 1 331.15 428.02 60.31 o 0 22 1 30.58 28.67 17.62 o 2 22 1 148.56 199.82 26.84 o 4 22 1 495.62 550.56 122.50 o -3 23 1 708.03 676.19 62.19 o -1 23 1 368.67 306.09 46.99 o 1 23 1 246.01 242.29 36.53 o 3 23 1 64.70 26.15 13.17 o -2 24 1 26.41 45.49 14.49 o 0 24 1 312.66 278.10 30.98 o 2 24 1 0.61 60.80 22.85 o -1 25 1 810.72 576.67 142.81 o 1 25 1 0.88 31.90 11.80 o -10 0 2 1020.52 1349.96 72.51 o -8 0 2 922.67 850.54 72.20 o -6 0 2 7964.34 8270.48 188.46 o -4 0 2 10549.76 10744.88 90.83 o -2 0 2 79.66 150.72 27.83 o 0 0 2 1109.58 866.84 101.36 o 2 0 2 553198.00 516724.75 11709.10 o 4 0 2 14729.37 15147.51 329.90 o 6 0 2 12575.29 13297.55 275.26 o -9 1 2 41.31 33.87 15.37 o -7 1 2 2589.09 2669.38 71.55 o -5 1 2 398.13 471.15 52.25 o -3 1 2 7659.68 7652.32 89.08 o -1 1 2 10083.27 10106.98 36.67 o 1 1 2 15457.09 15355.28 126.51 o 3 1 2 33922.00 31987.43 231.12 o 5 1 2 125.20 145.99 12.91 o 7 1 2 276.33 300.24 37.76 o 9 1 2 396.37 497.72 36.35 o -10 2 2 3.57 36.53 14.39 o -8 2 2 773.63 706.60 31.75 o -6 2 2 770.93 820.44 40.29 o -4 2 2 2464.36 2234.75 53.62 o -2 2 2 537.29 534.89 14.80 o 0 2 2 57900.36 59450.11 471.80 o 2 2 2 782.67 759.53 18.40 o 4 2 2 47755.84 49100.55 279.49 o 6 2 2 1118.40 1093.97 83.72 o 8 2 2 109.31 139.27 38.05 o -9 3 2 641.98 446.64 73.16 o -7 3 2 5284.08 5601.69 131.87 o -5 3 2 2112.03 1769.13 42.88 o -3 3 2 1797.78 1678.37 44.35 o -1 3 2 89.84 91.01 5.65 o 1 3 2 2603.33 2429.23 54.77 o 3 3 2 22414.88 20763.88 414.80 o 5 3 2 5117.04 5206.77 74.78 o 7 3 2 101.08 100.67 12.33 o 9 3 2 399.42 547.40 58.67 o -10 4 2 36.52 26.27 19.65 o -8 4 2 3517.67 3988.14 147.23 o -6 4 2 9279.79 9474.61 284.25 o -4 4 2 6628.25 6581.00 84.68 o -2 4 2 18988.52 19446.77 231.44 o 0 4 2 156.31 167.62 8.86 o 2 4 2 5454.78 4872.72 65.19 o 4 4 2 8563.14 8067.02 195.68 o 6 4 2 145.74 163.52 15.18 o 8 4 2 2101.36 1998.64 105.30 o -9 5 2 76.38 81.15 24.08 o -7 5 2 4751.16 4724.10 203.50 o -5 5 2 3816.55 3881.79 53.78 o -3 5 2 1484.16 1720.38 59.98 o -1 5 2 348.18 274.89 11.24 o 1 5 2 495.37 406.18 14.72 o 3 5 2 17656.26 17034.01 441.71 o 5 5 2 1127.61 1242.20 50.52 o 7 5 2 87.13 89.93 18.77 o 9 5 2 862.87 795.60 83.30 o -10 6 2 0.27 20.00 14.94 o -8 6 2 2.31 35.67 15.51 o -6 6 2 686.79 650.98 73.26 o -4 6 2 27651.31 27848.24 675.26 o -2 6 2 35.39 64.44 20.14 o 0 6 2 7351.70 7090.77 58.25 o 2 6 2 215.47 220.00 10.48 o 4 6 2 4954.61 4907.17 180.38 o 6 6 2 592.35 616.61 54.01 o 8 6 2 286.99 269.61 44.73 o -9 7 2 134.54 74.41 24.63 o -7 7 2 1137.75 1254.17 45.39 o -5 7 2 2400.05 2256.07 55.41 o -3 7 2 1276.31 1307.44 88.56 o -1 7 2 2734.42 2337.15 44.04 o 1 7 2 19208.29 18650.41 78.15 o 3 7 2 16390.78 16653.90 312.85 o 5 7 2 78.73 90.62 20.21 o 7 7 2 30.96 51.82 11.14 o 9 7 2 39.68 53.69 31.00 o -8 8 2 550.08 577.36 47.08 o -6 8 2 1602.94 1494.21 63.35 o -4 8 2 6733.02 6781.77 105.00 o -2 8 2 16966.60 15647.35 185.38 o 0 8 2 534.24 496.54 26.03 o 2 8 2 120760.75 120093.54 2844.85 o 4 8 2 8508.56 8006.85 365.10 o 6 8 2 2106.99 2044.29 52.65 o 8 8 2 83.97 84.78 18.89 o -9 9 2 3.67 58.11 21.14 o -7 9 2 1488.85 1667.30 56.93 o -5 9 2 468.96 359.05 24.02 o -3 9 2 8724.91 8648.69 71.18 o -1 9 2 15802.80 15381.63 228.65 o 1 9 2 5368.07 5170.86 83.32 o 3 9 2 16837.53 16244.04 392.36 o 5 9 2 358.42 364.02 42.56 o 7 9 2 109.51 119.37 18.73 o 9 9 2 517.70 447.02 64.48 o -8 10 2 801.28 846.58 182.65 o -6 10 2 424.79 458.92 36.48 o -4 10 2 135.72 126.37 40.48 o -2 10 2 371.20 400.35 26.83 o 0 10 2 21549.38 23212.91 308.36 o 2 10 2 440.46 474.69 20.68 o 4 10 2 19066.29 18704.48 406.56 o 6 10 2 681.63 794.76 78.55 o 8 10 2 85.21 71.87 20.96 o -9 11 2 812.17 569.76 73.38 o -7 11 2 1430.62 1522.01 97.21 o -5 11 2 140.14 146.92 16.61 o -3 11 2 2057.96 1877.33 57.28 o -1 11 2 243.06 197.33 12.09 o 1 11 2 2081.31 2115.35 27.41 o 3 11 2 8948.65 8532.10 332.42 o 5 11 2 5361.98 5578.86 142.56 o 7 11 2 166.12 122.16 42.44 o 9 11 2 39.25 19.93 17.71 o -8 12 2 1562.96 1726.67 72.04 o -6 12 2 1781.00 1847.28 68.67 o -4 12 2 2518.88 2713.65 109.56 o -2 12 2 80.73 53.44 14.51 o 0 12 2 106.07 118.13 14.97 o 2 12 2 2912.29 3038.31 52.55 o 4 12 2 3082.46 3281.93 55.84 o 6 12 2 22.00 45.24 13.66 o 8 12 2 956.25 867.36 132.36 o -7 13 2 1253.41 1455.46 79.49 o -5 13 2 2067.37 2240.35 134.07 o -3 13 2 2055.14 2058.14 42.86 o -1 13 2 770.37 727.87 26.20 o 1 13 2 414.89 378.33 20.79 o 3 13 2 2568.53 2618.66 58.72 o 5 13 2 4.57 46.86 13.22 o 7 13 2 214.90 197.62 36.63 o -8 14 2 81.49 94.03 25.15 o -6 14 2 248.13 209.15 33.74 o -4 14 2 17394.23 18671.32 362.00 o -2 14 2 10.14 19.86 8.36 o 0 14 2 16191.50 17450.85 273.99 o 2 14 2 0.59 48.78 18.15 o 4 14 2 667.81 621.70 30.65 o 6 14 2 127.57 137.09 23.04 o 8 14 2 708.56 556.44 81.13 o -7 15 2 69.04 53.78 16.46 o -5 15 2 1466.79 1361.71 53.33 o -3 15 2 207.34 221.04 28.52 o -1 15 2 466.46 419.70 20.47 o 1 15 2 4663.99 4563.12 74.18 o 3 15 2 1543.25 1517.44 43.98 o 5 15 2 98.92 118.24 22.52 o 7 15 2 113.91 83.51 23.80 o -8 16 2 140.50 108.25 35.77 o -6 16 2 121.32 57.19 34.66 o -4 16 2 1890.13 1783.52 75.97 o -2 16 2 21897.46 23265.47 403.10 o 0 16 2 133.28 139.65 19.84 o 2 16 2 2862.69 3331.78 84.16 o 4 16 2 2104.64 2256.42 76.29 o 6 16 2 355.32 294.90 33.16 o -7 17 2 175.19 140.67 47.60 o -5 17 2 669.43 713.16 34.99 o -3 17 2 4571.20 4976.54 128.90 o -1 17 2 6491.02 6706.93 99.55 o 1 17 2 720.37 724.78 35.07 o 3 17 2 3296.66 3438.11 100.17 o 5 17 2 34.28 36.19 11.01 o 7 17 2 5.82 22.37 14.10 o -6 18 2 123.28 79.86 44.00 o -4 18 2 13.85 55.08 38.19 o -2 18 2 101.11 93.79 25.78 o 0 18 2 1120.31 1267.72 49.54 o 2 18 2 168.99 157.52 38.17 o 4 18 2 1049.78 1068.02 118.72 o 6 18 2 149.68 81.17 24.42 o -5 19 2 18.42 20.64 21.36 o -3 19 2 1262.41 1212.61 49.69 o -1 19 2 5.47 23.70 22.75 o 1 19 2 716.96 689.20 59.04 o 3 19 2 1414.86 1416.83 56.64 o 5 19 2 1777.39 1779.99 109.05 o -6 20 2 11.25 37.47 12.48 o -4 20 2 468.72 473.35 37.93 o -2 20 2 1158.63 1281.32 81.35 o 0 20 2 19.13 39.42 17.41 o 2 20 2 71.72 73.76 15.12 o 4 20 2 555.82 505.66 58.81 o 6 20 2 36.65 44.89 15.23 o -5 21 2 271.80 243.41 70.67 o -3 21 2 740.64 768.63 109.05 o -1 21 2 601.45 733.75 64.87 o 1 21 2 317.71 315.84 33.51 o 3 21 2 10.91 31.09 15.15 o 5 21 2 53.85 15.11 9.38 o -4 22 2 1543.15 1371.55 144.28 o -2 22 2 7.65 55.49 14.43 o 0 22 2 1461.61 1374.19 96.33 o 2 22 2 13.93 37.73 17.18 o 4 22 2 118.45 88.05 31.96 o -3 23 2 106.22 157.51 32.05 o -1 23 2 81.34 47.80 13.96 o 1 23 2 174.11 109.80 27.83 o 3 23 2 1.73 21.17 11.13 o -2 24 2 4307.36 4979.76 80.52 o 0 24 2 11.31 40.66 24.96 o 2 24 2 10.31 57.65 18.40 o -1 25 2 1007.19 851.24 117.40 o -9 1 3 31.72 38.18 12.04 o -7 1 3 69.88 71.76 17.98 o -5 1 3 14161.39 15563.50 204.28 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1021.15 134.50 o -3 9 7 11954.03 12756.66 339.63 o -1 9 7 601.56 559.64 29.86 o 1 9 7 8515.34 8304.83 229.67 o 3 9 7 6473.96 7002.89 154.03 o 5 9 7 5.21 41.30 13.84 o 7 9 7 17.09 23.92 10.37 o -8 10 7 102.83 152.14 38.46 o -6 10 7 1427.08 1438.81 63.73 o -4 10 7 8487.62 9046.44 375.15 o -2 10 7 16336.67 17437.07 526.25 o 0 10 7 6367.01 6916.54 150.15 o 2 10 7 5735.72 5702.68 176.45 o 4 10 7 1054.89 1253.22 52.65 o 6 10 7 549.67 577.63 78.77 o 8 10 7 313.89 196.06 47.79 o -9 11 7 831.02 906.57 171.48 o -7 11 7 13.27 54.15 28.23 o -5 11 7 733.05 800.60 52.67 o -3 11 7 8410.23 8473.15 266.97 o -1 11 7 68.47 102.67 30.72 o 1 11 7 2473.66 2375.32 94.80 o 3 11 7 8.56 32.31 13.90 o 5 11 7 17.33 31.82 15.26 o 7 11 7 435.96 545.92 74.84 o -8 12 7 360.97 357.35 40.74 o -6 12 7 441.35 501.39 67.80 o -4 12 7 2580.11 2396.52 79.08 o -2 12 7 996.24 1050.31 49.42 o 0 12 7 1933.46 1877.96 34.99 o 2 12 7 910.20 974.78 56.03 o 4 12 7 40.36 30.56 28.52 o 6 12 7 20.35 35.40 34.05 o -7 13 7 1006.10 1167.61 88.05 o -5 13 7 1403.03 1409.08 64.06 o -3 13 7 38.67 36.68 23.97 o -1 13 7 207.66 158.87 22.53 o 1 13 7 135.42 97.07 11.81 o 3 13 7 1115.43 1155.05 32.75 o 5 13 7 16.78 20.92 14.97 o 7 13 7 89.72 56.68 14.76 o -8 14 7 1106.82 1111.70 49.87 o -6 14 7 6.61 55.54 20.57 o -4 14 7 473.12 537.07 62.41 o -2 14 7 476.39 552.34 33.80 o 0 14 7 370.17 364.95 38.96 o 2 14 7 1924.16 1958.85 38.29 o 4 14 7 821.28 779.04 37.31 o 6 14 7 291.32 299.52 40.06 o -7 15 7 11.68 70.68 65.04 o -5 15 7 2931.86 3512.55 179.93 o -3 15 7 1657.66 1769.01 125.88 o -1 15 7 301.26 321.98 39.23 o 1 15 7 2042.87 1997.10 94.33 o 3 15 7 1221.58 1239.92 98.00 o 5 15 7 202.65 166.91 36.73 o -6 16 7 1362.46 1445.71 122.32 o -4 16 7 35.13 46.79 22.22 o -2 16 7 636.74 587.41 47.09 o 0 16 7 232.19 218.44 35.15 o 2 16 7 24.28 31.34 9.78 o 4 16 7 363.94 403.79 37.55 o 6 16 7 223.14 212.64 32.79 o -7 17 7 0.51 36.72 20.56 o -5 17 7 378.70 376.16 108.21 o -3 17 7 2695.51 2897.54 173.25 o -1 17 7 0.68 55.25 14.40 o 1 17 7 2014.09 2011.06 39.04 o 3 17 7 1169.45 1197.00 47.96 o 5 17 7 63.94 44.85 18.96 o -6 18 7 54.56 49.72 50.09 o -4 18 7 2863.80 3249.69 144.05 o -2 18 7 2242.39 2338.67 78.93 o 0 18 7 1753.91 1618.60 63.91 o 2 18 7 2977.91 3053.62 86.12 o 4 18 7 122.57 76.53 26.14 o -5 19 7 26.21 29.49 38.13 o -3 19 7 1695.61 1801.81 88.15 o -1 19 7 250.13 246.43 58.59 o 1 19 7 1132.20 1208.43 67.65 o 3 19 7 17.86 24.63 18.12 o 5 19 7 54.70 28.37 20.38 o -4 20 7 393.83 440.89 80.29 o -2 20 7 1079.02 1140.61 62.46 o 0 20 7 281.05 229.43 43.20 o 2 20 7 639.20 632.80 41.54 o 4 20 7 92.03 39.05 25.37 o -5 21 7 422.58 242.98 76.38 o -3 21 7 38.96 73.17 25.25 o -1 21 7 1.67 20.34 11.72 o 1 21 7 200.88 200.03 73.80 o 3 21 7 514.31 424.38 39.56 o -4 22 7 408.74 262.35 94.03 o -2 22 7 7.27 34.23 28.07 o 0 22 7 273.50 251.07 51.69 o 2 22 7 145.79 171.50 65.99 o -1 23 7 15.13 49.94 26.76 o 1 23 7 60.21 17.15 10.94 o -10 0 8 106.34 220.84 74.72 o -8 0 8 5.12 36.90 23.25 o -6 0 8 2266.44 2174.62 74.31 o -4 0 8 768.84 786.39 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