# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' yu3 in monoclinic' _shelx_refln_list_code 4 _shelx_F_calc_maximum 315.77 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.8405 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 34.6610 _cell_length_b 6.5155 _cell_length_c 10.6632 _cell_angle_alpha 90.000 _cell_angle_beta 93.633 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 25815.22 26747.07 578.60 o 6 0 0 52.26 13.83 7.91 o 8 0 0 5699.87 6206.02 67.84 o 10 0 0 17915.03 18212.52 169.79 o 12 0 0 42850.22 41701.46 596.13 o 14 0 0 213.85 246.70 14.00 o 16 0 0 8696.57 8674.49 118.13 o 18 0 0 111.34 114.49 13.61 o 20 0 0 13516.52 13597.87 183.10 o 22 0 0 78.71 93.14 21.17 o 24 0 0 1622.72 1847.00 95.86 o 26 0 0 693.45 748.73 70.88 o 28 0 0 10146.28 9517.60 258.28 o 30 0 0 3435.51 3606.10 150.58 o 32 0 0 4.84 20.18 21.82 o 34 0 0 1294.28 1065.86 86.23 o 36 0 0 0.19 19.11 22.90 o 38 0 0 571.94 615.54 83.13 o 40 0 0 130.99 127.99 45.05 o 1 1 0 4023.39 3805.01 39.95 o 3 1 0 14601.64 14070.73 176.20 o 5 1 0 2236.28 2202.38 27.31 o 7 1 0 15.57 1.82 3.66 o 9 1 0 2348.96 2522.29 39.78 o 11 1 0 5562.03 5916.78 62.90 o 13 1 0 83.75 79.67 7.74 o 15 1 0 41.46 42.08 6.76 o 17 1 0 477.30 583.34 24.40 o 19 1 0 0.85 16.85 5.62 o 21 1 0 23.42 27.91 7.30 o 23 1 0 2265.79 2251.53 73.96 o 25 1 0 23.59 37.69 11.02 o 27 1 0 34.37 42.64 16.04 o 29 1 0 549.03 475.74 58.46 o 31 1 0 322.95 331.36 39.71 o 33 1 0 248.11 213.32 33.78 o 35 1 0 4.00 9.88 15.89 o 37 1 0 58.69 36.19 19.81 o 39 1 0 10.47 37.71 22.71 o 0 2 0 66608.91 61751.17 1632.12 o 2 2 0 8563.78 8339.89 75.73 o 4 2 0 18069.21 17453.66 143.93 o 6 2 0 1599.04 1644.28 29.71 o 8 2 0 37351.34 36047.23 275.85 o 10 2 0 10793.22 10944.29 103.56 o 12 2 0 927.24 773.54 21.42 o 14 2 0 4925.09 5351.07 66.57 o 16 2 0 2913.51 2726.13 45.61 o 18 2 0 370.49 426.58 19.21 o 20 2 0 16596.46 17275.02 228.90 o 22 2 0 53.49 27.13 10.85 o 24 2 0 417.08 326.78 35.80 o 26 2 0 960.59 910.81 175.08 o 28 2 0 7459.81 7428.85 164.38 o 30 2 0 2080.20 2081.98 106.88 o 32 2 0 888.42 923.63 61.29 o 34 2 0 64.75 38.69 18.81 o 36 2 0 117.22 119.52 31.30 o 38 2 0 265.37 214.46 38.19 o 1 3 0 20.81 16.27 5.92 o 3 3 0 635.00 626.17 19.80 o 5 3 0 5514.82 5814.46 60.56 o 7 3 0 1472.72 1494.98 28.79 o 9 3 0 52.23 75.78 8.54 o 11 3 0 1808.86 1790.45 49.04 o 13 3 0 1017.07 1170.44 29.35 o 15 3 0 545.62 569.60 22.58 o 17 3 0 1723.23 1843.40 64.55 o 19 3 0 670.95 714.62 30.36 o 21 3 0 59.12 77.08 20.25 o 23 3 0 1233.10 1339.52 47.54 o 25 3 0 15.73 10.41 12.51 o 27 3 0 150.08 146.28 28.59 o 29 3 0 8.39 -11.71 37.06 o 31 3 0 433.49 448.60 50.49 o 33 3 0 182.49 133.82 29.98 o 35 3 0 38.90 30.20 17.80 o 37 3 0 6.87 13.34 20.06 o 0 4 0 6557.75 6192.40 124.86 o 2 4 0 70.08 43.67 8.40 o 4 4 0 962.19 796.95 29.12 o 6 4 0 1042.35 1093.63 34.42 o 8 4 0 7664.79 7808.96 151.79 o 10 4 0 2598.85 2656.36 75.44 o 12 4 0 1373.46 1359.60 45.70 o 14 4 0 596.97 637.63 32.91 o 16 4 0 317.73 371.27 28.69 o 18 4 0 275.53 314.89 28.71 o 20 4 0 1514.55 1500.24 67.60 o 22 4 0 486.13 555.02 50.38 o 24 4 0 132.89 51.94 20.02 o 26 4 0 32.56 21.60 16.96 o 28 4 0 270.45 279.80 56.71 o 30 4 0 584.91 611.76 59.97 o 32 4 0 61.60 61.84 23.47 o 34 4 0 56.46 70.89 28.37 o 1 5 0 56.76 79.52 15.08 o 3 5 0 112.75 129.15 15.93 o 5 5 0 223.14 261.08 40.90 o 7 5 0 35.52 36.64 11.78 o 9 5 0 1343.54 1315.90 49.72 o 11 5 0 2724.06 2511.04 69.79 o 13 5 0 538.71 465.67 51.26 o 15 5 0 980.20 994.84 70.22 o 17 5 0 95.44 117.55 19.25 o 19 5 0 7.90 13.10 32.08 o 21 5 0 1.56 -1.61 12.03 o 23 5 0 208.19 164.13 31.38 o 25 5 0 12.77 49.90 20.87 o 27 5 0 154.30 194.66 36.81 o 29 5 0 1.03 -9.44 18.05 o 31 5 0 400.78 334.42 108.53 o 0 6 0 8.32 -0.74 11.29 o 2 6 0 766.80 725.20 42.44 o 4 6 0 30.74 15.47 11.26 o 6 6 0 52.88 37.64 17.32 o 8 6 0 76.96 50.30 20.11 o 10 6 0 148.46 138.96 28.08 o 12 6 0 593.80 694.84 72.59 o 14 6 0 90.06 87.94 20.04 o 16 6 0 153.10 101.63 41.68 o 18 6 0 200.06 244.79 40.08 o 20 6 0 54.73 40.05 42.62 o 22 6 0 8.79 11.78 17.44 o 24 6 0 67.43 59.31 69.80 o 26 6 0 50.09 43.84 23.76 o 1 7 0 3.23 11.25 11.99 o 3 7 0 156.69 170.50 23.95 o 5 7 0 9.36 8.68 12.35 o 7 7 0 33.44 76.62 49.74 o 9 7 0 0.15 7.60 15.87 o 11 7 0 52.27 2.34 16.31 o 13 7 0 10.77 -0.94 19.29 o 15 7 0 65.36 100.29 28.87 o 17 7 0 12.17 14.38 20.33 o -39 1 1 546.73 553.39 57.32 o -37 1 1 85.45 96.01 26.70 o -35 1 1 1.02 9.85 15.12 o -33 1 1 185.08 244.32 34.99 o -31 1 1 3415.77 3116.94 101.05 o -29 1 1 1.83 -4.25 10.11 o -27 1 1 326.72 358.82 32.75 o -25 1 1 462.63 525.36 29.56 o -23 1 1 1034.49 968.21 28.54 o -21 1 1 1364.50 1528.62 43.10 o -19 1 1 589.36 652.77 21.81 o -17 1 1 1191.67 1314.19 35.03 o -15 1 1 6026.85 5960.06 83.09 o -13 1 1 7067.42 7387.74 92.01 o -11 1 1 1718.50 1905.73 37.20 o -9 1 1 3243.96 3200.25 48.64 o -7 1 1 38151.05 37586.64 365.46 o -5 1 1 1503.21 1450.86 33.27 o -3 1 1 4019.24 3569.31 45.77 o -1 1 1 31226.95 30040.75 330.37 o 1 1 1 4938.68 4671.69 46.61 o 3 1 1 2800.37 2636.12 31.58 o 5 1 1 59398.04 59397.26 739.68 o 7 1 1 4386.74 4476.66 44.63 o 9 1 1 10662.92 10554.03 98.29 o 11 1 1 1145.17 1087.45 25.15 o 13 1 1 46837.28 48033.65 365.53 o 15 1 1 7425.34 7383.74 87.01 o 17 1 1 2778.36 2752.52 51.12 o 19 1 1 1466.25 1245.01 34.67 o 21 1 1 2963.59 2742.54 55.06 o 23 1 1 8788.44 8779.52 148.78 o 25 1 1 1007.83 935.53 40.09 o 27 1 1 372.15 394.11 32.42 o 29 1 1 677.07 705.91 42.69 o 31 1 1 354.00 313.95 39.27 o 33 1 1 6301.67 5948.94 190.06 o 35 1 1 1611.46 1516.84 76.09 o 37 1 1 452.47 624.54 60.28 o 39 1 1 477.88 502.48 55.26 o -38 2 1 2.39 41.68 26.02 o -36 2 1 478.66 513.20 54.05 o -34 2 1 495.73 543.45 55.17 o -32 2 1 727.98 860.64 63.11 o -30 2 1 2212.25 2214.63 85.72 o -28 2 1 2252.94 2197.13 83.05 o -26 2 1 126.53 141.19 48.18 o -24 2 1 45.05 50.38 17.20 o -22 2 1 556.62 591.04 30.05 o -20 2 1 2194.58 2046.00 50.41 o -18 2 1 2119.74 2235.17 51.18 o -16 2 1 7147.36 7168.05 100.68 o -14 2 1 2988.49 3319.87 60.65 o -12 2 1 1362.60 1191.82 45.75 o -10 2 1 155.75 153.13 16.87 o -8 2 1 1023.88 991.27 28.62 o -6 2 1 620.66 615.63 21.98 o -4 2 1 4750.58 4526.97 56.46 o -2 2 1 5046.18 5234.60 70.29 o 0 2 1 10578.06 10329.93 142.01 o 2 2 1 746.16 683.88 22.72 o 4 2 1 8.40 19.09 5.67 o 6 2 1 4494.35 4772.31 50.38 o 8 2 1 6307.99 6153.93 61.02 o 10 2 1 1892.87 2064.18 40.95 o 12 2 1 6432.11 6824.13 75.58 o 14 2 1 4402.23 4654.60 59.90 o 16 2 1 350.46 406.13 17.27 o 18 2 1 260.79 368.92 24.23 o 20 2 1 837.10 818.55 34.30 o 22 2 1 0.03 2.76 8.32 o 24 2 1 1305.98 1287.94 49.44 o 26 2 1 280.19 312.33 29.21 o 28 2 1 451.90 467.55 36.00 o 30 2 1 406.32 394.06 34.62 o 32 2 1 213.13 241.52 36.46 o 34 2 1 240.25 211.66 35.93 o 36 2 1 4.11 17.20 20.59 o 38 2 1 76.36 30.87 18.19 o -37 3 1 22.94 29.05 20.10 o -35 3 1 0.05 -2.65 27.01 o -33 3 1 26.52 32.82 21.95 o -31 3 1 1035.85 1144.46 109.25 o -29 3 1 376.37 303.34 40.79 o -27 3 1 897.44 931.72 56.17 o -25 3 1 342.84 243.89 33.46 o -23 3 1 122.66 88.51 21.61 o -21 3 1 159.35 161.38 21.65 o -19 3 1 1.87 3.58 8.15 o -17 3 1 1034.85 1143.95 39.70 o -15 3 1 6377.83 6423.02 169.65 o -13 3 1 177.39 137.28 16.54 o -11 3 1 4292.95 4692.34 80.71 o -9 3 1 45.47 66.19 20.31 o -7 3 1 1.16 8.39 6.77 o -5 3 1 302.10 294.42 18.84 o -3 3 1 625.45 563.76 21.37 o -1 3 1 0.02 3.77 4.82 o 1 3 1 1234.76 1206.26 35.84 o 3 3 1 320.93 318.71 18.25 o 5 3 1 15424.89 15845.97 179.06 o 7 3 1 971.32 1146.84 25.02 o 9 3 1 5041.39 5214.75 61.01 o 11 3 1 582.54 687.89 22.47 o 13 3 1 16972.05 16770.13 157.13 o 15 3 1 8670.06 8815.73 100.47 o 17 3 1 24.37 14.52 7.76 o 19 3 1 1323.37 1358.41 60.84 o 21 3 1 1520.51 1575.30 50.53 o 23 3 1 316.83 315.80 28.39 o 25 3 1 2994.38 3045.09 78.93 o 27 3 1 0.81 2.89 11.39 o 29 3 1 308.35 394.26 48.23 o 31 3 1 54.68 36.53 19.16 o 33 3 1 562.50 598.69 58.46 o 35 3 1 113.51 165.17 33.69 o 37 3 1 70.15 55.99 24.14 o -34 4 1 253.21 242.88 42.83 o -32 4 1 479.78 510.48 122.67 o -30 4 1 144.89 119.91 28.78 o -28 4 1 1484.45 1536.66 77.61 o -26 4 1 15.48 -3.64 14.24 o -24 4 1 2874.34 2983.00 102.06 o -22 4 1 11.13 4.63 14.25 o -20 4 1 8555.79 8852.04 139.16 o -18 4 1 649.90 673.21 51.11 o -16 4 1 1907.32 1880.84 56.14 o -14 4 1 434.33 378.88 29.56 o -12 4 1 1342.64 1328.69 45.74 o -10 4 1 114.95 109.13 17.79 o -8 4 1 16410.31 16137.71 196.66 o -6 4 1 1418.35 1465.29 40.33 o -4 4 1 7856.53 7534.25 100.22 o -2 4 1 1163.77 1150.61 35.27 o 0 4 1 8295.99 8155.40 121.82 o 2 4 1 3687.01 3688.52 65.08 o 4 4 1 1544.89 1280.94 37.37 o 6 4 1 666.79 583.45 37.97 o 8 4 1 1717.17 1524.91 52.77 o 10 4 1 21.17 30.29 11.56 o 12 4 1 3397.74 3354.79 73.04 o 14 4 1 1183.98 1207.70 42.66 o 16 4 1 304.46 314.92 26.14 o 18 4 1 1240.22 1193.34 63.94 o 20 4 1 727.22 796.19 86.16 o 22 4 1 722.29 760.02 57.78 o 24 4 1 2.43 49.41 19.10 o 26 4 1 3.80 18.63 23.64 o 28 4 1 260.90 295.20 42.04 o 30 4 1 2.82 4.24 15.30 o 32 4 1 153.79 208.01 38.84 o 34 4 1 84.54 51.27 25.63 o -31 5 1 116.45 144.63 32.70 o -29 5 1 34.61 27.18 21.01 o -27 5 1 13.33 -5.76 15.99 o -25 5 1 365.75 319.23 44.93 o -23 5 1 49.22 36.06 19.76 o -21 5 1 147.00 99.45 58.40 o -19 5 1 5.78 -3.94 10.52 o -17 5 1 179.85 203.38 25.24 o -15 5 1 1636.91 1566.41 77.77 o -13 5 1 91.80 90.60 18.14 o -11 5 1 148.77 169.79 22.31 o -9 5 1 1788.75 1644.67 55.74 o -7 5 1 104.01 117.55 18.83 o -5 5 1 384.82 383.49 27.77 o -3 5 1 12.79 -1.98 7.20 o -1 5 1 316.39 331.51 48.03 o 1 5 1 964.16 1007.01 36.67 o 3 5 1 3076.99 2834.90 63.13 o 5 5 1 626.01 574.41 32.91 o 7 5 1 725.11 775.53 98.48 o 9 5 1 123.97 112.44 23.08 o 11 5 1 9.43 -5.34 15.32 o 13 5 1 984.86 942.12 54.58 o 15 5 1 213.56 239.80 34.07 o 17 5 1 9.48 9.80 12.69 o 19 5 1 55.07 25.01 14.95 o 21 5 1 29.32 8.54 15.35 o 23 5 1 211.65 179.93 50.20 o 25 5 1 56.57 15.73 26.77 o 27 5 1 14.23 13.84 17.78 o 29 5 1 43.39 63.85 25.08 o 31 5 1 29.26 13.55 21.27 o -26 6 1 389.49 543.33 62.79 o -24 6 1 1025.22 1223.11 260.92 o -22 6 1 238.78 303.92 66.56 o -20 6 1 2089.50 2204.46 97.62 o -18 6 1 159.96 195.49 38.01 o -16 6 1 855.69 957.82 52.76 o -14 6 1 340.38 365.21 49.33 o -12 6 1 325.40 395.12 37.08 o -10 6 1 199.15 261.99 37.48 o -8 6 1 2547.26 2576.99 78.36 o -6 6 1 17.60 28.44 12.87 o -4 6 1 2295.07 2399.98 64.23 o -2 6 1 113.02 118.88 20.46 o 0 6 1 2706.32 2722.32 60.80 o 2 6 1 484.41 468.38 33.07 o 4 6 1 537.67 530.72 42.52 o 6 6 1 87.40 21.19 15.18 o 8 6 1 1003.84 1067.75 62.21 o 10 6 1 127.22 98.84 33.65 o 12 6 1 1590.55 1716.04 112.97 o 14 6 1 143.58 90.36 24.25 o 16 6 1 360.10 466.14 51.75 o 18 6 1 118.38 64.90 23.34 o 20 6 1 1034.19 1210.05 72.71 o 22 6 1 222.77 218.08 58.40 o 24 6 1 135.71 150.86 34.06 o -17 7 1 73.66 57.45 24.95 o -15 7 1 9.25 13.43 21.00 o -13 7 1 153.68 216.01 31.27 o -11 7 1 8.82 27.90 16.13 o -9 7 1 171.00 187.84 47.67 o -7 7 1 0.04 14.65 18.78 o -5 7 1 63.20 43.86 18.45 o -3 7 1 16.14 33.71 16.35 o -1 7 1 515.49 458.29 40.55 o 1 7 1 14.52 24.33 13.32 o 3 7 1 609.84 568.99 40.50 o 5 7 1 50.50 41.58 20.71 o 7 7 1 0.29 6.11 14.48 o 9 7 1 0.29 13.78 18.36 o 11 7 1 86.41 88.83 26.91 o 13 7 1 13.65 -4.08 16.43 o 15 7 1 191.18 181.46 35.93 o 17 7 1 49.11 47.73 49.87 o -40 0 2 234.32 228.33 55.52 o -38 0 2 51.13 48.10 31.54 o -36 0 2 31.27 68.52 31.30 o -34 0 2 232.47 191.68 45.80 o -32 0 2 507.84 313.25 54.30 o -30 0 2 53.09 27.76 21.50 o -28 0 2 1111.52 1146.34 78.24 o -26 0 2 5483.00 5725.77 117.70 o -24 0 2 2284.13 2164.20 65.16 o -22 0 2 2964.32 3095.01 184.48 o -20 0 2 1848.85 1691.86 52.85 o -18 0 2 22042.74 23294.23 446.04 o -16 0 2 4832.12 5077.57 135.83 o -14 0 2 2799.65 2939.04 63.35 o -12 0 2 13209.63 13849.59 177.70 o -10 0 2 960.32 1059.91 32.11 o -8 0 2 82123.76 84517.48 863.99 o -6 0 2 99710.47 103325.72 1045.13 o -4 0 2 36.04 78.99 13.34 o -2 0 2 2209.83 2154.53 59.70 o 0 0 2 31987.67 32830.70 495.42 o 2 0 2 21344.55 23110.14 354.63 o 4 0 2 21973.83 21642.01 190.52 o 6 0 2 11359.81 11481.74 134.84 o 8 0 2 1220.73 1289.16 39.97 o 10 0 2 1086.72 1083.65 65.74 o 12 0 2 9131.86 9235.70 282.97 o 14 0 2 3649.93 3597.22 150.10 o 16 0 2 452.58 430.92 28.08 o 18 0 2 490.70 494.55 34.27 o 20 0 2 116.69 154.49 42.09 o 22 0 2 193.77 190.29 26.63 o 24 0 2 50.93 48.02 17.04 o 26 0 2 3411.51 3583.07 101.12 o 28 0 2 2449.30 2336.36 83.19 o 30 0 2 69.90 73.92 21.19 o 32 0 2 1433.69 1482.12 80.68 o 34 0 2 129.48 103.86 35.33 o 36 0 2 6.77 49.00 25.94 o 38 0 2 192.56 171.24 49.26 o 40 0 2 55.43 47.27 31.38 o -39 1 2 163.81 107.07 48.64 o -37 1 2 458.54 390.63 78.22 o -35 1 2 52.37 42.79 19.07 o -33 1 2 104.35 95.26 26.23 o -31 1 2 889.26 825.65 59.92 o -29 1 2 236.83 200.82 22.63 o -27 1 2 283.01 272.19 25.09 o -25 1 2 538.73 557.99 25.27 o -23 1 2 1057.95 1054.95 31.47 o -21 1 2 207.84 280.87 18.47 o -19 1 2 114.09 135.90 13.13 o -17 1 2 3158.68 3342.76 52.89 o -15 1 2 754.60 714.15 22.15 o -13 1 2 1673.24 1703.64 33.38 o -11 1 2 1152.93 1189.84 30.07 o -9 1 2 1929.67 1975.77 37.39 o -7 1 2 3434.07 3396.20 49.42 o -5 1 2 27835.83 27062.86 242.63 o -3 1 2 4473.95 4715.78 106.29 o -1 1 2 1479.58 1425.71 25.58 o 1 1 2 3728.59 3785.99 36.06 o 3 1 2 2024.68 2000.77 28.17 o 5 1 2 25513.44 25319.15 175.00 o 7 1 2 1078.03 1108.05 20.22 o 9 1 2 1317.03 1238.59 22.82 o 11 1 2 396.24 432.84 14.10 o 13 1 2 175.30 172.85 12.26 o 15 1 2 13.42 2.42 4.69 o 17 1 2 3716.41 3702.25 69.64 o 19 1 2 1.57 3.01 5.94 o 21 1 2 1026.44 1112.61 35.11 o 23 1 2 62.37 59.00 13.98 o 25 1 2 78.18 54.49 12.11 o 27 1 2 193.82 214.97 21.62 o 29 1 2 33.09 40.71 12.96 o 31 1 2 37.53 27.97 13.70 o 33 1 2 5.64 11.62 11.60 o 35 1 2 441.04 429.08 58.75 o 37 1 2 67.45 30.30 18.91 o 39 1 2 89.85 49.13 45.79 o -38 2 2 402.67 484.31 54.94 o -36 2 2 444.21 509.02 54.39 o -34 2 2 1762.37 1732.21 80.52 o -32 2 2 43.04 19.45 15.69 o -30 2 2 28.36 20.42 13.84 o -28 2 2 21.42 23.33 10.50 o -26 2 2 3611.20 3794.16 83.17 o -24 2 2 1319.00 1395.89 45.50 o -22 2 2 3879.28 3940.81 94.07 o -20 2 2 7.60 5.33 6.95 o -18 2 2 4460.04 4360.67 151.26 o -16 2 2 3927.33 3719.73 68.73 o -14 2 2 2345.88 2182.40 48.95 o -12 2 2 3917.21 3882.34 78.97 o -10 2 2 27.73 21.31 12.50 o -8 2 2 1368.66 1240.64 32.79 o -6 2 2 3220.06 3199.01 54.92 o -4 2 2 4008.93 3960.18 52.36 o -2 2 2 1375.16 1282.68 34.20 o 0 2 2 596.17 614.55 18.15 o 2 2 2 11115.57 11138.68 91.78 o 4 2 2 6098.48 5941.94 76.50 o 6 2 2 477.06 475.09 14.75 o 8 2 2 3539.37 3725.93 46.12 o 10 2 2 3310.57 3563.89 46.64 o 12 2 2 14367.41 14859.22 125.94 o 14 2 2 1641.39 1746.81 33.85 o 16 2 2 974.76 1045.55 30.84 o 18 2 2 4209.67 4774.99 73.49 o 20 2 2 82.36 74.29 12.08 o 22 2 2 142.13 129.53 15.91 o 24 2 2 262.51 303.89 42.43 o 26 2 2 99.36 94.52 18.33 o 28 2 2 419.68 411.97 34.71 o 30 2 2 297.05 273.34 30.05 o 32 2 2 0.64 -10.09 10.09 o 34 2 2 30.88 26.36 14.40 o 36 2 2 562.79 587.63 47.50 o 38 2 2 198.45 121.34 31.24 o -37 3 2 0.00 2.82 16.27 o -35 3 2 175.23 167.96 34.69 o -33 3 2 145.08 144.33 30.81 o -31 3 2 26.75 50.87 19.83 o -29 3 2 1.91 6.80 13.68 o -27 3 2 476.13 533.45 49.54 o -25 3 2 19.69 -6.01 10.28 o -23 3 2 4586.16 4492.07 90.03 o -21 3 2 667.66 685.74 40.28 o -19 3 2 1293.32 1225.27 42.97 o -17 3 2 23.81 13.22 9.29 o -15 3 2 4631.58 4683.36 84.89 o -13 3 2 991.64 981.51 35.55 o -11 3 2 7055.78 6982.65 104.39 o -9 3 2 0.76 4.42 5.90 o -7 3 2 5595.64 5306.28 129.75 o -5 3 2 466.93 473.48 20.55 o -3 3 2 1185.74 1030.31 29.04 o -1 3 2 1282.68 1332.31 38.05 o 1 3 2 6411.56 6078.79 78.21 o 3 3 2 510.38 478.22 20.33 o 5 3 2 19121.66 18630.58 203.20 o 7 3 2 24.99 17.54 6.21 o 9 3 2 1026.11 777.72 24.84 o 11 3 2 3860.31 3954.37 65.88 o 13 3 2 5671.57 5138.12 73.73 o 15 3 2 3422.49 3429.15 68.88 o 17 3 2 4405.90 4595.27 84.08 o 19 3 2 1220.67 1222.42 56.63 o 21 3 2 1446.49 1519.44 50.24 o 23 3 2 1514.14 1510.14 52.35 o 25 3 2 2062.57 2235.17 66.46 o 27 3 2 28.16 4.40 13.13 o 29 3 2 498.58 604.78 43.15 o 31 3 2 81.97 87.43 19.45 o 33 3 2 984.23 1078.12 76.18 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