# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title 'Mn' _shelx_refln_list_code 4 _shelx_F_calc_maximum 206.48 _exptl_crystal_F_000 1736.00 _reflns_d_resolution_high 0.7880 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 10.5567 _cell_length_b 30.1870 _cell_length_c 11.6879 _cell_angle_alpha 90.000 _cell_angle_beta 93.734 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 986.06 800.73 41.13 o 6 0 0 6456.05 6379.20 61.04 o 8 0 0 2834.04 2974.90 72.39 o 10 0 0 26.79 93.76 51.35 o 12 0 0 120.59 128.81 32.82 o 1 1 0 531.86 625.04 72.75 o 2 1 0 15773.91 15430.44 112.86 o 3 1 0 1266.08 1228.23 41.34 o 4 1 0 324.88 276.41 29.55 o 5 1 0 1216.05 1199.98 27.86 o 6 1 0 7403.83 7325.91 46.31 o 7 1 0 4618.30 4489.67 43.32 o 8 1 0 12992.25 13396.94 125.52 o 9 1 0 6123.16 6139.30 71.27 o 10 1 0 7342.63 7700.48 107.17 o 11 1 0 2103.07 2083.70 59.60 o 12 1 0 834.64 752.20 32.82 o 13 1 0 89.51 91.78 20.56 o 0 2 0 6765.64 8606.25 96.32 o 1 2 0 25034.57 30126.06 120.66 o 2 2 0 1141.49 1098.29 52.20 o 3 2 0 8900.08 8714.88 48.46 o 4 2 0 43.37 13.26 29.94 o 5 2 0 3649.71 3639.35 30.92 o 6 2 0 69.06 105.28 22.51 o 7 2 0 1232.31 1233.17 23.40 o 8 2 0 62.02 78.26 20.80 o 9 2 0 12.44 76.36 22.23 o 10 2 0 299.35 321.23 26.51 o 11 2 0 110.87 151.90 24.44 o 12 2 0 120.45 121.02 24.00 o 13 2 0 4.99 35.66 20.47 o 1 3 0 203.09 208.79 54.75 o 2 3 0 1482.14 1469.87 46.91 o 3 3 0 1701.04 1695.89 39.10 o 4 3 0 284.99 326.78 30.28 o 5 3 0 4288.63 4285.65 52.92 o 6 3 0 499.94 568.41 24.67 o 7 3 0 1610.81 1484.04 24.25 o 8 3 0 64.73 88.47 21.75 o 9 3 0 858.36 896.35 28.39 o 10 3 0 247.08 270.37 25.16 o 11 3 0 199.66 186.06 24.31 o 12 3 0 1.85 8.46 23.62 o 13 3 0 9.19 15.17 20.83 o 0 4 0 18080.72 17683.26 98.54 o 1 4 0 3119.28 2840.30 47.96 o 2 4 0 796.66 824.80 52.70 o 3 4 0 335.54 247.19 39.39 o 4 4 0 777.37 906.16 31.76 o 5 4 0 1577.71 1698.42 29.72 o 6 4 0 1507.79 1504.01 25.89 o 7 4 0 65.90 63.56 22.44 o 8 4 0 0.03 30.81 20.97 o 9 4 0 177.98 190.95 26.78 o 10 4 0 2.03 0.62 26.06 o 11 4 0 167.05 158.61 25.39 o 12 4 0 29.17 55.33 19.38 o 13 4 0 0.73 25.95 19.47 o 1 5 0 415.33 441.75 39.82 o 2 5 0 3335.57 3536.21 48.73 o 3 5 0 351.46 379.13 34.66 o 4 5 0 37.49 56.83 27.40 o 5 5 0 1360.98 1357.21 28.72 o 6 5 0 118.46 125.76 23.76 o 7 5 0 402.57 456.57 20.96 o 8 5 0 4243.89 4294.05 52.95 o 9 5 0 532.65 573.97 32.47 o 10 5 0 2932.25 2787.72 108.82 o 11 5 0 89.49 120.34 26.33 o 12 5 0 146.33 182.97 20.68 o 13 5 0 38.75 82.56 19.38 o 2 6 0 42635.87 45950.59 181.57 o 3 6 0 9400.26 9875.37 185.85 o 4 6 0 3232.77 3513.00 73.54 o 5 6 0 1053.17 972.10 24.91 o 6 6 0 2209.48 2096.10 41.90 o 7 6 0 243.90 284.76 27.19 o 8 6 0 498.08 548.88 25.33 o 9 6 0 1.42 61.97 23.73 o 10 6 0 5.55 83.47 27.07 o 11 6 0 217.37 213.68 25.86 o 12 6 0 12.54 33.96 20.55 o 13 6 0 28.02 34.32 20.35 o 1 7 0 5196.20 5299.31 46.77 o 2 7 0 447.64 352.78 36.08 o 3 7 0 6522.30 6626.92 70.94 o 4 7 0 76.44 99.19 28.04 o 5 7 0 6121.36 5986.78 72.55 o 6 7 0 223.67 373.00 26.71 o 7 7 0 14427.33 14858.19 348.60 o 8 7 0 649.30 613.30 22.65 o 9 7 0 9368.36 9891.85 231.27 o 10 7 0 26.16 42.92 27.61 o 11 7 0 2650.79 2567.63 34.06 o 12 7 0 64.99 70.53 21.73 o 13 7 0 117.60 115.08 19.06 o 2 8 0 14794.87 15515.91 73.80 o 3 8 0 16912.73 17649.90 207.67 o 4 8 0 3438.67 3532.47 54.16 o 5 8 0 5226.08 5475.27 75.60 o 6 8 0 1553.54 1567.82 24.89 o 7 8 0 3721.18 3934.70 127.87 o 8 8 0 399.82 479.24 26.90 o 9 8 0 9.79 64.97 23.33 o 10 8 0 6.72 86.11 29.79 o 11 8 0 122.39 165.65 22.78 o 12 8 0 27.21 82.09 21.55 o 13 8 0 14.58 49.75 19.24 o 1 9 0 1301.15 1127.85 38.32 o 2 9 0 5428.85 5328.79 42.28 o 3 9 0 775.67 797.39 29.33 o 4 9 0 683.52 708.57 27.75 o 5 9 0 638.87 720.02 26.06 o 6 9 0 4190.25 4264.79 84.29 o 7 9 0 6520.41 6773.84 124.81 o 8 9 0 6445.92 7093.00 138.90 o 9 9 0 2778.32 2969.06 97.42 o 10 9 0 6165.60 6400.83 165.19 o 11 9 0 289.14 307.95 30.04 o 12 9 0 655.16 629.65 28.36 o 1 10 0 3713.88 3839.44 37.02 o 2 10 0 34289.63 33705.03 165.95 o 3 10 0 778.91 685.44 25.34 o 4 10 0 165.15 181.90 26.41 o 5 10 0 111.44 119.66 24.41 o 6 10 0 237.67 295.19 24.56 o 7 10 0 0.70 48.82 24.97 o 8 10 0 106.87 109.95 27.34 o 9 10 0 71.72 114.47 25.41 o 10 10 0 62.24 140.88 28.38 o 11 10 0 5.20 20.54 23.16 o 12 10 0 110.94 107.84 24.80 o 1 11 0 900.90 831.69 30.46 o 2 11 0 812.32 772.22 26.34 o 3 11 0 130.56 124.26 25.70 o 4 11 0 551.06 548.60 24.90 o 5 11 0 11.12 34.78 27.27 o 6 11 0 0.55 27.73 36.32 o 7 11 0 1549.51 1512.14 42.88 o 8 11 0 205.09 256.70 25.69 o 9 11 0 1369.90 1340.42 23.13 o 10 11 0 836.73 832.59 26.39 o 11 11 0 319.71 300.20 29.19 o 12 11 0 183.63 152.36 25.38 o 0 12 0 1844.79 2110.64 42.54 o 1 12 0 4090.96 4410.67 33.63 o 2 12 0 57.92 93.27 24.40 o 3 12 0 9870.13 9295.06 89.96 o 4 12 0 655.35 624.90 24.05 o 5 12 0 1205.68 1260.24 25.21 o 6 12 0 11.80 48.69 28.07 o 7 12 0 404.49 394.85 24.80 o 8 12 0 250.67 296.75 24.66 o 9 12 0 77.01 97.11 31.23 o 10 12 0 288.12 293.46 23.29 o 11 12 0 14.80 74.09 44.34 o 12 12 0 34.77 42.62 20.67 o 1 13 0 894.01 838.19 24.27 o 2 13 0 1557.02 1682.44 25.39 o 3 13 0 6222.06 6209.27 55.89 o 4 13 0 1119.67 1158.14 22.75 o 5 13 0 1278.99 1311.96 24.11 o 6 13 0 2466.68 2460.78 43.78 o 7 13 0 21.33 85.78 35.48 o 8 13 0 6121.65 6630.28 162.14 o 9 13 0 1574.68 1769.62 53.39 o 10 13 0 1024.54 1092.76 51.84 o 11 13 0 349.63 325.83 23.93 o 12 13 0 5.74 8.41 20.80 o 1 14 0 10257.28 10472.29 44.16 o 2 14 0 31234.43 33080.44 254.53 o 3 14 0 4190.51 4493.09 51.06 o 4 14 0 4122.21 4120.91 53.00 o 5 14 0 255.86 264.58 25.53 o 6 14 0 2573.14 2563.79 75.04 o 7 14 0 301.30 288.72 23.21 o 8 14 0 1982.71 2102.09 54.87 o 9 14 0 366.84 347.01 23.05 o 10 14 0 0.78 164.60 82.72 o 11 14 0 12.47 43.38 19.02 o 12 14 0 37.16 3.46 21.66 o 1 15 0 119.03 123.90 20.52 o 2 15 0 3312.82 3172.42 26.95 o 3 15 0 70.91 87.54 20.79 o 4 15 0 936.19 903.04 26.16 o 5 15 0 10.94 40.03 23.53 o 6 15 0 707.80 714.81 22.87 o 7 15 0 2.40 25.34 35.33 o 8 15 0 13655.28 14638.25 510.64 o 9 15 0 380.33 422.22 20.70 o 10 15 0 6377.36 6431.31 266.37 o 11 15 0 351.30 385.14 37.84 o 12 15 0 257.07 168.09 25.28 o 0 16 0 14297.77 13885.42 81.01 o 1 16 0 32589.31 32284.08 112.54 o 2 16 0 7794.09 7972.14 59.61 o 3 16 0 4441.91 4968.04 39.32 o 4 16 0 627.47 658.65 22.36 o 5 16 0 35.71 63.86 21.82 o 6 16 0 147.22 159.61 21.92 o 7 16 0 53.41 95.77 20.66 o 8 16 0 21.64 89.98 32.79 o 9 16 0 59.21 97.73 41.53 o 10 16 0 26.98 32.42 18.84 o 11 16 0 20.89 41.94 19.51 o 12 16 0 27.15 59.87 36.73 o 1 17 0 689.70 723.74 28.39 o 2 17 0 16.85 -12.28 20.16 o 3 17 0 1574.05 1726.04 22.27 o 4 17 0 1.37 33.29 21.60 o 5 17 0 522.84 531.84 20.92 o 6 17 0 142.45 151.68 22.53 o 7 17 0 2096.51 2385.25 64.78 o 8 17 0 47.88 74.11 22.06 o 9 17 0 7207.03 7438.65 304.40 o 10 17 0 37.41 67.94 18.93 o 11 17 0 481.58 408.90 20.35 o 0 18 0 6927.97 6640.27 47.24 o 1 18 0 8271.52 8553.61 75.14 o 2 18 0 2397.58 2627.96 31.75 o 3 18 0 4566.82 5084.40 46.17 o 4 18 0 1322.56 1382.43 21.58 o 5 18 0 232.63 297.79 20.46 o 6 18 0 238.56 272.67 25.39 o 7 18 0 0.34 44.52 20.32 o 8 18 0 58.10 68.99 20.43 o 9 18 0 12.68 98.59 25.87 o 10 18 0 8.24 2.38 19.05 o 11 18 0 41.19 -6.28 18.99 o 1 19 0 0.41 24.66 18.59 o 2 19 0 0.21 14.51 19.39 o 3 19 0 235.79 277.94 20.85 o 4 19 0 59.89 86.83 19.99 o 5 19 0 0.05 60.06 19.19 o 6 19 0 0.52 10.49 22.74 o 7 19 0 0.43 64.23 20.91 o 8 19 0 394.09 487.48 30.10 o 9 19 0 229.79 252.90 28.46 o 10 19 0 70.79 81.71 19.31 o 11 19 0 3.12 44.35 23.73 o 0 20 0 2204.36 2191.38 53.86 o 1 20 0 192.46 227.37 19.70 o 2 20 0 1857.92 1942.95 21.13 o 3 20 0 349.60 376.45 19.53 o 4 20 0 210.70 255.39 19.72 o 5 20 0 13.16 50.21 20.68 o 6 20 0 268.67 375.47 21.44 o 7 20 0 25.49 37.07 20.11 o 8 20 0 2.49 32.73 22.94 o 9 20 0 87.06 94.08 18.74 o 10 20 0 1.59 38.75 22.20 o 11 20 0 21.37 39.48 18.79 o 1 21 0 24.42 20.56 18.44 o 2 21 0 78.03 86.40 19.92 o 3 21 0 317.77 346.55 18.99 o 4 21 0 176.27 214.33 19.84 o 5 21 0 941.10 1027.67 22.35 o 6 21 0 608.75 639.47 21.58 o 7 21 0 2378.76 2589.99 113.20 o 8 21 0 6.18 16.82 18.99 o 9 21 0 368.20 437.78 19.81 o 10 21 0 70.31 104.18 25.18 o 11 21 0 252.61 219.64 23.83 o 0 22 0 339.38 313.08 24.71 o 1 22 0 14857.76 15202.73 111.37 o 2 22 0 219.13 251.32 19.09 o 3 22 0 4799.56 5187.02 66.70 o 4 22 0 0.70 15.34 17.86 o 5 22 0 2671.79 2960.11 33.11 o 6 22 0 5.59 109.18 19.16 o 7 22 0 1498.36 1607.43 64.54 o 8 22 0 7.07 40.37 22.69 o 9 22 0 6.73 25.81 17.28 o 10 22 0 27.81 19.88 18.40 o 1 23 0 513.87 564.33 17.86 o 2 23 0 639.73 602.06 18.72 o 3 23 0 1199.55 1264.35 20.16 o 4 23 0 1243.88 1182.54 19.91 o 5 23 0 1224.21 1333.94 36.23 o 6 23 0 2018.81 2137.27 70.05 o 7 23 0 2637.70 2875.19 101.12 o 8 23 0 2181.34 2357.19 92.28 o 9 23 0 629.03 572.72 24.00 o 10 23 0 850.46 711.88 38.35 o 0 24 0 5559.91 5624.28 114.26 o 1 24 0 342.99 356.58 17.43 o 2 24 0 6280.76 6559.12 110.42 o 3 24 0 46.08 58.16 17.83 o 4 24 0 2275.73 2161.43 23.15 o 5 24 0 0.08 32.49 17.24 o 6 24 0 2139.83 2206.83 70.11 o 7 24 0 0.07 29.85 39.28 o 8 24 0 359.79 370.30 30.18 o 9 24 0 0.47 16.34 18.54 o 10 24 0 21.37 24.80 18.91 o 1 25 0 161.55 183.07 17.88 o 2 25 0 392.69 462.61 18.09 o 3 25 0 21.52 51.00 16.82 o 4 25 0 25.18 67.94 16.99 o 5 25 0 230.59 230.96 27.63 o 6 25 0 348.27 312.68 17.14 o 7 25 0 37.33 82.05 19.92 o 8 25 0 1437.32 1503.54 62.84 o 9 25 0 72.36 64.65 18.61 o 10 25 0 780.99 620.06 46.46 o 0 26 0 781.96 951.77 37.59 o 1 26 0 5631.31 5669.05 80.39 o 2 26 0 313.80 388.45 17.30 o 3 26 0 160.98 163.15 16.85 o 4 26 0 483.89 508.03 17.03 o 5 26 0 1330.75 1189.39 21.40 o 6 26 0 170.38 145.04 17.65 o 7 26 0 5.57 29.38 27.46 o 8 26 0 13.42 24.49 18.83 o 9 26 0 0.07 40.21 17.87 o 1 27 0 2.73 53.79 16.78 o 2 27 0 3.85 18.65 16.93 o 3 27 0 68.27 94.58 15.78 o 4 27 0 15.99 34.00 16.85 o 5 27 0 834.06 900.00 29.60 o 6 27 0 18.25 43.85 19.27 o 7 27 0 36.51 58.75 17.76 o 8 27 0 0.55 47.15 19.08 o 9 27 0 72.15 56.69 18.14 o 0 28 0 874.64 926.56 40.79 o 1 28 0 166.39 280.47 22.26 o 2 28 0 167.30 224.16 16.50 o 3 28 0 2.05 7.24 16.15 o 4 28 0 82.21 165.74 20.21 o 5 28 0 304.65 330.39 17.36 o 6 28 0 9.09 -2.80 17.55 o 7 28 0 69.46 74.19 18.01 o 8 28 0 0.96 1.64 18.45 o 9 28 0 31.49 41.76 28.21 o 1 29 0 13.02 54.49 15.82 o 2 29 0 406.74 377.24 19.98 o 3 29 0 5.27 41.83 20.01 o 4 29 0 707.82 743.61 19.01 o 5 29 0 8.86 46.98 16.01 o 6 29 0 552.29 533.57 25.65 o 7 29 0 5.94 39.56 27.74 o 8 29 0 382.32 300.84 29.84 o 0 30 0 8421.20 7999.12 351.05 o 1 30 0 1501.42 1320.74 26.15 o 2 30 0 1810.95 1692.95 31.25 o 3 30 0 637.36 731.73 25.99 o 4 30 0 666.79 630.70 15.50 o 5 30 0 108.41 112.78 19.07 o 6 30 0 296.78 254.42 22.91 o 7 30 0 26.67 -9.56 17.29 o 8 30 0 84.37 19.80 17.34 o 1 31 0 15.17 26.39 14.42 o 2 31 0 10.33 10.72 15.50 o 3 31 0 46.42 59.34 16.08 o 4 31 0 18.22 31.55 15.69 o 5 31 0 356.94 372.45 20.80 o 6 31 0 90.19 96.71 16.01 o 7 31 0 543.01 439.57 20.78 o 0 32 0 34.89 3.98 25.16 o 1 32 0 1387.31 1285.40 39.21 o 2 32 0 306.48 302.79 15.52 o 3 32 0 234.42 257.35 16.07 o 4 32 0 143.91 161.60 15.75 o 5 32 0 432.55 332.42 40.06 o 6 32 0 13.64 53.82 16.39 o 7 32 0 32.91 44.91 20.68 o 1 33 0 3.29 46.04 18.87 o 2 33 0 14.55 32.35 15.34 o 3 33 0 0.63 17.66 15.08 o 4 33 0 77.21 90.52 14.78 o 5 33 0 239.84 192.56 15.34 o 6 33 0 201.70 205.21 16.77 o 0 34 0 583.98 557.76 23.77 o 1 34 0 46.02 64.86 14.70 o 2 34 0 6.99 38.93 14.80 o 3 34 0 21.67 34.82 15.24 o 4 34 0 1.51 42.39 15.09 o 5 34 0 0.22 8.17 15.78 o 6 34 0 75.45 95.79 16.47 o 1 35 0 0.04 30.30 14.80 o 2 35 0 13.51 55.85 16.27 o 3 35 0 1.42 23.98 15.26 o 4 35 0 40.80 84.20 14.97 o 5 35 0 52.51 89.50 16.88 o 0 36 0 24.37 107.98 19.89 o 1 36 0 138.24 156.68 14.27 o 2 36 0 137.71 138.55 14.71 o 3 36 0 354.68 270.99 15.26 o 4 36 0 77.57 91.79 14.52 o 1 37 0 17.39 46.05 13.72 o 2 37 0 7.69 43.97 15.41 o 3 37 0 233.89 189.32 16.07 o 0 38 0 488.14 286.83 20.18 o 1 38 0 127.85 117.05 15.96 o -13 0 1 281.36 194.94 27.88 o -11 0 1 143.87 217.62 37.50 o -9 0 1 127.13 163.89 36.49 o -7 0 1 1088.62 1168.74 36.47 o -5 0 1 14695.54 14777.22 163.97 o -3 0 1 10008.42 10231.19 106.02 o 7 0 1 7154.56 6773.08 191.15 o 9 0 1 1105.58 1022.34 38.15 o 11 0 1 40.90 56.49 33.10 o 13 0 1 32.47 62.02 34.00 o -13 1 1 360.58 304.74 23.70 o -12 1 1 301.32 325.34 19.60 o -11 1 1 1674.57 1682.58 27.28 o -10 1 1 147.96 220.31 24.81 o -9 1 1 1294.07 1256.96 25.07 o -8 1 1 819.40 1023.37 55.28 o -7 1 1 3132.32 3242.45 29.68 o -6 1 1 2697.61 2811.29 53.66 o -5 1 1 14153.57 14010.48 88.93 o -4 1 1 144.93 97.16 31.55 o -3 1 1 1228.79 1221.16 39.82 o -2 1 1 720.02 537.83 51.72 o -1 1 1 97.94 145.50 58.43 o 0 1 1 4762.72 5196.51 60.67 o 1 1 1 451.73 541.78 49.89 o 2 1 1 761.69 704.82 42.00 o 3 1 1 3182.90 3010.80 42.77 o 4 1 1 229.20 242.04 28.06 o 5 1 1 15837.41 15420.85 97.95 o 6 1 1 27.38 143.05 22.84 o 7 1 1 3260.34 3256.95 52.93 o 8 1 1 207.22 229.40 23.10 o 9 1 1 1296.52 1227.82 41.87 o 10 1 1 76.01 73.28 23.31 o 11 1 1 1423.97 1323.34 33.45 o 12 1 1 123.99 163.24 23.59 o 13 1 1 397.61 318.58 24.69 o -13 2 1 4.03 23.96 18.80 o -12 2 1 114.59 115.53 19.12 o -11 2 1 6.63 24.15 22.49 o -10 2 1 8.57 62.83 23.72 o -9 2 1 58.15 83.35 22.20 o -8 2 1 15.01 42.14 20.71 o -7 2 1 176.49 214.65 23.86 o -6 2 1 1120.36 1109.19 24.77 o -5 2 1 1633.23 1526.48 30.71 o -4 2 1 846.81 659.00 28.97 o -3 2 1 2.21 28.23 41.18 o -2 2 1 747.17 1111.44 48.19 o -1 2 1 707.95 740.72 49.80 o 0 2 1 19946.57 21153.55 201.94 o 1 2 1 5.62 23.83 45.76 o 2 2 1 16081.53 17249.63 102.81 o 3 2 1 3271.96 3225.08 38.34 o 4 2 1 2050.26 2163.99 33.05 o 5 2 1 450.79 434.07 28.12 o 6 2 1 145.17 193.71 22.45 o 7 2 1 1066.04 993.31 23.27 o 8 2 1 8.47 38.24 23.85 o 9 2 1 684.74 601.09 22.88 o 10 2 1 21.37 84.81 25.58 o 11 2 1 693.10 666.81 24.74 o 12 2 1 0.41 19.39 23.34 o 13 2 1 151.26 132.43 23.21 o -13 3 1 3.96 19.85 19.45 o -12 3 1 50.23 57.14 19.66 o -11 3 1 0.23 13.58 20.82 o -10 3 1 457.28 430.25 22.77 o -9 3 1 35.49 90.47 26.28 o -8 3 1 447.50 462.50 24.57 o -7 3 1 146.17 240.07 23.47 o -6 3 1 3785.70 3850.54 34.53 o -5 3 1 2626.14 2644.27 29.40 o -4 3 1 917.58 815.44 31.27 o -3 3 1 1961.73 1770.29 38.35 o -2 3 1 2701.50 2744.29 48.31 o -1 3 1 679.58 799.62 44.55 o 0 3 1 567.39 639.79 43.78 o 1 3 1 2180.44 2285.67 40.91 o 2 3 1 116.83 162.76 42.66 o 3 3 1 303.55 270.86 34.69 o 4 3 1 505.01 478.94 26.86 o 5 3 1 256.38 317.28 28.15 o 6 3 1 1158.36 1154.99 23.67 o 7 3 1 37.10 36.42 20.72 o 8 3 1 617.08 586.61 25.11 o 9 3 1 56.18 97.58 26.66 o 10 3 1 466.11 381.64 24.50 o 11 3 1 4.23 15.12 25.51 o 12 3 1 10.67 25.79 31.32 o 13 3 1 97.46 65.71 24.55 o -13 4 1 10.59 22.52 18.00 o -12 4 1 0.24 24.35 19.06 o -11 4 1 4.77 0.47 21.73 o -10 4 1 5.82 32.15 21.51 o -9 4 1 52.08 80.94 23.47 o -8 4 1 13.24 40.63 25.35 o -7 4 1 154.04 163.07 23.54 o -6 4 1 1054.47 1134.99 24.02 o -5 4 1 434.22 495.53 29.07 o -4 4 1 2143.36 2026.10 31.66 o -3 4 1 1753.19 1705.85 37.78 o -2 4 1 2602.12 2680.16 43.76 o -1 4 1 4058.60 3961.40 48.83 o 0 4 1 3.17 26.44 40.55 o 1 4 1 2676.73 2542.60 39.15 o 2 4 1 1234.58 1173.88 36.34 o 3 4 1 500.91 476.31 35.27 o 4 4 1 2099.90 2008.65 31.62 o 5 4 1 9787.39 9698.69 107.49 o 6 4 1 20.23 70.80 26.92 o 7 4 1 387.50 418.19 22.10 o 8 4 1 111.03 135.99 24.08 o 9 4 1 49.29 77.56 26.24 o 10 4 1 82.07 70.55 24.82 o 11 4 1 46.59 110.38 27.74 o 12 4 1 136.01 174.29 25.33 o 13 4 1 72.96 66.49 20.99 o -13 5 1 17.19 26.69 19.10 o -12 5 1 38.47 46.45 21.36 o -11 5 1 432.85 451.91 23.36 o -10 5 1 80.96 70.46 22.11 o -9 5 1 1204.64 1116.51 29.06 o -8 5 1 374.87 422.02 21.59 o -7 5 1 1751.84 1718.24 21.87 o -6 5 1 483.39 464.90 22.75 o -5 5 1 159.25 132.14 26.54 o -4 5 1 223.35 274.12 29.73 o -3 5 1 5392.88 5065.23 39.34 o -2 5 1 80.52 96.17 37.80 o -1 5 1 46.25 54.18 40.14 o 0 5 1 218.91 287.61 41.18 o 1 5 1 12.30 33.74 35.64 o 2 5 1 80.52 82.93 36.04 o 3 5 1 158.29 155.27 32.74 o 4 5 1 5935.87 5890.50 80.09 o 5 5 1 367.71 381.72 25.93 o 6 5 1 3197.56 3260.49 49.02 o 7 5 1 440.26 464.73 21.97 o 8 5 1 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28.84 o -7 12 2 0.52 13.66 26.89 o -6 12 2 1212.92 1249.04 24.37 o -5 12 2 818.48 868.64 25.03 o -4 12 2 2966.59 2899.33 25.93 o -3 12 2 9615.58 9711.94 52.96 o -2 12 2 1666.07 1711.63 23.62 o -1 12 2 162.28 105.84 22.23 o 0 12 2 157.30 155.91 22.57 o 1 12 2 6.71 63.36 21.38 o 2 12 2 33.05 48.68 20.37 o 3 12 2 7158.96 7116.37 102.82 o 4 12 2 1472.75 1466.15 26.49 o 5 12 2 708.61 759.16 24.21 o 6 12 2 203.18 206.04 22.07 o 7 12 2 1246.88 1164.90 47.47 o 8 12 2 1080.10 1165.75 53.37 o 9 12 2 224.79 263.05 28.89 o 10 12 2 975.46 1023.87 54.99 o 11 12 2 3.42 42.36 27.39 o 12 12 2 374.64 309.66 24.29 o -12 13 2 19.03 48.90 20.74 o -11 13 2 66.57 90.92 18.66 o -10 13 2 94.30 107.83 20.61 o -9 13 2 715.06 764.51 23.48 o -8 13 2 2258.49 2287.05 38.52 o -7 13 2 37.34 92.83 26.47 o -6 13 2 1778.13 1688.51 25.95 o -5 13 2 3757.99 3854.57 45.95 o -4 13 2 54.79 80.60 22.47 o -3 13 2 14151.02 14081.09 115.68 o -2 13 2 2321.68 2310.08 25.48 o -1 13 2 2668.84 2536.97 24.07 o 0 13 2 465.78 553.82 22.23 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728.41 73.93 o 10 14 2 98.45 123.42 20.63 o 11 14 2 122.68 147.12 25.39 o 12 14 2 36.77 47.36 20.51 o -12 15 2 181.11 166.32 19.37 o -11 15 2 118.35 124.51 19.36 o -10 15 2 1449.18 1595.07 41.28 o -9 15 2 2.70 45.05 20.55 o -8 15 2 3515.11 3515.65 113.23 o -7 15 2 2.44 57.45 22.38 o -6 15 2 1226.88 1243.87 27.44 o -5 15 2 201.52 249.70 21.73 o -4 15 2 7238.38 7355.02 50.65 o -3 15 2 860.75 859.91 21.60 o -2 15 2 1485.29 1421.88 22.74 o -1 15 2 2870.47 2761.23 25.08 o 0 15 2 8.84 45.41 22.56 o 1 15 2 969.92 952.78 22.60 o 2 15 2 240.29 264.97 20.99 o 3 15 2 417.23 509.02 20.60 o 4 15 2 645.92 701.60 22.20 o 5 15 2 113.36 112.81 21.92 o 6 15 2 712.08 770.68 27.12 o 7 15 2 318.90 347.56 27.35 o 8 15 2 2286.39 2365.30 87.07 o 9 15 2 143.36 120.39 34.37 o 10 15 2 370.61 379.38 20.21 o 11 15 2 8.59 61.00 23.29 o 12 15 2 69.49 15.72 40.58 o -12 16 2 0.87 63.17 20.05 o -11 16 2 119.27 148.86 19.56 o -10 16 2 73.60 91.33 20.35 o -9 16 2 150.55 194.62 26.37 o -8 16 2 443.07 479.08 22.25 o -7 16 2 39.87 94.82 22.35 o -6 16 2 11.17 51.46 27.61 o -5 16 2 699.46 761.58 22.43 o -4 16 2 712.26 774.53 22.09 o -3 16 2 3660.07 3794.60 25.29 o -2 16 2 2997.77 2999.74 23.18 o -1 16 2 342.75 330.16 22.28 o 0 16 2 199.33 220.44 19.68 o 1 16 2 563.20 559.68 21.61 o 2 16 2 1755.91 1674.84 23.14 o 3 16 2 4449.30 4436.49 50.25 o 4 16 2 2559.75 2526.03 31.93 o 5 16 2 669.97 704.22 21.93 o 6 16 2 214.69 235.52 22.27 o 7 16 2 3.21 40.02 23.76 o 8 16 2 526.82 564.44 35.70 o 9 16 2 336.60 340.27 21.49 o 10 16 2 147.89 171.77 22.39 o 11 16 2 82.37 52.23 23.00 o -11 17 2 2.97 25.53 19.42 o -10 17 2 9.55 27.09 18.56 o -9 17 2 498.60 550.63 24.08 o -8 17 2 6.35 15.68 20.08 o -7 17 2 39.02 75.56 19.68 o -6 17 2 86.01 117.63 25.68 o -5 17 2 2509.32 2543.99 22.43 o -4 17 2 373.47 401.20 21.20 o -3 17 2 1950.98 2012.47 25.43 o -2 17 2 883.71 875.95 21.08 o -1 17 2 151.30 142.75 20.43 o 0 17 2 5055.91 4953.76 56.76 o 1 17 2 8.05 45.80 19.23 o 2 17 2 1418.10 1375.14 20.60 o 3 17 2 25.83 62.30 20.22 o 4 17 2 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282.68 307.50 17.75 o 5 20 2 337.52 377.65 22.47 o 6 20 2 1237.92 1250.01 54.66 o 7 20 2 363.23 390.94 20.96 o 8 20 2 53.95 102.57 18.80 o 9 20 2 214.17 177.71 19.44 o 10 20 2 11.84 45.65 44.69 o 11 20 2 35.26 81.83 22.28 o -11 21 2 76.16 71.96 18.90 o -10 21 2 131.49 178.25 19.36 o -9 21 2 7.25 27.69 24.69 o -8 21 2 65.51 125.71 20.28 o -7 21 2 1102.80 1123.98 39.82 o -6 21 2 2247.90 2287.02 41.37 o -5 21 2 370.81 423.65 22.16 o -4 21 2 3451.81 3421.30 32.57 o -3 21 2 15.61 11.80 21.80 o -2 21 2 1259.59 1318.45 21.60 o -1 21 2 273.95 283.49 17.51 o 0 21 2 176.69 195.91 17.63 o 1 21 2 18.14 38.41 17.19 o 2 21 2 823.11 870.46 20.47 o 3 21 2 1901.19 1928.19 21.60 o 4 21 2 1922.67 1862.65 19.48 o 5 21 2 1642.11 1778.89 59.37 o 6 21 2 82.60 88.25 36.58 o 7 21 2 1250.35 1231.05 52.52 o 8 21 2 50.70 114.50 18.36 o 9 21 2 20.86 24.21 17.54 o 10 21 2 20.22 62.18 28.04 o -10 22 2 1.56 30.14 18.03 o -9 22 2 53.01 65.97 17.54 o -8 22 2 111.78 124.82 19.01 o -7 22 2 273.56 331.87 22.72 o -6 22 2 594.28 688.76 19.49 o -5 22 2 1310.93 1389.38 34.99 o -4 22 2 2154.73 2151.98 23.53 o -3 22 2 3471.10 3445.70 34.23 o -2 22 2 630.88 623.78 18.97 o -1 22 2 3004.37 3044.17 47.73 o 0 22 2 7.75 42.57 17.97 o 1 22 2 3225.95 3321.10 53.09 o 2 22 2 0.56 31.38 17.59 o 3 22 2 2892.57 2995.42 51.88 o 4 22 2 124.13 203.13 18.36 o 5 22 2 2334.05 2504.09 69.78 o 6 22 2 36.76 57.71 19.64 o 7 22 2 1102.30 1042.98 40.25 o 8 22 2 3.24 51.22 25.05 o 9 22 2 5.14 36.83 24.09 o 10 22 2 5.79 37.44 19.02 o -10 23 2 220.54 241.35 18.87 o -9 23 2 5.16 12.04 19.60 o -8 23 2 855.06 957.64 37.95 o -7 23 2 1297.45 1265.23 39.30 o -6 23 2 2762.82 2754.43 49.74 o -5 23 2 1087.67 1173.76 19.71 o -4 23 2 2254.06 2202.39 21.31 o -3 23 2 852.56 934.34 20.43 o -2 23 2 529.51 539.38 19.17 o -1 23 2 304.10 309.89 18.06 o 0 23 2 310.34 334.64 18.11 o 1 23 2 123.54 162.81 17.52 o 2 23 2 93.32 140.95 23.27 o 3 23 2 12.16 53.34 18.65 o 4 23 2 511.25 516.60 24.42 o 5 23 2 464.71 477.49 20.22 o 6 23 2 321.52 291.75 19.88 o 7 23 2 674.88 690.41 48.22 o 8 23 2 270.35 273.52 19.31 o 9 23 2 3.74 22.80 19.34 o 10 23 2 67.31 66.72 22.17 o -10 24 2 118.88 134.99 19.06 o -9 24 2 59.36 97.51 39.58 o -8 24 2 2.12 44.54 20.58 o -7 24 2 438.84 470.97 50.00 o -6 24 2 66.84 66.15 17.00 o -5 24 2 831.25 875.69 20.72 o -4 24 2 976.78 933.69 24.24 o -3 24 2 391.71 425.84 19.70 o -2 24 2 703.79 788.00 20.00 o -1 24 2 120.76 125.11 18.16 o 0 24 2 926.06 826.58 20.96 o 1 24 2 17.62 26.41 16.94 o 2 24 2 613.16 708.45 21.39 o 3 24 2 67.80 67.35 22.75 o 4 24 2 2235.91 2150.52 39.71 o 5 24 2 32.77 34.23 16.87 o 6 24 2 2221.33 2300.43 70.10 o 7 24 2 193.15 186.62 18.86 o 8 24 2 165.28 166.22 19.89 o 9 24 2 117.13 178.50 28.67 o 10 24 2 30.13 35.16 18.35 o -10 25 2 70.83 73.45 19.85 o -9 25 2 44.58 57.96 19.19 o -8 25 2 81.85 97.01 18.77 o -7 25 2 8.06 25.98 18.06 o -6 25 2 184.20 169.92 16.83 o -5 25 2 3.36 36.58 17.23 o -4 25 2 177.13 203.10 16.99 o -3 25 2 172.42 246.23 19.56 o -2 25 2 2.59 52.01 18.91 o -1 25 2 2540.88 2602.32 50.44 o 0 25 2 708.00 742.39 19.27 o 1 25 2 1374.88 1454.58 31.71 o 2 25 2 847.28 819.47 21.59 o 3 25 2 163.56 188.68 17.41 o 4 25 2 653.89 647.65 18.26 o 5 25 2 1460.74 1458.22 37.20 o 6 25 2 507.08 496.49 18.76 o 7 25 2 505.41 513.75 18.29 o 8 25 2 148.20 169.85 18.27 o 9 25 2 57.06 91.89 17.83 o -9 26 2 32.94 80.04 18.48 o -8 26 2 172.09 146.16 17.31 o -7 26 2 3.67 43.15 18.60 o -6 26 2 177.73 154.51 18.24 o -5 26 2 487.73 482.30 18.64 o -4 26 2 64.34 87.89 16.97 o -3 26 2 54.15 54.22 17.76 o -2 26 2 552.94 573.96 17.84 o -1 26 2 230.25 262.08 18.76 o 0 26 2 103.92 108.42 17.58 o 1 26 2 973.21 979.12 21.93 o 2 26 2 89.96 93.22 17.27 o 3 26 2 21.32 46.88 15.16 o 4 26 2 409.31 376.06 18.72 o 5 26 2 476.98 454.80 18.26 o 6 26 2 527.36 526.65 19.68 o 7 26 2 10.54 36.48 22.26 o 8 26 2 310.32 346.73 21.85 o 9 26 2 8.47 14.37 22.90 o -9 27 2 46.96 44.40 18.11 o -8 27 2 36.54 109.82 23.93 o -7 27 2 40.73 50.36 18.96 o -6 27 2 152.76 127.72 17.71 o -5 27 2 840.41 783.37 18.94 o -4 27 2 85.60 96.12 16.77 o -3 27 2 278.15 279.81 16.93 o -2 27 2 88.01 106.36 22.45 o -1 27 2 118.39 157.83 16.58 o 0 27 2 719.38 756.83 30.51 o 1 27 2 28.44 74.30 16.86 o 2 27 2 359.70 374.41 16.38 o 3 27 2 15.07 43.86 15.77 o 4 27 2 200.91 234.82 16.90 o 5 27 2 263.25 259.63 15.64 o 6 27 2 274.93 279.64 19.00 o 7 27 2 5.09 40.86 18.79 o 8 27 2 42.89 77.54 17.73 o 9 27 2 16.07 5.25 19.62 o -8 28 2 125.50 118.84 22.40 o -7 28 2 40.21 56.24 16.48 o -6 28 2 403.38 454.04 35.81 o -5 28 2 5.00 67.17 16.93 o -4 28 2 206.84 223.82 16.34 o -3 28 2 58.70 62.87 16.18 o -2 28 2 374.93 367.93 16.04 o -1 28 2 197.13 255.58 23.31 o 0 28 2 1489.14 1619.71 40.33 o 1 28 2 245.99 300.03 16.09 o 2 28 2 284.75 302.67 15.76 o 3 28 2 2.80 25.54 15.43 o 4 28 2 122.39 147.72 15.44 o 5 28 2 222.85 229.61 15.84 o 6 28 2 0.10 53.74 18.12 o 7 28 2 85.02 72.02 26.56 o 8 28 2 3.43 46.16 27.31 o -8 29 2 329.37 257.77 19.10 o -7 29 2 0.75 21.43 16.33 o -6 29 2 608.53 503.36 17.32 o -5 29 2 6.46 39.62 17.16 o -4 29 2 844.91 857.74 17.15 o -3 29 2 0.26 23.54 15.81 o -2 29 2 412.01 455.51 15.81 o -1 29 2 744.24 642.23 15.77 o 0 29 2 42.54 70.29 15.91 o 1 29 2 685.14 648.94 17.29 o 2 29 2 0.02 16.80 15.75 o 3 29 2 266.97 290.56 15.91 o 4 29 2 35.53 21.14 14.56 o 5 29 2 102.78 116.38 17.68 o 6 29 2 139.35 175.72 37.60 o 7 29 2 55.96 44.97 21.49 o 8 29 2 66.73 42.84 17.15 o -8 30 2 0.02 -6.01 17.49 o -7 30 2 43.81 78.45 16.69 o -6 30 2 0.52 27.21 18.20 o -5 30 2 205.99 162.37 17.41 o -4 30 2 46.90 81.95 15.87 o -3 30 2 284.29 319.47 16.77 o -2 30 2 456.45 476.22 16.84 o -1 30 2 370.58 389.11 16.77 o 0 30 2 2564.75 2558.48 35.02 o 1 30 2 477.64 537.54 20.80 o 2 30 2 291.42 307.74 18.07 o 3 30 2 424.28 411.67 15.17 o 4 30 2 831.30 802.82 15.73 o 5 30 2 36.09 57.02 15.17 o 6 30 2 466.30 357.96 28.00 o 7 30 2 0.48 -5.86 17.11 o -7 31 2 260.13 175.71 16.80 o -6 31 2 98.36 86.95 16.81 o -5 31 2 570.34 505.97 28.90 o -4 31 2 72.78 84.88 15.67 o -3 31 2 186.43 223.84 15.77 o -2 31 2 14.42 44.23 14.99 o -1 31 2 90.49 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