# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ox0086 in P2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 299.63 _exptl_crystal_F_000 962.00 _reflns_d_resolution_high 0.8255 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 9.1550 _cell_length_b 13.6852 _cell_length_c 14.5359 _cell_angle_alpha 90.000 _cell_angle_beta 92.570 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 -15 0 326.32 456.34 486.63 o 5 -14 0 111.45 0.00 446.87 o 3 -13 0 165.16 244.26 284.97 o 4 -13 0 593.47 422.25 296.33 o 5 -13 0 35.55 35.71 261.01 o 6 -13 0 282.48 178.06 266.31 o 0 -12 0 737.59 551.96 201.66 o 1 -12 0 809.30 785.36 140.78 o 2 -12 0 2291.02 2192.63 153.77 o 3 -12 0 530.05 639.06 284.03 o 4 -12 0 3002.03 2898.96 327.58 o 5 -12 0 228.77 227.33 249.48 o 6 -12 0 2527.16 2449.44 278.90 o 7 -12 0 3.28 380.32 329.94 o 1 -11 0 428.19 368.89 132.33 o 2 -11 0 1359.39 1445.30 145.64 o 3 -11 0 200.99 147.93 141.50 o 4 -11 0 1688.25 1785.58 301.07 o 5 -11 0 78.25 116.70 234.56 o 6 -11 0 338.23 352.78 247.17 o 7 -11 0 338.65 120.99 247.69 o 8 -11 0 102.18 136.80 255.99 o 0 -10 0 1295.53 1041.43 175.15 o 1 -10 0 577.47 668.64 125.51 o 2 -10 0 5639.31 5636.99 172.15 o 3 -10 0 1039.14 1337.76 289.71 o 4 -10 0 7366.60 7082.66 392.90 o 5 -10 0 518.12 445.18 244.85 o 6 -10 0 4186.29 4001.33 276.91 o 7 -10 0 4.64 64.20 241.85 o 8 -10 0 1311.79 1580.04 263.20 o 1 -9 0 4467.91 4353.12 152.90 o 2 -9 0 3077.41 3045.09 149.18 o 3 -9 0 136.47 97.52 264.14 o 4 -9 0 3853.08 3623.23 337.04 o 5 -9 0 95.55 69.91 243.14 o 6 -9 0 843.65 833.95 228.24 o 7 -9 0 673.21 850.30 239.49 o 8 -9 0 84.85 163.12 231.75 o 0 -8 0 10442.43 10606.48 220.59 o 1 -8 0 2626.44 2518.39 116.46 o 2 -8 0 7910.05 7800.30 292.55 o 3 -8 0 2718.80 2898.01 284.03 o 4 -8 0 9730.13 9249.40 235.27 o 5 -8 0 1785.35 1837.61 243.36 o 6 -8 0 6324.14 5911.90 274.69 o 7 -8 0 656.70 507.60 219.30 o 8 -8 0 3017.88 3210.90 255.35 o 9 -8 0 29.00 43.55 320.95 o 1 -7 0 6758.51 6807.22 131.94 o 2 -7 0 895.01 807.35 121.23 o 3 -7 0 428.17 392.31 112.66 o 4 -7 0 2648.40 2657.15 124.26 o 5 -7 0 1010.35 958.98 89.53 o 6 -7 0 818.90 656.22 170.44 o 7 -7 0 1104.35 928.99 172.70 o 8 -7 0 63.71 34.45 189.53 o 9 -7 0 449.64 485.68 333.26 o 10 -7 0 109.12 155.27 352.19 o 0 -6 0 9429.73 9674.88 176.10 o 1 -6 0 468.59 433.66 83.09 o 2 -6 0 6009.92 5616.55 139.18 o 3 -6 0 2786.21 2678.34 115.84 o 4 -6 0 7836.51 7820.79 134.96 o 5 -6 0 3378.81 3450.41 92.11 o 6 -6 0 6317.50 6535.56 207.23 o 7 -6 0 120.10 340.16 160.70 o 8 -6 0 2842.27 3005.01 211.09 o 10 -6 0 1711.23 1370.90 360.71 o 1 -5 0 420.89 354.75 93.70 o 2 -5 0 750.42 568.64 88.53 o 3 -5 0 630.20 617.07 80.62 o 4 -5 0 4576.39 4808.44 154.14 o 5 -5 0 5111.07 5306.03 102.86 o 6 -5 0 479.03 684.62 87.15 o 7 -5 0 1835.79 1481.87 162.05 o 8 -5 0 509.58 690.05 171.44 o 9 -5 0 593.24 778.23 313.38 o 10 -5 0 703.45 925.93 340.83 o 0 -4 0 39742.66 40486.98 960.01 o 1 -4 0 1424.08 1522.15 127.34 o 2 -4 0 2909.93 2690.11 93.56 o 3 -4 0 1840.69 1976.68 81.04 o 4 -4 0 4100.83 4051.61 86.90 o 5 -4 0 1240.70 1316.61 88.98 o 6 -4 0 5508.82 5535.60 100.98 o 7 -4 0 286.32 384.04 164.19 o 8 -4 0 1390.42 1735.40 302.96 o 9 -4 0 517.15 508.41 315.27 o 10 -4 0 1468.85 1496.82 374.91 o 1 -3 0 2698.29 2406.14 79.73 o 2 -3 0 317.78 303.57 59.93 o 3 -3 0 336.20 341.81 63.42 o 4 -3 0 1748.44 1961.07 82.21 o 5 -3 0 4547.77 5114.91 172.10 o 6 -3 0 64.17 581.09 99.85 o 7 -3 0 2742.40 2512.11 133.58 o 8 -3 0 1477.97 1568.77 301.07 o 9 -3 0 1252.35 1386.05 326.63 o 10 -3 0 1239.62 1132.32 343.67 o 0 -2 0 89779.73 92915.57 814.11 o 1 -2 0 4943.41 4609.74 124.02 o 2 -2 0 34493.96 32855.11 516.45 o 3 -2 0 3480.58 3507.82 138.13 o 4 -2 0 20839.57 20501.25 271.80 o 5 -2 0 2148.69 2211.81 137.28 o 6 -2 0 3821.58 3845.59 173.26 o 7 -2 0 652.40 889.00 279.29 o 8 -2 0 1859.64 1626.75 131.62 o 9 -2 0 590.92 651.37 303.91 o 10 -2 0 2057.96 2207.83 373.02 o 1 -1 0 11166.81 11185.30 195.03 o 2 -1 0 5943.63 6066.58 78.37 o 3 -1 0 2612.59 2709.39 84.80 o 4 -1 0 130.50 167.24 50.20 o 5 -1 0 10859.13 11376.70 271.72 o 6 -1 0 199.58 707.73 106.34 o 7 -1 0 3708.61 3739.26 126.22 o 8 -1 0 1157.34 1352.91 301.07 o 9 -1 0 2005.47 1849.96 327.58 o 10 -1 0 1455.89 1354.80 343.67 o 11 -1 0 565.00 125.92 367.34 o 1 0 0 4023.14 4138.26 88.99 o 2 0 0 70618.84 72511.20 1126.16 o 3 0 0 1858.05 1920.44 63.69 o 4 0 0 12878.76 12556.75 432.67 o 5 0 0 2048.51 2060.14 89.94 o 6 0 0 4165.34 4360.75 288.76 o 7 0 0 439.80 593.61 271.72 o 8 0 0 437.45 387.22 290.65 o 9 0 0 535.95 633.38 317.16 o 10 0 0 1268.30 1458.95 350.30 o 11 0 0 278.86 363.55 369.23 o 1 1 0 11160.45 10955.76 97.49 o 2 1 0 5982.06 6167.59 126.60 o 3 1 0 2635.15 2601.68 239.53 o 8 1 0 1172.56 1240.25 303.91 o 9 1 0 2044.13 1947.47 329.47 o 10 1 0 1421.04 1673.49 253.73 o 11 1 0 546.32 600.24 358.82 o 0 2 0 89364.26 94675.37 1301.79 o 1 2 0 5266.63 5337.41 55.80 o 2 2 0 34593.93 34166.75 238.86 o 3 2 0 4007.80 4378.78 161.45 o 9 2 0 551.28 664.62 319.06 o 10 2 0 2068.73 2090.46 234.45 o 1 3 0 2613.83 2675.37 74.07 o 2 3 0 323.84 335.10 66.21 o 3 3 0 317.61 353.67 129.19 o 9 3 0 1206.60 1494.92 286.87 o 10 3 0 1237.17 1384.20 229.46 o 0 4 0 39424.03 41939.94 693.97 o 1 4 0 1335.45 1413.59 76.08 o 2 4 0 3270.80 3293.51 83.23 o 3 4 0 1848.54 2040.25 213.97 o 8 4 0 1405.27 1576.34 290.65 o 9 4 0 427.29 434.56 296.33 o 10 4 0 1487.13 1590.55 317.16 o 1 5 0 412.85 355.18 75.25 o 2 5 0 775.18 752.32 66.81 o 3 5 0 624.86 656.04 86.05 o 7 5 0 1943.39 1978.72 301.07 o 8 5 0 473.13 471.48 299.17 o 9 5 0 602.89 1067.94 314.32 o 10 5 0 658.30 756.46 324.74 o 0 6 0 8698.25 8538.77 228.17 o 1 6 0 509.01 456.51 76.62 o 2 6 0 6177.86 6290.07 110.92 o 3 6 0 2699.55 2783.73 107.50 o 4 6 0 8010.96 8220.66 313.38 o 5 6 0 3421.86 3494.47 303.91 o 6 6 0 6715.99 6624.44 360.71 o 7 6 0 99.90 253.73 287.81 o 8 6 0 2745.60 2781.56 326.63 o 9 6 0 7.03 56.81 308.64 o 10 6 0 1677.03 1154.09 357.87 o 1 7 0 6397.02 6528.67 240.52 o 2 7 0 793.65 797.28 89.40 o 3 7 0 418.47 474.33 100.73 o 4 7 0 2706.93 2663.48 118.19 o 5 7 0 1066.02 1169.24 289.71 o 6 7 0 754.48 730.89 292.55 o 7 7 0 1078.73 1235.51 308.64 o 8 7 0 102.46 174.20 304.85 o 9 7 0 431.43 351.25 335.15 o 10 7 0 153.71 190.30 364.50 o 0 8 0 10034.14 10287.43 282.13 o 1 8 0 2751.09 2894.26 163.56 o 2 8 0 7916.93 7862.15 156.36 o 3 8 0 2780.57 2637.27 131.98 o 4 8 0 9653.66 9124.38 175.92 o 5 8 0 1876.12 2093.27 308.64 o 6 8 0 6149.14 6254.25 380.60 o 7 8 0 704.83 759.30 313.38 o 8 8 0 3131.19 3253.05 363.55 o 9 8 0 19.13 108.88 329.47 o 1 9 0 4456.41 4436.74 132.35 o 2 9 0 3229.36 3518.18 159.03 o 3 9 0 139.72 77.78 119.64 o 4 9 0 4154.37 4105.10 156.08 o 5 9 0 78.96 239.53 305.80 o 6 9 0 930.66 960.01 318.11 o 7 9 0 648.88 711.96 323.79 o 8 9 0 109.09 190.30 328.52 o 9 9 0 312.23 256.57 351.25 o 0 10 0 1159.24 1050.90 224.38 o 1 10 0 615.58 528.60 155.37 o 2 10 0 5481.73 5415.19 189.58 o 3 10 0 1094.35 1167.31 146.40 o 4 10 0 7223.39 6936.96 217.75 o 5 10 0 513.05 615.39 300.12 o 6 10 0 4241.41 3987.73 372.07 o 7 10 0 12.19 55.86 321.90 o 8 10 0 1330.82 1500.60 371.13 o 1 11 0 485.93 580.53 156.28 o 2 11 0 1447.59 1472.03 166.38 o 3 11 0 185.47 147.66 142.86 o 4 11 0 1788.23 1698.58 151.37 o 5 11 0 73.09 32.19 297.28 o 6 11 0 263.69 286.87 324.74 o 7 11 0 384.78 415.62 341.78 o 8 11 0 102.02 0.00 363.55 o 0 12 0 625.78 758.35 231.01 o 1 12 0 871.45 904.94 171.05 o 2 12 0 2265.34 2467.72 175.65 o 3 12 0 537.97 659.47 151.52 o 4 12 0 2864.41 2759.79 341.78 o 5 12 0 185.69 193.14 307.69 o 6 12 0 2474.47 2507.00 370.18 o 7 12 0 6.70 223.43 352.19 o 1 13 0 303.19 366.95 170.79 o 2 13 0 255.72 206.13 159.86 o 3 13 0 187.71 251.23 155.84 o 4 13 0 551.84 462.96 312.43 o 5 13 0 32.03 0.00 325.68 o 6 13 0 222.57 75.74 337.04 o 0 14 0 1858.05 2103.69 274.56 o 1 14 0 32.27 4.75 166.70 o 2 14 0 1382.54 1664.85 189.94 o 3 14 0 331.89 347.46 298.23 o 4 14 0 1797.30 1734.45 342.72 o 5 14 0 99.82 71.95 336.10 o 1 15 0 910.52 838.57 182.71 o 2 15 0 265.04 117.40 290.65 o 3 15 0 148.87 63.43 303.91 o 4 15 0 265.29 259.41 331.36 o 0 16 0 899.05 1553.62 306.75 o 1 16 0 32.03 0.00 184.67 o 2 16 0 1159.28 1588.65 328.52 o -4 -15 1 1319.74 856.81 480.95 o -3 -15 1 242.71 50.18 462.96 o -5 -14 1 120.35 103.20 422.25 o -4 -14 1 154.80 0.00 443.08 o -3 -14 1 111.17 190.30 440.24 o 5 -14 1 609.37 296.33 452.55 o -6 -13 1 726.69 1146.52 444.03 o -5 -13 1 601.57 425.09 419.41 o -4 -13 1 1543.82 1422.97 434.56 o 0 -13 1 3994.77 3921.45 265.09 o 1 -13 1 193.67 124.02 245.21 o 2 -13 1 1778.50 1635.99 306.75 o 3 -13 1 4.57 0.00 297.28 o 4 -13 1 462.47 380.60 331.36 o 5 -13 1 237.56 227.22 337.04 o 6 -13 1 707.08 710.60 295.99 o -7 -12 1 596.85 386.28 383.44 o -6 -12 1 170.36 378.85 250.45 o -5 -12 1 337.85 280.47 231.18 o -4 -12 1 157.51 70.99 146.96 o -3 -12 1 164.69 246.91 144.32 o -2 -12 1 502.98 558.24 143.31 o -1 -12 1 878.10 777.11 144.80 o 0 -12 1 2546.57 2698.25 234.79 o 1 -12 1 250.78 133.49 235.74 o 2 -12 1 2376.20 2143.45 295.39 o 3 -12 1 330.67 217.75 304.85 o 4 -12 1 521.76 291.60 338.94 o 5 -12 1 997.11 757.40 338.94 o 7 -12 1 394.81 269.46 279.54 o -8 -11 1 88.77 90.89 372.07 o -7 -11 1 443.71 237.64 361.66 o -6 -11 1 732.11 585.26 233.16 o -5 -11 1 256.75 229.58 225.36 o -4 -11 1 3656.75 3627.00 415.62 o -3 -11 1 208.89 357.26 149.35 o -2 -11 1 8000.51 7740.52 202.64 o -1 -11 1 421.19 313.39 134.83 o 0 -11 1 10096.33 10717.26 285.45 o 1 -11 1 601.48 551.84 122.11 o 2 -11 1 6787.20 6571.10 179.41 o 3 -11 1 702.74 517.94 136.03 o 4 -11 1 1451.13 1138.94 341.78 o 5 -11 1 732.43 516.93 333.26 o 6 -11 1 961.31 1116.96 273.58 o 7 -11 1 972.67 1195.09 282.84 o 8 -11 1 512.00 645.84 275.79 o -8 -10 1 889.23 1165.45 359.77 o -7 -10 1 836.60 627.70 335.15 o -6 -10 1 932.21 1110.30 233.87 o -5 -10 1 102.91 166.27 213.00 o -4 -10 1 1460.00 1218.73 232.57 o -3 -10 1 450.27 450.65 250.89 o -2 -10 1 877.74 745.92 141.26 o -1 -10 1 1717.71 1767.83 139.23 o 0 -10 1 3557.35 4000.29 144.16 o 1 -10 1 719.77 782.74 116.51 o 2 -10 1 4622.49 4514.28 163.32 o 3 -10 1 100.50 105.09 291.60 o 4 -10 1 714.88 862.49 319.06 o 5 -10 1 1506.83 1555.52 354.09 o 6 -10 1 30.24 98.37 255.14 o 7 -10 1 627.99 682.75 251.33 o 8 -10 1 203.79 336.27 251.26 o -8 -9 1 609.76 845.45 320.00 o -7 -9 1 68.61 171.36 324.74 o -6 -9 1 1461.53 1250.48 217.17 o -5 -9 1 552.06 540.74 216.43 o -4 -9 1 4060.94 3671.57 360.71 o -3 -9 1 809.22 815.15 249.94 o -2 -9 1 11815.70 11312.63 208.73 o -1 -9 1 1991.78 1803.32 128.49 o 0 -9 1 14141.26 14683.35 186.52 o 1 -9 1 971.49 1058.88 108.48 o 2 -9 1 5441.57 5235.33 149.69 o 3 -9 1 141.90 96.57 298.23 o 4 -9 1 1327.44 1228.93 159.28 o 5 -9 1 883.38 711.01 361.66 o 6 -9 1 821.81 1067.31 255.40 o 7 -9 1 2117.37 1721.00 262.27 o 8 -9 1 1451.65 1779.41 256.90 o 9 -9 1 701.90 373.97 404.26 o -9 -8 1 482.26 736.57 340.83 o -8 -8 1 1384.03 1822.14 231.03 o -7 -8 1 762.53 1000.72 302.01 o -6 -8 1 3342.96 3460.71 245.08 o -5 -8 1 202.81 305.08 214.82 o -4 -8 1 1208.89 1423.31 209.27 o -3 -8 1 1327.84 1387.94 252.78 o -2 -8 1 2000.26 1691.85 212.07 o -1 -8 1 1269.56 1203.19 112.37 o 0 -8 1 6891.50 7425.80 231.48 o 1 -8 1 2267.28 2330.25 115.98 o 2 -8 1 1719.30 1465.62 220.59 o 3 -8 1 292.60 256.34 144.08 o 4 -8 1 127.33 155.58 136.69 o 5 -8 1 1886.89 1949.37 365.45 o 6 -8 1 224.20 336.29 239.53 o 7 -8 1 246.28 134.47 222.02 o 8 -8 1 571.12 693.38 233.13 o -10 -7 1 1227.21 1155.99 390.06 o -9 -7 1 327.60 240.48 330.42 o -8 -7 1 1321.04 1353.38 209.49 o -7 -7 1 217.86 478.87 194.39 o -6 -7 1 2430.11 2243.66 179.98 o -5 -7 1 1768.30 1432.92 207.36 o -4 -7 1 4500.26 4551.64 231.48 o -3 -7 1 2713.51 2713.40 246.16 o -2 -7 1 11196.11 11004.12 282.13 o -1 -7 1 242.84 198.10 93.66 o 0 -7 1 6389.51 6361.97 117.14 o 1 -7 1 479.88 474.82 72.12 o 2 -7 1 3587.14 3408.60 144.11 o 3 -7 1 2928.19 3031.85 146.26 o 4 -7 1 5688.96 5743.24 364.03 o 5 -7 1 3026.07 3107.89 138.54 o 6 -7 1 2754.32 2606.33 257.87 o 7 -7 1 1850.54 2108.21 179.99 o 8 -7 1 2478.57 2292.43 190.35 o 9 -7 1 440.91 500.83 323.79 o -10 -6 1 2195.90 2293.98 394.80 o -9 -6 1 269.72 247.10 307.69 o -8 -6 1 1665.95 1732.60 205.64 o -7 -6 1 1778.51 1816.05 209.71 o -6 -6 1 5868.44 6077.22 236.54 o -5 -6 1 897.82 970.79 152.73 o -4 -6 1 3886.82 3792.76 202.20 o -3 -6 1 2905.00 2666.54 168.11 o -2 -6 1 4658.12 4779.21 211.13 o -1 -6 1 4930.99 4820.33 147.22 o 0 -6 1 5281.60 5495.43 92.86 o 1 -6 1 4968.52 4956.28 90.44 o 2 -6 1 4410.37 4474.75 139.09 o 3 -6 1 36.63 87.51 101.70 o 4 -6 1 821.69 834.62 110.56 o 5 -6 1 2517.64 2455.39 115.72 o 6 -6 1 435.04 527.49 160.07 o 7 -6 1 408.70 669.18 164.59 o 8 -6 1 709.67 852.27 165.82 o 9 -6 1 81.39 96.57 289.71 o 10 -6 1 507.48 291.60 320.95 o -10 -5 1 1400.05 1260.13 355.03 o -9 -5 1 61.98 15.15 320.00 o -8 -5 1 2708.87 2608.47 199.75 o -7 -5 1 258.70 191.48 176.09 o -6 -5 1 5402.45 4852.16 173.24 o -5 -5 1 3593.84 3375.14 160.97 o -4 -5 1 2804.28 2631.04 170.94 o -3 -5 1 1355.23 1207.12 148.17 o -2 -5 1 3337.31 3175.41 193.14 o -1 -5 1 329.07 356.93 129.71 o 0 -5 1 9362.25 9686.57 185.52 o 1 -5 1 3175.97 2959.65 124.02 o 2 -5 1 8690.96 8248.80 145.36 o 3 -5 1 2882.39 2880.47 115.74 o 4 -5 1 9249.30 9213.72 221.32 o 5 -5 1 4797.27 4908.08 168.25 o 6 -5 1 8704.91 8873.43 198.55 o 7 -5 1 1638.60 1967.63 165.37 o 8 -5 1 3100.31 3323.56 252.95 o 9 -5 1 499.81 501.78 297.28 o 10 -5 1 1462.94 1353.86 350.30 o -10 -4 1 845.18 849.24 342.72 o -9 -4 1 162.78 306.75 313.38 o -8 -4 1 2280.09 1931.38 324.74 o -7 -4 1 965.23 1038.39 168.26 o -6 -4 1 7572.59 7828.08 204.39 o -5 -4 1 354.04 391.02 55.77 o -4 -4 1 4953.83 4974.95 143.32 o -3 -4 1 5692.46 5740.87 178.69 o -2 -4 1 2891.98 2940.62 182.72 o -1 -4 1 1481.13 1616.86 112.91 o 0 -4 1 6032.42 5931.19 75.92 o 1 -4 1 7419.10 7532.79 244.74 o 2 -4 1 2349.69 2329.32 103.98 o 3 -4 1 1378.20 1317.57 74.49 o 4 -4 1 350.96 220.91 88.21 o 5 -4 1 5252.59 5284.97 142.25 o 6 -4 1 432.25 520.19 64.93 o 7 -4 1 1657.03 1969.09 198.12 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