# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1385 in C2/c, 1385am MS4 Co(saloph)(py)2.ClO4' _shelx_refln_list_code 4 _shelx_F_calc_maximum 508.11 _exptl_crystal_F_000 2592.00 _reflns_d_resolution_high 0.7108 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 33.4032 _cell_length_b 10.6586 _cell_length_c 16.3498 _cell_angle_alpha 90.000 _cell_angle_beta 112.179 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 150225.05 135746.75 2945.90 o 6 0 0 80.01 185.11 18.55 o 8 0 0 43169.87 40583.63 614.45 o 10 0 0 35004.29 31505.15 481.02 o 12 0 0 4324.31 3904.51 110.06 o 14 0 0 971.17 740.16 89.90 o 16 0 0 4291.75 4600.65 88.83 o 18 0 0 2281.47 2060.83 52.40 o 20 0 0 7672.64 6395.72 93.11 o 22 0 0 16874.58 16325.41 231.11 o 24 0 0 439.07 501.78 24.13 o 26 0 0 3444.53 3662.21 139.03 o 28 0 0 950.52 800.17 67.37 o 30 0 0 94.93 74.67 48.92 o 32 0 0 16579.34 16384.24 428.24 o 34 0 0 49.02 -36.39 49.43 o 36 0 0 1042.46 929.38 81.18 o 38 0 0 6627.33 6401.62 220.73 o 40 0 0 71.95 51.30 59.83 o 42 0 0 2107.42 1914.79 117.30 o 3 1 0 10356.21 10311.32 98.53 o 5 1 0 104555.84 103358.00 971.90 o 7 1 0 10388.12 9968.81 98.04 o 9 1 0 2711.52 2508.94 31.43 o 11 1 0 628.39 656.27 17.10 o 13 1 0 28.08 88.97 30.13 o 15 1 0 27503.80 25315.52 305.75 o 17 1 0 26178.08 24844.90 241.65 o 19 1 0 4453.58 4326.05 54.11 o 21 1 0 1746.29 1773.96 37.93 o 23 1 0 1599.44 1453.93 30.64 o 25 1 0 11555.28 11169.08 163.59 o 27 1 0 16723.54 15876.38 284.51 o 29 1 0 450.92 496.64 44.67 o 31 1 0 960.00 836.93 53.20 o 33 1 0 2368.80 2498.12 130.30 o 35 1 0 1153.90 1175.43 53.97 o 37 1 0 1974.28 2172.37 67.06 o 39 1 0 618.62 587.94 55.04 o 41 1 0 1167.52 1076.15 66.35 o 43 1 0 412.02 421.80 46.45 o 0 2 0 74530.89 74732.30 927.71 o 2 2 0 17987.01 18207.49 155.47 o 4 2 0 11777.72 12045.91 114.43 o 6 2 0 12107.75 12458.15 121.16 o 8 2 0 416.33 349.03 13.94 o 10 2 0 54726.90 52932.36 527.44 o 12 2 0 7346.14 6901.01 68.01 o 14 2 0 2667.14 2448.71 35.52 o 16 2 0 10417.97 10983.94 114.43 o 18 2 0 6149.97 6425.50 97.89 o 20 2 0 11065.33 9817.83 106.31 o 22 2 0 14377.48 14128.94 157.50 o 24 2 0 269.80 266.20 19.79 o 26 2 0 290.55 253.80 25.00 o 28 2 0 3975.63 4072.74 87.29 o 30 2 0 1041.38 1143.60 49.70 o 32 2 0 6775.94 7092.17 242.76 o 34 2 0 1668.59 1684.68 74.90 o 36 2 0 16.16 -28.48 36.34 o 38 2 0 2206.75 1951.30 119.34 o 40 2 0 0.62 -21.55 51.66 o 42 2 0 2075.17 2062.67 110.44 o 1 3 0 1235.83 1334.58 19.16 o 3 3 0 12377.26 11920.73 105.77 o 5 3 0 43206.25 41489.00 382.05 o 7 3 0 3981.97 3373.04 41.15 o 9 3 0 9283.06 9972.32 101.70 o 11 3 0 6575.84 7245.34 78.03 o 13 3 0 238.69 314.37 14.45 o 15 3 0 68760.95 70735.52 660.59 o 17 3 0 5543.33 4998.73 61.06 o 19 3 0 3702.53 3522.61 48.79 o 21 3 0 324.85 396.49 18.80 o 23 3 0 4063.18 4020.18 63.13 o 25 3 0 591.77 604.97 29.43 o 27 3 0 8332.51 8520.27 131.10 o 29 3 0 29.41 -11.19 33.37 o 31 3 0 9.92 -9.99 42.31 o 33 3 0 1803.92 1722.98 74.75 o 35 3 0 344.19 365.29 46.01 o 37 3 0 2193.41 2156.93 99.59 o 39 3 0 3.16 79.45 40.74 o 41 3 0 518.96 546.74 106.69 o 0 4 0 18241.65 17100.27 211.00 o 2 4 0 5623.84 6102.42 59.69 o 4 4 0 2071.59 2274.54 33.59 o 6 4 0 8453.81 8430.12 86.98 o 8 4 0 3696.98 3696.25 46.60 o 10 4 0 34917.26 35043.74 333.60 o 12 4 0 22935.40 23245.81 226.65 o 14 4 0 1896.59 2131.49 35.49 o 16 4 0 31.62 19.68 13.18 o 18 4 0 1378.72 1473.01 31.20 o 20 4 0 11950.02 12340.34 131.71 o 22 4 0 1591.84 1606.59 34.76 o 24 4 0 1868.33 1793.56 43.14 o 26 4 0 2377.77 2414.76 59.19 o 28 4 0 1649.26 1677.78 68.45 o 30 4 0 361.87 400.62 43.15 o 32 4 0 7515.57 7353.87 162.08 o 34 4 0 101.99 129.21 40.28 o 36 4 0 277.20 347.82 47.80 o 38 4 0 189.26 163.99 43.09 o 40 4 0 497.67 452.65 57.24 o 1 5 0 784.66 652.05 17.72 o 3 5 0 191.01 237.36 16.33 o 5 5 0 9679.06 8876.31 87.83 o 7 5 0 8728.05 8605.38 104.63 o 9 5 0 1738.94 1926.60 33.20 o 11 5 0 452.26 349.10 16.40 o 13 5 0 939.35 951.15 25.97 o 15 5 0 13987.04 14401.07 149.52 o 17 5 0 10624.37 11322.71 122.66 o 19 5 0 31.80 62.33 16.36 o 21 5 0 963.65 950.34 30.42 o 23 5 0 2381.18 2447.27 51.09 o 25 5 0 1905.68 1984.98 47.18 o 27 5 0 3558.94 3643.13 85.68 o 29 5 0 3020.83 2877.86 89.61 o 31 5 0 343.94 280.78 43.99 o 33 5 0 4474.06 4335.62 118.54 o 35 5 0 57.71 57.55 39.75 o 37 5 0 141.91 124.57 42.57 o 39 5 0 6.76 1.00 39.21 o 41 5 0 264.36 152.55 43.60 o 0 6 0 285.18 248.73 19.45 o 2 6 0 3830.41 4101.02 47.63 o 4 6 0 1102.76 1117.42 23.25 o 6 6 0 30.48 20.25 11.00 o 8 6 0 271.22 302.76 16.01 o 10 6 0 6984.39 6588.86 77.82 o 12 6 0 879.30 1001.78 34.48 o 14 6 0 15438.94 15444.69 160.93 o 16 6 0 93.17 120.61 17.11 o 18 6 0 3059.49 3089.22 50.48 o 20 6 0 324.10 307.53 21.93 o 22 6 0 18.45 -1.54 17.89 o 24 6 0 1435.38 1328.41 40.52 o 26 6 0 70.64 59.78 28.48 o 28 6 0 557.50 528.96 35.81 o 30 6 0 1299.84 1314.02 67.30 o 32 6 0 627.43 676.11 83.69 o 34 6 0 345.17 264.13 45.62 o 36 6 0 67.11 120.32 42.13 o 38 6 0 127.99 137.73 44.85 o 1 7 0 10.29 -7.05 10.98 o 3 7 0 40.61 18.60 11.62 o 5 7 0 123.38 125.23 13.29 o 7 7 0 1493.62 1566.16 32.13 o 9 7 0 44.30 21.46 15.08 o 11 7 0 33.35 3.74 14.78 o 13 7 0 9796.45 9685.67 110.17 o 15 7 0 43.60 43.34 17.15 o 17 7 0 14082.13 14322.96 154.77 o 19 7 0 2846.09 2847.75 51.11 o 21 7 0 51.44 12.52 20.23 o 23 7 0 152.11 141.64 23.22 o 25 7 0 1509.03 1478.46 44.60 o 27 7 0 29.63 42.20 26.73 o 29 7 0 6.18 16.08 35.95 o 31 7 0 30.72 13.64 38.58 o 33 7 0 1.66 -12.18 38.89 o 35 7 0 118.26 70.93 43.03 o 37 7 0 30.67 -46.67 70.16 o 0 8 0 14.47 31.97 18.45 o 2 8 0 196.31 162.70 15.62 o 4 8 0 480.69 414.99 23.14 o 6 8 0 51.63 42.76 14.56 o 8 8 0 29.14 0.75 15.38 o 10 8 0 5860.17 5838.84 75.79 o 12 8 0 5867.65 6016.59 78.71 o 14 8 0 373.48 314.15 22.47 o 16 8 0 6877.69 6785.69 87.63 o 18 8 0 2332.33 2314.28 47.41 o 20 8 0 2300.50 2366.96 71.05 o 22 8 0 3899.94 3766.76 70.35 o 24 8 0 4.62 16.84 21.97 o 26 8 0 436.90 435.06 35.54 o 28 8 0 29.28 22.97 45.11 o 30 8 0 2.62 -21.42 50.47 o 32 8 0 9.63 12.92 52.13 o 34 8 0 982.51 1048.00 91.38 o 36 8 0 3.04 -5.75 52.82 o 1 9 0 389.02 441.57 20.98 o 3 9 0 685.87 616.36 29.98 o 5 9 0 742.74 642.62 26.50 o 7 9 0 0.31 -7.16 19.36 o 9 9 0 450.54 524.74 25.75 o 11 9 0 1061.94 994.55 37.62 o 13 9 0 87.00 69.69 22.77 o 15 9 0 1468.46 1566.43 45.98 o 17 9 0 5469.17 5747.08 136.05 o 19 9 0 5.23 5.28 22.76 o 21 9 0 1437.38 1402.75 70.49 o 23 9 0 307.94 393.76 36.64 o 25 9 0 21.16 8.64 28.15 o 27 9 0 183.99 185.12 39.30 o 29 9 0 211.80 325.42 43.21 o 31 9 0 0.42 14.65 54.59 o 33 9 0 45.59 35.48 55.25 o 0 10 0 13699.23 12381.87 224.82 o 2 10 0 423.58 339.76 28.93 o 4 10 0 2238.37 2150.72 91.81 o 6 10 0 898.34 706.67 38.67 o 8 10 0 208.64 172.17 25.83 o 10 10 0 3890.75 3650.50 82.23 o 12 10 0 223.18 214.15 58.76 o 14 10 0 584.13 698.48 63.21 o 16 10 0 372.44 438.73 37.16 o 18 10 0 335.53 315.44 35.80 o 20 10 0 38.70 19.23 37.03 o 22 10 0 691.88 699.32 52.81 o 24 10 0 715.21 742.00 67.51 o 26 10 0 20.04 12.43 34.77 o 28 10 0 87.62 89.60 50.68 o 1 11 0 1249.15 1258.69 66.90 o 3 11 0 63.95 -14.89 23.42 o 5 11 0 3348.06 3331.23 79.24 o 7 11 0 1129.87 1091.26 42.14 o 9 11 0 319.37 419.00 37.51 o 11 11 0 919.91 942.85 47.24 o 13 11 0 18.90 1.73 29.18 o 15 11 0 16.76 14.63 31.90 o 17 11 0 456.73 462.95 74.93 o 19 11 0 12.24 -32.79 35.33 o 21 11 0 512.40 551.07 50.27 o 23 11 0 293.83 341.64 56.18 o 25 11 0 1225.23 1354.97 69.82 o 27 11 0 227.72 280.50 59.10 o 29 11 0 255.08 346.47 60.22 o 0 12 0 54.41 102.34 44.23 o 2 12 0 6.18 -18.82 25.43 o 4 12 0 328.64 390.92 37.96 o 6 12 0 435.22 436.69 34.40 o 8 12 0 1159.48 1120.57 52.49 o 10 12 0 1606.09 1575.54 61.92 o 12 12 0 536.35 409.47 45.37 o 14 12 0 262.10 408.66 39.96 o 16 12 0 233.37 193.24 36.20 o 18 12 0 13.28 -26.93 31.85 o 20 12 0 238.72 247.98 44.99 o 22 12 0 199.21 222.79 43.47 o 24 12 0 3205.11 2959.97 116.92 o 26 12 0 47.62 33.98 46.44 o 1 13 0 54.46 54.18 32.27 o 3 13 0 93.46 42.57 31.76 o 5 13 0 3159.86 3076.80 71.82 o 7 13 0 206.73 267.47 38.87 o 9 13 0 1180.85 1112.38 69.76 o 11 13 0 226.56 191.45 37.33 o 13 13 0 833.43 792.80 49.52 o 15 13 0 1514.35 1476.36 99.08 o 17 13 0 2285.46 2286.64 82.94 o 19 13 0 707.12 926.23 67.73 o 21 13 0 28.13 -31.83 37.91 o 0 14 0 4342.17 4631.91 175.37 o 2 14 0 88.61 144.89 41.55 o 4 14 0 280.07 217.75 33.44 o 6 14 0 905.79 866.87 52.00 o 8 14 0 15.44 -31.09 32.94 o 10 14 0 1978.28 2118.52 73.65 o 12 14 0 9.09 9.11 36.00 o 14 14 0 1285.59 1239.44 59.81 o -43 1 1 893.79 968.85 65.24 o -41 1 1 167.48 184.91 35.10 o -39 1 1 3.02 -16.96 31.09 o -37 1 1 246.88 163.52 40.32 o -35 1 1 430.27 348.99 46.48 o -33 1 1 1.25 82.20 35.84 o -31 1 1 380.54 313.54 47.23 o -29 1 1 485.26 565.66 44.00 o -27 1 1 1064.70 1128.13 44.80 o -25 1 1 923.48 909.39 42.17 o -23 1 1 2466.29 2505.33 45.07 o -21 1 1 5.16 60.30 23.94 o -19 1 1 5778.45 6309.90 89.63 o -17 1 1 10008.68 11059.92 113.84 o -15 1 1 11541.87 12500.83 138.71 o -13 1 1 16388.54 16228.13 158.67 o -11 1 1 35383.31 37743.01 355.73 o -9 1 1 15221.61 15322.65 148.09 o -7 1 1 16486.84 16201.32 154.90 o -5 1 1 11047.20 10192.75 125.72 o -3 1 1 2664.22 2524.80 35.20 o 1 1 1 1802.82 2008.62 32.78 o 3 1 1 5048.97 4946.09 50.21 o 5 1 1 41896.53 42945.55 399.63 o 7 1 1 3444.97 4021.63 44.24 o 9 1 1 3.48 -6.33 10.52 o 11 1 1 22396.26 23284.81 366.37 o 13 1 1 2404.90 2820.96 45.71 o 15 1 1 5399.53 5599.29 74.96 o 17 1 1 3079.36 3696.66 48.09 o 19 1 1 254.53 239.85 15.15 o 21 1 1 300.07 267.03 16.29 o 23 1 1 560.82 500.81 23.37 o 25 1 1 0.38 21.83 21.10 o 27 1 1 48.31 -22.54 28.93 o 29 1 1 17.81 27.13 29.31 o 31 1 1 2226.18 2075.81 64.41 o 33 1 1 1604.99 1479.85 72.33 o 35 1 1 55.42 68.52 38.58 o 37 1 1 398.85 299.18 63.26 o 39 1 1 27.38 14.01 39.82 o 41 1 1 707.15 579.84 44.96 o -42 2 1 727.55 669.22 56.79 o -40 2 1 16.04 -38.72 35.70 o -38 2 1 237.20 254.83 43.03 o -36 2 1 10.53 -33.70 27.73 o -34 2 1 29.12 16.66 27.34 o -32 2 1 258.09 245.19 41.95 o -30 2 1 2549.86 2593.13 116.57 o -28 2 1 1529.04 1543.25 67.92 o -26 2 1 1819.10 1877.21 52.82 o -24 2 1 453.44 515.57 29.60 o -22 2 1 6093.99 6596.42 77.54 o -20 2 1 6662.97 6164.23 72.01 o -18 2 1 23934.78 26835.42 260.94 o -16 2 1 778.61 652.60 28.74 o -14 2 1 39033.79 42833.97 405.37 o -12 2 1 3111.30 3383.53 56.26 o -10 2 1 997.16 934.35 18.91 o -8 2 1 2058.84 2411.73 30.66 o -6 2 1 4858.33 4988.76 51.75 o -4 2 1 6066.32 6206.82 61.81 o -2 2 1 1245.76 1212.92 17.75 o 0 2 1 4598.87 4860.35 49.83 o 2 2 1 82151.07 83415.96 983.39 o 4 2 1 645.89 635.88 14.09 o 6 2 1 30904.89 32492.65 305.40 o 8 2 1 10612.59 11932.98 118.18 o 10 2 1 21490.46 22661.91 217.40 o 12 2 1 386.89 381.40 16.70 o 14 2 1 288.60 323.78 28.96 o 16 2 1 18131.11 18829.44 227.26 o 18 2 1 5479.22 5388.56 64.69 o 20 2 1 773.10 868.49 24.85 o 22 2 1 5219.36 4795.79 61.65 o 24 2 1 51.83 33.20 17.46 o 26 2 1 18.92 47.78 21.67 o 28 2 1 1886.35 1893.62 72.36 o 30 2 1 79.25 64.25 33.63 o 32 2 1 159.24 133.93 37.43 o 34 2 1 11.36 -25.32 35.61 o 36 2 1 280.23 275.16 43.95 o 38 2 1 51.64 75.30 53.56 o 40 2 1 314.35 260.14 46.69 o 42 2 1 295.32 232.31 47.30 o -43 3 1 55.40 -58.45 49.07 o -41 3 1 225.34 172.67 42.20 o -39 3 1 544.17 470.22 54.80 o -37 3 1 1078.97 1007.03 61.03 o -35 3 1 3062.27 3127.49 100.06 o -33 3 1 442.50 503.09 49.34 o -31 3 1 400.10 377.45 95.14 o -29 3 1 2145.90 2076.82 167.33 o -27 3 1 353.55 329.04 31.23 o -25 3 1 10490.48 10423.71 118.16 o -23 3 1 1575.01 1580.85 47.87 o -21 3 1 5429.19 5402.60 61.60 o -19 3 1 5211.39 4998.54 57.11 o -17 3 1 1706.32 1710.96 30.95 o -15 3 1 388.76 224.02 14.38 o -13 3 1 3999.72 4635.52 55.04 o -11 3 1 12421.33 13123.23 131.00 o -9 3 1 1812.51 1953.91 29.17 o -7 3 1 5527.19 5742.12 60.48 o -5 3 1 2210.21 1966.10 33.87 o -3 3 1 4308.30 3911.44 36.88 o -1 3 1 232.69 167.09 9.45 o 1 3 1 22473.97 22804.23 195.65 o 3 3 1 38177.89 39316.14 350.43 o 5 3 1 2074.53 2245.64 28.21 o 7 3 1 6374.25 6361.25 68.80 o 9 3 1 260.25 192.40 14.66 o 11 3 1 9705.28 10501.92 108.64 o 13 3 1 12564.49 12724.63 130.01 o 15 3 1 530.99 451.58 17.40 o 17 3 1 117.33 77.95 17.08 o 19 3 1 306.29 435.72 18.91 o 21 3 1 78.00 106.37 14.99 o 23 3 1 1727.34 1636.45 34.89 o 25 3 1 287.76 336.93 28.31 o 27 3 1 3010.13 2927.81 65.69 o 29 3 1 1.84 50.33 34.86 o 31 3 1 1208.38 1182.50 65.27 o 33 3 1 422.49 523.31 50.48 o 35 3 1 971.36 990.32 62.38 o 37 3 1 536.49 586.65 73.45 o 39 3 1 9.09 21.22 37.70 o 41 3 1 197.56 311.77 51.17 o -42 4 1 28.99 67.30 43.00 o -40 4 1 4.93 -56.04 37.36 o -38 4 1 1230.91 1065.33 63.66 o -36 4 1 52.13 31.69 36.13 o -34 4 1 3889.29 3876.05 158.89 o -32 4 1 90.07 160.49 42.46 o -30 4 1 6649.55 6891.35 151.33 o -28 4 1 666.53 714.29 37.26 o -26 4 1 2583.12 2716.18 54.03 o -24 4 1 701.55 562.66 26.85 o -22 4 1 523.87 524.00 25.29 o -20 4 1 15511.87 16097.06 165.46 o -18 4 1 80.36 85.27 14.42 o -16 4 1 18527.53 20194.59 200.28 o -14 4 1 7904.04 8064.41 88.66 o -12 4 1 2921.64 3113.52 47.72 o -10 4 1 12592.34 12465.94 126.48 o -8 4 1 15.40 10.86 10.01 o -6 4 1 14811.13 15154.29 146.89 o -4 4 1 106.45 123.57 9.24 o -2 4 1 7918.50 7505.61 70.79 o 0 4 1 4464.40 4422.76 45.98 o 2 4 1 435.94 398.07 12.24 o 4 4 1 16114.96 16689.45 173.87 o 6 4 1 4206.95 4630.48 50.04 o 8 4 1 9057.29 8631.47 91.93 o 10 4 1 827.69 1077.14 25.61 o 12 4 1 10786.99 10721.21 112.89 o 14 4 1 3140.92 3573.64 49.08 o 16 4 1 3467.68 3523.53 49.91 o 18 4 1 7507.46 7691.24 88.93 o 20 4 1 83.20 41.45 15.38 o 22 4 1 13681.10 13085.08 140.90 o 24 4 1 955.50 926.43 38.62 o 26 4 1 1773.50 1844.22 53.17 o 28 4 1 2238.71 2233.37 60.57 o 30 4 1 1696.48 1831.93 76.11 o 32 4 1 3540.70 3510.41 105.43 o 34 4 1 1861.14 1841.55 141.93 o 36 4 1 1549.94 1575.32 78.27 o 38 4 1 73.67 105.99 39.46 o 40 4 1 274.26 284.50 45.78 o -41 5 1 5.78 -19.15 40.51 o -39 5 1 11.54 22.57 57.73 o -37 5 1 994.49 960.12 64.78 o -35 5 1 3268.47 3301.23 120.20 o -33 5 1 38.94 -24.19 36.27 o -31 5 1 1895.46 2033.12 84.36 o -29 5 1 427.56 418.65 45.28 o -27 5 1 12.48 -28.42 18.95 o -25 5 1 3290.41 3425.37 61.90 o -23 5 1 437.01 543.93 27.72 o -21 5 1 5754.49 6117.50 77.41 o -19 5 1 9333.80 9479.01 106.75 o -17 5 1 11658.37 12480.35 132.94 o -15 5 1 16369.62 17154.76 174.47 o -13 5 1 6182.24 6474.15 75.82 o -11 5 1 19690.93 20282.66 200.83 o -9 5 1 5617.49 5995.30 79.30 o -7 5 1 3264.08 2974.87 40.31 o -5 5 1 12559.86 11942.37 110.56 o -3 5 1 3914.03 3919.77 43.94 o -1 5 1 227.79 83.80 10.18 o 1 5 1 1438.67 1455.72 24.29 o 3 5 1 343.34 156.78 11.64 o 5 5 1 6079.77 6291.56 65.61 o 7 5 1 11250.29 10737.69 104.70 o 9 5 1 12133.04 12668.46 131.19 o 11 5 1 5990.75 6229.36 73.68 o 13 5 1 21588.88 21459.51 213.81 o 15 5 1 302.54 379.98 19.56 o 17 5 1 17803.06 17977.68 184.51 o 19 5 1 48.29 66.88 16.83 o 21 5 1 16020.04 16664.88 175.49 o 23 5 1 2365.03 2412.07 66.24 o 25 5 1 3823.73 3928.82 80.17 o 27 5 1 4920.28 5064.07 95.16 o 29 5 1 0.49 5.78 36.25 o 31 5 1 5027.51 5149.10 130.66 o 33 5 1 848.31 890.84 65.40 o 35 5 1 3453.93 3290.04 105.82 o 37 5 1 2112.26 2096.24 87.04 o 39 5 1 1611.46 1350.12 73.60 o -40 6 1 204.11 295.99 51.36 o -38 6 1 91.48 100.25 45.87 o -36 6 1 72.97 97.57 45.50 o -34 6 1 1991.19 2262.12 87.26 o -32 6 1 43.14 23.17 57.81 o -30 6 1 4733.62 4837.70 123.50 o -28 6 1 872.77 900.67 64.80 o -26 6 1 528.84 594.08 30.05 o -24 6 1 3281.69 3182.29 77.79 o -22 6 1 544.54 478.93 27.72 o -20 6 1 34709.61 36432.04 356.46 o -18 6 1 754.51 821.93 28.14 o -16 6 1 6717.71 7043.59 85.18 o -14 6 1 9985.20 9738.70 108.58 o -12 6 1 2432.09 2699.79 45.64 o -10 6 1 24545.84 24250.91 235.19 o -8 6 1 2773.99 2302.92 36.99 o -6 6 1 5472.93 4780.22 58.53 o -4 6 1 867.13 960.42 22.15 o 0 6 1 8101.40 9750.59 94.16 o 2 6 1 1913.54 2325.01 33.23 o 4 6 1 6615.46 6199.56 65.58 o 6 6 1 2.12 16.28 10.51 o 8 6 1 19417.20 20257.84 202.69 o 10 6 1 898.39 990.63 27.60 o 12 6 1 35349.29 35022.40 339.62 o 14 6 1 900.01 944.47 29.20 o 16 6 1 1935.79 1888.59 39.44 o 18 6 1 12492.18 13358.65 145.24 o 20 6 1 421.44 387.15 23.77 o 22 6 1 3663.93 3738.29 59.16 o 24 6 1 252.39 242.11 25.49 o 26 6 1 1346.93 1372.16 51.08 o 28 6 1 2049.39 2333.34 64.23 o 30 6 1 1056.69 1125.16 62.75 o 32 6 1 2396.04 2251.06 85.28 o 34 6 1 213.19 238.01 45.98 o 36 6 1 942.80 974.70 79.40 o 38 6 1 222.34 343.43 76.34 o -39 7 1 597.74 646.59 86.03 o -37 7 1 768.52 666.92 86.22 o -35 7 1 2441.48 2497.60 136.44 o -33 7 1 889.38 942.13 60.85 o -31 7 1 255.21 296.98 46.61 o -29 7 1 3719.78 3853.98 108.39 o -27 7 1 18.60 2.45 23.13 o -25 7 1 4132.95 4602.21 78.84 o -23 7 1 1.59 22.54 22.60 o -21 7 1 1033.03 1136.95 35.24 o -19 7 1 2802.38 2925.19 59.57 o -17 7 1 297.91 259.63 21.49 o -15 7 1 6987.55 7526.61 91.52 o -13 7 1 5881.32 5793.25 74.39 o -11 7 1 14316.15 14394.65 137.31 o -9 7 1 5257.98 5187.82 65.71 o -7 7 1 8494.17 8215.10 92.01 o -5 7 1 2725.30 2417.61 36.07 o -3 7 1 4267.09 4263.78 51.47 o -1 7 1 2217.64 1708.19 29.87 o 1 7 1 13.93 -0.44 11.47 o 3 7 1 10133.90 9489.91 94.96 o 5 7 1 6370.70 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