# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' G7-22 IPDS2 -100DEGC' _shelx_refln_list_code 4 _shelx_F_calc_maximum 64.02 _exptl_crystal_F_000 312.00 _reflns_d_resolution_high 0.8356 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 14.6060 _cell_length_b 3.9970 _cell_length_c 11.5650 _cell_angle_alpha 90.000 _cell_angle_beta 94.470 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 52.94 70.47 2.87 o 4 0 0 708.07 806.02 7.55 o 5 0 0 1912.06 2188.01 11.08 o 6 0 0 324.14 244.11 3.75 o 7 0 0 574.48 535.15 5.59 o 8 0 0 521.36 647.49 5.96 o 9 0 0 231.76 194.22 3.24 o 10 0 0 16.73 17.56 1.62 o 11 0 0 633.10 573.38 5.30 o 12 0 0 313.87 298.48 3.94 o 13 0 0 0.22 0.80 1.52 o 14 0 0 2.23 4.27 1.61 o 15 0 0 29.53 34.61 2.54 o 16 0 0 4.18 3.62 1.57 o 17 0 0 94.23 96.24 9.16 o 1 1 0 1445.70 1595.71 32.34 o 2 1 0 4098.78 4415.52 36.71 o 3 1 0 10.36 32.90 10.97 o 4 1 0 588.80 559.42 24.83 o 5 1 0 870.85 725.15 132.30 o 6 1 0 9.47 7.76 1.14 o 7 1 0 641.25 547.01 4.32 o 8 1 0 3.45 1.75 1.33 o 9 1 0 18.24 12.14 1.48 o 10 1 0 230.37 206.08 2.72 o 11 1 0 329.20 285.08 2.92 o 12 1 0 124.07 108.39 1.95 o 13 1 0 439.65 409.16 3.66 o 14 1 0 40.41 35.35 1.55 o 15 1 0 13.39 13.21 1.79 o 16 1 0 40.59 57.24 2.33 o 0 2 0 661.79 607.52 43.83 o 1 2 0 350.85 326.36 10.61 o 2 2 0 1.28 0.30 0.59 o 3 2 0 25.67 29.38 2.68 o 4 2 0 23.71 21.54 1.56 o 5 2 0 190.24 151.40 6.32 o 6 2 0 680.17 648.55 86.51 o 7 2 0 44.98 43.63 2.59 o 8 2 0 80.55 72.52 1.37 o 9 2 0 314.89 286.82 2.96 o 10 2 0 8.09 7.25 1.15 o 11 2 0 724.12 663.77 3.94 o 12 2 0 177.78 166.27 2.23 o 13 2 0 21.32 20.32 1.33 o 14 2 0 32.24 32.37 1.50 o 15 2 0 49.01 41.45 1.67 o 1 3 0 10.38 11.63 0.80 o 2 3 0 142.84 137.24 1.41 o 3 3 0 4.28 4.27 0.92 o 4 3 0 213.80 218.13 2.64 o 5 3 0 8.07 7.74 0.82 o 6 3 0 18.51 18.62 2.65 o 7 3 0 90.41 96.32 7.93 o 8 3 0 27.07 27.80 4.30 o 9 3 0 85.42 89.05 10.70 o 10 3 0 1.26 0.84 1.02 o 11 3 0 0.06 -0.92 1.68 o 12 3 0 3.58 4.81 1.25 o 13 3 0 40.88 38.00 1.60 o 0 4 0 25.38 28.69 1.34 o 1 4 0 27.45 32.14 1.01 o 2 4 0 2.11 1.56 0.97 o 3 4 0 34.69 38.01 1.15 o 4 4 0 0.27 0.04 1.03 o 5 4 0 39.87 44.56 8.09 o 6 4 0 15.46 19.29 2.12 o 7 4 0 5.68 8.01 1.06 o 8 4 0 0.36 -0.10 1.26 o 9 4 0 5.96 6.76 1.11 o -17 1 1 8.63 11.72 2.00 o -16 1 1 0.59 0.52 1.77 o -15 1 1 36.24 33.36 1.99 o -14 1 1 7.51 8.14 1.26 o -13 1 1 14.14 13.09 1.21 o -12 1 1 13.85 12.92 1.65 o -11 1 1 8.53 6.34 1.15 o -10 1 1 130.05 112.17 1.94 o -9 1 1 114.23 119.58 2.30 o -8 1 1 35.86 35.60 1.25 o -7 1 1 335.01 322.38 4.77 o -6 1 1 148.33 126.98 8.32 o -5 1 1 129.70 109.05 6.69 o -4 1 1 5.22 6.70 1.05 o -3 1 1 8.69 7.40 0.68 o -2 1 1 1783.12 1666.16 147.99 o -1 1 1 1263.88 1571.24 37.23 o 1 1 1 665.41 794.06 5.56 o 2 1 1 61.30 56.90 0.98 o 3 1 1 368.24 406.77 9.06 o 4 1 1 454.26 499.39 32.23 o 5 1 1 128.09 139.53 14.00 o 6 1 1 229.66 250.18 26.44 o 7 1 1 714.13 746.05 34.60 o 8 1 1 552.20 541.27 17.65 o 9 1 1 0.26 1.04 0.95 o 10 1 1 30.93 28.11 1.34 o 11 1 1 62.05 60.11 1.67 o 12 1 1 31.28 25.55 1.35 o 13 1 1 1.45 1.31 1.09 o 14 1 1 85.99 84.56 2.23 o 15 1 1 4.45 4.54 1.22 o 16 1 1 11.86 10.75 1.87 o -15 2 1 35.25 32.20 1.57 o -14 2 1 24.65 24.75 1.45 o -13 2 1 81.76 79.96 1.78 o -12 2 1 40.67 42.59 1.48 o -11 2 1 46.31 40.08 1.42 o -10 2 1 13.81 11.90 1.14 o -9 2 1 151.48 130.01 3.71 o -8 2 1 440.57 386.86 3.35 o -7 2 1 64.10 54.32 3.88 o -6 2 1 123.43 114.14 8.17 o -5 2 1 280.72 278.36 24.70 o -4 2 1 9.64 9.45 0.68 o -3 2 1 560.24 545.54 59.28 o -2 2 1 94.78 110.40 7.17 o -1 2 1 0.54 2.60 0.61 o 0 2 1 0.05 0.74 0.74 o 1 2 1 83.74 75.48 0.99 o 2 2 1 224.85 203.29 5.69 o 3 2 1 795.28 708.34 33.55 o 4 2 1 105.08 96.76 4.23 o 5 2 1 268.46 260.33 6.94 o 6 2 1 367.09 351.65 40.48 o 7 2 1 91.88 88.11 3.28 o 8 2 1 49.32 46.28 3.82 o 9 2 1 197.12 182.04 2.20 o 10 2 1 0.57 1.16 1.03 o 11 2 1 4.95 5.32 1.58 o 12 2 1 0.60 1.26 1.12 o 13 2 1 0.45 0.06 1.14 o 14 2 1 13.06 12.10 1.31 o 15 2 1 16.16 14.58 1.41 o -13 3 1 9.48 11.08 1.88 o -12 3 1 12.91 13.65 1.34 o -11 3 1 192.96 190.81 9.23 o -10 3 1 29.89 35.67 3.91 o -9 3 1 8.13 9.58 1.06 o -8 3 1 119.49 119.09 2.67 o -7 3 1 184.34 193.01 24.54 o -6 3 1 8.83 8.83 1.49 o -5 3 1 45.68 40.76 1.56 o -4 3 1 474.26 470.90 17.93 o -3 3 1 170.70 179.06 5.37 o -2 3 1 159.38 148.29 6.03 o -1 3 1 163.69 153.03 7.35 o 0 3 1 5.52 7.49 0.95 o 1 3 1 60.46 54.07 1.49 o 2 3 1 183.39 168.96 6.15 o 3 3 1 114.11 110.89 5.90 o 4 3 1 285.52 286.87 3.72 o 5 3 1 213.57 241.60 29.12 o 6 3 1 0.80 0.05 0.76 o 7 3 1 136.29 139.22 2.30 o 8 3 1 135.93 140.57 16.95 o 9 3 1 95.18 104.73 5.67 o 10 3 1 4.60 5.66 1.19 o 11 3 1 45.11 43.66 1.53 o 12 3 1 1.45 1.87 1.24 o 13 3 1 17.34 16.29 1.95 o -9 4 1 115.31 143.29 12.71 o -8 4 1 57.10 60.96 1.65 o -7 4 1 2.96 3.21 1.04 o -6 4 1 124.07 152.81 21.53 o -5 4 1 50.78 63.39 9.46 o -4 4 1 39.30 39.29 1.18 o -3 4 1 57.84 69.22 7.17 o -2 4 1 15.86 20.57 2.45 o -1 4 1 0.73 2.40 0.97 o 0 4 1 41.56 47.57 1.45 o 1 4 1 16.70 20.07 1.89 o 2 4 1 113.28 117.31 2.41 o 3 4 1 111.03 129.16 1.75 o 4 4 1 4.66 2.75 4.05 o 5 4 1 5.78 9.09 0.91 o 6 4 1 83.78 99.30 12.85 o 7 4 1 5.87 5.14 2.87 o 8 4 1 2.19 2.99 1.28 o 9 4 1 26.13 31.01 1.49 o -17 0 2 49.81 49.23 2.99 o -16 0 2 2.12 0.86 1.25 o -15 0 2 165.18 167.03 8.00 o -14 0 2 161.34 153.71 14.20 o -13 0 2 30.87 27.78 3.39 o -12 0 2 879.63 906.84 166.23 o -11 0 2 385.26 404.49 77.15 o -10 0 2 226.38 194.03 3.26 o -4 0 2 5.71 8.14 1.44 o -3 0 2 3293.45 3549.34 10.57 o -2 0 2 88.23 91.48 3.81 o -1 0 2 2959.27 3394.31 10.96 o 0 0 2 631.59 654.39 16.44 o 2 0 2 19.06 19.65 2.29 o 3 0 2 22.41 19.93 4.42 o 4 0 2 178.96 116.15 10.33 o 5 0 2 1355.77 1476.43 101.55 o 6 0 2 2174.32 2092.25 587.36 o 7 0 2 664.63 806.98 65.09 o 8 0 2 948.59 981.28 56.19 o 9 0 2 285.62 238.46 3.46 o 10 0 2 34.25 30.58 1.73 o 11 0 2 488.16 509.77 4.36 o 12 0 2 1037.63 985.26 6.15 o 13 0 2 9.81 9.92 1.69 o 14 0 2 198.77 179.78 3.30 o 15 0 2 12.72 23.27 2.40 o 16 0 2 1.11 3.39 2.58 o -16 1 2 52.46 57.06 2.27 o -15 1 2 0.11 0.28 1.67 o -14 1 2 67.34 57.58 1.74 o -13 1 2 106.68 95.49 1.92 o -12 1 2 453.51 398.72 5.53 o -11 1 2 9.28 7.14 0.82 o -10 1 2 560.43 446.54 6.33 o -9 1 2 137.55 132.69 1.79 o -8 1 2 1030.47 845.68 25.91 o -7 1 2 592.56 420.06 90.03 o -6 1 2 204.54 152.52 18.66 o -5 1 2 815.62 684.72 163.52 o -4 1 2 4.37 1.95 0.98 o -3 1 2 116.76 103.71 16.95 o -2 1 2 392.63 375.60 22.13 o 0 1 2 1739.36 2028.93 72.26 o 1 1 2 1782.32 2081.63 11.04 o 2 1 2 42.43 42.84 1.66 o 3 1 2 598.30 643.14 26.54 o 4 1 2 1528.33 1492.51 232.78 o 5 1 2 540.10 478.49 48.22 o 6 1 2 40.20 39.38 3.74 o 7 1 2 62.51 47.15 2.49 o 8 1 2 97.62 80.70 2.70 o 9 1 2 76.20 72.77 3.12 o 10 1 2 1031.43 937.71 24.37 o 11 1 2 436.32 443.42 3.78 o 12 1 2 2.92 2.83 1.51 o 13 1 2 58.41 66.56 2.04 o 14 1 2 25.62 28.24 1.84 o 15 1 2 18.80 17.75 1.43 o 16 1 2 72.16 88.26 2.59 o -15 2 2 4.50 6.33 1.80 o -14 2 2 127.25 108.88 2.03 o -13 2 2 1.67 2.22 1.20 o -12 2 2 12.09 9.68 1.20 o -11 2 2 4.98 5.56 1.55 o -10 2 2 39.21 36.97 1.40 o -9 2 2 0.80 0.22 0.85 o -8 2 2 24.57 21.98 1.40 o -7 2 2 0.16 0.51 0.63 o -6 2 2 380.66 328.83 17.39 o -5 2 2 192.72 193.94 15.52 o -4 2 2 413.84 454.23 52.81 o -3 2 2 1360.56 1528.03 148.72 o -2 2 2 191.85 198.43 20.47 o -1 2 2 1622.11 1688.42 135.47 o 0 2 2 686.68 706.47 63.93 o 1 2 2 209.92 213.89 12.01 o 2 2 2 88.69 80.85 1.91 o 3 2 2 1169.10 1056.11 42.55 o 4 2 2 5.22 7.82 1.12 o 5 2 2 108.88 99.20 7.23 o 6 2 2 396.28 342.21 23.40 o 7 2 2 105.39 101.52 13.31 o 8 2 2 110.31 92.55 3.33 o 9 2 2 11.78 10.21 1.08 o 10 2 2 87.36 82.48 2.08 o 11 2 2 1.21 1.28 1.09 o 12 2 2 174.17 186.98 2.50 o 13 2 2 18.33 19.39 1.79 o 14 2 2 1.26 2.18 1.24 o 15 2 2 21.61 20.03 1.49 o -13 3 2 48.90 46.42 1.61 o -12 3 2 20.57 18.48 1.38 o -11 3 2 2.73 1.44 1.24 o -10 3 2 0.09 0.59 0.95 o -9 3 2 0.72 0.81 0.94 o -8 3 2 43.45 45.01 0.97 o -7 3 2 122.43 134.02 16.74 o -6 3 2 3.50 2.32 0.77 o -5 3 2 0.12 2.85 1.87 o -4 3 2 31.86 35.94 2.49 o -3 3 2 9.77 8.64 1.60 o -2 3 2 278.28 265.25 6.11 o -1 3 2 110.43 102.23 2.78 o 0 3 2 16.94 18.03 0.94 o 1 3 2 7.90 7.34 1.17 o 2 3 2 2.78 3.05 0.73 o 3 3 2 0.00 -0.15 0.74 o 4 3 2 160.91 151.38 3.21 o 5 3 2 178.20 187.95 9.34 o 6 3 2 0.16 0.10 0.76 o 7 3 2 14.46 14.82 0.86 o 8 3 2 50.17 54.30 1.36 o 9 3 2 53.85 55.07 2.38 o 10 3 2 149.98 149.86 6.13 o 11 3 2 1.13 0.67 1.25 o 12 3 2 0.38 0.27 1.26 o 13 3 2 0.29 0.81 1.30 o -9 4 2 8.32 8.51 2.07 o -8 4 2 29.83 31.85 4.50 o -7 4 2 0.10 0.75 0.89 o -6 4 2 2.19 3.13 1.03 o -5 4 2 13.30 13.44 2.02 o -4 4 2 16.89 18.65 1.77 o -3 4 2 7.82 8.01 0.78 o -2 4 2 0.00 0.18 0.73 o -1 4 2 0.25 0.25 0.73 o 0 4 2 11.98 13.12 0.87 o 1 4 2 0.01 0.62 0.73 o 2 4 2 13.43 14.30 1.45 o 3 4 2 0.03 0.43 0.75 o 4 4 2 4.21 4.97 0.99 o 5 4 2 5.66 6.52 0.88 o 6 4 2 9.85 13.21 1.27 o 7 4 2 2.84 2.62 1.03 o 8 4 2 24.38 27.93 2.48 o -16 1 3 0.04 0.41 1.28 o -15 1 3 1.31 0.61 1.17 o -14 1 3 21.31 20.28 1.05 o -13 1 3 27.42 28.95 1.11 o -12 1 3 281.02 265.18 12.18 o -11 1 3 1.66 1.77 0.85 o -10 1 3 19.88 20.92 1.12 o -9 1 3 3.16 2.08 1.01 o -8 1 3 40.14 25.57 1.29 o -7 1 3 6.07 10.88 1.06 o -6 1 3 59.67 51.28 1.07 o -5 1 3 150.66 141.07 19.83 o -4 1 3 783.22 796.69 140.29 o -3 1 3 14.16 13.61 3.00 o -2 1 3 572.28 575.06 110.10 o -1 1 3 2658.88 2974.90 170.81 o 0 1 3 147.23 169.58 4.07 o 1 1 3 423.02 477.15 2.66 o 2 1 3 1284.01 1394.01 31.28 o 3 1 3 297.47 321.89 12.35 o 4 1 3 444.02 417.88 51.28 o 5 1 3 0.14 2.08 0.85 o 6 1 3 137.81 133.13 16.72 o 7 1 3 67.58 85.38 6.70 o 8 1 3 13.28 14.45 1.24 o 9 1 3 12.34 13.57 0.87 o 10 1 3 13.98 13.59 0.84 o 11 1 3 26.33 22.02 2.49 o 12 1 3 27.48 24.97 2.29 o 13 1 3 1.04 0.78 1.56 o 14 1 3 0.27 -0.01 1.66 o 15 1 3 1.19 0.57 1.23 o 16 1 3 25.13 29.01 2.17 o -15 2 3 13.00 12.23 1.86 o -14 2 3 20.03 18.82 1.82 o -13 2 3 3.64 4.32 1.19 o -12 2 3 226.76 212.00 8.06 o -11 2 3 36.54 37.48 2.78 o -10 2 3 52.21 49.65 4.71 o -9 2 3 7.04 7.18 0.90 o -8 2 3 154.84 178.83 17.72 o -7 2 3 0.01 0.99 0.63 o -6 2 3 119.11 131.00 14.78 o -5 2 3 19.88 18.36 1.80 o -4 2 3 114.39 156.69 14.25 o -3 2 3 840.40 875.77 13.02 o -2 2 3 46.90 49.66 1.28 o -1 2 3 1863.29 1958.49 116.87 o 0 2 3 72.17 58.35 1.13 o 1 2 3 0.42 3.65 0.73 o 2 2 3 9.13 9.66 1.36 o 3 2 3 254.16 208.78 10.97 o 4 2 3 275.12 267.03 11.48 o 5 2 3 6.85 9.85 0.69 o 6 2 3 180.45 168.21 4.36 o 7 2 3 284.34 259.07 4.25 o 8 2 3 58.03 54.00 1.78 o 9 2 3 188.59 183.75 3.81 o 10 2 3 67.76 63.58 2.27 o 11 2 3 41.58 44.79 2.53 o 12 2 3 1.37 0.46 0.83 o 13 2 3 10.87 10.51 1.76 o 14 2 3 38.31 44.31 2.08 o -13 3 3 72.20 70.81 1.83 o -12 3 3 0.53 1.29 1.24 o -11 3 3 30.69 29.07 2.44 o -10 3 3 171.82 198.88 17.51 o -9 3 3 186.51 201.57 18.52 o -8 3 3 18.54 21.71 2.04 o -7 3 3 162.07 187.90 23.07 o -6 3 3 7.68 7.74 0.67 o -5 3 3 28.76 29.98 0.75 o -4 3 3 69.94 64.22 0.98 o -3 3 3 39.50 38.40 1.27 o -2 3 3 56.22 56.41 6.33 o -1 3 3 23.85 25.57 1.88 o 0 3 3 13.03 14.13 1.62 o 1 3 3 276.12 257.46 1.40 o 2 3 3 116.98 111.60 2.54 o 3 3 3 2.10 2.26 0.75 o 4 3 3 60.35 61.26 0.99 o 5 3 3 202.19 206.19 5.51 o 6 3 3 1.36 1.86 0.68 o 7 3 3 79.27 75.64 3.24 o 8 3 3 141.99 147.37 3.97 o 9 3 3 9.64 9.85 0.89 o 10 3 3 246.06 255.76 3.20 o 11 3 3 21.63 21.79 1.42 o 12 3 3 47.47 44.20 1.62 o -8 4 3 18.81 19.53 1.04 o -7 4 3 2.59 2.59 0.90 o -6 4 3 20.20 26.40 2.75 o -5 4 3 40.90 43.95 0.91 o -4 4 3 0.14 -0.22 0.76 o -3 4 3 43.27 45.71 1.24 o -2 4 3 34.20 37.54 0.88 o -1 4 3 91.40 104.31 3.29 o 0 4 3 144.50 162.12 3.65 o 1 4 3 4.52 8.11 1.01 o 2 4 3 14.24 15.13 0.84 o 3 4 3 152.41 164.71 3.20 o 4 4 3 20.99 20.23 2.21 o 5 4 3 19.43 20.75 0.81 o 6 4 3 52.15 59.50 3.89 o 7 4 3 23.95 24.51 1.80 o 8 4 3 39.65 39.98 1.22 o -16 0 4 0.83 0.74 1.04 o -15 0 4 185.67 203.32 29.66 o -14 0 4 10.53 10.33 2.91 o -13 0 4 211.61 179.58 2.31 o -12 0 4 185.77 238.74 2.70 o -11 0 4 735.67 563.57 3.49 o -10 0 4 48.21 67.66 1.87 o -9 0 4 1235.50 1097.77 4.55 o -8 0 4 585.60 519.45 3.18 o -7 0 4 15.12 15.49 1.14 o -6 0 4 1739.52 1642.59 5.50 o -5 0 4 82.15 114.58 2.17 o -4 0 4 2316.17 2767.91 7.30 o -3 0 4 842.94 831.18 29.75 o -2 0 4 1436.98 1589.64 3.92 o -1 0 4 60.83 66.30 1.22 o 0 0 4 917.07 1081.45 10.60 o 1 0 4 136.25 117.21 13.02 o 3 0 4 2069.28 2069.82 187.00 o 4 0 4 292.63 284.38 50.08 o 5 0 4 331.24 273.62 18.86 o 6 0 4 1381.17 1120.50 94.65 o 7 0 4 65.21 78.54 10.95 o 8 0 4 152.41 195.24 18.50 o 9 0 4 1227.55 1287.56 32.25 o 10 0 4 793.35 687.91 108.86 o 11 0 4 4.56 5.40 1.13 o 12 0 4 75.59 79.81 4.24 o 13 0 4 43.65 43.21 2.00 o 14 0 4 99.75 109.67 2.67 o 15 0 4 80.31 81.11 2.72 o 16 0 4 1.54 1.08 2.31 o -16 1 4 52.78 48.49 1.89 o -15 1 4 34.70 26.90 1.32 o -14 1 4 5.56 7.61 1.00 o -13 1 4 172.28 173.41 26.28 o -12 1 4 7.18 6.75 1.60 o -11 1 4 54.69 44.33 1.50 o -10 1 4 109.32 124.61 2.25 o -9 1 4 6.93 4.29 1.07 o -8 1 4 594.54 472.85 3.28 o -7 1 4 895.01 817.30 117.43 o -6 1 4 227.00 180.77 7.11 o -5 1 4 498.56 440.51 26.55 o -4 1 4 1689.15 1494.08 200.62 o -3 1 4 95.39 75.15 1.11 o -2 1 4 469.72 476.67 20.75 o -1 1 4 223.72 212.26 5.30 o 0 1 4 774.55 936.93 15.77 o 1 1 4 169.43 149.54 15.55 o 2 1 4 815.53 863.06 42.34 o 3 1 4 299.08 314.37 1.67 o 4 1 4 1648.93 1661.49 155.35 o 5 1 4 1252.06 1213.35 78.88 o 6 1 4 66.09 75.13 5.54 o 7 1 4 1128.74 945.64 96.46 o 8 1 4 15.92 11.42 0.81 o 9 1 4 21.18 23.81 1.65 o 10 1 4 57.76 58.27 2.85 o 11 1 4 462.22 398.43 30.24 o 12 1 4 5.22 5.27 1.13 o 13 1 4 109.79 110.15 9.27 o 14 1 4 0.36 1.05 1.69 o 15 1 4 26.98 25.18 2.05 o -15 2 4 46.98 48.28 1.69 o -14 2 4 33.08 28.34 1.47 o -13 2 4 0.44 0.25 1.30 o -12 2 4 48.94 47.42 7.93 o -11 2 4 4.71 5.25 0.93 o -10 2 4 170.87 198.13 25.86 o -9 2 4 642.25 607.18 93.13 o -8 2 4 131.12 115.71 8.80 o -7 2 4 22.34 25.41 0.97 o -6 2 4 155.17 156.93 21.09 o -5 2 4 162.00 195.07 9.03 o -4 2 4 65.00 51.71 0.97 o -3 2 4 259.75 239.28 23.25 o -2 2 4 1846.63 1748.75 93.00 o -1 2 4 561.13 580.26 9.65 o 0 2 4 490.56 477.19 4.74 o 1 2 4 1.50 4.69 0.76 o 2 2 4 25.00 19.34 0.82 o 3 2 4 579.95 514.06 29.51 o 4 2 4 189.45 173.59 12.05 o 5 2 4 234.99 230.47 17.25 o 6 2 4 5.98 5.20 0.72 o 7 2 4 0.53 1.89 0.65 o 8 2 4 299.54 269.81 3.34 o 9 2 4 349.73 324.21 8.53 o 10 2 4 20.11 21.63 0.90 o 11 2 4 35.31 36.90 2.43 o 12 2 4 4.69 4.02 0.86 o 13 2 4 21.25 24.37 1.31 o 14 2 4 42.96 49.95 2.13 o -12 3 4 1.91 1.64 0.96 o -11 3 4 13.53 15.51 1.61 o -10 3 4 4.93 4.02 0.77 o -9 3 4 3.04 1.93 0.74 o -8 3 4 4.24 4.37 0.68 o -7 3 4 118.52 120.06 4.44 o -6 3 4 8.48 9.19 0.68 o -5 3 4 15.87 16.19 1.58 o -4 3 4 106.81 108.35 4.37 o -3 3 4 53.81 52.26 3.67 o -2 3 4 349.33 330.79 9.68 o -1 3 4 57.59 63.39 6.06 o 0 3 4 21.96 23.19 1.74 o 1 3 4 2.49 2.77 0.64 o 2 3 4 18.93 20.62 0.78 o 3 3 4 18.85 18.66 0.75 o 4 3 4 32.21 30.55 0.79 o 5 3 4 26.56 27.18 0.75 o 6 3 4 5.20 4.69 0.79 o 7 3 4 25.76 24.30 1.18 o 8 3 4 21.31 21.83 1.22 o 9 3 4 7.16 7.52 0.78 o 10 3 4 81.52 83.40 2.06 o 11 3 4 4.69 4.95 1.30 o 12 3 4 4.10 4.08 1.09 o -8 4 4 16.44 16.44 0.93 o -7 4 4 13.43 13.42 1.16 o -6 4 4 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