Acta Cryst. (2009). E65, i67  [ doi:10.1107/S160053680903147X ]

Cs₂Bi(PO₄)(WO₄)

K. V. Terebilenko, I. V. Zatovsky, V. N. Baumer and N. S. Slobodyanik

Online 15 August 2009

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (W-O) = 0.009 Å
• R factor = 0.052
• wR factor = 0.115
• Data-to-parameter ratio = 22.9

checkCIF/PLATON results

No syntax errors found



Alert level A
DIFF020_ALERT_1_A  _diffrn_standards_interval_count and
            _diffrn_standards_interval_time are missing. Number of measurements
            between standards or time (min) between standards.
DIFF022_ALERT_1_A  _diffrn_standards_decay_% is missing
            Percentage decrease in standards intensity.
GEOM006_ALERT_1_A  _geom_angle_atom_site_label_2 is missing
            Label identifying the atom site 2.
GEOM007_ALERT_1_A  _geom_angle_atom_site_label_3 is missing
            Label identifying the atom site 3.

Alert level C
RINTA01_ALERT_3_C  The value of Rint is greater than 0.12
            Rint given   0.156
PLAT158_ALERT_4_C The Input Unitcell is NOT Standard/Reduced .....          ?

Alert level G
ABSTM02_ALERT_3_G  When printed, the submitted absorption T values will be
            replaced by the scaled T values. Since the ratio of scaled T's
            is identical to the ratio of reported T values, the scaling
            does not imply a change to the absorption corrections used in
            the study.
            Ratio of Tmax expected/reported      0.868
            Tmax scaled      0.151 Tmin scaled      0.053
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large.      22.40      
PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size ....       0.08 mm   
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported   _diffrn_ambient_temperature        293 K    

   4 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   2 ALERT level C = Check and explain
   5 ALERT level G = General alerts; check

   6 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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