Acta Cryst. (2009). E65, m1117-m1118  [ doi:10.1107/S1600536809032589 ]

(2,2'-Bipyridine-²N,N')chlorido[4'-(2,5-dimethoxyphenyl)-2,2':6',2''-terpyridine-³N,N',N'']ruthenium(II) hexafluoridophosphate acetonitrile monosolvate

D. Oyama, M. Kido, A. Orita and T. Takase

Online 22 August 2009

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.004 Å
• Disorder in solvent or counterion
• R factor = 0.037
• wR factor = 0.111
• Data-to-parameter ratio = 16.3

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT198_ALERT_1_A Missing              _diffrn_ambient_temperature          ?

Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.60 Ratio
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.26 Ratio
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru1    --  Cl1     ..       5.80 su   
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         O1     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          P1     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         C34     

Alert level G
PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size ....       0.60 mm   
PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ...................      29.00 Perc.

   1 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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