Acta Cryst. (2009). E65, m1127-m1128  [ doi:10.1107/S1600536809032395 ]

trans-(Pyrimidine-2-thiolato-²N,S)[tris(2-aminoethyl)amine-⁴N,N',N'',N''']cobalt(III) chloride hexafluoridophosphate

K. Fujihara and T. Yonemura

Online 22 August 2009

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.006 Å
• R factor = 0.057
• wR factor = 0.174
• Data-to-parameter ratio = 18.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT420_ALERT_2_C D-H Without Acceptor       N6     -   H20    ...          ?      
PLAT042_ALERT_1_C Calc. and Reported MoietyFormula Strings  Differ          ?
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          P1     

Alert level G
PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large..       0.11      
PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size ....       0.45 mm   

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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