# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' JAMISCA_I' _shelx_refln_list_code 4 _shelx_F_calc_maximum 160.02 _exptl_crystal_F_000 784.00 _reflns_d_resolution_high 0.8027 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 11.5130 _cell_length_b 12.6390 _cell_length_c 13.5560 _cell_angle_alpha 78.578 _cell_angle_beta 71.880 _cell_angle_gamma 89.300 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3887.16 4088.13 57.96 o 3 0 0 20033.95 20159.41 256.13 o 4 0 0 1100.31 1113.74 27.68 o 5 0 0 86.92 112.54 17.00 o 6 0 0 4815.21 4984.46 89.53 o 7 0 0 135.49 192.71 61.77 o 8 0 0 405.48 450.28 28.24 o 9 0 0 1896.00 1949.71 52.69 o 10 0 0 528.87 431.63 54.13 o 11 0 0 814.96 1076.48 85.22 o 12 0 0 211.58 228.73 175.40 o 13 0 0 331.67 183.14 118.46 o -13 1 0 20.70 -121.71 209.38 o -12 1 0 286.60 315.31 137.08 o -11 1 0 182.00 232.36 51.90 o -10 1 0 20.77 31.01 40.27 o -9 1 0 213.97 241.25 27.63 o -8 1 0 697.33 740.37 33.26 o -7 1 0 194.92 200.80 36.55 o -6 1 0 3222.20 3431.58 59.10 o -5 1 0 5126.65 4861.48 77.85 o -4 1 0 269.92 255.98 22.67 o -3 1 0 9347.38 9273.43 123.98 o -2 1 0 12.10 22.33 13.88 o 2 1 0 3201.81 3049.28 50.00 o 3 1 0 1866.65 1786.61 66.79 o 4 1 0 421.36 451.19 25.23 o 5 1 0 2423.08 2763.41 52.97 o 6 1 0 29.77 41.08 17.00 o 7 1 0 1.90 -20.24 21.05 o 8 1 0 487.97 407.29 32.26 o 9 1 0 709.70 720.84 34.06 o 10 1 0 12.81 11.39 67.72 o 11 1 0 124.27 100.62 150.17 o 12 1 0 44.10 58.27 93.59 o 13 1 0 95.97 32.24 113.05 o -13 2 0 0.42 -69.81 166.60 o -12 2 0 5.08 -112.67 114.46 o -11 2 0 1645.63 1674.44 81.35 o -10 2 0 748.17 859.93 127.27 o -9 2 0 158.59 175.21 28.06 o -8 2 0 1288.49 1295.57 41.65 o -7 2 0 375.87 401.31 23.65 o -6 2 0 15.04 22.74 16.22 o -5 2 0 16.40 -16.19 21.05 o -4 2 0 898.91 989.69 30.92 o -3 2 0 1113.04 1179.81 28.77 o -2 2 0 9551.53 9130.07 132.23 o -1 2 0 8169.68 7684.51 122.63 o 0 2 0 2188.54 1679.36 85.85 o 1 2 0 62.87 92.20 9.64 o 2 2 0 5895.73 5654.11 79.41 o 3 2 0 505.62 471.67 27.79 o 4 2 0 429.55 465.30 22.59 o 5 2 0 734.46 841.80 61.53 o 6 2 0 77.74 48.66 14.58 o 7 2 0 9.75 -14.85 14.85 o 8 2 0 52.42 49.87 28.33 o 9 2 0 274.49 301.32 90.96 o 10 2 0 670.22 637.26 77.46 o 11 2 0 272.81 293.12 59.61 o 12 2 0 22.34 48.14 104.82 o 13 2 0 21.21 119.83 112.93 o -13 3 0 122.53 231.21 226.67 o -12 3 0 237.94 145.37 238.02 o -11 3 0 40.11 -13.65 35.54 o -10 3 0 348.94 432.43 38.72 o -9 3 0 203.33 205.28 31.45 o -8 3 0 23.91 30.63 17.56 o -7 3 0 442.71 451.19 25.79 o -6 3 0 1.86 -5.53 16.22 o -5 3 0 249.29 266.96 20.84 o -4 3 0 115.17 84.44 17.29 o -3 3 0 37.61 31.29 13.31 o -2 3 0 16413.84 15977.90 251.86 o -1 3 0 8526.59 8177.60 185.16 o 0 3 0 3362.89 3349.47 87.57 o 1 3 0 1853.55 1763.06 69.09 o 2 3 0 5827.18 5505.35 86.08 o 3 3 0 326.68 346.77 17.43 o 4 3 0 3.70 14.17 16.03 o 5 3 0 78.37 78.77 16.03 o 6 3 0 608.31 606.96 31.75 o 7 3 0 962.94 936.90 35.40 o 8 3 0 516.20 565.30 51.02 o 9 3 0 1887.05 1969.27 104.66 o 10 3 0 2.51 31.97 50.50 o 11 3 0 551.10 489.88 87.54 o 12 3 0 1.39 -61.06 135.71 o 13 3 0 23.79 44.18 110.50 o -13 4 0 0.70 237.99 176.80 o -12 4 0 11.26 -35.06 118.94 o -11 4 0 108.44 100.34 49.36 o -10 4 0 233.84 218.30 45.81 o -9 4 0 268.15 277.08 35.95 o -8 4 0 1219.46 1291.28 47.93 o -7 4 0 1785.94 1730.87 52.66 o -6 4 0 493.22 528.29 28.02 o -5 4 0 51.86 46.10 39.38 o -4 4 0 212.84 256.67 21.94 o -3 4 0 1183.04 1193.36 60.43 o -2 4 0 1906.65 1842.78 49.74 o -1 4 0 865.28 828.84 30.11 o 0 4 0 175.87 154.71 45.06 o 1 4 0 5653.61 5757.25 90.98 o 2 4 0 552.50 567.56 25.23 o 3 4 0 921.01 1005.17 30.92 o 4 4 0 186.99 197.91 17.02 o 5 4 0 222.14 219.90 18.44 o 6 4 0 85.76 103.94 70.55 o 7 4 0 18.36 38.48 21.65 o 8 4 0 66.65 108.95 20.62 o 9 4 0 7.39 22.44 31.45 o 10 4 0 500.41 563.62 70.38 o 11 4 0 9.34 -1.27 71.21 o 12 4 0 8.03 -52.60 80.60 o -12 5 0 52.84 -1.64 175.38 o -11 5 0 438.84 424.97 96.64 o -10 5 0 12.49 14.86 46.22 o -9 5 0 1265.92 1291.77 59.09 o -8 5 0 10.13 36.88 32.18 o -7 5 0 6.83 48.07 25.90 o -6 5 0 41.97 54.52 23.84 o -5 5 0 144.98 102.78 28.62 o -4 5 0 193.99 206.94 45.91 o -3 5 0 51.87 15.11 25.34 o -2 5 0 496.04 494.37 31.83 o -1 5 0 435.73 436.53 30.71 o 0 5 0 4884.12 4881.55 106.39 o 1 5 0 2675.63 2682.32 52.03 o 2 5 0 104.52 136.01 21.62 o 3 5 0 455.50 403.60 47.90 o 4 5 0 683.10 633.06 46.78 o 5 5 0 85.33 67.20 23.06 o 6 5 0 160.26 114.81 24.46 o 7 5 0 6.61 10.57 27.49 o 8 5 0 61.63 85.93 50.72 o 9 5 0 1.96 -59.54 59.54 o 10 5 0 119.19 262.85 71.72 o 11 5 0 35.79 76.50 80.14 o 12 5 0 14.24 96.05 124.10 o -12 6 0 130.17 222.74 135.65 o -11 6 0 16.43 32.91 62.21 o -10 6 0 28.46 159.65 74.75 o -9 6 0 14.07 -45.37 45.37 o -8 6 0 5.63 17.06 42.22 o -7 6 0 260.08 249.94 32.06 o -6 6 0 16.14 -24.40 25.97 o -5 6 0 302.97 357.08 31.32 o -4 6 0 406.15 368.45 30.43 o -3 6 0 38.72 43.08 36.83 o -2 6 0 413.85 429.67 31.87 o -1 6 0 1097.08 1076.45 51.91 o 0 6 0 642.71 576.89 34.47 o 1 6 0 551.07 570.06 24.95 o 2 6 0 623.36 702.44 70.59 o 3 6 0 64.22 26.19 17.70 o 4 6 0 86.16 84.21 21.86 o 5 6 0 6.23 5.67 28.05 o 6 6 0 296.68 268.99 34.27 o 7 6 0 86.32 163.93 48.17 o 8 6 0 329.41 369.48 46.77 o 9 6 0 401.54 460.04 71.85 o 10 6 0 21.94 50.46 77.69 o 11 6 0 52.68 1.66 108.27 o 12 6 0 312.66 479.05 126.66 o -12 7 0 207.08 -36.70 123.87 o -11 7 0 360.64 499.87 100.88 o -10 7 0 70.06 69.38 68.41 o -9 7 0 208.09 302.52 72.09 o -8 7 0 469.67 287.72 60.10 o -7 7 0 3.03 -34.05 34.05 o -6 7 0 331.22 323.93 37.61 o -5 7 0 9.94 15.36 24.11 o -4 7 0 135.46 157.70 28.65 o -3 7 0 1140.94 1078.97 47.14 o -2 7 0 79.08 47.00 33.88 o -1 7 0 596.85 582.95 35.84 o 0 7 0 2385.28 2545.31 69.86 o 1 7 0 0.87 4.38 16.06 o 2 7 0 21.88 16.15 27.49 o 3 7 0 26.45 13.52 23.47 o 4 7 0 88.10 102.33 45.05 o 5 7 0 7.77 44.98 25.78 o 6 7 0 131.46 82.09 50.72 o 7 7 0 1671.36 1814.52 62.71 o 8 7 0 7.62 -61.11 61.11 o 9 7 0 44.82 49.87 68.00 o 10 7 0 488.35 623.19 91.78 o 11 7 0 196.43 237.22 164.91 o -11 8 0 225.40 148.35 75.95 o -10 8 0 20.64 26.68 73.74 o -9 8 0 23.78 31.17 85.00 o -8 8 0 0.01 -8.55 44.07 o -7 8 0 167.69 243.94 54.24 o -6 8 0 401.30 352.59 43.68 o -5 8 0 11.91 46.82 29.61 o -4 8 0 10.63 -0.79 29.76 o -3 8 0 61.25 59.58 45.33 o -2 8 0 80.44 110.05 29.45 o -1 8 0 150.65 179.04 58.94 o 0 8 0 628.54 598.77 51.45 o 1 8 0 342.67 319.34 53.85 o 2 8 0 3.47 0.03 30.87 o 3 8 0 344.98 341.89 40.75 o 4 8 0 36.77 83.07 76.22 o 5 8 0 68.04 62.20 31.17 o 6 8 0 560.88 624.76 42.36 o 7 8 0 388.30 337.28 47.72 o 8 8 0 13.03 113.54 65.02 o 9 8 0 347.30 491.50 84.96 o 10 8 0 0.05 22.86 90.66 o 11 8 0 9.77 226.66 165.46 o -11 9 0 101.21 40.12 198.34 o -10 9 0 5.86 -38.86 79.09 o -9 9 0 71.25 157.54 84.03 o -8 9 0 395.00 399.44 94.73 o -7 9 0 371.26 379.26 69.86 o -6 9 0 341.75 429.66 60.36 o -5 9 0 85.86 53.41 51.15 o -4 9 0 114.14 232.70 59.79 o -3 9 0 61.31 16.31 37.67 o -2 9 0 0.18 30.58 53.55 o -1 9 0 22.55 71.31 45.33 o 0 9 0 417.68 472.30 157.58 o 1 9 0 3469.21 3470.40 136.32 o 2 9 0 0.01 -37.07 37.84 o 3 9 0 717.99 764.07 62.79 o 4 9 0 1489.40 1376.49 131.87 o 5 9 0 4.42 2.55 43.94 o 6 9 0 1.42 -39.47 39.47 o 7 9 0 472.53 665.89 109.39 o 8 9 0 24.75 -33.55 81.69 o 9 9 0 139.25 272.73 99.40 o 10 9 0 852.92 485.44 138.49 o -10 10 0 116.25 -67.49 95.22 o -9 10 0 67.70 34.87 86.27 o -8 10 0 392.40 463.57 215.09 o -7 10 0 13.91 -22.40 59.86 o -6 10 0 5.40 46.91 52.03 o -5 10 0 873.35 897.35 68.13 o -4 10 0 3.57 -47.11 90.38 o -3 10 0 714.79 688.02 73.00 o -2 10 0 4786.93 4557.66 287.59 o -1 10 0 39.24 75.04 48.62 o 0 10 0 701.74 672.89 114.23 o 1 10 0 2086.34 2123.00 106.41 o 2 10 0 15.84 112.53 130.62 o 3 10 0 433.60 414.69 65.27 o 4 10 0 2727.75 2784.92 117.99 o 5 10 0 270.95 272.72 62.77 o 6 10 0 241.96 162.23 64.00 o 7 10 0 20.21 -4.21 83.15 o 8 10 0 2.00 -41.33 93.67 o 9 10 0 25.49 22.67 163.77 o -9 11 0 26.00 163.77 113.90 o -8 11 0 351.14 187.59 111.23 o -7 11 0 1479.28 1911.10 481.16 o -6 11 0 563.94 742.72 126.01 o -5 11 0 7.53 17.81 153.28 o -4 11 0 343.52 258.22 60.51 o -3 11 0 116.53 209.53 116.74 o -2 11 0 12.60 -26.48 62.33 o -1 11 0 1686.90 1828.70 114.05 o 0 11 0 1236.05 1256.97 95.87 o 1 11 0 0.89 37.89 65.99 o 2 11 0 180.54 199.87 64.17 o 3 11 0 78.11 86.59 67.26 o 4 11 0 127.75 387.05 90.37 o 5 11 0 96.82 145.18 70.27 o 6 11 0 143.56 255.37 85.29 o 7 11 0 44.09 39.28 113.49 o 8 11 0 107.39 -73.67 119.00 o -8 12 0 133.75 188.31 103.78 o -7 12 0 21.99 85.03 98.75 o -6 12 0 216.21 -25.62 87.71 o -5 12 0 1.73 29.83 82.28 o -4 12 0 0.08 -2.27 57.03 o -3 12 0 202.29 263.88 94.92 o -2 12 0 172.39 115.25 65.26 o -1 12 0 72.11 118.32 138.84 o 0 12 0 50.88 37.02 63.07 o 1 12 0 136.27 110.33 92.22 o 2 12 0 95.39 181.66 91.01 o 3 12 0 32.64 29.49 70.43 o 4 12 0 139.11 13.95 99.22 o 5 12 0 57.56 17.48 79.64 o 6 12 0 1.20 -8.59 78.58 o 7 12 0 12.58 -24.50 94.06 o -7 13 0 154.02 237.34 111.50 o -6 13 0 124.09 135.31 129.77 o -5 13 0 262.48 299.71 141.11 o -4 13 0 9.48 34.28 67.72 o -3 13 0 145.75 115.25 106.03 o -2 13 0 189.69 188.77 97.36 o -1 13 0 14.42 -31.49 62.29 o 0 13 0 114.94 101.89 71.65 o 1 13 0 63.10 167.18 83.55 o 2 13 0 0.78 78.76 101.43 o 3 13 0 166.91 -76.82 87.20 o 4 13 0 290.71 361.05 102.58 o 5 13 0 0.18 -101.81 101.81 o 6 13 0 543.03 495.50 162.44 o -6 14 0 69.74 136.00 170.57 o -5 14 0 128.31 180.39 212.51 o -4 14 0 22.53 159.92 127.78 o -3 14 0 168.73 335.48 96.57 o -2 14 0 30.55 108.24 90.76 o -1 14 0 183.88 76.05 76.87 o 0 14 0 17.33 -47.92 104.27 o 1 14 0 73.10 133.69 90.48 o 2 14 0 0.06 -43.00 77.38 o 3 14 0 54.95 62.33 181.90 o 4 14 0 92.65 -14.57 215.62 o -3 15 0 3.69 -57.95 138.55 o -2 15 0 2.48 -29.49 260.66 o -1 15 0 66.55 184.46 94.63 o 0 15 0 35.32 -88.31 153.28 o 1 15 0 13.96 215.33 170.00 o 2 15 0 9.16 61.79 99.16 o 0 -15 1 0.01 -88.67 102.85 o 1 -15 1 25.72 67.55 218.16 o 2 -15 1 160.18 66.44 238.30 o -4 -14 1 74.39 136.00 124.67 o -3 -14 1 78.32 -65.57 115.76 o -2 -14 1 450.60 521.39 97.77 o -1 -14 1 74.36 149.17 86.47 o 0 -14 1 127.68 189.78 89.31 o 1 -14 1 10.40 58.52 115.60 o 2 -14 1 14.55 221.47 210.51 o 3 -14 1 44.12 -23.35 115.88 o 4 -14 1 5.55 -30.08 113.95 o 5 -14 1 6.24 -22.67 151.86 o 6 -14 1 184.88 40.24 147.34 o -5 -13 1 59.23 -56.49 92.98 o -4 -13 1 0.69 -30.47 161.50 o -3 -13 1 0.24 -0.21 72.53 o -2 -13 1 598.15 626.31 141.70 o -1 -13 1 0.67 96.62 160.93 o 0 -13 1 86.43 7.65 54.33 o 1 -13 1 153.78 225.93 121.56 o 2 -13 1 188.54 251.65 166.33 o 3 -13 1 1.92 29.19 121.83 o 4 -13 1 584.58 910.72 130.74 o 5 -13 1 52.57 -78.77 107.10 o 6 -13 1 495.03 741.72 155.58 o 7 -13 1 35.48 -68.57 153.57 o -7 -12 1 58.55 48.79 164.62 o -6 -12 1 47.47 -113.58 147.62 o -5 -12 1 42.36 59.57 79.74 o -4 -12 1 0.08 115.09 78.36 o -3 -12 1 90.50 178.05 89.42 o -2 -12 1 22.49 -64.38 64.77 o -1 -12 1 533.05 642.27 88.17 o 0 -12 1 215.01 246.14 88.09 o 1 -12 1 10.79 -89.29 89.29 o 2 -12 1 152.38 -25.45 68.54 o 3 -12 1 2.66 -9.83 54.20 o 4 -12 1 8.70 74.97 70.25 o 5 -12 1 4.38 -44.98 130.33 o 6 -12 1 156.19 202.15 80.25 o 7 -12 1 0.03 -62.33 90.66 o 8 -12 1 2.98 222.80 108.83 o -8 -11 1 114.27 187.57 125.80 o -7 -11 1 283.24 50.89 93.94 o -6 -11 1 2.96 -20.88 90.39 o -5 -11 1 20.75 92.88 91.31 o -4 -11 1 11.34 -6.73 54.10 o -3 -11 1 213.54 208.21 73.45 o -2 -11 1 21.74 132.08 73.32 o -1 -11 1 153.20 135.07 67.72 o 0 -11 1 46.70 174.10 67.72 o 1 -11 1 123.73 207.87 107.39 o 2 -11 1 7.08 7.08 59.50 o 3 -11 1 61.30 32.70 52.03 o 4 -11 1 4.81 6.63 101.71 o 5 -11 1 0.02 -53.88 60.48 o 6 -11 1 46.30 56.16 57.17 o 7 -11 1 64.49 230.32 90.21 o 8 -11 1 41.83 11.36 92.96 o 9 -11 1 190.90 270.72 127.51 o 10 -11 1 158.56 -214.21 214.21 o -9 -10 1 123.81 215.34 159.24 o -8 -10 1 33.72 299.04 138.04 o -7 -10 1 105.21 147.57 111.39 o -6 -10 1 0.22 60.14 88.11 o -5 -10 1 298.38 312.92 107.96 o -4 -10 1 15.63 25.35 68.23 o -3 -10 1 1.47 -15.65 49.42 o -2 -10 1 186.04 206.59 96.63 o -1 -10 1 25.71 14.47 57.05 o 0 -10 1 122.12 157.23 110.79 o 1 -10 1 55.24 111.80 82.17 o 2 -10 1 1.83 -14.55 45.04 o 3 -10 1 82.26 30.88 71.12 o 4 -10 1 1189.25 1275.86 122.48 o 5 -10 1 408.94 479.59 58.37 o 6 -10 1 232.21 261.23 57.42 o 7 -10 1 232.68 288.17 79.34 o 8 -10 1 4.69 56.14 99.82 o 9 -10 1 55.04 232.51 79.33 o 10 -10 1 483.77 499.67 115.23 o -9 -9 1 3.00 -127.40 166.60 o -8 -9 1 442.96 352.45 107.58 o -7 -9 1 45.12 8.75 47.97 o -6 -9 1 531.85 600.11 64.73 o -5 -9 1 45.59 -30.25 46.06 o -4 -9 1 332.95 335.03 60.64 o -3 -9 1 17.87 35.94 37.84 o -2 -9 1 522.09 534.88 86.16 o -1 -9 1 3491.92 3682.86 124.86 o 0 -9 1 324.78 261.67 79.63 o 1 -9 1 94.56 43.16 49.60 o 2 -9 1 161.16 78.25 45.72 o 3 -9 1 79.47 149.36 51.53 o 4 -9 1 131.47 157.60 45.81 o 5 -9 1 401.17 397.65 60.08 o 6 -9 1 99.14 141.69 42.27 o 7 -9 1 186.51 155.35 62.06 o 8 -9 1 86.00 44.50 169.72 o 9 -9 1 7.24 21.19 70.55 o 10 -9 1 278.44 286.50 305.18 o 11 -9 1 1.80 25.04 119.73 o -10 -8 1 222.70 97.16 88.97 o -9 -8 1 5.63 -54.28 70.83 o -8 -8 1 9.83 60.68 121.55 o -7 -8 1 1018.95 1167.97 93.86 o -6 -8 1 118.15 196.17 36.36 o -5 -8 1 113.85 121.68 42.13 o -4 -8 1 30.25 79.30 33.95 o -3 -8 1 12.53 -11.78 67.72 o -2 -8 1 1161.01 1037.34 117.40 o -1 -8 1 309.95 290.66 33.56 o 0 -8 1 48.21 85.60 36.55 o 1 -8 1 1124.55 1045.26 83.09 o 2 -8 1 717.35 648.99 57.08 o 3 -8 1 359.05 323.20 52.50 o 4 -8 1 0.25 3.38 34.05 o 5 -8 1 227.19 198.90 37.53 o 6 -8 1 127.75 136.44 47.33 o 7 -8 1 89.17 141.63 49.74 o 8 -8 1 0.38 -22.13 43.68 o 9 -8 1 0.92 22.67 85.00 o 10 -8 1 18.64 -25.69 72.35 o 11 -8 1 0.01 43.86 241.11 o 12 -8 1 1.62 238.00 181.33 o -11 -7 1 381.78 533.88 102.80 o -10 -7 1 8.59 35.20 118.71 o -9 -7 1 111.74 181.48 89.48 o -8 -7 1 348.23 262.25 83.03 o -7 -7 1 66.13 13.99 33.12 o -6 -7 1 65.86 62.25 28.25 o -5 -7 1 141.26 177.96 27.03 o -4 -7 1 114.90 68.88 27.32 o -3 -7 1 107.30 133.47 28.25 o -2 -7 1 103.52 83.83 33.72 o -1 -7 1 594.86 587.54 33.26 o 0 -7 1 942.60 964.74 44.68 o 1 -7 1 111.48 138.94 28.25 o 2 -7 1 634.23 506.55 38.16 o 3 -7 1 682.08 647.42 35.95 o 4 -7 1 9.58 43.40 27.49 o 5 -7 1 247.86 227.27 28.05 o 6 -7 1 3.36 48.73 33.88 o 7 -7 1 10.52 33.38 82.17 o 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